Hach-Lange SD900 User Manual

DOC026.52.80437
SD900 Portable Sampler
03/2014, Edition 1
User Manual
Table of Contents
Specifications..............................................................................................................3
General information..................................................................................................4
Safety information........................................................................................................5
Precautionary labels.............................................................................................5
Certification........................................................................................................... 5
Product overview.........................................................................................................6
Product components....................................................................................................7
Installation.....................................................................................................................8
Confined space precautions........................................................................................8
Mechanical installation
Site installation guidelines....................................................................................8
Install the sampler in a manhole...........................................................................9
Install the distributor or full-bottle shutoff (optional)..............................................9
Prepare the sampler.............................................................................................9
Clean the sample bottles...............................................................................9
Install a single bottle......................................................................................9
Install the first bottle for multiple sample collections.....................................9
Install multiple bottles..................................................................................10
Plumb the sampler......................................................................................11
Electrical installation..................................................................................................12
Controller connections........................................................................................12
Connect a flow meter.......................................................................................... 13
Connect a PC or communications network........................................................13
Connect an SDI-12 device.................................................................................. 14
Connect the sampler to power............................................................................ 14
Calculate the pump cycle time............................................................................ 15
Close the cover..........................................................................................................16
................................................................................................. 8
Set the power to on.................................................................................................16
User interface and navigation............................................................................16
Operation.....................................................................................................................17
Main menu overview..................................................................................................17
Configure the system settings...................................................................................17
Configure the SDI-12 device..............................................................................18
Set up a sampling program........................................................................................ 19
Time based collection.........................................................................................21
Use variable volume....................................................................................21
Do not use variable volume.........................................................................21
Flow based collection.........................................................................................21
Use counts for the flow source....................................................................21
Use 4–20 mA input for the flow source.......................................................22
Review or modify program settings....................................................................22
Save or load programs.......................................................................................22
Restore the default settings................................................................................22
Constant Time Variable Volume (CTVV) sampling............................................23
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Table of Contents
Start or stop a program..............................................................................................24
View the program status............................................................................................24
Manual operation.......................................................................................................24
Collect a grab sample.........................................................................................24
Move the distributor arm.....................................................................................25
Start or stop the pump........................................................................................25
View data...................................................................................................................25
View the sample history...................................................................................... 25
View the event log..............................................................................................26
Event log information
Erase the event log.....................................................................................26
View data from SDI-12 devices..........................................................................26
Volume calibration.....................................................................................................27
Calibrate the liquid sensor..................................................................................27
Restore the default calibration............................................................................27
Calibrate the sample volume with the liquid sensor...........................................27
Calibrate the sample volume manually............................................................... 28
Verify the sample volume...................................................................................28
Full bottle shutoff.......................................................................................................28
Activate the full bottle shutoff.............................................................................. 29
Enable the full bottle shutoff...............................................................................29
Full bottle shutoff in non-continuous mode.........................................................29
Full bottle shut off in continuous mode...............................................................29
Full bottle shutoff and timed bottle mode....................................................30
Full bottle shutoff exception conditions............................................................... 30
................................................................................... 26
Advanced sampling................................................................................................30
Send output signal at program completion................................................................30
Send output signal with sample cycle (special output)..............................................31
Operate from an external signal (setpoint sample)....................................................31
Use an SDI-12 device for setpoint sampling .....................................................31
Set multiple start and stop times................................................................................ 32
Collect first flush stormwater samples.......................................................................33
Set variable intervals.................................................................................................33
Timed bottle sets.......................................................................................................34
Maintenance...............................................................................................................34
Clean the instrument.................................................................................................. 35
Replace the desiccant...............................................................................................35
Pump maintenance....................................................................................................36
Replace the pump tubing.................................................................................... 36
Clean the rotor....................................................................................................38
Replace the distributor arm tube................................................................................ 39
Fuse replacement......................................................................................................39
Troubleshooting.......................................................................................................39
General troubleshooting............................................................................................39
Error messages.........................................................................................................40
Diagnostic tests.........................................................................................................42
Replacement parts and accessories...............................................................42
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Specifications

Specifications are subject to change without notice.
SD900 Portable Sampler
Specification Standard base Compact base Composite base
Dimensions Diameter: 50.5 cm (19.9 in.)
Height: 69.4 cm (27.3 in.)
Weight 15 kg (35.6 lb) with 1-L
Enclosure Impact-resistant ABS, 3-section construction; double-walled base with 2.54 cm (1 in.)
Sample temperature
Strainers 316 stainless steel in standard size, high velocity or low profile for shallow depth applications
Sample intake tubing
Sample bottle capacity
polyethylene bottles (24x)
14.8 kg (32.6 lb) with 10-L (2.5 gal) polyethylene container (1x)
insulation—direct bottle contact with ice.
0–60 °C (32–140 °F)
and Teflon® or 316 stainless steel in standard size
9.5 mm (3/8 in.) I.D. vinyl or Teflon-lined polyethylene
1-L (0.26 gal) polyethylene and/or 350-mL (11.83 oz) glass bottles (24x)
2.3-L (0.6 gal) polyethylene and/or
1.9-L (0.5 gal) glass bottles (8x)
3.8-L (1 gal) polyethylene and/or
3.8-L (1 gal) glass bottles (4x)
3.8-L (1 gal) polyethylene and/or
3.8-L (1 gal) glass bottles (2x)
21-L (5.5 gal) or 15-L (4 gal) polyethylene composite container or 20-L (5.25 gal) polyethylene or 10-L (2.5 gal) polyethylene or 10-L (2.5 gal) glass (1x)
Diameter: 44.1 cm (17.4 in.)
Height: 61 cm (24 in.)
12.2 kg (27 lb) with 575-mL (19.44 oz) polyethylene bottles (24x)
12.9 kg (28.3 lb) with 10-L (2.5 gal) polyethylene container (1x)
575-mL (19.44 oz) polyethylene bottles (24x)
950-mL (32.12 oz) glass bottles (8x)
10-L (2.5 gal) polyethylene bottle (1x)
10-L (2.5 gal) glass bottle (1x)
Diameter: 50.28 cm (19.8 in.)
Height: 79.75 cm (31.4 in.)
15 kg (36 lb) with 950­mL (32.12 oz) glass bottles (12x)
21-L (5.5 gal) polyethylene bottle (1x)
SD controller
Specification Details
Dimensions (W x H x D) 29.2 x 17.1 x 26.4 cm (11½ x 6¾ x 103/8 in.)
Weight 4.2 kg (9.26 lb)
Enclosure PC/ABS blend, NEMA 4X, 6, IP 67
Power requirements 15 VDC supplied by a 8754500 power supply; 15 VDC supplied by an integral
Overload protection 7 A, DC line fuse for the pump
Operating temperature 0 to 50 °C (32 to 122 °F)
Storage temperature –30 to 60 °C (–22 to 140 °F)
power supply
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Specification Details
Storage/operating humidity 100% condensing
Pump Peristaltic high speed, with spring-mounted Nylatron rollers
Pump enclosure IP37
Pump tubing 9.5 mm ID x 15.9 OD mm (3/8 in. ID x 5/8 in. OD) silicone
Pump tubing life 20,000 sample cycles with: 1 L (0.3 gal) sample volume, 1 rinse, 6 minute
Vertical sample lift Maximum 8.5 m (28 ft) for: 8.8 m (29 ft) of 3/8-in. vinyl intake tube at sea level
Pump flow rate 4.8 L/min (1.25 gpm) at 1 m (3 ft) vertical lift with 3/8-in. intake tube typical
Sample volume Programmable in 10-mL (0.34 oz) increments from 10 to 10,000 mL (3.38 oz
Sample volume repeatability (typical)
Sample volume accuracy (typical)
Sampling modes Pacing: Time-fixed, flow-fixed, time-variable, flow-variable, constant time
Run modes Continuous or non-continuous with user-entered number of samples
Multiple programs Stores up to three sampling programs
Transfer velocity (typical) 0.9 m/s (2.9 ft/s) with: 4.6 m (15 ft) vertical lift, 4.9 m (16 ft) of 3/8-in. vinyl
Liquid sensor Ultrasonic. Body: Ultem® NSF ANSI standard 51 approved, USP Class VI
Sample history Up to 510 records
Air purge Air purged automatically before and after each sample. The duration
Event log 510 records
Connections Power, auxiliary, serial communications, distributor, SDI-12
Wetted materials Stainless steel, polyethylene, Teflon, Ultem, silicone
Communications RS232, Modbus, SDI-12
Warranty 1 year
pacing interval, 4.9 m (16 ft) of 3/8 in. intake tube, 4.6 m (15 ft) of vertical lift, 21 °C (70 °F) sample temperature
at 20–25 °C (68–77 °F)
to 2.6 gal)
±5% of 200 mL sample volume using uncalibrated liquid detect with: 4.6 m (15 ft) vertical lift, 4.9 m (16 ft) of 3/8-in. vinyl intake tube, single bottle, full bottle shut-off at room temperature and 1524 m (5000 ft) elevation
±10% of 200 mL sample volume using uncalibrated liquid detect with: 4.6 m (15 ft) vertical lift, 4.9 m (16 ft) of 3/8-in. vinyl intake tube, single bottle, full bottle shut-off at room temperature and 1524 m (5000 ft) elevation
variable volume (CTVV). Refer to Constant Time Variable Volume (CTVV) sampling on page 23.
Distribution: Single bottle composite, multi-bottle composite, multi-bottle discrete, bottles per sample, samples per bottle, combination of bottles per sample, samples per bottle
intake tubing, 21 °C (70 °F) and 1524 m (5000 ft) elevation
compliant
automatically compensates for varying intake tube lengths.

General information

In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential damages resulting from any defect or omission in this manual. The manufacturer reserves the right to make changes in this manual and the products it describes at any time, without notice or obligation. Revised editions are found on the manufacturer’s website.
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Safety information

N O T I C E
The manufacturer is not responsible for any damages due to misapplication or misuse of this product including, without limitation, direct, incidental and consequential damages, and disclaims such damages to the full extent permitted under applicable law. The user is solely responsible to identify critical application risks and install appropriate mechanisms to protect processes during a possible equipment malfunction.
Please read this entire manual before unpacking, setting up or operating this equipment. Pay attention to all danger and caution statements. Failure to do so could result in serious injury to the operator or damage to the equipment.
Make sure that the protection provided by this equipment is not impaired. Do not use or install this equipment in any manner other than that specified in this manual.

Use of hazard information

Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.
Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious injury.
Indicates a potentially hazardous situation that may result in minor or moderate injury.
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special emphasis.

Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol on the instrument is referenced in the manual with a precautionary statement.
This is the safety alert symbol. Obey all safety messages that follow this symbol to avoid potential injury. If on the instrument, refer to the instruction manual for operation or safety information.
D A N G E R
W A R N I N G
C A U T I O N
N O T I C E
This symbol indicates a potential pinch hazard.
Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.

Certification

Canadian Radio Interference-Causing Equipment Regulation, IECS-003, Class A:
Supporting test records reside with the manufacturer.
This Class A digital apparatus meets all requirements of the Canadian Interference-Causing Equipment Regulations.
Cet appareil numérique de classe A répond à toutes les exigences de la réglementation canadienne sur les équipements provoquant des interférences.
FCC Part 15, Class "A" Limits
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Supporting test records reside with the manufacturer. The device complies with Part 15 of the FCC Rules. Operation is subject to the following conditions:
1. The equipment may not cause harmful interference.
2. The equipment must accept any interference received, including interference that may cause
undesired operation.
Changes or modifications to this equipment not expressly approved by the party responsible for compliance could void the user's authority to operate the equipment. This equipment has been tested and found to comply with the limits for a Class A digital device, pursuant to Part 15 of the FCC rules. These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment. This equipment generates, uses and can radiate radio frequency energy and, if not installed and used in accordance with the instruction manual, may cause harmful interference to radio communications. Operation of this equipment in a residential area is likely to cause harmful interference, in which case the user will be required to correct the interference at their expense. The following techniques can be used to reduce interference problems:
1. Disconnect the equipment from its power source to verify that it is or is not the source of the interference.
2. If the equipment is connected to the same outlet as the device experiencing interference, connect the equipment to a different outlet.
3. Move the equipment away from the device receiving the interference.
4. Reposition the receiving antenna for the device receiving the interference.
5. Try combinations of the above.

Product overview

D A N G E R
Chemical or biological hazards. If this instrument is used to monitor a treatment process and/or chemical feed system for which there are regulatory limits and monitoring requirements related to public health, public safety, food or beverage manufacture or processing, it is the responsibility of the user of this instrument to know and abide by any applicable regulation and to have sufficient and appropriate mechanisms in place for compliance with applicable regulations in the event of malfunction of the instrument.
C A U T I O N
Fire hazard. This product is not designed for use with flammable liquids.
The SD900 Portable Sampler collects liquid samples at specified intervals and keeps the samples in bottles or containers. Use the sampler for a wide variety of aqueous applications and for toxic pollutants and suspended solids. Set up
the sampler with different retainers, bottles or containers.
Refer to Figure 1.
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Figure 1 Product overview
1 Compact base 6 Controller connections
2 Standard insulated base 7 Pump
3 Center section 8 Controller
4 Power source 9 Liquid sensor
5 Top cover 10 Standard insulated base for 21-L (5.5 gal)
container

Product components

Make sure that all components have been received. Refer to Figure 2. If any items are missing or damaged, contact the manufacturer or a sales representative immediately.
Figure 2 Product components
1 Base (Standard, compact or composite) 6 Battery charger (optional)
2 Components for a single-bottle option (bottle and
support can change)
3 Center section with controller 8 Strainer
4 Battery (optional) 9 Intake tubing, vinyl or Teflon-lined
5 Top cover 10 Components for a multiple-bottle option (bottles
7 AC power supply (optional)
and retainers can change)
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Installation

D A N G E R
Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document.

Confined space precautions

D A N G E R
Explosion hazard. Training in pre-entry testing, ventilation, entry procedures, evacuation/rescue procedures and safety work practices is necessary before entering confined spaces.
The information that follows is supplied to help users understand the dangers and risks that are associated with entry into confined spaces.
On April 15, 1993, OSHA's final ruling on CFR 1910.146, Permit Required Confined Spaces, became law. This standard directly affects more than 250,000 industrial sites in the United States and was created to protect the health and safety of workers in confined spaces.
Definition of a confined space:
A confined space is any location or enclosure that has (or has the immediate potential for) one or more of the following conditions:
• An atmosphere with an oxygen concentration that is less than 19.5% or more than 23.5% and/or a
hydrogen sulfide (H2S) concentration that is more than 10 ppm.
An atmosphere that can be flammable or explosive due to gases, vapors, mists, dusts or fibers.
• Toxic materials which upon contact or inhalation can cause injury, impairment of health or death.
Confined spaces are not designed for human occupancy. Confined spaces have a restricted entry and contain known or potential hazards. Examples of confined spaces include manholes, stacks, pipes, vats, switch vaults and other similar locations.
Standard safety procedures must always be obeyed before entry into confined spaces and/or locations where hazardous gases, vapors, mists, dusts or fibers can be present. Before entry into a confined space, find and read all procedures that are related to confined space entry.

Mechanical installation

Site installation guidelines

D A N G E R
Explosion hazard. The instrument is not approved for installation in hazardous locations.
Refer to the guidelines that follow for the site location evaluation.
• Obey all the safety precautions if the sampler is installed in a confined space. Refer to Confined
space precautions on page 8.
• Make sure that the temperature at the location is in the specification range. Refer to Specifications
on page 3.
• Install the sampler on a level surface or hang the sampler with the suspension harness, the
support bracket or the spanner bar. Refer to Install the sampler in a manhole on page 9 and to the applicable installation documentation.
• As near the sample source as possible to decrease analysis delay. Refer to Plumb the sampler
on page 11.
• For limitations on transport velocity and maximum vertical lift, refer to Specifications on page 3.
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Install the sampler in a manhole

Install the sampler above the sample water in a manhole. Install the sampler support bracket. Install the spanner bar inside the manhole. The spanner bar is supported by pressure against the walls. The support bracket has the same width as the manhole cover. Install the support bracket directly below the cover for support. Refer to Replacement parts and accessories on page 42. Refer to the documentation supplied with the accessories to install the sampler.
with a spanner bar or a

Install the distributor or full-bottle shutoff (optional)

The distributor or full-bottle shutoff assembly is typically installed at the factory. Refer to the distributor or full-bottle shutoff documentation for installation.

Prepare the sampler

Clean the sample bottles
Clean the sample bottles and caps with a brush, water and a mild detergent. Flush the containers with fresh water followed by a distilled water rinse.
Install a single bottle
Use a single bottle to collect one composite sample. When the bottle is full, the full bottle shut-off stops the sample program.
1. Clean the sample bottles. Refer to Clean the sample bottles on page 9.
2. Install the sample bottle as shown in Figure 3.
Figure 3 Single bottle installation
1 Polyethylene bottle, 10 L (2.5 gal) (1918) 6 Polyethylene bottle, 21 L (5.5 gal) (6494)
2 Glass bottle, 10 L (2.5 gal) (6559) 7 Compact base (8975)
3 Support (1502) 8 Standard insulated base (8976)
4 Polyethylene bottle, 15 L (4 gal) (1367) 9 Standard insulated base for 21 L (5.5 gal) bottle
5 Polyethylene bottle, 19 L (5 gal) (6498)
(8561)
Install the first bottle for multiple sample collections
Use multiple bottles to collect samples into separate bottles or into more than one bottle. The distributor moves the sample tube above each bottle. Install the bottles in the sampler base as shown in Figure 4. Install the first sample bottle (number 1) below the label in the sampler base. Install the remaining bottles in increasing numbers in the direction shown by the label. Refer to Figure 5 on page 11 for a diagram of necessary components.
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English
Figure 4 Bottle number 1 installation
1 Bottle number 1 location (compact base) 6 Elastic straps
2 Bottle number 1 location for 24 bottles 7 Standard insulated base for 21 L (5.5 gal) bottle
3 Bottle number 1 location for 8 bottles 8 Standad insulated base
4 Bottle number 1 location for 2 or 4 bottles 9 Compact base
5 Retainer
Install multiple bottles
When multiple bottles are installed, a distributor arm moves the sample tube over each bottle. Sample collection automatically stops when the specified number of samples have been collected.
1. Clean the sample bottles. Refer to Clean the sample bottles on page
9.
2. Install the first sample bottle (number 1) below the label in the sampler base. Refer to Install the
first bottle for multiple sample collections
on page 9.
3. Assemble the sample bottles as shown in Figure 5. For eight or more bottles, make sure that the first bottle goes next to the bottle one indicator in the clockwise direction.
4. Put the bottle assembly in the sampler. For eight or more bottles, align the wires in the slots in the bottom tray.
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Figure 5 Multiple bottle installation
1 Positioner/retainer (2347) 8 Glass bottles, 3.8 L (1 gal), (4x) (2216) or
2 Retainer (1422) 9 Glass bottles, 1.9 L (0.5 gal), (8x) (1118) or
3 Retainer (2190) 10 Polyethylene bottles, 1 L (0.26 gal), (24x) (737)
4 Retainer (2189) 11 Glass bottles, 350 mL (11.83 oz), (24x) (732)
5 Glass bottles, 950 mL (32.12 oz) (8x) (2348) 12 Compact base (8975)
6 Polyethylene bottles, 575 mL (19.44 oz), (24x)
(1369)
7 Glass bottles, 3.8 L (1 gal), (2x) (2214) or
polyethylene bottles, 3.8 L (1 gal), (2x) (2215)
polyethylene bottles, 3.8 L (1 gal), (4x) (2217)
polyethylene bottles, 2.3 L (0.61 gal), (8x) (657)
13 Standard base (8976)
Plumb the sampler
Install the strainer in the middle of the sample stream (not near the surface or the bottom) to make sure that a representative sample is collected. Refer to Figure 6. Refer to Figure 7 for the intake tube installation.
1. Connect the tubing to the sampler as shown in Figure 7.
Note: Use connection kit 2186 if Teflon-lined tubing is used.
2. Install the intake tube and strainer in the main stream of the sample source where the water is turbulent and well-mixed.
• Make the intake tube as short as possible.
Keep the intake tube at a maximum vertical slope so that the tube drains completely between samples.
Note: If a vertical slope is not possible or if the tube is pressurized, disable the liquid sensor. Calibrate the sample volume manually. Refer to Calibrate the sample volume manually on page 28.
• Make sure that the intake tube is not pinched.
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Figure 6 Instrument installation
1 Strainer 3 Intake tube
2 Vertical lift
Figure 7 Intake tube installation

Electrical installation

Controller connections

W A R N I N G
Electrical shock hazard. Externally connected equipment must have an applicable country safety standard assessment.
Figure 8 shows the connections that can be made to the controller.
12 English
Figure 8 Controller connectors
1 Auxiliary device 4 SDI-12 device option
2 Power supply 5 Distributor/full bottle shut-off
3 Serial communications

Connect a flow meter

Connect a flow meter to the controller to start or stop the sampler when the sample flow goes above or below a specified value.
Items to collect:
• Multi-purpose full cable for Sigma flow meters (or 980 half cable for the model 980 flow meter).
Optional splitter for additional connections. Two or more splitters can be connected in series.
1. Connect one end of the cable to the flow meter. For the model 980 flow meter, refer to the model 980 flow meter user manual.
2. Connect the other end of the cable to the auxiliary device connector on the controller.
Note: If the flow meter has a 6-pin cable, use the 6-pin to 7-pin adapter cable.

Connect a PC or communications network

Connect a PC or a communications network to the controller to transfer data or to configure the sampler.
Items to collect:
• Serial cable, 7-pin RS232 to DB-9 (refer to Figure 9). Connections: B to 5 (signal ground); D to
3 (RCD); F to 2 (TXD); G (ground).
1. Connect one end of the serial cable to the communications device or network.
2. Connect the other end of the cable to the serial communications connector on the controller.
Figure 9 Serial communications cable
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