Hach-Lange POLYMETRON 9523 User Manual [en, ru, de, es, fr, it, pl]
DOC023.98.93065
Polymetron 9523 pH Calculator
11/2013, Edition 3
Basic User Manual
Manuale dell'utente di base
Manuel d'utilisation de base
Manual básico del usuario
Manual de operações básicas
Basisgebruikershandleiding
Podstawowa instrukcja obsługi
Начальное руководство пользователя
Basishandbuch
基本用户手册
Peruskäyttöohje
English..............................................................................................................................3
Deutsch..........................................................................................................................25
Italiano............................................................................................................................48
Français.........................................................................................................................71
Español..........................................................................................................................94
Português....................................................................................................................118
中文...............................................................................................................................141
Nederlands.................................................................................................................160
Polski............................................................................................................................184
Suomi............................................................................................................................207
Русский........................................................................................................................229
2
Table of contents
Specifications on page 3 Operation on page 18
General information on page 5 Maintenance on page 22
Installation on page 8
User interface and navigation on page 17
Additional information
Additional information is available on the manufacturer's website.
Specifications
Specifications are subject to change without notice.
Analyzer
Specification Details
Dimensions 748 x 250 x 236 mm (29.4 x 9.8 x 9.3 in.)
Weight 7 kg (15.4 lb)
Sample flow rate 5—20 liters/hour
Ambient temperature 0—60 °C (32—140 °F)
Relative humidity 10—90%
Temperature sensor Pt100
Accuracy ± 1% of displayed value; temperature < ± 0.2 °C
Calculated pH
Display range
Display resolution Conductivity/resistivity: automatic point drift (minimum resolution 0.001 μS/cm) < 0.1 °C
Sample tubing
Certifications EN 61326-1: 2006; EN 61010-1: 2010
Accuracy on conductivity measurement: ± 2%; Maximum difference calculated-theoretical
value: 0.1 pH
NH3; 7 < pH < 10; 2.8 μS/cm < C1 < 28 μS/cm; C2 < 0.5 μS/cm
NaOH; 7 < pH < 10.7; 2.5 μS/cm < C1 < 125 μS/cm; C2 < 100 μS/cm
Polyethylene or PTFE or FEP; 0.2 to 6 bars (3 to 90 psi); 5 to 50 °C (40 to 120 °F); Input:
6-mm (standard) or 1/4-inch (with adapter); Output: 12-mm or 1/2-inch
Sensor
Specification Details
Sensor body material Black PSU
Conductivity electrodes, internal and external Stainless steel 316L
Cell constant K 0.01 (cm-1)
Conductivity range 0.01—200 μS.cm-1; Resistivity range: 5k Ω.cm—100 MΩ.cm
Maximum pressure 10 bar
Maximum temperature 125 °C (257 °F)
Accuracy < 2%
English 3
Specification Details
Temperature response < 30 seconds
Insulator PSU
Connector Glass polyester (IP65)
Controller
Specification Details
Component description Microprocessor-controlled and menu-driven controller that operates the sensor and
Operating temperature -20 to 60 ºC (-4 to 140 ºF); 95% relative humidity, non-condensing with sensor load
Storage temperature -20 to 70 ºC (-4 to 158 ºF); 95% relative humidity, non-condensing
Enclosure
1
Power requirements AC powered controller: 100-240 VAC ±10%, 50/60 Hz; Power 50 VA with 7 W
Altitude requirements Standard 2000 m (6562 ft) ASL (Above Sea Level)
Pollution
degree/Installation
category
Outputs Two analog (0-20 mA or 4-20 mA) outputs. Each analog output can be assigned to
Relays Four SPDT, user-configured contacts, rated 250 VAC, 5 Amp resistive maximum for
Dimensions ½ DIN—144 x 144 x 180.9 mm (5.7 x 5.7 x 7.12 in.)
Weight 1.7 kg (3.75 lb)
Compliance information2CE approved (with all sensor types). Listed for use in general locations to UL and
Digital communication Optional Modbus, RS232/RS485, Profibus DPV1 or HART network connection for
Data logging Secure Digital Card (32 GB maximum) or special RS232 cable connector for data
Warranty 2 years
1
Units that have the Underwriters Laboratories (UL) certification are intended for indoor use only and do not
have a NEMA 4X/IP66 rating.
2
DC powered units are not listed by UL.
displays measured values.
<7 W; -20 to 50 ºC (-4 to 104 ºF) with sensor load <28 W
NEMA 4X/IP66 metal enclosure with a corrosion-resistant finish
sensor/network module load, 100 VA with 28 W sensor/network module load
(optional Modbus, RS232/RS485, Profibus DPV1 or HART network connection).
24 VDC powered controller: 24 VDC—15%, + 20%; Power 15 W with 7 W
sensor/network module load, 40 W with 28 W sensor/network module load (optional
Modbus, RS232/RS485, Profibus DPV1 or HART network connection).
Polution Degree 2; Installation Category II
represent a measured parameter such as pH, temperature, flow or calculated
values. Optional module supplies three additional analog outputs (5 total).
the AC powered controller and 24 VDC, 5A resistive maximum for the DC powered
controller. Relays are designed for connection to AC Mains circuits (i.e., whenever
the controller is operated with 115 - 240 VAC power) or DC circuits (i.e., whenever
the controller is operated with 24 VDC power).
CSA safety standards by ETL (with all sensor types).
Certain AC mains powered models are listed for use in general safety locations to
UL and CSA safety standards by Underwriters Laboratories (with all sensor types).
data transmission
logging and performing software updates. The controller will keep approximately
20,000 data points per sensor.
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English
General information
In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential
damages resulting from any defect or omission in this manual. The manufacturer reserves the right to
make changes in this manual and the products it describes at any time, without notice or obligation.
Revised editions are found on the manufacturer’s website.
Safety information
N O T I C E
The manufacturer is not responsible for any damages due to misapplication or misuse of this product including,
without limitation, direct, incidental and consequential damages, and disclaims such damages to the full extent
permitted under applicable law. The user is solely responsible to identify critical application risks and install
appropriate mechanisms to protect processes during a possible equipment malfunction.
Please read this entire manual before unpacking, setting up or operating this equipment. Pay
attention to all danger and caution statements. Failure to do so could result in serious injury to the
operator or damage to the equipment.
Make sure that the protection provided by this equipment is not impaired. Do not use or install this
equipment in any manner other than that specified in this manual.
Use of hazard information
Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.
Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious
injury.
Indicates a potentially hazardous situation that may result in minor or moderate injury.
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special
emphasis.
Precautionary labels
Read all labels and tags attached to the product. Personal injury or damage to the product could
occur if not observed. A symbol on the instrument is referenced in the manual with a precautionary
statement.
D A N G E R
W A R N I N G
C A U T I O N
N O T I C E
This symbol, when noted on a product, indicates a potential hazard which could cause serious
personal injury and/or death. The user should reference this instruction manual for operation and/or
safety information.
This symbol, when noted on a product enclosure or barrier, indicates that a risk of electrical shock
and/or electrocution exists and indicates that only individuals qualified to work with hazardous
voltages should open the enclosure or remove the barrier.
This symbol, when noted on the product, indicates the presence of devices sensitive to electrostatic
discharge and indicates that care must be taken to prevent damage to them.
This symbol, when noted on a product, indicates the instrument is connected to alternate current.
English 5
Electrical equipment marked with this symbol may not be disposed of in European public disposal
systems. In conformity with European local and national regulations, European electrical equipment
users must now return old or end-of-life equipment to the manufacturer for disposal at no charge to
the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return
end-of-life equipment, producer-supplied electrical accessories, and all auxiliary items for proper disposal.
Products marked with this symbol indicates that the product contains toxic or hazardous substances
or elements. The number inside the symbol indicates the environmental protection use period in
years.
Products marked with this symbol indicates that the product conforms to relevant South Korean
EMC standards.
EMC compliance statement (Korea)
Type of equipment Additional information
A 급 기기
( 업무용 방송통신기자재 )
Class A equipment
(Industrial Broadcasting and Communication
Equipment)
이 기기는 업무용 (A 급 ) 전자파적합기기로서 판매자 또
는 사용자는 이 점을 주의하시기 바라며, 가정외의 지역
에서 사용하는 것을 목적으로 합니다.
This equipment meets Industrial (Class A) EMC
requirements. This equipment is for use in industrial
environments only.
Certification
Canadian Radio Interference-Causing Equipment Regulation, IECS-003, Class A:
Supporting test records reside with the manufacturer.
This Class A digital apparatus meets all requirements of the Canadian Interference-Causing
Equipment Regulations.
FCC Part 15, Class "A" Limits
Supporting test records reside with the manufacturer. The device complies with Part 15 of the FCC
Rules. Operation is subject to the following conditions:
1. The equipment may not cause harmful interference.
2. The equipment must accept any interference received, including interference that may cause
undesired operation.
Changes or modifications to this equipment not expressly approved by the party responsible for
compliance could void the user's authority to operate the equipment. This equipment has been tested
and found to comply with the limits for a Class A digital device, pursuant to Part 15 of the FCC rules.
These limits are designed to provide reasonable protection against harmful interference when the
equipment is operated in a commercial environment. This equipment generates, uses and can
radiate radio frequency energy and, if not installed and used in accordance with the instruction
manual, may cause harmful interference to radio communications. Operation of this equipment in a
residential area is likely to cause harmful interference, in which case the user will be required to
correct the interference at their expense. The following techniques can be used to reduce
interference problems:
1. Disconnect the equipment from its power source to verify that it is or is not the source of the
interference.
2. If the equipment is connected to the same outlet as the device experiencing interference, connect
the equipment to a different outlet.
3. Move the equipment away from the device receiving the interference.
4. Reposition the receiving antenna for the device receiving the interference.
5. Try combinations of the above.
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English
Product components
Make sure that all components have been received. If any items are missing or damaged, contact the
manufacturer or a sales representative immediately.
Product overview
The analyzer measures conductivity and calculates the pH in low-conductivity applications. The
system can include the controller as shown in Figure 1 or the controller can be installed as an
external component.
The system can be configured to function in numerous applications in the following industry sectors:
• Measurement in pure and ultrapure water, power plants, semiconductor industry, pharmaceutical
• Drinking water
• Industrial processes (chemistry, paper mills, sugar refineries, etc.)
Figure 1 Analyzer overview
1 Mounting panel 6 Cationic resin cartridge
2 Controller 7 Sample output
3 Channel 1 conductivity probe 8 Sample input
4 Degassing valve 9 Measurement cell
5 Sample flow adjustment valve 10 Channel 2 conductivity probe
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Principle of operation (pH calculation)
The 9523 analyzer adheres to the recommendations contained in the guidelines for feedwaters,
boiler water and steam quality for power and industrial plants.
The pH calculations can only be applied under the following strict chemical conditions:
• The sample must only contain an alkaline agent (ammonia, sodium hydroxide or ethanolamine)
• Any impurity is principally NaCl (sodium chloride)
• The concentration of impurity must be negligible in comparison to the alkaline agent
Installation
C A U T I O N
Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the
document.
Analyzer mounting
Attach the analyzer to a stable, vertical surface. Refer to the guidelines that follow and Figure 2.
Note: If an external controller is used, refer to the controller documentation for mounting instructions.
• Put the instrument in a location that has access for operation, service and calibration.
• Make sure that there is good view of the display and controls.
• Keep the instrument away from a heat source.
• Keep the instrument away from vibrations.
• Keep the sample tubing as short as possible to minimize the response time.
• Make sure that there is no air in the sample supply line.
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Figure 2 Dimensions
Resin cartridge installation
Refer to the steps that follow and Figure 3 to install the resin cartridge.
1. Insert the steel tube into the quick lock connector.
2. Push the steel tube as far as possible into the measuring cell.
3. Take the resin cartridge and turn it upside down 2 or 3 times until the resin comes away from the
sides of the cartridge and settles at the bottom, at the opposite end to the marker line.
4. Unscrew the cap off the top of the cartridge, by the marker line. Discard this cap and the flat black
sealing cap following the safety and disposal information for used cartridges.
5. Place the end of the steel tube into the center of the cartridge.
6. Slowly raise the cartridge to the measuring cell and screw into place to obtain an airtight and
watertight fitting.
English
9
Figure 3 Resin cartridge installation
Wiring overview
Figure 4 shows an overview of the wiring connections inside the controller with the high voltage
barrier removed. The left side of the figure shows the back side of the controller cover.
Note: Remove connector caps from the connectors before module installation.
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English
Figure 4 Wiring connections overview
1 Service cable connection 5 AC and DC power connector
2 4-20 mA output
3 Sensor module connector 7 Relay connections
4 Communication module
connector (e.g., Modbus,
Profibus, HART, optional
4-20 mA module, etc.)
1
Terminals can be removed for improved access.
1
6 Ground terminals 10 Digital sensor connector
1
8 Digital sensor connector
1
9 Discrete input wiring connector
1
1
High-voltage barrier
High-voltage wiring for the controller is located behind the high-voltage barrier in the controller
enclosure. The barrier must remain in place except when installing modules or when a qualified
installation technician is wiring for power, alarms, outputs or relays. Do not remove the barrier while
power is applied to the controller.
Wiring for power
W A R N I N G
Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical
connections.
W A R N I N G
Potential Electrocution Hazard. If this equipment is used outdoors or in potentially wet locations, a
Ground Fault Interrupt device must be used for connecting the equipment to its mains power source.
1
English 11
D A N G E R
Electrocution Hazard. Do not connect AC power to a 24 VDC powered model.
W A R N I N G
Potential Electrocution Hazard. A protective earth (PE) ground connection is required for both
100-240 VAC and 24 VDC wiring applications. Failure to connect a good PE ground connection can
result in shock hazards and poor performance due to electromagnetic interferences. ALWAYS connect
a good PE ground to the controller terminal.
Install the device in a location and position that gives easy access to the disconnect device and its operation.
N O T I C E
The controller can be purchased as either a 100-240 VAC powered model or a 24 VDC powered
model. Follow the appropriate wiring instructions for the purchased model.
The controller can be wired for line power by hard-wiring in conduit or wiring to a power cord.
Regardless of the wire used, the connections are made at the same terminals. A local disconnect
designed to meet local electrical code is required and must be identified for all types of installation. In
hard-wired applications, the power and safety ground service drops for the instrument must be 18 to
12 AWG.
Notes:
• The voltage barrier must be removed before making any electrical connections. After making all
connections, replace the voltage barrier before closing the controller cover.
• A sealing type strain relief and a power cord less than 3 meters (10 feet) in length with three 18gauge conductors (including a safety ground wire) can be used to maintain the NEMA
4X/IP66 environmental rating.
• Controllers can be ordered with AC power cords pre-installed. Additional power cords may also be
ordered.
• The DC power source that supplies power to the 24 VDC powered controller must maintain
voltage regulation within the specified 24 VDC-15% +20% voltage limits. The DC power source
must also provide adequate protection against surges and line transients.
Wiring procedure
Refer to the illustrated steps that follow and Table 1 or Table 2 to wire the controller for power. Insert
each wire into the appropriate terminal until the insulation is seated against the connector with no
bare wire exposed. Tug gently after insertion to make sure that there is a secure connection. Seal
any unused openings in the controller box with conduit opening sealing plugs.
Table 1 AC power wiring information (AC powered models only)
Terminal Description Color—North America Color—EU
1 Hot (L1) Black Brown
2 Neutral (N) White Blue
— Protective Earth (PE) Ground lug Green Green with yellow stripe
Table 2 DC power wiring information (DC powered models only)
Terminal Description Color—North America Color—EU
1 +24 VDC Red Red
2 24 VDC return Black Black
— Protective Earth (PE) Ground lug Green Green with yellow stripe
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Alarms and relays
The controller is equipped with four unpowered, single pole relays rated 100-250 VAC, 50/60 Hz,
5 amp resistive maximum. Contacts are rated 250 VAC, 5 amp resistive maximum for the AC
English
13
powered controller and 24 VDC, 5A resistive maximum for the DC powered controller. The relays are
not rated for inductive loads.
Wiring relays
W A R N I N G
Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical
connections.
W A R N I N G
Potential fire hazard. The relay contacts are rated 5A and are not fused. External loads connected to
the relays must have current limiting devices provided to limit current to < 5 A.
W A R N I N G
Potential fire hazard. Do not daisy-chain the common relay connections or jumper wire from the mains
power connection inside the instrument.
W A R N I N G
Potential electrocution hazard. In order to maintain the NEMA/IP environmental ratings of the
enclosure, use only conduit fittings and cable glands rated for at least NEMA 4X/IP66 to route cables in
to the instrument.
AC line (100—250 V) powered controllers
Potential electrocution hazard. AC mains powered controllers (115 V–230 V) are designed for relay
connections to AC mains circuits (i.e., voltages greater than 16 V-RMS, 22.6 V-PEAK or 35 VDC).
The wiring compartment is not designed for voltage connections in excess of 250 VAC.
24 VDC powered controllers
Potential electrocution hazard. 24 V powered controllers are designed for relay connections to low
voltage circuits (i.e., voltages less than 16 V-RMS, 22.6 V-PEAK or 35 VDC).
W A R N I N G
W A R N I N G
The 24 VDC controller relays are designed for the connection to low voltage circuits (i.e., voltages
less than 30 V-RMS, 42.2 V-PEAK or 60 VDC). The wiring compartment is not designed for voltage
connections above these levels.
The relay connector accepts 18–12 AWG wire (as determined by load application). Wire gauge less
than 18 AWG is not recommended.
The Normally Open (NO) and Common (COM) relay contacts will be connected when an alarm or
other condition is active. The Normally Closed (NC) and Common relay contacts will be connected
when an alarm or other condition is inactive (unless the Fail Safe is set to Yes) or when power is
removed from the controller.
Most relay connections use either the NO and COM terminals or the NC and COM terminals. The
numbered installation steps show connection to the NO and COM terminals.
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English
English 15
Analog output connections
W A R N I N G
Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical
connections.
W A R N I N G
Potential electrocution hazard. In order to maintain the NEMA/IP environmental ratings of the
enclosure, use only conduit fittings and cable glands rated for at least NEMA 4X/IP66 to route cables in
to the instrument.
Two isolated analog outputs (1 and 2) are provided (Figure 5). Such outputs are commonly used for
analog signaling or to control other external devices.
Make wiring connections to the controller as shown in Figure 5 and Table 3.
Note: Figure 5 shows the back of the controller cover and not the inside of the main controller compartment.
Table 3 Output connections
Recorder wires Circuit board position
Output 2– 4
Output 2+ 3
Output 1– 2
Output 1+ 1
1. Open the controller cover.
2. Feed the wires through the strain relief.
3. Adjust the wire as necessary and tighten the strain relief.
4. Make connections with twisted-pair shielded wire and connect the shield at the controlled
component end or at the control loop end.
• Do not connect the shield at both ends of the cable.
• Use of non-shielded cable may result in radio frequency emission or susceptibility levels higher
than allowed.
• Maximum loop resistance is 500 ohm.
5. Close the controller cover and tighten the cover screws.
6. Configure outputs in the controller.
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English
Figure 5 Analog output connections
Connect the optional digital communication output
The manufacturer supports Modbus RS485, Modbus RS232, Profibus DPV1 and HART
communication protocols. The optional digital output module is installed in the location indicated by
item 4 in Figure 4 on page 11. Refer to the instructions supplied with the network module for more
details.
For information about Modbus registers, go to http://www.hach-lange.com or http://www.hach.com
and search Modbus registers or go to any sc200 product page.
Plumb the sample and drain lines
After the panel is attached to a wall, connect the sample and drain lines to the fittings on the panel.
Make sure that the tubing meets the Specifications on page 3. Refer to the steps that follow and
Figure 1 on page 7.
1. Insert the sample tubing into the input quick-connect fitting under the flow chamber (Figure 1
on page 7).
2. Connect a drain line to sample output fitting. Keep the drain line as short as possible to prevent
back-pressure.
Analyzer startup
1. Open the degassing valve.
2. Open the sample flow adjustment valve and ensure everything is watertight and there are no
leaks.
3. Close the degassing valve when the measuring cell is free of air.
4. Set the sample flow to the required rate (between 5 and 20 L/h).
5. Pass about 10 liters of sample through the resin to thoroughly rinse it and prepare the analyzer
for measurements.
User interface and navigation
User interface
The keypad has four menu keys and four directional keys as shown in Figure 6.
English
17
Figure 6 Keypad and front panel overview
1 Instrument display 5 BACK key. Moves back one level in the menu
2 Cover for secure digital memory card slot 6 MENU key. Moves to the Settings Menu from other
3 HOME key. Moves to the Main Measurement
screen from other screens and submenus.
4 ENTER key. Accepts input values, updates, or
displayed menu options.
structure.
screens and submenus.
7 Directional keys. Used to navigate through the
menus, change settings, and increment or
decrement digits.
Inputs and outputs are set up and configured through the front panel using the keypad and display
screen. This user interface is used to set up and configure inputs and outputs, create log information
and calculated values, and calibrate sensors. The SD interface can be used to save logs and update
software.
Operation
Contacting conductivity sensor configuration
Use the CONFIGURE menu to enter identification information for the sensor and to change options
for data handling and storage.
1. Push the menu key and select SENSOR SETUP>[Select Sensor]>CONFIGURE.
2. Select an option and push enter. To enter numbers, characters or punctuation, push and hold the
up or down arrow keys. Push the right arrow key to advance to the next space.
Option Description
EDIT NAME Changes the name that corresponds to the sensor on the top of the measure screen.
SENSOR S/N Allows the user to enter the serial number of the sensor, limited to 16 characters in any
SELECT MEASURE Changes the measured parameter to CONDUCTIVITY (default), TDS (total dissolved
The name is limited to 16 characters in any combination of letters, numbers, spaces or
punctuation. Only the first 12 characters are displayed on the controller.
combination of letters, numbers, spaces or punctuation.
solids), SALINITY or RESISTIVITY. All other configured settings are reset to the
default values.
Note: If SALINITY is selected, the measurement unit is defined as ppt (parts per
thousand) and cannot be changed.
18 English
Option Description
DISPLAY FORMAT Changes the number of decimal places that are shown on the measure screen. When
MEAS UNITS Changes the units for the selected measurement—select the unit from the list
TEMP UNITS Sets the temperature units to °C (default) or °F.
T-COMPENSATION Adds a temperature-dependent correction to the measured value:
set to auto, the number of decimal places changes automatically with changes in the
measured value.
available.
• NONE—Temperature compensation not required
• USP—Set the alarm level for the standard USP definition table
• ULTRA PURE WATER—Not available for TDS. Set the compensation type
according to the sample characteristics—Select NaCl , HCl, AMMONIA or ULTRA
PURE WATER
• USER—Select BUILT IN LINEAR, LINEAR or TEMP TABLE:
• BUILT IN LINEAR—Use the pre-defined linear table (slope defined as 2.0%/°C,
reference temperature as 25 °C)
• LINEAR—Set the slope and reference temperature parameters if different from
the built-in parameters
• TEMP TABLE—Set the temperature and multiplication factor points (refer to the
conductivity module documentation)
• NATURAL WATER—Not available for TDS
CONFIG TDS TDS only—changes the factor that is used to convert conductivity to TDS: NaCl
CABLE PARAM Sets the sensor cable parameters to improve measurement accuracy when the sensor
TEMP ELEMENT Sets the temperature element to PT100 or PT1000 for automatic temperature
FILTER Sets a time constant to increase signal stability. The time constant calculates the
LOG SETUP Sets the time interval for data storage in the data log—5, 30 seconds, 1, 2, 5, 10,
RESET DEFAULTS Sets the configuration menu to the default settings. All sensor information is lost.
(0.49 ppm/µS) or CUSTOM (enter factor between 0.01 and 99.99 ppm/µS).
cable is extended or shortened from the standard 5 m. Enter the cable length,
resistance and capacitance.
compensation. If no element is used, the type can be set to MANUAL and a value for
temperature compensation can be entered.
average value during a specified time—0 (no effect) to 60 seconds (average of signal
value for 60 seconds). The filter increases the time for the sensor signal to respond to
actual changes in the process.
15 (default), 30, 60 minutes.
Resin option
Use the RESIN option to view and change the parameters related to the resin cartridge. These
parameters must be defined before the analyzer is used for the first time.
1. Push the menu key and select TEST/MAINT>RESIN.
2. To monitor the status of the resin select the TRACK option and push enter.
Option Description
YES Monitor the resin status. When the life expectancy of the resin is less than 10 days a warning
message is triggered. When the life expectancy reaches 0 days a system error is triggered.
NO The resin is not monitored.
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3. To view the current status of the resin select the STATUS option and push enter. The date the
resin was last changed and the current life expectancy are displayed. Push back to return to the
menu or enter to reset the parameters.
4. To reset the resin parameters select PARAMETERS and push enter. Based on the values input,
the life expectancy of the resin is recalculated.
Option Description
CAPACITY Use the arrow keys to enter the resin exchange capacity (0.5 to 5.0 mole/liter).
VOLUME Use the arrow keys to enter the volume of resin (0.5 to 20 liters).
FLOW Use the arrow keys to enter the sample flow rate through the cartridge (2 to
CONCENTRATION Use the arrow keys to enter the resin concentration (0 to 20 ppm).
20 liters/hour).
Calibration
About sensor calibration
The sensor characteristics slowly shift over time and cause the sensor to lose accuracy. The sensor
must be calibrated regularly to maintain accuracy. The calibration frequency varies with the
application and is best determined by experience.
Use air (zero calibration) and the process sample to define the calibration curve. When the process
sample is used, the reference value must be determined with a secondary verification instrument.
Cell constant
Before making a calibration make sure the sensor cell parameters are correct.
1. Push the menu key and select SENSOR SETUP>[Select Sensor]>CALIBRATE.
2. If the pass code is enabled in the security menu for the controller, enter the pass code.
3. Select CELL CONSTANT and push enter.
4. Contacting conductivity sensors: Select the cell K range for the sensor (0.01, 0.1 or 1.0) then
enter the actual K value as printed on the label attached to the sensor.
Inductive conductivity sensors: Enter the actual K value as printed on the label attached to the
sensor.
Temperature calibration
It is recommended to calibrate the temperature sensor once a year. Calibrate the temperature sensor
before calibrating the measurement sensor.
1. Measure the temperature of the water with an accurate thermometer or independent instrument.
2. Push the menu key and select SENSOR SETUP>CALIBRATE.
3. If the pass code is enabled in the security menu for the controller, enter the pass code.
4. Select 1 PT TEMP CAL and push enter.
5. The raw temperature value is displayed. Push enter.
6. Enter the correct value if different from that displayed and push enter.
7. Push enter to confirm the calibration. The temperature offset is displayed.
Zero calibration procedure
Use the zero calibration procedure to define the unique zero point of the sensor.
1. Remove the sensor from the process. Wipe with a clean towel to make sure the sensor is dry.
2. Push the menu key and select SENSOR SETUP>[Select Sensor]>CALIBRATE.
3. If the pass code is enabled in the security menu for the controller, enter the pass code.
4. Select ZERO CAL and push enter.
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English
5. Select the option for the output signal during calibration:
Option Description
ACTIVE The instrument sends the current measured output value during the calibration procedure.
HOLD The sensor output value is held at the current measured value during the calibration procedure.
TRANSFER A preset output value is sent during calibration. Refer to the controller user manual to change
the preset value.
6. Place the sensor in air, push enter.
7. Review the calibration result:
• PASS—the sensor is calibrated and ready to measure samples.
• FAIL—the calibration is outside of accepted limits. Clean the sensor and retry. Refer to
Troubleshooting on page 24 for more information.
8. If the calibration passed, push enter to continue.
9. If the option for operator ID is set to YES in the CAL OPTIONS menu, enter an operator ID. Refer
to Change calibration options on page 22.
10. On the NEW SENSOR screen, select whether the sensor is new:
Option Description
YES The sensor was not calibrated previously with this controller. The days of operation and previous
calibration curves for the sensor are reset.
NO The sensor was calibrated previously with this controller.
11. Return the sensor to the process and push enter. The output signal returns to the active state
and the measured sample value is shown on the measure screen.
Note: If the output mode is set to hold or transfer, select the delay time when the outputs return to the active
state.
Calibration with the process sample
The sensor can remain in the process sample.
1. Push the menu key and select SENSOR SETUP>CALIBRATE.
2. If the pass code is enabled in the security menu for the controller, enter the pass code.
3. Select SAMPLE CAL and push enter.
4. Select the option for the output signal during calibration:
Option Description
ACTIVE The instrument sends the current measured output value during the calibration procedure.
HOLD The sensor output value is held at the current measured value during the calibration procedure.
TRANSFER A preset output value is sent during calibration. Refer to the controller user manual to change
the preset value.
5. With the sensor in the process sample, push enter. The measured value is shown. Wait for the
value to stabilize and push enter.
6. With a certified secondary verification instrument measure the concentration value of the sample.
To avoid impurities in the sample take the measurement before the sample enters the flow
chamber. Use the arrow keys to enter this value if different from the value displayed and push
enter.
7. Review the calibration result:
• PASS—the sensor is calibrated and the calibration factor is displayed.
• FAIL—the calibration is outside of accepted limits. Clean the sensor and retry. Refer to
Troubleshooting on page 24 for more information.
English
21
8. If the calibration passed, push enter to continue.
9. If the option for operator ID is set to YES in the CAL OPTIONS menu, enter an operator ID. Refer
to Change calibration options on page 22.
10. On the NEW SENSOR screen, select whether the sensor is new:
Option Description
YES The sensor was not calibrated previously with this controller. The days of operation and previous
calibration curves for the sensor are reset.
NO The sensor was calibrated previously with this controller.
11. With the sensor still in the process push enter. The output signal returns to the active state and
the measured sample value is shown on the measure screen.
Note: If the output mode is set to hold or transfer, select the delay time when the outputs return to the active
state.
Change calibration options
The user can set a calibration reminder or include an operator ID with calibration data from this
menu.
1. Push the menu key and select SENSOR SETUP>[Select Sensor]>CALIBRATE.
2. If the pass code is enabled in the security menu for the controller, enter the pass code.
3. Select CAL OPTIONS and push enter.
4. Use the arrow keys to select an option and push enter.
Option Description
CAL REMINDER Sets a reminder for the next calibration in days, months or years—select the required
OP ID ON CAL Includes an operator ID with calibration data—YES or NO (default). The ID is entered
delay from the list.
during the calibration.
Maintenance
D A N G E R
Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document.
Service schedule
The following table shows the recommended service schedule:
Validation (check with referenced measure) X X X X
Calibration (measure) X X
Calibration (temperature) X
22 English
Every 3 Months Every 6 Months Yearly As Needed
Cleaning the controller
D A N G E R
Always remove power from the controller before performing maintenance activities.
Note: Never use flammable or corrosive solvents to clean any part of the controller. Use of these solvents may
degrade the environmental protection of the unit and may void the warranty.
1. Make sure the controller cover is securely closed.
2. Wipe the controller exterior with a cloth dampened with water, or with a mixture of water and mild
detergent.
Replace the resin
C A U T I O N
Chemical exposure hazard. Dispose of chemicals and wastes in accordance with local, regional and
national regulations.
The cartridge of resin can be replaced with a new cartridge, or as an alternative, keep the cartridge
and replace only the resin. In order to take advantage of the full system specifications, we
recommend the use of nuclear grade cationic resin.
1. Stop the sample flow using the sample flow adjustment valve.
2. Replace the cartridge or resin:
• Cartridge—refer to Resin cartridge installation on page 9.
• Resin—refer to Figure 7. Make sure to add deionized water at regular intervals when new resin
is added to compact the resin.
3. Open the degassing valve.
4. Open the sample flow adjustment valve and ensure everything is watertight and there are no
leaks.
5. Close the degassing valve when the measuring cell is free of air.
6. Set the sample flow to the required rate (between 5 and 20 L/h).
7. Reset the resin options. Refer to Resin option on page 19.
English
23
Figure 7 Resin replacement
Troubleshooting
Additional information
Additional information is available on the manufacturer's website.
24
English
Inhaltsverzeichnis
Spezifikationen auf Seite 25 Betrieb auf Seite 41
Allgemeine Informationen auf Seite 27 Wartung auf Seite 46
Installation auf Seite 31
Benutzeroberfläche und Navigation auf Seite 41
Zusätzliche Informationen
Zusätzliche Informationen finden Sie auf der Website des Herstellers.
Spezifikationen
Die Spezifikationen können ohne Vorankündigung Änderungen unterliegen.
Analysator
Spezifikation Details
Abmessungen 748 x 250 x 236 mm (29.4 x 9.8 x 9.3 Zoll)
Gewicht 7 kg / 15.4 lb
Probenflussrate 5—20 l/h
Umgebungstemperatur 0—60 °C (32—140 °F)
Relative Feuchtigkeit 10—90%
Temperatursensor Pt 100
Genauigkeit ± 1% des angezeigten Werts; Temperatur < ± 0,2°C
Berechneter pH-Wert
Anzeigebereich
Anzeigeauflösung
Probenleitung
Zertifikationen EN 61326-1: 2006; EN 61010-1: 2010
Genauigkeit der Leitfähigkeitsmessung: ±2 %; Maximale Abweichung von´m
errechneten theoretischen Wert: 0,1 pH
NH3; 7 < pH < 10; 2,8 μS/cm < C1 < 28 μS/cm; C2 < 0,5 μS/cm
NaOH; 7 < pH < 10,7; 2,5 μS/cm < C1 < 125 μS/cm; C2 < 100 μS/cm
Leitfähigkeit/Resistivität; automatische Punktverschiebung (Mindestauflösung
0,001 μS/cm) < 0,1 °C
Polyethylen oder PTFE oder FEP; 0,2 bis 6 bar (3 bis 90 psi); 5 bis 50 °C; Eingang:
6 mm (Standard) oder 1/4 Zoll (mit Adapter); Ausgang: 12 mm oder 1/2 Zoll
Sensor
Spezifikation Details
Material des Sensorgehäuses PSU schwarz
Leitfähigkeitselektroden, intern und extern Edelstahl 316L
Zellkonstante K 0,01 (cm-1)
Leitfähigkeitsbereich 0,01 - 200 μS.cm-1; Resistivitätsbereich: 5 kΩ.cm - 100 MΩ.cm
Max. Druck 10 bar
Max. Temperatur 125 °C (257 °F)
Genauigkeit < 2%
Deutsch 25
Spezifikation Details
Temperaturverhalten < 30 Sekunden
Isoliermaterial PSU
Stecker Glas Polyester (IP65)
Controller
Technische Daten Details
Beschreibung der Komponenten Mikroprozessor- und menügesteuerter Controller, der Sensoren
Betriebstemperatur –20 bis 60 °C (–4 bis 140 °F); 95 % relative Luftfeuchtigkeit, nicht
Lagertemperatur –20 bis 70 ºC (-4 bis 158 ºF); 95 % relative Luftfeuchtigkeit, nicht
1
Gehäuse
Stromversorgung Controller mit Wechselspannungsversorgung:100-240 V~ ±10 %,
Aufstellungshöhe Standardmäßig 2000 m ü. M. (über Meeresspiegel)
Verschmutzungsgrad/Einbaukategorie Verschmutzungsgrad 2; Einbaukategorie II
Ausgänge Zwei Analogausgänge (0-20 mA oder 4-20 mA). Jeder analoge Ausgang
Relais Für SPDT, benutzerkonfigurierte Kontakte, mit folgenden Nennwerten:
Abmessungen ½ DIN—144 x 144 x 180,9 mm (5,7 x 5,7 x 7.12 Zoll)
Gewicht 1.7 kg (3.75 lbs)
Einhaltungsinformationen
2
Digitale Kommunikation Optionaler Modbus-, RS232/RS485-, Profibus DPV1- oder HART-
ansteuert und Messwerte anzeigt.
kondensierend mit Sensorleistung <7 W; –20 bis 50 °C (–4 bis 104 °F)
mit Sensorleistung <28 W
kondensierend
Metallgehäuse, Schutzart NEMA 4X/IP66, mit korrosionsbeständiger
Oberfläche
50/60 Hz; Leistung 50 VA bei Sensor-/Netzwerkmodullast von 7 W,
100 VA bei Sensor-/Netzwerkmodullast von 28 W (Modbus-,
RS232/RS485-, Profibus DPV1- oder HART-Netzwerkverbindung
optional).
Controller mit 24-Volt-Gleichstromversorgung:24 V= -15 % + 20 %;
Leistung 15 W bei Sensor-/Netzwerkmodullast von 7 W, 40 W bei
Sensor-/Netzwerkmodullast von 28 W (Modbus-, RS232/RS485-,
Profibus DPV1- oder HART-Netzwerkverbindung optional).
lässt sich Messgrößen wie pH, Temperatur, Durchfluss oder
berechneten Werten zuordnen. Das optionale Modul wendet drei
zusätzliche analoge Ausgänge an (insgesamt 5).
250 V~, max. Schaltlast 5 A bei wechselstrombetriebenen Controllern
bzw. 24 V=, max. Schaltlast 5 A bei gleichstrom betriebenen Controllern.
Relais sind für den Anschluss an das Stromnetz (bei Betrieb des
Controllers mit 115 - 240 V~) oder eine Gleichspannungsversorgung (bei
Betrieb des Controllers mit 24 V=) ausgelegt.
CE-Zulassung (alle Sensortypen). UL- und CSA-Zulassung für den
Einsatz an allgemeinen Aufstellungsorten durch ETL (alle Sensortypen).
Bestimmte Modelle mit Anschluss an das Stromnetz werden für den
Einsatz an allgemeinen Sicherheitsstandorten mit UL- und CSAZulassung von Underwriter Laboratories aufgeführt (alle Sensortypen).
Netzwerkanschluss für die Datenübertragung
26 Deutsch
Technische Daten Details
Datenprotokollierung Secure Digital-Speicherkarte (maximal 32 GB) oder spezieller RS(232-
Gewährleistung 2 Jahre
1
Geräte mit einer Zertifizierung von Underwriters Laboratories (UL) eignen sich nur zur Verwendung in
geschlossenen Räumen und verfügen nicht über die Schutzart NEMA 4X/IP66.
2
Geräte mit Gleichstromversorgung werden nicht von UL aufgeführt.
Kabelanschluss für Datenprotokollierung und Software-Updates. Der
Controller speichert ca. 20.000 Datenpunkte pro Sensor.
Allgemeine Informationen
Der Hersteller ist nicht verantwortlich für direkte, indirekte, versehentliche oder Folgeschäden, die
aus Fehlern oder Unterlassungen in diesem Handbuch entstanden. Der Hersteller behält sich
jederzeit und ohne vorherige Ankündigung oder Verpflichtung das Recht auf Verbesserungen an
diesem Handbuch und den hierin beschriebenen Produkten vor. Überarbeitete Ausgaben der
Bedienungsanleitung sind auf der Hersteller-Webseite erhältlich.
Sicherheitshinweise
H I N W E I S
Der Hersteller ist nicht für Schäden verantwortlich, die durch Fehlanwendung oder Missbrauch dieses Produkts
entstehen, einschließlich, aber ohne Beschränkung auf direkte, zufällige oder Folgeschäden, und lehnt jegliche
Haftung im gesetzlich zulässigen Umfang ab. Der Benutzer ist selbst dafür verantwortlich, schwerwiegende
Anwendungsrisiken zu erkennen und erforderliche Maßnahmen durchzuführen, um die Prozesse im Fall von
möglichen Gerätefehlern zu schützen.
Bitte lesen Sie dieses Handbuch komplett durch, bevor Sie dieses Gerät auspacken, aufstellen oder
bedienen. Beachten Sie alle Gefahren- und Warnhinweise. Nichtbeachtung kann zu schweren
Verletzungen des Bedieners oder Schäden am Gerät führen.
Stellen Sie sicher, dass die durch dieses Messgerät bereitgestellte Sicherheit nicht beeinträchtigt
wird. Verwenden bzw. installieren Sie das Messsystem nur wie in diesem Handbuch beschrieben.
Bedeutung von Gefahrenhinweisen
Kennzeichnet eine mögliche oder drohende Gefahrensituation, die, wenn sie nicht vermieden wird, zum Tod oder
zu schweren Verletzungen führt.
G E F A H R
W A R N U N G
Kennzeichnet eine mögliche oder drohende Gefahrensituation, die, wenn sie nicht vermieden wird, zum Tod oder
zu schweren Verletzungen führen kann.
Kennzeichnet eine mögliche Gefahrensituation, die zu geringeren oder moderaten Verletzungen führen kann.
Kennzeichnet eine Situation, die, wenn sie nicht vermieden wird, das Gerät beschädigen kann. Informationen, die
besonders beachtet werden müssen.
V O R S I C H T
H I N W E I S
Deutsch 27
Warnaufkleber
Bitte lesen Sie alle Aufkleber und Schilder, die am Produkt angebracht sind. Die Nichtbeachtung
kann zu Verletzungen von Personen oder Beschädigungen des Produkts führen. Im Handbuch
werden auf die am Gerät angebrachten Symbole in Form von Warnhinweisen verwiesen.
Dieses Symbol auf einem Produkt zeigt eine potenzielle Gefahr an, die zu ernsthaften Verletzungen
und/oder zum Tod führen kann. Der Benutzer soll dieses Handbuch bei der Bedienung des Geräts
und/oder für Sicherheitsinformationen verwenden.
Dieses Symbol auf einer Verkleidung oder Schranke des Produkts weist auf die Gefahr von
Stromschlägen hin und macht darauf aufmerksam, dass ausschließlich für die Arbeit mit
gefährlichen Spannungen qualifiziertes Personal die Verkleidung öffnen oder die Schranke
entfernen sollte.
Dieses Symbol auf dem Produkt weist auf das Vorhandensein von Bauteilen hin, die durch
elektrostatische Entladungen gestört werden können und macht darauf aufmerksam, dass mit
Vorsicht vorgegangen werden muss, um Schäden an diesen Bauteilen zu vermeiden.
Dieses Symbol weist darauf hin, dass das Instrument an Wechselstrom angeschlossen werden
muss.
Elektrogeräte, die mit diesem Symbol gekennzeichnet sind, dürfen in der Europäischen Union nicht
als Haushaltsabfall entsorgt werden. Den lokalen und nationalen europäischen Bestimmungen
gemäß müssen Benutzer von Elektrogeräten diese jetzt an den Hersteller zurückgeben. Dieser
Rücknahmeservice ist für den Benutzer kostenlos.
Hinweis: Bitte wenden Sie sich für Anweisungen zur Rücklieferung für die ordnungsgemäße Entsorgung von alten
oder nicht mehr benutzten elektrischen Geräten an den Hersteller oder Händler.
Produkte, die mit diesem Symbol gekennzeichnet sind, enthalten toxische oder gefährliche
Substanzen oder Elemente. Die Ziffer in diesem Symbol gibt den Umweltschutzzeitraum in Jahren
an.
Produkte, die mit diesem Symbol gekennzeichnet sind, entsprechen den EMV-Standards
Südkoreas.
EMV-Konformitätserklärung (Korea)
Gerätetyp Zusätzliche Informationen
A 급 기기
( 업무용 방송통신기자재 )
Geräteklasse A
(Industrielle Übertragungs- und Kommunikationsgeräte)
이 기기는 업무용 (A 급 ) 전자파적합기기로서 판매자 또
는 사용자는 이 점을 주의하시기 바라며, 가정외의 지역
에서 사용하는 것을 목적으로 합니다.
Dieses Gerät ist mit den Anforderungen der EMVRichtliniene für industrielle Geräte (Klasse A) konform.
Dieses Gerät ist ausschließlich für den industriellen
Gebrauch bestimmt.
Zertifizierungen
Kanadische Vorschriften zu Störungen verursachenden Einrichtungen, IECS-003, Klasse A:
Entsprechende Prüfprotokolle hält der Hersteller bereit.
Dieses digitale Gerät der Klasse A erfüllt alle Vorgaben der kanadischen Normen für Interferenz
verursachende Geräte.
FCC Teil 15, Beschränkungen der Klasse "A"
Entsprechende Prüfprotokolle hält der Hersteller bereit. Das Gerät entspricht Teil 15 der FVVVorschriften. Der Betrieb unterliegt den folgenden Bedingungen:
1. Das Gerät darf keine Störungen verursachen.
2. Das Gerät muss jegliche Störung, die es erhält, einschließlich jener Störungen, die zu
unerwünschtem Betrieb führen, annehmen.
28
Deutsch
Änderungen oder Modifizierungen an diesem Gerät, die nicht ausdrücklich durch die für die
Einhaltung der Standards verantwortliche Stelle bestätigt wurden, können zur Aufhebung der
Nutzungsberechtigung für des Geräts führen. Dieses Gerät wurde geprüft, und es wurde festgestellt,
dass es die Grenzwerte für digitale Geräte der Klasse A entsprechend Teil 15 der FCC-Vorschriften
einhält. Diese Grenzwerte bieten beim Einsatz der Ausrüstung in gewerblichen Umgebungen einen
ausreichenden Schutz gegen Verletzungen. Dieses Gerät erzeugt und nutzt hochfrequente Energie
und kann diese auch abstrahlen, und es kann, wenn es nicht in Übereinstimmung mit der
Bedienungsanleitung installiert und eingesetzt wird, schädliche Störungen der Funkkommunikation
verursachen. Der Betrieb dieses Geräts in Wohngebieten kann schädliche Störungen verursachen.
In diesem Fall muss der Benutzer die Störungen auf eigene Kosten beseitigen. Probleme mit
Interferenzen lassen sich durch folgende Methoden mindern:
1. Trennen Sie das Gerät von der Stromversorgung, um sicherzugehen, dass dieser die Störungen
nicht selbst verursacht.
2. Wenn das Gerät an die gleiche Steckdose angeschlossen ist wie das gestörte Gerät, schließen
Sie das störende Gerät an eine andere Steckdose an.
3. Vergrößern Sie den Abstand zwischen diesem Gerät und dem gestörten Gerät.
4. Ändern Sie die Position der Empfangsantenne des gestörten Geräts.
5. Versuchen Sie auch, die beschriebenen Maßnahmen miteinander zu kombinieren.
Produktkomponenten
Stellen Sie sicher, dass Sie alle Teile erhalten haben. Wenn Komponenten fehlen oder beschädigt
sind, kontaktieren Sie bitte den Hersteller oder Verkäufer.
Produktübersicht
Der Analysator misst Leitfähigkeit und berechnet den pH-Wert in Anwendungen mit geringer
Leitfähigkeit. Das System kann einen Controller wie in Abbildung 1 gezeigt umfassen. Alternativ kann
der Controller als externe Komponente installiert werden.
Das System kann für den Betrieb in zahlreichen Anwendungen in den folgenden Branchen
konfiguriert werden:
• Messung in Rein- und Reinstwasser, Kraftwerken, Halbleiterindustrie, pharmazeutische Industrie.
• Trinkwasser
• industrielle Prozesse (chemische Industrie, Papierfabriken, Zuckerraffinerien usw.)
Deutsch
29
Abbildung 1 Übersicht über den Analysator
1 Montagepaneel 6 Patrone kationisches Harz
2 Controller 7 Probenauslass
3 Kanal 1 Sonde Leitfähigkeit 8 Probeneinlass
4 Entlüftungsventil 9 Messzelle
5 Probenflusseinstellventil 10 Kanal 2 Sonde Leitfähigkeit
Betriebsweise (pH-Wertberechnung)
Der Analysator 9523 entspricht den Empfehlungen der Richtlinien für Speisewasser, Boilerwasser
und Dampfqualität für Kraftwerke und Industrieanlagen.
Die pH-Wertberechnung kann nur unter den folgenden strengen chemischen Bedingungen erfolgen:
• Die Probe darf ausschließlich alkaline Arbeitsstoffe (Ammoniak, Natriumhydroxid oder
Äthanolamin) enthalten.
• Bei eventuellen Verunreinigungen handelt es sich überwiegend um NaCl (Natriumchlorid).
• Die Konzentration der Verunreinigung muss im Vergleich zu dem alkalinen Arbeitsstoff
vernachlässigbar sein
30
Deutsch
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