Hach-Lange POLYMETRON 8398 User Manual

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Document Number 221=183=098

POLYMETRON Model 8398

Inductive probe

USER MANUAL

April 2010, Version D

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Restriction of hazardous substances (RoHS)

The European Union RoHS Directive and subsequent regulations introduced in member states and other countries limits the use of six hazardous substances used in the manufacturing of electrical and electronic equipment.

Currently, monitoring and control instruments do not fall within the scope of the RoHS Directive, however Hach Lange has taken the decision to adopt the recommendations in the Directive as the target for all future product design and component purchasing.

Note: The following only applies to exports of this product into the People’s Republic of China.

Conductivity plastic sensor (8310, 8311, 8312)

Conductivity stainless steel sensor (8314, 8394)

Digital sensor PCB O O

Glass electrode O O

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Inductive Probe 8398

Table of contents

1. INTRODUCTION................................................................................................ 3

1.1 General ....................................................................................................................3

1.2 Probes...................................................................................................................... 3

2. OPERATING PRINCIPLE.................................................................................. 4

2.1 Conductivity reminder ..............................................................................................4

2.2 Principle of inductive technology.............................................................................. 5

3. TECHNICAL SPECIFICATIONS ....................................................................... 6

3.1 Specifications...........................................................................................................6

3.2 Compliance ..............................................................................................................7

4. PROBE START-UP ........................................................................................... 7

4.1 Cable connection .....................................................................................................7

4.2 Use with a 8921 conductimeter................................................................................ 8

4.3 Use with a 9125 conductimeter................................................................................ 9

5. PROBE CALIBRATION..................................................................................... 9

6. INSTALLATION PRECAUTION ...................................................................... 11

7. ACCESSORIES ............................................................................................... 13

7.1 Probe 8398.2, 2" clamp model (08398=A=2000)...................................................13

7.2 Probe 8398.3, DIN 11851 / DN50 dairy connection model (08398=A=3000) ........14

7.3 Probe 8398.5, 1" threaded model gas ...................................................................16

8. MAINTENANCE............................................................................................... 18

9. PRECAUTIONARY LABELS........................................................................... 19

10. CHEMICAL RESISTANCE TABLE ................................................................. 20

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Inductive Probe 8398

1. INTRODUCTION

1.1 General

The 8398 range of probes makes use of inductive technology, which is particularly recommended for corrosive and soiling uses, making use of conductivity or concentration measurements. The main uses are as follows:

- Determination of solution concentrations: in-place cleaning, regeneration of resin in water processing plants, surface treatment.

- Accurate interface control in conduits: in-place cleaning in the food and pharmaceutical industries.

- Waste water testing: industrial and town sewerage plants.

1.2 Probes

WARNING: Non-removable cable!

8398.2 8398.3 8398.5 2''clamp DN50 dairy connection 1'' Gas

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Inductive Probe 8398

2. OPERATING PRINCIPLE

2.1 Conductivity reminder

Electrolytic conductivity refers to the ability of a liquid to conduct an electrical current (conductivity is the opposite of resistivity). In metals, the electrical current flows by electron displacement, in liquids it flows by ion transport. The conductivity of a solution is dependent both upon the solution’s ionic concentration and temperature.

To obtain a solution's actual conductivity (in S.cm-1), it is necessary to multiply the measured conductance 1/R (in S) by a coefficient dependent solely upon the geometry of the probe and termed "cell or K constant", expressed in cm

-1

C (S.cm

-1)

In order to allow the comparison between measurements made at different temperatures, this measurement needs to be brought back to a

temperature

(generally 25 °C). This temperature dependency can be easily

reference

expressed in the form of relative variation in degrees Celsius. It is referred to as the temperature coefficient (D).

= C T [1 + D (T - T

Tref

)]-1

ref

: Conductivity compensated to the reference temperature

Tref

: Conductivity measured at T

: Reference temperature (generally 25 °C)

ref

: Temperature coefficient of the solution (% / °C)

Examples:

Product Soda (NaOH)

5 %

D :

2.01 1.45

Nitric acid (HNO

10 %

)

REMARK:

1 S = 1000 mS (R = 1 :) 1 mS = 1000 μS (R = 1 k:)

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Inductive Probe 8398

2.2 Principle of inductive technology

1 : Receiver 2 : Oscillator 3 : Cables 4 : Thermoplastic insulator 5 : Receiver 6 : Transmitter 7 : Induced current

The 8398 probes are made up of two coils that are completely insulated from the process:

x The primary (or transmitter) coil, supplied with alternating voltage, produces an

alternating electromagnetic field that generates an electrical current in the solution.

x The secondary (or receiver) coil detects the size of the weak current induced by

the movement of ions in the solution.

The absence of contact between the electrical part and the solution (magnetic coupling) provides a large number of advantages compared to the traditional technique using metallic electrodes:

No polarisation and hence a broad measurement range.

x High chemical and mechanical resistance. x Possibility of performing measurements in soiling products. x Perfectly hygienic design.

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Inductive Probe 8398

3. TECHNICAL SPECIFICATIONS

3.1 Specifications

Measurement range 0 to 2000 mS/cm

Precision

r 2 % of the displayed value or r 0.004 mS/cm

Conductivity response < 1 s

Temperature response T 50 % = 20 s

T 90 % = 2 mn

Cell constant K = 2.35 cm-1

Roughness Ra < 0.5 μm (roughness certificate on request,

Ref.: 08398=T=1111)

Chemical resistance Our mono-block probe is made from PEEC

(poly ether ether Ketone), whose chemical resistance is summarised in the table §9.

WARNING: PEEC is not resistant to high concentrations of oxidative acids (nitric and sulphuric acid > 70 %, etc.) In the case of probe 8398.5, one must consider the other materials in contact with the process (EPDM or VITON gaskets, PP or 316 stainless steel extension, etc.).

Mechanical resistance PEEC possesses a flexion temperature

(pressure: 18 bars) of approximately 300 °C.

In the case of probe 8398.5, take account of extensions, if any.

Heat resistance PEEC is a polymer that is particularly well-

suited to sterilisation, it can therefore withstand temperatures of 140 °C.

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Inductive Probe 8398

3.2 Compliance

i Probes are factory tested and are delivered with a certificate of compliance with

specifications. Models 8398.2 and 8398.3 are particularly well-suited to applications where sanitary requirements are extremely stringent (compliance with the European food directive 90/128/CE modified by directive 93/9/CE). Indeed, these probes do not possess any retention zones that could allow the development of bacteria (interstices, slits, joints, etc.) and have a roughness inferior to 0.5 μm (optional certificate, ref. 08398=T=1111).

i The measurement chain, made up of an 8398 probe and of our conductivity

transmitters, complies with European directives 89/336/CEE and 73/23/CEE modified by directive 93/68/CEE.

4. PROBE START-UP

4.1 Cable connection

WARNING: Fit the DN50 clamping nut or the immersion rod onto the probe before

wiring!

Make the following connections

COND 9125 COND 8921

(channels 1 and 2)

1 : GREEN or yellow (Pt100) TEMP + 14 and 19

2 : YELLOW or green (Pt100) TEMP - 15 and 20

GND 30 and 32 3 : BLACK (secondary coil shielding)

4 : WHITE (secondary coil)

IN 31 and 33

GND 16 and 21 5 : BLACK (primary coil shielding)

6 : BROWN (primary coil)

7 : WHITE (external shielding) EXTERNAL

OUT 17 and 22

EXTERNAL SHIELDING

SHIELDING

REMARK: The probe is fitted as standard with 5 metres of cable. We recommend

not cutting this cable in order to avoid any connection errors. If the length is insufficient, please order the following accessories:

x Junction box, ref.: 08335=A=6000 x Cable (per metre, maximum 50 m), ref.: 150727,10000

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Inductive Probe 8398

4.2 Use with a 8921 conductimeter

EPROM

The use of a type 8398 inductive probe connected to a type 8921 2-channel conductimeter requires that this latter be fitted with a software version greater than or equal to the following versions:

Software Minimum

Memory reference

version no.

Standard 3.76 08921=A=6200

Concentration 1.04 08921=A=6400

Special 4.07 08921=A=6305

To install your new software version, proceed as follows:

x Remove the transmitter's front panel (4 screws). x On the rear of the front panel, there are two circuit boards. Remove the first of

these two circuit boards (4 screws).

x At the rear of this printed circuit board, carefully change the integrated circuit

(EPROM) represented on the figure opposite.

x Check that the memory has been inserted in the correct position, otherwise it

would be irreversibly damaged.

x Re-fit the front panel and initialise the instrument's default parameters using

command 900.

x Reprogram the instrument to your configuration and configure command

(102)

with Argument 2, which corresponds to the 8398 probe's cell constant,

C101

equal to 2.35.

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Inductive Probe 8398



4.3 Use with a 9125 conductimeter

Set the two switches (I/K) inside the instrument to position I. Check that the measurement type is set to inductive.

5. PROBE CALIBRATION

REMARK: For more detailed information, see the user instructions of out 9125 and

8921 transmitters. We recommend proceeding in the following order:

Set the cell constant value on your transmitter to 2.35 cm

-1

Calibrate your temperature sensor:

Submerge the probe in a solution for approximately 10 min., raise the temperature of this solution using a thermometer (accurate to r 0.1°C if possible). Set the transmitter to process calibration mode, then adjust the temperature value.

Calibrate conductivity (two solutions)

Electrical calibration:

Perform the "electrical" calibration of the probe with a decade box, using a wire no longer than 50 cm and with a minimum cross-section of 0.38 mm². The resistance values to use are: f for zero adjustment (decade box disconnected):

then 200 Ohms (default instrument value) for slope adjustment:

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Inductive Probe 8398

REMARK

: After returning to measurement mode, the value displayed by the

transmitter takes account of the cell constant and also of temperature compensation.

Example: 200 Ohms on decade box, T = 20 °C, transmitter set for 25 °C

compensation with a coefficient of 2 %, unit mS/cm:

DISPLAY: [2.35/200]. [1 + 0.02 u (20 - 25)]

-1

= 13.06 mS/cm (c.f. Ch. 2-1)

Process calibration (9125 only):

During the first calibration of the chain, process calibration must be performed at two distinct points (probe in air, then in the control solution). After this, calibration can be performed on a single point (control solution only).

WARNING:

If you are using a 9125 with software version < 1.12, the cell constant value must be set prior to calibration. Any alteration of the cell constant value after calibration would cancel the calibration for this probe (slope reset to 100 %).

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6. INSTALLATION PRECAUTION

Inductive Probe 8398

Minimum distance between probe and conduit

When the electrical field lines are partially obstructed by a wall, the measured conductivity is altered (increased if the wall is a conductor, decreased if it is an insulator). With our "high performance" shielding system, 100 % of the field lines of our probe are channelled to within less than 10 mm, thus allowing

be made without disturbance in DN65 conduits

measurements to

It is also possible to perform measurements in DN50 conduits, using our DN65 / DN50 converging / diverging T-pieces (reference 08398=A=6000 for 8398.3 probes and 08398=A=7000 for 8398.2 probes). These T-pieces therefore allow users to connect to DN50 conduits, while performing their measurements in a DN65 diameter.

WARNING: In order to work optimally, the probe must be completely submerged in

the liquid. We therefore recommend the use of a U-bend tube.

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Inductive Probe 8398

Installation direction

The opening of the probe must face the conduit's flow direction, thus avoiding the influence of flow rate and to perform the self-cleaning of this opening. For optimal operation, the "POLYMETRON" marking should be positioned in the conduit's flow direction, as shown in the following figure:

: flow direction in the conduit

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Inductive Probe 8398

7. ACCESSORIES

There are three probe versions, that are distinguished by the type of connector used.

7.1 Probe 8398.2, 2" clamp model (08398=A=2000)

APPLICATION: FREE FLOW

Number: Reference: Designation Installation

1 581=000=510

2" stainless steel clamp collar

2 429=500=510 EPDM joint for 2" clamp -

6 581=100=510 2" stainless steel ferrule to weld Min. DN65

1+2+6 08398=A=0510 Kit with 2" stainless collar

Min. DN65

+ 2" EPDM joint + 2" stainless ferrule

1+2+3 08398=A=7500 Kit with 2" stainless collar

DN65 + 2" EPDM joint + DN65 stainless T-piece

1+2+4 08398=A=7000 Kit with 2" stainless collar + 2" EPDM

DN50 joint + DN65/50 stainless T-piece

1+2+5 08398=A=8200 Kit with 2" stainless collar

Derivation + 2" EPDM joint + Stainless flow chamber (inlet / outlet 1/4" NPT)

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7.2 Probe 8398.3, DIN 11851 / DN50 dairy connection model (08398=A=3000)

APPLICATION: FREE FLOW

Inductive Probe 8398

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Inductive Probe 8398

Number: Reference:

1 402=400=500

Designation

Stainless steel DN50 DIN screw

2 429=600=500 EPDM DIN DN50 joint

7 429=600=501 VITON DIN DN50 joint

6 581=200=500 DIN DN50 stainless steel ferrule to weld

(H = 35 mm)

1+2+6 08398=A=0500 Kit with DN50 stainless screw + EPDM

DN50 joint + DN50 stainless ferrule to weld (H = 35 mm)

1+7+8 08398=A=5310 Kit with DN50 stainless screw + VITON

DN50 joint + PVC ferrule to glue (H = 23 mm)

1+2+9 08398=A=5320 Kit with DN50 stainless screw + EPDM

DN50 joint + PP ferrule to weld (H = 23 mm)

1+7+10 08398=A=5330 Kit with DN50 stainless screw + VITON

DN50 joint + PVDF ferrule to weld (H = 23 mm)

1+2+4 08398=A=6000 Kit with DN50 stainless screw + EPDM

DN50 joint + DN65/50 T-piece

1+2+3 08398=A=6500 Kit with DN50 stainless screw + EPDM

DN50 joint + DN65 stainless T-piece

1+2+5 08398=A=8300 Kit with DN50 stainless screw + EPDM

DN50 joint + Stainless flow chamber (inlet / outlet 1/4" NPT)

1+7+11 08398=A=8310 Kit with DN50 stainless screw + VITON

DN50 joint + PVC flow chamber (inlet / outlet 1/2" gas)

1+2+12 08398=A=8320 Kit with DN50 stainless screw + EPDM

DN50 joint + PP flow chamber (inlet / outlet 1/2" gas)

1+7+13 08398=A=8330 Kit with DN50 stainless screw + VITON

DN50 joint + PVDF flow chamber (inlet / outlet 1/2" gas)

Installation

Min. DN65

DN50

DN65

Derivation

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7.3 Probe 8398.5, 1" threaded model gas

Inductive Probe 8398

Remark: Flanges are not supplied individually.

This model is a universal model, specially adapted to immersion measurements. it is supplied as standard with an EPDM sheet gasket, an optional Viton joint (ref. 08398=C=3438) is also available, along with the stainless steel 1"G screw (402=700=010). We propose as standard several PP and 316 L stainless steel accessories for immersion at various depths (0.5/1/1.5/2 m):

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Inductive Probe 8398

Reference Material Immersion (m) Flange Immersion

setting

08335=A=5005 PP 0.5 DN65 PVC Adjustable

08335=A=5010 PP 1 DN65 PVC Adjustable 08398=A=1014

08335=A=5015 PP 1.5 DN65 PVC Adjustable 08398=A=1014

08335=A=5020 PP 2 DN65 PVC Adjustable 08398=A=1014

08398=A=6005 PP 0.5 DN50 PP Fixed -

08398=A=6010 PP 1 DN50 PP Fixed -

08398=A=6015 PP 1.5 DN50 PP Fixed -

08398=A=6020 PP 2 DN50 PP Fixed -

08398=A=6605 PP 0.5 DN50 PVC Adjustable -

08398=A=6610 PP 1 DN50 PVC Adjustable -

08398=A=6615 PP 1.5 DN50 PVC Adjustable -

08398=A=6620 PP 2 DN50 PVC Adjustable -

08350=A=1105 PP 0.5 - Clip

08350=A=1110 PP 1 - Clip 08398=C=0300

08350=A=1115 PP 1.5 - Clip 08398=C=0300

08350=A=1120 PP 2 - Clip 08398=C=0300

08878=A=1500 STAINLESS 1.5 (*) Adjustable 08398=C=0500

Adapter required

08398=A=1014

(H = 150 mm)

08398=C=0300

(H = 130 mm)

(*): No flange, to be used with 08878=C=1600 support

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Inductive Probe 8398

8. MAINTENANCE

WARNING: Read the "installation precaution" and "cable connection" chapters

carefully.

o If there is a doubt concerning the operation of a probe, disconnect it from the

transmitter, leaving it in place on your process and ensure that you obtain the following resistance values (see 4.1 Cable connection):

R (1-2) | 110 : (at 25 °C) (Temperature sensor Pt100) R (3-4) | [1…2] : (Secondary coil) R (5-6) | [1…2] : (Primary coil) R (3-5) f : (Coil electrical insulation)

o If the checks performed do not generate any erroneous resistance values, the

probe can be considered to be working properly.

o If the measurement is still not satisfactory, remove the probe from the process and

calibrate it (see "probe calibration" chapter), set the transmitter to "no temperature compensation", then check the following points:

Displayed conductivity (K = 2.35) Simulated resistance

470 μS/cm 5 k:

4.7 mS/cm 500 :

47 mS/cm 50 :

470 mS/cm 5 :

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Inductive Probe 8398

9. PRECAUTIONARY LABELS

Read all labels and tags attached to the instrument. Personal injury or damage to this instrument could occur if not observed.

This symbol, if noted on the instrument, references the instruction

manual for operation and / or safety information.

Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of life equipment to the Producer for disposal at no charge to the user.

Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return end-of-life equipment for proper disposal.

Important document. Retain with product records.

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Inductive Probe 8398

10. CHEMICAL RESISTANCE TABLE

0: yes, -: no, x: momentarily

% 20 60 100 20 60 100 20 60 100

Sulphuric acid 10

Hydrochloric acid 10

Nitric acid < 25

Phosphoric acid < 25

Hydrofluoric acid 40

Acetic acid 10

Formic acid 80 x x x 0 0 0 0 0 -

Citric acid 50 0 0 0 0 0 0 0 0 0

Calcium hydroxide Sat 0 0 0 0 0 0 0 0 -

Potassium hydroxide 50 0 0 0 0 0 x 0 0 -

Sodium hydroxide 10

Ammonia 10

Ammonium chloride Sat 0 0 0 0 0 0 0 0 0

Zinc chloride 50 0 0 0 0 0 0 0 0 -

Iron chloride 50 0 0 0 0 0 0 0 0 0

Sodium sulphite Sat 0 0 0 0 0 0 0 0 -

Sodium carbonate Sat 0 0 0 0 0 0 0 0 -

Potassium chloride Sat 0 0 0 0 0 0 0 0 0

Sodium sulphate Sat 0 0 0 0 0 0 0 0 0

Calcium chloride Sat 0 0 0 0 0 0 0 0 0

Sodium chloride Sat 0 0 0 0 0 0 0 0 0

Sodium nitrate 50 0 0 0 0 0 0 0 0 -

Aluminium chloride Sat 0 0 0 0 0 0 0 0 0

Hydrogen peroxide 30 0 0 0 0 0 0 0 0 -

Sodium hypochlorite 50 0 0 0 0 0 0 x x -

Potassium dichromate Sat 0 0 0 0 0 0 0 0 0

Chlorinated salt water 0 0 0 0 x - - - -

Ethanol 80 0 0 0 0 0 x 0 0 0

Cyclohexane 0 0 0 0 0 x - - -

Toluene 0 0 0 0 0 0 x - -

Trichloroethane 0 0 0 x x x - - -

Water 0 0 0 0 0 0 0 0 0

(°C)

Sat

glacial

PEEK

0 0 0 0 x

0 0 0 0 0 x 0 0 0 x 0 - 0 0 0 x 0

0 0 0 0 0 0 0 0 x

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 -

PVDF

0 0 0 0 0 0 0 0 0 0 x

0 0 0 0 0 0 0 0 0 0 -

0 - x 0 0 0 0 0 -

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Inductive Probe 8398

0: yes, -: no, x: momentarily

20 60 100 20 60 100 20 60 100

Sulphuric acid 10

Hydrochloric acid 10

Nitric acid < 25

Phosphoric acid < 25

Hydrofluoric acid 40

Acetic acid 10

Formic acid 80 0 0 x - - - 0 x x

Citric acid 50 0 0 0 0 0 0 0 0 0

Calcium hydroxide Sat 0 0 0 0 0 0 0 0 0

Potassium hydroxide 50 0 0 x x x - 0 0 0

Sodium hydroxide 10

Ammonia 10

Ammonium chloride Sat 0 0 0 0 0 0 x x x

Zinc chloride 50 0 0 0 0 0 0 x x x

Iron chloride 50 0 0 0 0 0 0 - - -

Sodium sulphite Sat 0 0 0 0 0 - 0 0 0

Sodium carbonate Sat 0 0 - 0 0 0 0 0 0

Potassium chloride Sat 0 x - 0 0 0 0 x x

Sodium sulphate Sat 0 0 0 0 0 0 0 0 0

Calcium chloride Sat 0 0 0 0 0 0 0 0 x

Sodium chloride Sat 0 0 0 0 0 0 x x x

Sodium nitrate 50 0 0 0 0 0 0 x x x

Aluminium chloride Sat 0 0 0 0 0 0 - - -

Hydrogen peroxide 30 0 0 - 0 0 0 0 0 0

Sodium hypochlorite 50 x x - 0 0 x x x x

Potassium dichromate Sat 0 x x 0 0 0 0 0 x

Chlorinated salt water - - - 0 x - - - -

Ethanol 80 0 0 0 0 x x 0 0 0

Cyclohexane - - - 0 0 0 0 0 0

Toluene - - - - - - 0 0 0

Trichloroethane - - - x x x 0 0 -

Water 0 0 0 0 0 0 0 0 0

sat

glacial

EPDM

0 - 0 - 0 - 0 0 0 0 0 0 - - - - -

0 0 0 x 0 - x

0 0 0 0 x

0 0 0 0 0

VITON

0 0 0 0 0 0 - - - - -

0 0 x

- - 0 0 0 0 x

- - 0 0 0 0 0

316 L

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Hach-Lange POLYMETRON 8398 User Manual

Specifications and Main Features

Frequently Asked Questions

User Manual