Hach-Lange ORBISPHERE K1100, ORBISPHERE M1100 User Manual

DOC024.52.93023
ORBISPHERE Model K-M1100 Sensor and Model
410 Analyzer
User Manual
12/2013, Edition 9
Section 1 General Information.........................................................................................................5
1.1 Disclaimer .................................................................................................................................... 5
1.2 Contact information......................................................................................................................5
1.3 Safety information ........................................................................................................................ 5
1.3.1 Use of hazard information................................................................................................... 5
1.3.2 Safety precautions ..............................................................................................................6
1.3.3 Service and repairs .............................................................................................................6
1.3.4 Precautionary labels............................................................................................................7
1.3.5 Intended use of this equipment........................................................................................... 7
1.4 Product recycling information.......................................................................................................8
1.5 Product disposal ........................................................................................................................ 10
1.6 Restriction of hazardous substances (RoHS) ............................................................................11
Section 2 Specifications.................................................................................................................. 13
2.1 Sensor descriptions ................................................................................................................... 13
2.2 Technical data............................................................................................................................13
2.3 General principle of operation.................................................................................................... 15
2.4 Hardware description .................................................................................................................16
2.5 Security level table.....................................................................................................................17
2.6 Default parameters .................................................................................................................... 18
2.7 M1100 EHEDG Certification ...................................................................................................... 19
Section 3 Installation........................................................................................................................21
3.1 Unpacking .................................................................................................................................. 21
3.2 Installation check list ..................................................................................................................22
3.3 Wall mount and pipe mount instruments.................................................................................... 23
3.3.1 Instrument dimensions......................................................................................................23
3.3.2 Wall mounting ...................................................................................................................24
3.3.3 Pipe mounting ...................................................................................................................24
3.3.4 Connections (bottom of instrument)..................................................................................25
3.4 Panel mount instrument ............................................................................................................. 26
3.4.1 Instrument dimensions......................................................................................................26
3.4.2 Mounting ...........................................................................................................................27
3.4.3 Connections (bottom of instrument)..................................................................................28
3.5 Connectors assembly instructions .............................................................................................29
3.5.1 Cable gland wiring instructions ......................................................................................... 29
3.5.2 USB-B client adapter cable............................................................................................... 30
3.6 Connection to mains power supply ............................................................................................30
3.6.1 Power supply connection (low voltage instruments) ......................................................... 30
3.6.2 Power supply connection (high voltage instruments)........................................................ 31
3.7 Connections to electronic boards...............................................................................................33
3.7.1 Electronic boards connectors............................................................................................ 33
3.7.2 Main board connections....................................................................................................33
3.7.3 Measurement board..........................................................................................................34
3.8 Measurement alarm relays ........................................................................................................ 34
3.9 Sensor installation......................................................................................................................35
3.9.1 Sensor positioning information.......................................................................................... 35
3.9.2 Recommended sample flow rate.......................................................................................35
3.9.3 Sensor insertion ................................................................................................................35
3.9.4 Sensor removal................................................................................................................. 36
3.9.5 Weld-on stainless steel socket..........................................................................................36
3.9.6 The 32003 insertion/extraction valve ................................................................................ 37
3.9.7 The 33095 and 33096 sensor housing..............................................................................37
3.9.8 Tuchenhagen Varivent® in-line access unit...................................................................... 37
3.9.9 Instrument connections.....................................................................................................38
3.10 Calibration devices...................................................................................................................38
3.10.1 Portable calibration device.............................................................................................. 38
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Table of Contents
3.10.2 ORBISPHERE flow chambers.........................................................................................39
Section 4 User Interface ..................................................................................................................41
4.1 Instrument ..................................................................................................................................41
4.2 Touch screen..............................................................................................................................41
4.2.1 Function keys on the header bar.......................................................................................42
4.2.2 Menu navigation ................................................................................................................43
4.2.3 Rolling list ..........................................................................................................................43
4.2.4 Virtual keyboard ................................................................................................................43
4.2.5 Identification and authorization level .................................................................................44
4.2.6 Warning windows ..............................................................................................................44
4.3 Main menu structure...................................................................................................................45
Section 5 View Menu ........................................................................................................................47
5.1 Selection of the view style..........................................................................................................48
5.2 Configuration of the view styles..................................................................................................49
Section 6 Measurement Menu........................................................................................................51
6.1 Instrument configuration.............................................................................................................51
6.2 Measurement configuration........................................................................................................52
6.3 Measured data storage ..............................................................................................................54
Section 7 Calibration Menu.............................................................................................................55
7.1 Sensor calibration.......................................................................................................................56
7.2 Calibration configuration.............................................................................................................57
7.3 Zero calibration...........................................................................................................................58
7.4 100% humid air calibration (high range sensors only) ...............................................................58
7.5 High level adjustment.................................................................................................................58
7.6 Sensor verification......................................................................................................................58
7.7 Barometric pressure calibration..................................................................................................59
7.8 Calibration reports......................................................................................................................59
Section 8 Inputs/Outputs Menu .....................................................................................................61
8.1 Configure snooze .......................................................................................................................62
8.2 View inputs/outputs ....................................................................................................................62
8.3 Relays ........................................................................................................................................62
8.4 Analog outputs ...........................................................................................................................63
8.5 Analog output characteristics .....................................................................................................67
Section 9 Communication Menu....................................................................................................71
9.1 RS-485 simple mode configuration ............................................................................................72
9.1.1 Data available....................................................................................................................73
9.1.2 Example of use..................................................................................................................76
9.2 PROFIBUS-DP communication (optional)..................................................................................77
9.2.1 Installation .........................................................................................................................77
9.2.2 Input/Output data...............................................................................................................78
9.3 USB-A port (host).......................................................................................................................81
9.4 HTTP/TCP-IP .............................................................................................................................82
9.4.1 Overview ...........................................................................................................................82
9.4.2 PC interface.......................................................................................................................82
9.5 Data file transfer through the USB-B port (client).......................................................................84
9.5.1 PC software installation.....................................................................................................84
9.5.2 Microsoft synchronization software ...................................................................................84
9.5.3 Upload report files .............................................................................................................84
9.6 Printer.........................................................................................................................................86
9.6.1 Printer error messages......................................................................................................86
Section 10 Security Menu................................................................................................................87
10.1 Access rights management......................................................................................................87
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Table of Contents
10.2 Configure security ....................................................................................................................88
10.3 User management ................................................................................................................... 88
10.4 User action log file ................................................................................................................... 88
Section 1 1 Products Menu..............................................................................................................89
Section 12 Global Configuration Menu........................................................................................91
Section 13 Services Menu............................................................................................................... 93
13.1 Sensor diagnostics...................................................................................................................95
13.2 Language selection.................................................................................................................. 95
13.3 Clock ........................................................................................................................................ 95
13.4 Screen......................................................................................................................................96
13.5 Buzzer...................................................................................................................................... 96
13.6 Boards info............................................................................................................................... 96
13.7 Batteries................................................................................................................................... 96
13.8 Software download .................................................................................................................. 96
13.9 End application ........................................................................................................................ 96
Section 14 Maintenance and Troubleshooting .......................................................................... 97
14.1 Instrument maintenance .......................................................................................................... 97
14.2 Sensor maintenance ................................................................................................................97
14.2.1 Equipment required......................................................................................................... 97
14.2.2 Sensor spot removal .......................................................................................................97
14.2.3 Sensor spot replacement ................................................................................................ 98
14.3 Storage, handling and transportation.......................................................................................99
14.4 Troubleshooting ....................................................................................................................... 99
14.5 List of events and alarms ....................................................................................................... 101
Section 15 Accessories and Spare Parts.................................................................................. 103
15.1 Instrument .............................................................................................................................. 103
15.2 Sensor....................................................................................................................................103
15.3 Insertion and sampling devices..............................................................................................104
15.4 K1100 kits to order (KTO’s) ................................................................................................... 104
15.5 M1100 kits to order (KTO’s)...................................................................................................105
15.6 Instrument options ................................................................................................................. 107
Section 16 Glossary .......................................................................................................................109
16.1 Gas units................................................................................................................................ 109
16.2 Generic terms and definitions ................................................................................................ 109
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Table of Contents
4

Section 1 General Information

1.1 Disclaimer

The information in this manual has been carefully checked and is believed to be accurate. However, Hach Lange assumes no responsibility for any inaccuracies that may be contained in this manual. In no event will Hach Lange be liable for direct, indirect, special, incidental, or consequential damages resulting from any defect or omission in this manual, even if advised of the possibility of such damages. In the interest of continued product development, Hach Lange reserves the right to make improvements in this manual and the products it describes at any time, without notice or obligation.
Copyright © 2009-2013 by Hach Lange. All rights reserved. No part of the contents of this manual may be reproduced or transmitted in any form or by any means without the written permission of Hach Lange.

1.2 Contact information

Manufacturing site:
HACH LANGE Sàrl 6, route de Compois 1222 Vésenaz SWITZERLAND Tel. +41 22 594 6400 Fax +41 22 594 6499

1.3 Safety information

For safe operation, please read the entire manual before unpacking, setting up, or operating this instrument.
Pay particular attention to all warning and caution statements. Failure to do so could result in serious injury to the operator or damage to the equipment.
To ensure the protection provided by this equipment is not impaired, do not use or install this equipment in any manner other than that which is specified in this manual.

1.3.1 Use of hazard information

Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.
European HQ:
HACH LANGE GmbH Willstätterstraße 11 40549 Düsseldorf GERMANY Tel. +49 211 52 880 Fax +49 211 52 88143
DANGER
WARNING
Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious injury.
CAUTION
Indicates a potentially or imminently hazardous situation that may result in minor or moderate injury.
NOTICE
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special emphasis.
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General Information

1.3.2 Safety precautions

Always remove power from the controller before performing maintenance activities.
Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical connections.
Potential Electrocution Hazard. If this equipment is used outdoors or in potentially wet locations a Ground Fault Interrupt device must be used for connecting the equipment to its main power source.
DANGER
WARNING
WARNING
WARNING
Potential Electrocution Hazard. Connect only safety low voltage < 33 VAC RMS.
CAUTION
Personal Injury Hazard. Only qualified personnel should conduct the tasks described in this manual.
NOTICE
Install the device in a location and position that gives easy access to the disconnect device and its operation.
NOTICE
Potential Instrument Damage. Delicate internal electronic components can be damaged by static electricity, resulting in degraded performance or eventual failure.
The power cord plug connection is also used as a main power switch.
The instrument must be connected to an electrical system which complies with applicable local regulations.
All the cables connected to the instrument must be fire resistant, type UL94V-1
The operator must read and understand this manual before using the instrument .
The instrument will not be used as a safety device. It does not provide a security function in a hazardous process.

1.3.3 Service and repairs

None of the analyzer’s components can be serviced by the user. Only personnel from Hach Lange or its approved representative(s) is (are) authorized to attempt repairs to the system and only components formally approved by the manufacturer should be used. Any attempt at repairing the analyzer in contravention of these principles could cause damage to the analyzer and corporal injury to the person carrying out the repair. It renders the warranty null and void and could compromise the correct working of the analyzer and the electrical integrity or the CE compliance of the analyzer.
6

1.3.4 Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed.
This symbol, when noted on a product, indicates a potential hazard which could cause serious personal injury and/or death. The user should reference this instruction manual for operation and/or safety information.
This symbol, when noted on a product enclosure or barrier, indicates that a risk of electrical shock and/or electrocution exists and indicates that only individuals qualified to work with hazardous voltages should open the enclosure or remove the barrier.
This symbol, when noted on the product, indicates that the marked item can be hot and should not be touched without care.
This symbol, when noted on the product, indicates the presence of devices sensitive to electrostatic discharge and indicates that care must be taken to prevent damage to them.
This symbol, when noted on the product, identifies a risk of chemical harm and indicates that only individuals qualified and trained to work with chemicals should handle chemicals or perform maintenance on chemical delivery systems associated with the equipment.
General Information
This symbol, if noted on the product, indicates the need for protective eye wear.
This symbol, when noted on the product, identifies the location of the connection for protective earth (ground).
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems. In conformity with European local and national regulations, European electrical equipment users must now return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.
Products marked with this symbol indicates that the product contains toxic or hazardous substances or elements. The number inside the symbol indicates the environmental protection use period in years.

1.3.5 Intended use of this equipment

This high accuracy ORBISPHERE instrument and sensor is designed for the measurement of dissolved oxygen in power applications using the K1100 sensor or in beverage applications using the M1100 sensor.
ORBISPHERE 410 analyzers are available as wall or pipe mount, and rack mount versions. This version of the instrument uses a luminescent dissolved oxygen sensor to determine dissolved oxygen concentrations in the measured sample.
NOTICE
Use of the instrument outside of the environmental conditions described in Technical data on
page 13 may cause damage to the instrument but without endangering the user.
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General Information

1.4 Product recycling information

ENGLISH
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.
Note: For return for recycling, please contact the equipment
manufacturer or supplier for instructions on how to return end-of-life equipment for proper disposal.
DEUTSCH
Elektrogeräte, die mit diesem Symbol gekennzeichnet sind, dürfen in Europa nach dem 12. August 2005 nicht mehr über die öffentliche Abfallentsorgung entsorgt werden. In Übereinstimmung mit lokalen und nationalen europäischen Bestimmungen (EU-Richtlinie 2002/96/EC), müssen Benutzer von Elektrogeräten in Europa ab diesem Zeitpunkt alte bzw. zu verschrottende Geräte zur Entsorgung kostenfrei an den Hersteller zurückgeben.
Hinweis: Bitte wenden Sie sich an den Hersteller bzw. an den Händler, von dem Sie das Gerät bezogen haben, um Informationen zur Rückgabe des Altgeräts zur ordnungsgemäßen Entsorgung zu erhalten.
FRANCAIS
A partir du 12 août 2005, il est interdit de mettre au rebut le matériel électrique marqué de ce symbole par les voies habituelles de déchetterie publique. Conformément à la réglementation européenne (directive UE 2002/96/EC), les utilisateurs de matériel électrique en Europe doivent désormais retourner le matériel usé ou périmé au fabricant pour élimination, sans frais pour l'utilisateur.
Remarque: Veuillez vous adresser au fabricant ou au fournisseur du matériel pour les instructions de retour du matériel usé ou périmé aux fins d'élimination conforme.
ITALIANO
Le apparecchiature elettriche con apposto questo simbolo non possono essere smaltite nelle discariche pubbliche europee successivamente al 12 agosto 2005. In conformità alle normative europee locali e nazionali (Direttiva UE 2002/96/EC), gli utilizzatori europei di apparecchiature elettriche devono restituire al produttore le apparecchiature vecchie o a fine vita per lo smaltimento senza alcun costo a carico dell’utilizzatore.
Nota: Per conoscere le modalità di restituzione delle apparecchiature a fine vita da riciclare, contattare il produttore o il fornitore dell’apparecchiatura per un corretto smaltimento.
DANSK
Elektriske apparater, der er mærket med dette symbol, må ikke bortskaffes i europæiske offentlige affaldssystemer efter den 12. august 2005. I henhold til europæiske lokale og nationale regler (EU-direktiv 2002/96/EF) skal europæiske brugere af elektriske apparater nu returnere gamle eller udtjente apparater til producenten med henblik på bortskaffelse uden omkostninger for brugeren.
Bemærk: I forbindelse med returnering til genbrug skal du kontakte producenten eller leverandøren af apparatet for at få instruktioner om, hvordan udtjente apparater bortskaffes korrekt.
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General Information
SVENSKA
Elektronikutrustning som är märkt med denna symbol kanske inte kan lämnas in på europeiska offentliga sopstationer efter 2005-08-12. Enligt europeiska lokala och nationella föreskrifter (EU-direktiv 2002/96/EC) måste användare av elektronikutrustning i Europa nu återlämna gammal eller utrangerad utrustning till tillverkaren för kassering utan kostnad för användaren.
Obs! Om du ska återlämna utrustning för återvinning ska du kontakta tillverkaren av utrustningen eller återförsäljaren för att få anvisningar om hur du återlämnar kasserad utrustning för att den ska bortskaffas på rätt sätt.
ESPANOL
A partir del 12 de agosto de 2005, los equipos eléctricos que lleven este símbolo no deberán ser desechados en los puntos limpios europeos. De conformidad con las normativas europeas locales y nacionales (Directiva de la UE 2002/96/EC), a partir de esa fecha, los usuarios europeos de equipos eléctricos deberán devolver los equipos usados u obsoletos al fabricante de los mismos para su reciclado, sin coste alguno para el usuario.
Nota: Sírvase ponerse en contacto con el fabricante o proveedor de los equipos para solicitar instrucciones sobre cómo devolver los equipos obsoletos para su correcto reciclado.
NEDERLANDS
Elektrische apparatuur die is voorzien van dit symbool mag na 12 augustus 2005 niet meer worden afgevoerd naar Europese openbare afvalsystemen. Conform Europese lokale en nationale wetgegeving (EU-richtlijn 2002/96/EC) dienen gebruikers van elektrische apparaten voortaan hun oude of afgedankte apparatuur kosteloos voor recycling of vernietiging naar de producent terug te brengen.
Nota: Als u apparatuur voor recycling terugbrengt, moet u contact opnemen met de producent of leverancier voor instructies voor het terugbrengen van de afgedankte apparatuur voor een juiste verwerking.
POLSKI
Sprzęt elektryczny oznaczony takim symbolem nie może być likwidowany w europejskich systemach utylizacji po dniu 12 sierpnia 2005. Zgodnie z europejskimi, lokalnymi i państwowymi przepisami prawa (Dyrektywa Unii Europejskiej 2002/96/EC), użytkownicy sprzętu elektrycznego w Europie muszą obecie przekazywać Producentowi stary sprzęt lub sprzęt po okresie użytkowania do bezpłatnej utylizacji.
Uwaga: Aby przekazać sprzęt do recyklingu, należy zwrócić się do producenta lub dostawcy sprzętu w celu uzyskania instrukcji dotyczących procedur przekazywania do utylizacji sprzętu po okresie użytkownia.
PORTUGUES
Qualquer equipamento eléctrico que ostente este símbolo não poderá ser eliminado através dos sistemas públicos europeus de tratamento de resíduos sólidos a partir de 12 de Agosto de 2005. De acordo com as normas locais e europeias (Directiva Europeia 2002/96/EC), os utilizadores europeus de equipamentos eléctricos deverão agora devolver os seus equipamentos velhos ou em fim de vida ao produtor para o respectivo tratamento sem quaisquer custos para o utilizador.
Nota: No que toca à devolução para reciclagem, por favor, contacte o produtor ou fornecedor do equipamento para instruções de devolução de equipamento em fim de vida para a sua correcta eliminação.
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General Information

1.5 Product disposal

Note: The following only applies to European customers.
Hach Lange is committed to ensuring that the risk of any environmental damage or pollution caused by any of its products is minimized as far as possible. The European Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC) that came into force on August 13 2005 aims to reduce the waste arising from electrical and electronic equipment; and improve the environmental performance of all those involved in the life cycle of electrical and electronic equipment.
In conformity with European local and national regulations (EU Directive 2002/96/EC stated above), electrical equipment marked with the above symbol may not be disposed of in European public disposal systems after 12 August 2005.
Hach Lange will offer to take back (free of charge to the customer) any old, unserviceable or redundant analyzers and systems which carry the above symbol, and which were originally supplied by Hach Lange. Hach Lange will then be responsible for the disposal of this equipment.
In addition, Hach Lange will offer to take back (at cost to the customer) any old, unserviceable or redundant analyzers and systems which do not carry the above symbol, but which were originally supplied by Hach Lange. Hach Lange will then be responsible for the disposal of this equipment.
Should you wish to arrange for the disposal of any piece of equipment originally supplied by Hach Lange, please contact your supplier or our After Sales Service department in Geneva for instructions on how to return this equipment for proper disposal.
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1.6 Restriction of hazardous substances (RoHS)

The European Union RoHS Directive and subsequent regulations introduced in member states and other countries limits the use of six hazardous substances used in the manufacturing of electrical and electronic equipment.
Currently, monitoring and control instruments do not fall within the scope of the RoHS Directive, however Hach Lange has taken the decision to adopt the recommendations in the Directive as the target for all future product design and component purchasing.
Note: The following only applies to exports of this product into the People’s Republic of China.
General Information
Locking system X Spacer X External connectors X Sensor head X
O:
X:
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General Information
12

Section 2 Specifications

2.1 Sensor descriptions

ORBISPHERE K1100 sensor
The high accuracy K1100 sensor is a luminescent sensor measuring dissolved oxygen, and has been optimized specifically for measurements in water processes in the power industry.
ORBISPHERE M1100 sensor
The high accuracy M1100 sensor is a luminescent sensor measuring dissolved oxygen, and has been optimized specifically for measurements in beer processes in the beverage industry.

2.2 Technical data

IP 65 Totally protected against dust. Protected against low pressure jets of water from all directions.
Enclosure ratings
NEMA4X (wall mount only) Totally protected against dust.
Protected against pressure jets of water from all directions. EMC requirements EN61326-1:2006 Directive 2004/108/EEC
Certifications
Analog outputs
Measurement alarm relays on the measurement board
CE compliance EN61010-1: 2010 Directive 2006/95/EEC
Safety rating
3 Smart 0/4 – 20 mA (500 Ohms), programmable as linear or tri-linear, configurable to send diagnostics or alarm information.
Three alarm relays 1A-30 VAC or 0.5A-50 VDC on a resistance load Configurable to Normally Open [NO] or Normally Closed [NC] contacts by changing the
jumper positions.
Controller
ETL, conforming to UL 61010-1 and CSA 22.2 No. 61010-1
WARNING
System alarm relay on the main board
Digital communication
Data storage
User interface
Potential Electrocution Hazard. Connect only safety low voltage < 33 VAC RMS.
One "instrument system alarm" relay per instrument 1A-30 VAC or 0.5A-50 VDC on a resistance load Normally closed [NC] (NO relay also available) when instrument is turned on. Opens when
a system alarm is detected, and when it does not receive any signal.
WARNING
Potential Electrocution Hazard. Connect only safety low voltage < 33 VAC RMS.
RS485 Profibus DP (optional) Ethernet USB-client to download data to and from a computer USB-host to download data with a USB memory stick Rolling buffer or store once mode for up to 1000 measurements and 1000 operator actions Holds calibration records for the last 10 calibrations
Touch-screen panel
Password protection
Displays concentration, trend graph, diagnostics, alarm status, historical data.
Five levels of authorised access to configuration and data management
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Specifications
Sensor
Sample temperature
Sample pressure 1 to 20 bar absolute (14.5 to 290 psia) Sample flow rate requirement 50 to 300 mL/min
Sample types
CIP
Measurement range
Repeatability
Reproducibility
Accuracy
Limit of detection (LOD)
Response time (90%)
Warm-up time None Display resolution 0.1 ppb
Calibration
Calibration sample
Measurement from -5 to 50°C (23 to 122°F) Sensor resistant to temperature from -5 to 100°C (23 to 212°F)
K1100 sensor Water only M1100 sensor (low range) Water and beer M1100 sensor (high range) Water, beer, wine, wort and carbonated drinks K1100 sensor Not designed for use in CIP processes M1100 sensor Resistant to all common CIP methods Low range sensors: 0 to 2,000 ppb (dissolved)
High range sensors: 0 to 40 ppm (dissolved) Low range sensors: ± 0.4 ppb or 1%, whichever is the greater
High range sensors: ± 0.015 ppm or ± 2% whichever is the greater Low range sensors: ± 0.8 ppb or 2%, whichever is the greater
High range sensors: ± 0.02 ppm or ± 3% whichever is the greater Low range sensors: ± 0.8 ppb or 2%, whichever is the greater
High range sensors: ± 0.02 ppm or ± 3% whichever is the greater Low range sensors: 0.6 ppb
High range sensors: 0.015 ppm Low range sensors: < 10 seconds in gas phase; < 30 seconds in liquid phase
High range sensors: < 10 seconds in gas phase; < 50 seconds in liquid phase
Low range sensors: Single point calibration (zero) High range sensors: Two at cap replacement (zero and air), one during use (air)
Low range sensors: Standard 99.999% N High range sensors: Standard 99.999% N2 (quality 30) or equivalent oxygen free gas, air
(quality 50) or equivalent oxygen free gas
2
Accessories
Active spots, spare sensors, tool kit, portable calibration setup, etc.
Accessories
In process sensor installation devices
Ambient temperature -5 to 50 °C (23 to 122 °F) Humidity 0 to 95% non-condensing relative humidity
Power supply
Wall (pipe) mount controller 3.8 kg Panel mount controller 2.9 kg M1100 12 mm (PG 13.5) sensor 0.6 kg K1100 and M1100 28 mm sensor 0.74 kg Calibration device 0.7 kg
Ask your local Hach Lange representative for more details on all available spare parts and accessories.
Installation
ORBISPHERE insertion/extraction valve for installation on Varinline® access units ORBISPHERE 28 mm sensor weld-on socket PG 13.5 stationary housing for installation on Varinline® access units
Note: This device is only available for the M1100 sensor
28 mm stationary housing for installation on Varinline® access units
Universal 85-264 VAC @ 50/60 Hz, 25 VA 10-36 VDC, 25 W
Weights
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2.3 General principle of operation

Optical sensing of oxygen originates from the work of Kautsky in 1939 where he demonstrated that oxygen can dynamically quench the fluorescence of an indicator (decrease the quantum yield). This principle has been reported in various fields of application such as monitoring aquatic biology in waste water, tests for blood gas analysis and cell culture monitoring. The method is now recognized by ASTM (American Society for Testing and Materials) for the measurement of oxygen in water. Compared to classical oxygen detection using electrochemical sensors, luminescent technology offers several advantages such as no oxygen consumption, independence from sample flow velocity, no electrolyte and low maintenance.
Optical sensing of oxygen is based on the measurement of the red fluorescence of a dye/indicator illuminated with a blue light as shown in Figure 1.
Specifications
Figure 1 Principle of optical oxygen detection using fluorescent dye
The dye fluorescence is quenched by the presence of oxygen. The oxygen concentration can be calculated by measuring the decay time of the fluorescence intensity as shown by Figure 2 left. The higher the oxygen concentration is, the shorter the decay time will be. By modulating the excitation, the decay time is transformed into a phase-shift of the modulated fluorescence signal, which is independent of fluorescent intensity and thus of potential aging (Figure 2 right).
Figure 2 Fluorescence decay time (left) and modulated signals (right)
15
Specifications
The oxygen partial pressure (pO2) is then linked to the corresponding phase-shift measurement (Φ) to build the sensor calibration curve (shown right in Figure 3). This curve is described by the Stern-Volmer equation (shown left in Figure 3) where K
-1
mbar
) representing the quenching efficiency of the oxygen and thus the sensor sensitivity, f0 is
a constant and Φ
is the phase-shift at zero oxygen representing the unquenched fluorescence
0
is the indicator quenching constant (in
sv
decay time of the dye. The calibration curve thus relies on two parameters: the phase-shift at zero oxygen and the luminescent spot sensitivity, K
. The dissolved oxygen concentration is
sv
then calculated with Henry’s law using the water solubility curve as a function of the temperature.

2.4 Hardware description

The instrument hardware is made of one main board, and one measurement board for the measurement channel (= the sensor).
The main board includes the controls for power, display, the touch screen, the barometric sensor, the alarms, and communication ports. The measurement board performs measurements and executes commands from the main board. It holds the "Analog output" and "Relays" that send information to external systems.
A hardware watchdog is activated at program start up, to check that the system is not frozen (i.e. infinite loop, system crash, etc.). If the watchdog is not refreshed by the software every minute, the measurement display, the relays and the analog output are frozen up to 2 minutes. Then the reset shuts down the instrument for 10 seconds and the start-up procedure is performed. At the same time all the hardware (sensor, measurement board) are reset.
Figure 3 Stern-Volmer equation and calibration curve
16

2.5 Security level table

Main 01234View 01234
iew XXXXX Numeric
Measurement XXXXX Graphic
Calibration X X X Statistical XXXXX Inputs/outputs X X X Event Communication X X Diagnostic Securit
y
X X Configure Products X X X Global config X X Measurement 01234
Services X X Config instrument
Config channel Measurement file
Gas senso
r
01234
Calibration
Calibration 01234
erification
Gas senso
r
Configuration
Baromete
r
Reports
Reports
Reports 0 1234
Inputs/Outputs 01234 Senso
r
Snooze
Baromete
r
iew Relays Analog outputs
Communication 01234
RS 485 RS 485 simple Profibus DP USB-
A
HTTP / TCPIP
Securit
y
01234
Configuration Access tabl
e
iew log file
Products 01234
Select product Modify produc
Global config 01234
Save config Select config
Services 01234
Diagnostic Language Clock Screen Buzzer Boards info Batteries Soft download More
Security level : 01234
vailable
Optional
Not available today
Diagram Legend:
A cross means that the user who has this user security level can access this function or setting (see User management on page 88).
Note: When not shown, the sub-levels carry the same security level as the level above.
Specifications
V
Note: For the USB-A option in the Communication Menu, level 4 access is required to import the access table data.
XXXXX
XXXXX
XXXXX
XXXXX
XX
XX XX XX
XXX
XX
XXX
V
XX
XXX
XX XX
XX XX XX XX XX
V
tXX
XX
XXX
XX XX
XX XX XX XX XX XX XX
A
V
X X
X X
XXX
XX XX
XXX XXX
XX
XXX
XXX
XX
17
Specifications

2.6 Default parameters

The table below indicates the factory default configurations. The instrument has these settings when started for the first time.
Parameter Default settings Customer settings Security Disabled Measurement
Measurement mode Continuous Measurement interval 2 seconds Data filter Disabled Medium Liquid Gas unit type Dissolved Gas unit ppm-ppb
Liquid
Display resolution XXX.X Storage mode Rolling buffer User offset Disabled Out of range protection Enabled
Temp unit °C
K1100 low and high range - Water M1100 low range - Beer M1100 high range - Water
Pressure unit bar Calibration
Mode Zero calibration Hold Enabled Auto-end Enabled Interferences Disabled
Analog outputs
Range 4-20 mA Outputs Gas measurement Extended mode Disabled Characteristics Monolinear mode
Alarm relays Disabled Thermal cutoff Enabled
Thermal cutoff temp
Calibration timer Disabled Service timer Disabled Buzzer
Screen tap Enabled Alarm sound Disabled
Display
K1100 - 40°C M1100 - 30°C
18
Minigraph Enabled Temperature Disabled

2.7 M1100 EHEDG Certification

Specifications
19
Specifications
20

Section 3 Installation

This section provides necessary information to install and connect the analyzer. The installation of the analyzer should be performed in accordance with relevant local regulations.
Electrocution Hazard. Do not connect AC power to a 5 VDC powered model.
Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical connections.
Potential Electrocution Hazard. If this equipment is used outdoors or in potentially wet locations a Ground Fault Interrupt device must be used for connecting the equipment to its main power source.
DANGER
WARNING
WARNING
WARNING
Personal Injury Hazard. Only qualified personnel should conduct the tasks described in this section of the manual.
Install the device in a location and position that gives easy access to the disconnect device and its operation.

3.1 Unpacking

Remove carefully the instrument and its accessories from the box and packing material, referring to the packing list included to confirm that everything has been delivered.
Potential Electrocution Hazard. A protective earth (PE) ground connection is required for both 100-240 VAC and 5 VDC wiring applications. Failure to connect a good PE ground connection can result in shock hazards and poor performance due to electromagnetic interferences. ALWAYS connect a good PE ground to the controller terminal.
CAUTION
NOTICE
NOTICE
Potential Instrument Damage. Delicate internal electronic components can be damaged by static electricity, resulting in degraded performance or eventual failure.
Please visually inspect the instrument for shipping damage. If anything is missing or damaged, contact the manufacturer or your dealer immediately.
You may want to retain the box and other packing material in case later you need to ship the instrument (see Storage, handling and transportation on page 99). Please dispose safely and ecologically of the box and packing material (if not stored for future use).
Please read through this manual thoroughly before carrying out the installation.
21
Installation

3.2 Installation check list

For a complete installation, proceed to the following actions following the instructions in this manual very carefully:
1. Install the 410 analyzer (section 3.3 on page 23 through section 3.8 on page 34).
2. Install the sensor in the sample pipe or flow chamber and connect it to the instrument
(section 3.9 on page 35).
3. Turn the instrument on and set the operating language (section 13.2 on page 95).
4. Set the security levels, users ID’s and passwords (Section 10 on page 87).
5. Verify that the sensor cap selected (i.e. low or high range: K/M1100-L or K/M1100-H)
corresponds to the sensor in use (section 6.2 on page 52).
6. The measurement liquid is set by default to water for the K1100 and M1100 high range
sensors, and beer for the M1100 low range sensor. For the M1100 low range sensor, change this to water if the sample being measured is not beer (section 6.2 on page 52).
7. Enable thermal cutoff and set it to the minimum possible value (e.g. 10°C if the liquid in the
sample line is at 0-5°C). This is critical to ensure long-term stability (section 6.2 on
page 52).
8. Set the measurement interval according to your response time needs (section 6.2 on
page 52).
9. Enable the calibration timer and set the number of days to 180 days (6 months) or
according to your quality needs (section 13.2 on page 95), to ensure a regular sensor calibration.
10. Enable the service timer and set the number of days to 360 days (1 year) or according to
your quality needs (Service timer on page 95), to ensure a regular sensor service.
11. If required, program the relay and analog outputs to ensure an event is set when a
calibration or service is required. These can be programmed for each as custom events (Section 8 on page 61). Note that when a calibration or service timer has expired, the instrument will automatically display this information as a warning message (see the table entitled List of Events on page 101).
As the system is factory calibrated and does not require an initial calibration (refer to Calibration
Menu on page 55 for more details), the instrument and sensor should now be ready for
operation. If a problem should arise, please refer initially to Troubleshooting on page 99. If the difficulty cannot be overcome, please contact your Hach Lange representative who will be happy to assist you.
22

3.3 Wall mount and pipe mount instruments

3.3.1 Instrument dimensions

Installation
Figure 4 Wall/Pipe mount instrument dimensions (in millimeters)
23
Installation

3.3.2 Wall mounting

Attach the U bracket (provided) to the wall with two screws (not provided).
Tilt the instrument slightly backwards to align the bracket pins and the insertion slots, and slide the instrument onto the bracket as shown.
Insert the 2 locking screws with washers through the side slots.
Adjust instrument angle for better screen vision, and lock both side screws.
Figure 5 Wall mount bracket

3.3.3 Pipe mounting

Assemble the pipe mount bracket to the U-bracket, using the two screws provided
Attach this assembly to the pipe using two clamps (not provided) as shown on the left
The rest of the procedure is similar to the wall mount version, pictured above.
Slide the instrument onto the bracket.
Insert the 2 locking screws with washers through the side slots.
Adjust the instrument angle for better screen vision, and lock both side screws.
Figure 6 Pipe mount diagram
24

3.3.4 Connections (bottom of instrument)

A square key is provided to open the instrument front panel locks. The two locks are located on the right side of the instrument on the top and bottom panels (bottom panel indicated with the number 9 in Figure 7 below).
The front panel can be easily pivoted to the left as shown below. To retain the instrument waterproof tightness, make sure the seal is clean and in good condition before closing the front panel.
Installation
Figure 7 Wall and pipe mount connection
panel
1 - Power cable 6 - External pressure sensor connection 2 - USB-B client 4 pin connector 7 - Input/Output 2 cable gland 3 - Ethernet cable gland 8 - Input/Output 1 cable gland 4 - Sensor connection 9 - Keylock 5 - USB-A host connector for mass storage device
Note: The type of power cable connection will vary depending on the instrument specification.
25
Installation

3.4 Panel mount instrument

3.4.1 Instrument dimensions

26
Figure 8 Panel mount instrument dimensions (in millimeters)

3.4.2 Mounting

Figure 9 Panel mount bracket frame
Installation
1. Cut an opening in the panel to accommodate
the bracket frame provided (this is the same size as previous generations of ORBISPHERE type 3600 instruments).
Figure 10 Opening dimensions
2. Install the provided frame in the opening.
3. Fold the 6 tabs over the panel lips, using
adjustable joint pliers.
4. Slide the instrument in the bracket frame. The
instrument should go over the four “T” pins. Rotate the 4 fast locking screws on both sides of the front panel and slide it in.
5. Rotate the 4 fast locking screws 1/4 turn twice in
the lock direction as indicated on the side of the front panel. This locks the instrument in place on the four “T” pins.
6. To access the connections inside the
instrument, remove the instrument housing (six screws on the back panel, and slide the housing back out)
7. Pass the cables through the housing, then
through the cable gland (if applicable) and then perform the connections as detailed below.
Note: Do not forget to pass the cable through the housing before passing it through the cable gland on the back panel.
27
Installation
Alternative Instrument Mounting Procedure
When it is not convenient to work from the back of the panel, the instrument can be connected before fitting in the panel.
1. Install the panel support frame in the panel opening
2. Slip the cables through the panel opening
3. Remove the instrument cover
4. Slip the cables through the instrument cover
5. Slip the cables through the instrument back panel cable glands
6. Connect the cables to the instrument electronic boards
7. Tighten the cable glands
8. Reinstall the instrument cover
9. Install the instrument in the panel opening

3.4.3 Connections (bottom of instrument)

28
Figure 11 Panel mount connection panel
1 - Power cable 5 - Input/Output 1 cable gland 2 - Ethernet cable gland 6 - Sensor connection 3 - USB-A host connector for mass storage device 7 - External pressure sensor connection 4 - USB-B client 4 pin connector 8 - Input/Output 2 cable gland
Note: The type of power cable connection will vary depending on the instrument specification.
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