Hach-Lange ORBISPHERE K1100, ORBISPHERE M1100 User Manual

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DOC024.52.93023

ORBISPHERE Model K-M1100 Sensor and Model

410 Analyzer

User Manual

12/2013, Edition 9

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Page 3

Table of Contents

Section 1 General Information.........................................................................................................5

1.1 Disclaimer .................................................................................................................................... 5

1.2 Contact information......................................................................................................................5

1.3 Safety information ........................................................................................................................ 5

1.3.1 Use of hazard information................................................................................................... 5

1.3.2 Safety precautions ..............................................................................................................6

1.3.3 Service and repairs .............................................................................................................6

1.3.4 Precautionary labels............................................................................................................7

1.3.5 Intended use of this equipment........................................................................................... 7

1.4 Product recycling information.......................................................................................................8

1.5 Product disposal ........................................................................................................................ 10

1.6 Restriction of hazardous substances (RoHS) ............................................................................11

Section 2 Specifications.................................................................................................................. 13

2.1 Sensor descriptions ................................................................................................................... 13

2.2 Technical data............................................................................................................................13

2.3 General principle of operation.................................................................................................... 15

2.4 Hardware description .................................................................................................................16

2.5 Security level table.....................................................................................................................17

2.6 Default parameters .................................................................................................................... 18

2.7 M1100 EHEDG Certification ...................................................................................................... 19

Section 3 Installation........................................................................................................................21

3.1 Unpacking .................................................................................................................................. 21

3.2 Installation check list ..................................................................................................................22

3.3 Wall mount and pipe mount instruments.................................................................................... 23

3.3.1 Instrument dimensions......................................................................................................23

3.3.2 Wall mounting ...................................................................................................................24

3.3.3 Pipe mounting ...................................................................................................................24

3.3.4 Connections (bottom of instrument)..................................................................................25

3.4 Panel mount instrument ............................................................................................................. 26

3.4.1 Instrument dimensions......................................................................................................26

3.4.2 Mounting ...........................................................................................................................27

3.4.3 Connections (bottom of instrument)..................................................................................28

3.5 Connectors assembly instructions .............................................................................................29

3.5.1 Cable gland wiring instructions ......................................................................................... 29

3.5.2 USB-B client adapter cable............................................................................................... 30

3.6 Connection to mains power supply ............................................................................................30

3.6.1 Power supply connection (low voltage instruments) ......................................................... 30

3.6.2 Power supply connection (high voltage instruments)........................................................ 31

3.7 Connections to electronic boards...............................................................................................33

3.7.1 Electronic boards connectors............................................................................................ 33

3.7.2 Main board connections....................................................................................................33

3.7.3 Measurement board..........................................................................................................34

3.8 Measurement alarm relays ........................................................................................................ 34

3.9 Sensor installation......................................................................................................................35

3.9.1 Sensor positioning information.......................................................................................... 35

3.9.2 Recommended sample flow rate.......................................................................................35

3.9.3 Sensor insertion ................................................................................................................35

3.9.4 Sensor removal................................................................................................................. 36

3.9.5 Weld-on stainless steel socket..........................................................................................36

3.9.6 The 32003 insertion/extraction valve ................................................................................ 37

3.9.7 The 33095 and 33096 sensor housing..............................................................................37

3.9.8 Tuchenhagen Varivent® in-line access unit...................................................................... 37

3.9.9 Instrument connections.....................................................................................................38

3.10 Calibration devices...................................................................................................................38

3.10.1 Portable calibration device.............................................................................................. 38

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Table of Contents

3.10.2 ORBISPHERE flow chambers.........................................................................................39

Section 4 User Interface ..................................................................................................................41

4.1 Instrument ..................................................................................................................................41

4.2 Touch screen..............................................................................................................................41

4.2.1 Function keys on the header bar.......................................................................................42

4.2.2 Menu navigation ................................................................................................................43

4.2.3 Rolling list ..........................................................................................................................43

4.2.4 Virtual keyboard ................................................................................................................43

4.2.5 Identification and authorization level .................................................................................44

4.2.6 Warning windows ..............................................................................................................44

4.3 Main menu structure...................................................................................................................45

Section 5 View Menu ........................................................................................................................47

5.1 Selection of the view style..........................................................................................................48

5.2 Configuration of the view styles..................................................................................................49

Section 6 Measurement Menu........................................................................................................51

6.1 Instrument configuration.............................................................................................................51

6.2 Measurement configuration........................................................................................................52

6.3 Measured data storage ..............................................................................................................54

Section 7 Calibration Menu.............................................................................................................55

7.1 Sensor calibration.......................................................................................................................56

7.2 Calibration configuration.............................................................................................................57

7.3 Zero calibration...........................................................................................................................58

7.4 100% humid air calibration (high range sensors only) ...............................................................58

7.5 High level adjustment.................................................................................................................58

7.6 Sensor verification......................................................................................................................58

7.7 Barometric pressure calibration..................................................................................................59

7.8 Calibration reports......................................................................................................................59

Section 8 Inputs/Outputs Menu .....................................................................................................61

8.1 Configure snooze .......................................................................................................................62

8.2 View inputs/outputs ....................................................................................................................62

8.3 Relays ........................................................................................................................................62

8.4 Analog outputs ...........................................................................................................................63

8.5 Analog output characteristics .....................................................................................................67

Section 9 Communication Menu....................................................................................................71

9.1 RS-485 simple mode configuration ............................................................................................72

9.1.1 Data available....................................................................................................................73

9.1.2 Example of use..................................................................................................................76

9.2 PROFIBUS-DP communication (optional)..................................................................................77

9.2.1 Installation .........................................................................................................................77

9.2.2 Input/Output data...............................................................................................................78

9.3 USB-A port (host).......................................................................................................................81

9.4 HTTP/TCP-IP .............................................................................................................................82

9.4.1 Overview ...........................................................................................................................82

9.4.2 PC interface.......................................................................................................................82

9.5 Data file transfer through the USB-B port (client).......................................................................84

9.5.1 PC software installation.....................................................................................................84

9.5.2 Microsoft synchronization software ...................................................................................84

9.5.3 Upload report files .............................................................................................................84

9.6 Printer.........................................................................................................................................86

9.6.1 Printer error messages......................................................................................................86

Section 10 Security Menu................................................................................................................87

10.1 Access rights management......................................................................................................87

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10.2 Configure security ....................................................................................................................88

10.3 User management ................................................................................................................... 88

10.4 User action log file ................................................................................................................... 88

Section 1 1 Products Menu..............................................................................................................89

Section 12 Global Configuration Menu........................................................................................91

Section 13 Services Menu............................................................................................................... 93

13.1 Sensor diagnostics...................................................................................................................95

13.2 Language selection.................................................................................................................. 95

13.3 Clock ........................................................................................................................................ 95

13.4 Screen......................................................................................................................................96

13.5 Buzzer...................................................................................................................................... 96

13.6 Boards info............................................................................................................................... 96

13.7 Batteries................................................................................................................................... 96

13.8 Software download .................................................................................................................. 96

13.9 End application ........................................................................................................................ 96

Section 14 Maintenance and Troubleshooting .......................................................................... 97

14.1 Instrument maintenance .......................................................................................................... 97

14.2 Sensor maintenance ................................................................................................................97

14.2.1 Equipment required......................................................................................................... 97

14.2.2 Sensor spot removal .......................................................................................................97

14.2.3 Sensor spot replacement ................................................................................................ 98

14.3 Storage, handling and transportation.......................................................................................99

14.4 Troubleshooting ....................................................................................................................... 99

14.5 List of events and alarms ....................................................................................................... 101

Section 15 Accessories and Spare Parts.................................................................................. 103

15.1 Instrument .............................................................................................................................. 103

15.2 Sensor....................................................................................................................................103

15.3 Insertion and sampling devices..............................................................................................104

15.4 K1100 kits to order (KTO’s) ................................................................................................... 104

15.5 M1100 kits to order (KTO’s)...................................................................................................105

15.6 Instrument options ................................................................................................................. 107

Section 16 Glossary .......................................................................................................................109

16.1 Gas units................................................................................................................................ 109

16.2 Generic terms and definitions ................................................................................................ 109

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Section 1 General Information

1.1 Disclaimer

The information in this manual has been carefully checked and is believed to be accurate. However, Hach Lange assumes no responsibility for any inaccuracies that may be contained in this manual. In no event will Hach Lange be liable for direct, indirect, special, incidental, or consequential damages resulting from any defect or omission in this manual, even if advised of the possibility of such damages. In the interest of continued product development, Hach Lange reserves the right to make improvements in this manual and the products it describes at any time, without notice or obligation.

Copyright © 2009-2013 by Hach Lange. All rights reserved. No part of the contents of this manual may be reproduced or transmitted in any form or by any means without the written permission of Hach Lange.

1.2 Contact information

Manufacturing site:

HACH LANGE Sàrl 6, route de Compois 1222 Vésenaz SWITZERLAND Tel. +41 22 594 6400 Fax +41 22 594 6499

1.3 Safety information

For safe operation, please read the entire manual before unpacking, setting up, or operating this instrument.

Pay particular attention to all warning and caution statements. Failure to do so could result in serious injury to the operator or damage to the equipment.

To ensure the protection provided by this equipment is not impaired, do not use or install this equipment in any manner other than that which is specified in this manual.

1.3.1 Use of hazard information

Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.

European HQ:

HACH LANGE GmbH Willstätterstraße 11 40549 Düsseldorf GERMANY Tel. +49 211 52 880 Fax +49 211 52 88143

DANGER

WARNING

Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious injury.

CAUTION

Indicates a potentially or imminently hazardous situation that may result in minor or moderate injury.

NOTICE

Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special emphasis.

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General Information

1.3.2 Safety precautions

Always remove power from the controller before performing maintenance activities.

Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical connections.

Potential Electrocution Hazard. If this equipment is used outdoors or in potentially wet locations a Ground Fault Interrupt device must be used for connecting the equipment to its main power source.

DANGER

WARNING

Potential Electrocution Hazard. Connect only safety low voltage < 33 VAC RMS.

CAUTION

Personal Injury Hazard. Only qualified personnel should conduct the tasks described in this manual.

NOTICE

Install the device in a location and position that gives easy access to the disconnect device and its operation.

NOTICE

Potential Instrument Damage. Delicate internal electronic components can be damaged by static electricity, resulting in degraded performance or eventual failure.

• The power cord plug connection is also used as a main power switch.

• The instrument must be connected to an electrical system which complies with applicable local regulations.

• All the cables connected to the instrument must be fire resistant, type UL94V-1

• The operator must read and understand this manual before using the instrument .

• The instrument will not be used as a safety device. It does not provide a security function in a hazardous process.

1.3.3 Service and repairs

None of the analyzer’s components can be serviced by the user. Only personnel from Hach Lange or its approved representative(s) is (are) authorized to attempt repairs to the system and only components formally approved by the manufacturer should be used. Any attempt at repairing the analyzer in contravention of these principles could cause damage to the analyzer and corporal injury to the person carrying out the repair. It renders the warranty null and void and could compromise the correct working of the analyzer and the electrical integrity or the CE compliance of the analyzer.

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1.3.4 Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed.

This symbol, when noted on a product, indicates a potential hazard which could cause serious personal injury and/or death. The user should reference this instruction manual for operation and/or safety information.

This symbol, when noted on a product enclosure or barrier, indicates that a risk of electrical shock and/or electrocution exists and indicates that only individuals qualified to work with hazardous voltages should open the enclosure or remove the barrier.

This symbol, when noted on the product, indicates that the marked item can be hot and should not be touched without care.

This symbol, when noted on the product, indicates the presence of devices sensitive to electrostatic discharge and indicates that care must be taken to prevent damage to them.

This symbol, when noted on the product, identifies a risk of chemical harm and indicates that only individuals qualified and trained to work with chemicals should handle chemicals or perform maintenance on chemical delivery systems associated with the equipment.

General Information

This symbol, if noted on the product, indicates the need for protective eye wear.

This symbol, when noted on the product, identifies the location of the connection for protective earth (ground).

Electrical equipment marked with this symbol may not be disposed of in European public disposal systems. In conformity with European local and national regulations, European electrical equipment users must now return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.

Products marked with this symbol indicates that the product contains toxic or hazardous substances or elements. The number inside the symbol indicates the environmental protection use period in years.

1.3.5 Intended use of this equipment

This high accuracy ORBISPHERE instrument and sensor is designed for the measurement of dissolved oxygen in power applications using the K1100 sensor or in beverage applications using the M1100 sensor.

ORBISPHERE 410 analyzers are available as wall or pipe mount, and rack mount versions. This version of the instrument uses a luminescent dissolved oxygen sensor to determine dissolved oxygen concentrations in the measured sample.

NOTICE

Use of the instrument outside of the environmental conditions described in Technical data on

page 13 may cause damage to the instrument but without endangering the user.

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General Information

1.4 Product recycling information

ENGLISH

Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.

Note: For return for recycling, please contact the equipment

manufacturer or supplier for instructions on how to return end-of-life equipment for proper disposal.

DEUTSCH

Elektrogeräte, die mit diesem Symbol gekennzeichnet sind, dürfen in Europa nach dem 12. August 2005 nicht mehr über die öffentliche Abfallentsorgung entsorgt werden. In Übereinstimmung mit lokalen und nationalen europäischen Bestimmungen (EU-Richtlinie 2002/96/EC), müssen Benutzer von Elektrogeräten in Europa ab diesem Zeitpunkt alte bzw. zu verschrottende Geräte zur Entsorgung kostenfrei an den Hersteller zurückgeben.

Hinweis: Bitte wenden Sie sich an den Hersteller bzw. an den Händler, von dem Sie das Gerät bezogen haben, um Informationen zur Rückgabe des Altgeräts zur ordnungsgemäßen Entsorgung zu erhalten.

FRANCAIS

A partir du 12 août 2005, il est interdit de mettre au rebut le matériel électrique marqué de ce symbole par les voies habituelles de déchetterie publique. Conformément à la réglementation européenne (directive UE 2002/96/EC), les utilisateurs de matériel électrique en Europe doivent désormais retourner le matériel usé ou périmé au fabricant pour élimination, sans frais pour l'utilisateur.

Remarque: Veuillez vous adresser au fabricant ou au fournisseur du matériel pour les instructions de retour du matériel usé ou périmé aux fins d'élimination conforme.

ITALIANO

Le apparecchiature elettriche con apposto questo simbolo non possono essere smaltite nelle discariche pubbliche europee successivamente al 12 agosto 2005. In conformità alle normative europee locali e nazionali (Direttiva UE 2002/96/EC), gli utilizzatori europei di apparecchiature elettriche devono restituire al produttore le apparecchiature vecchie o a fine vita per lo smaltimento senza alcun costo a carico dell’utilizzatore.

Nota: Per conoscere le modalità di restituzione delle apparecchiature a fine vita da riciclare, contattare il produttore o il fornitore dell’apparecchiatura per un corretto smaltimento.

DANSK

Elektriske apparater, der er mærket med dette symbol, må ikke bortskaffes i europæiske offentlige affaldssystemer efter den 12. august 2005. I henhold til europæiske lokale og nationale regler (EU-direktiv 2002/96/EF) skal europæiske brugere af elektriske apparater nu returnere gamle eller udtjente apparater til producenten med henblik på bortskaffelse uden omkostninger for brugeren.

Bemærk: I forbindelse med returnering til genbrug skal du kontakte producenten eller leverandøren af apparatet for at få instruktioner om, hvordan udtjente apparater bortskaffes korrekt.

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General Information

SVENSKA

Elektronikutrustning som är märkt med denna symbol kanske inte kan lämnas in på europeiska offentliga sopstationer efter 2005-08-12. Enligt europeiska lokala och nationella föreskrifter (EU-direktiv 2002/96/EC) måste användare av elektronikutrustning i Europa nu återlämna gammal eller utrangerad utrustning till tillverkaren för kassering utan kostnad för användaren.

Obs! Om du ska återlämna utrustning för återvinning ska du kontakta tillverkaren av utrustningen eller återförsäljaren för att få anvisningar om hur du återlämnar kasserad utrustning för att den ska bortskaffas på rätt sätt.

ESPANOL

A partir del 12 de agosto de 2005, los equipos eléctricos que lleven este símbolo no deberán ser desechados en los puntos limpios europeos. De conformidad con las normativas europeas locales y nacionales (Directiva de la UE 2002/96/EC), a partir de esa fecha, los usuarios europeos de equipos eléctricos deberán devolver los equipos usados u obsoletos al fabricante de los mismos para su reciclado, sin coste alguno para el usuario.

Nota: Sírvase ponerse en contacto con el fabricante o proveedor de los equipos para solicitar instrucciones sobre cómo devolver los equipos obsoletos para su correcto reciclado.

NEDERLANDS

Elektrische apparatuur die is voorzien van dit symbool mag na 12 augustus 2005 niet meer worden afgevoerd naar Europese openbare afvalsystemen. Conform Europese lokale en nationale wetgegeving (EU-richtlijn 2002/96/EC) dienen gebruikers van elektrische apparaten voortaan hun oude of afgedankte apparatuur kosteloos voor recycling of vernietiging naar de producent terug te brengen.

Nota: Als u apparatuur voor recycling terugbrengt, moet u contact opnemen met de producent of leverancier voor instructies voor het terugbrengen van de afgedankte apparatuur voor een juiste verwerking.

POLSKI

Sprzęt elektryczny oznaczony takim symbolem nie może być likwidowany w europejskich systemach utylizacji po dniu 12 sierpnia 2005. Zgodnie z europejskimi, lokalnymi i państwowymi przepisami prawa (Dyrektywa Unii Europejskiej 2002/96/EC), użytkownicy sprzętu elektrycznego w Europie muszą obecie przekazywać Producentowi stary sprzęt lub sprzęt po okresie użytkowania do bezpłatnej utylizacji.

Uwaga: Aby przekazać sprzęt do recyklingu, należy zwrócić się do producenta lub dostawcy sprzętu w celu uzyskania instrukcji dotyczących procedur przekazywania do utylizacji sprzętu po okresie użytkownia.

PORTUGUES

Qualquer equipamento eléctrico que ostente este símbolo não poderá ser eliminado através dos sistemas públicos europeus de tratamento de resíduos sólidos a partir de 12 de Agosto de 2005. De acordo com as normas locais e europeias (Directiva Europeia 2002/96/EC), os utilizadores europeus de equipamentos eléctricos deverão agora devolver os seus equipamentos velhos ou em fim de vida ao produtor para o respectivo tratamento sem quaisquer custos para o utilizador.

Nota: No que toca à devolução para reciclagem, por favor, contacte o produtor ou fornecedor do equipamento para instruções de devolução de equipamento em fim de vida para a sua correcta eliminação.

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General Information

1.5 Product disposal

Note: The following only applies to European customers.

Hach Lange is committed to ensuring that the risk of any environmental damage or pollution caused by any of its products is minimized as far as possible. The European Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC) that came into force on August 13 2005 aims to reduce the waste arising from electrical and electronic equipment; and improve the environmental performance of all those involved in the life cycle of electrical and electronic equipment.

In conformity with European local and national regulations (EU Directive 2002/96/EC stated above), electrical equipment marked with the above symbol may not be disposed of in European public disposal systems after 12 August 2005.

Hach Lange will offer to take back (free of charge to the customer) any old, unserviceable or redundant analyzers and systems which carry the above symbol, and which were originally supplied by Hach Lange. Hach Lange will then be responsible for the disposal of this equipment.

In addition, Hach Lange will offer to take back (at cost to the customer) any old, unserviceable or redundant analyzers and systems which do not carry the above symbol, but which were originally supplied by Hach Lange. Hach Lange will then be responsible for the disposal of this equipment.

Should you wish to arrange for the disposal of any piece of equipment originally supplied by Hach Lange, please contact your supplier or our After Sales Service department in Geneva for instructions on how to return this equipment for proper disposal.

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1.6 Restriction of hazardous substances (RoHS)

The European Union RoHS Directive and subsequent regulations introduced in member states and other countries limits the use of six hazardous substances used in the manufacturing of electrical and electronic equipment.

Currently, monitoring and control instruments do not fall within the scope of the RoHS Directive, however Hach Lange has taken the decision to adopt the recommendations in the Directive as the target for all future product design and component purchasing.

Note: The following only applies to exports of this product into the People’s Republic of China.

General Information

Locking system X Spacer X External connectors X Sensor head X

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General Information

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Section 2 Specifications

2.1 Sensor descriptions

ORBISPHERE K1100 sensor

The high accuracy K1100 sensor is a luminescent sensor measuring dissolved oxygen, and has been optimized specifically for measurements in water processes in the power industry.

ORBISPHERE M1100 sensor

The high accuracy M1100 sensor is a luminescent sensor measuring dissolved oxygen, and has been optimized specifically for measurements in beer processes in the beverage industry.

2.2 Technical data

IP 65 Totally protected against dust. Protected against low pressure jets of water from all directions.

Enclosure ratings

NEMA4X (wall mount only) Totally protected against dust.

Protected against pressure jets of water from all directions. EMC requirements EN61326-1:2006 Directive 2004/108/EEC

Certifications

Analog outputs

Measurement alarm relays on the measurement board

CE compliance EN61010-1: 2010 Directive 2006/95/EEC

Safety rating

3 Smart 0/4 – 20 mA (500 Ohms), programmable as linear or tri-linear, configurable to send diagnostics or alarm information.

Three alarm relays 1A-30 VAC or 0.5A-50 VDC on a resistance load Configurable to Normally Open [NO] or Normally Closed [NC] contacts by changing the

jumper positions.

Controller

ETL, conforming to UL 61010-1 and CSA 22.2 No. 61010-1

WARNING

System alarm relay on the main board

Digital communication

Data storage

User interface

Potential Electrocution Hazard. Connect only safety low voltage < 33 VAC RMS.

One "instrument system alarm" relay per instrument 1A-30 VAC or 0.5A-50 VDC on a resistance load Normally closed [NC] (NO relay also available) when instrument is turned on. Opens when

a system alarm is detected, and when it does not receive any signal.

WARNING

Potential Electrocution Hazard. Connect only safety low voltage < 33 VAC RMS.

RS485 Profibus DP (optional) Ethernet USB-client to download data to and from a computer USB-host to download data with a USB memory stick Rolling buffer or store once mode for up to 1000 measurements and 1000 operator actions Holds calibration records for the last 10 calibrations

Touch-screen panel

Password protection

Displays concentration, trend graph, diagnostics, alarm status, historical data.

Five levels of authorised access to configuration and data management

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Specifications

Sensor

Sample temperature

Sample pressure 1 to 20 bar absolute (14.5 to 290 psia) Sample flow rate requirement 50 to 300 mL/min

Sample types

CIP

Measurement range

Repeatability

Reproducibility

Accuracy

Limit of detection (LOD)

Response time (90%)

Warm-up time None Display resolution 0.1 ppb

Calibration

Calibration sample

Measurement from -5 to 50°C (23 to 122°F) Sensor resistant to temperature from -5 to 100°C (23 to 212°F)

K1100 sensor Water only M1100 sensor (low range) Water and beer M1100 sensor (high range) Water, beer, wine, wort and carbonated drinks K1100 sensor Not designed for use in CIP processes M1100 sensor Resistant to all common CIP methods Low range sensors: 0 to 2,000 ppb (dissolved)

High range sensors: 0 to 40 ppm (dissolved) Low range sensors: ± 0.4 ppb or 1%, whichever is the greater

High range sensors: ± 0.015 ppm or ± 2% whichever is the greater Low range sensors: ± 0.8 ppb or 2%, whichever is the greater

High range sensors: ± 0.02 ppm or ± 3% whichever is the greater Low range sensors: ± 0.8 ppb or 2%, whichever is the greater

High range sensors: ± 0.02 ppm or ± 3% whichever is the greater Low range sensors: 0.6 ppb

High range sensors: 0.015 ppm Low range sensors: < 10 seconds in gas phase; < 30 seconds in liquid phase

High range sensors: < 10 seconds in gas phase; < 50 seconds in liquid phase

Low range sensors: Single point calibration (zero) High range sensors: Two at cap replacement (zero and air), one during use (air)

Low range sensors: Standard 99.999% N High range sensors: Standard 99.999% N2 (quality 30) or equivalent oxygen free gas, air

(quality 50) or equivalent oxygen free gas

Accessories

Active spots, spare sensors, tool kit, portable calibration setup, etc.

Accessories

In process sensor installation devices

Ambient temperature -5 to 50 °C (23 to 122 °F) Humidity 0 to 95% non-condensing relative humidity

Power supply

Wall (pipe) mount controller 3.8 kg Panel mount controller 2.9 kg M1100 12 mm (PG 13.5) sensor 0.6 kg K1100 and M1100 28 mm sensor 0.74 kg Calibration device 0.7 kg

Ask your local Hach Lange representative for more details on all available spare parts and accessories.

Installation

ORBISPHERE insertion/extraction valve for installation on Varinline® access units ORBISPHERE 28 mm sensor weld-on socket PG 13.5 stationary housing for installation on Varinline® access units

Note: This device is only available for the M1100 sensor

28 mm stationary housing for installation on Varinline® access units

Universal 85-264 VAC @ 50/60 Hz, 25 VA 10-36 VDC, 25 W

Weights

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2.3 General principle of operation

Optical sensing of oxygen originates from the work of Kautsky in 1939 where he demonstrated that oxygen can dynamically quench the fluorescence of an indicator (decrease the quantum yield). This principle has been reported in various fields of application such as monitoring aquatic biology in waste water, tests for blood gas analysis and cell culture monitoring. The method is now recognized by ASTM (American Society for Testing and Materials) for the measurement of oxygen in water. Compared to classical oxygen detection using electrochemical sensors, luminescent technology offers several advantages such as no oxygen consumption, independence from sample flow velocity, no electrolyte and low maintenance.

Optical sensing of oxygen is based on the measurement of the red fluorescence of a dye/indicator illuminated with a blue light as shown in Figure 1.

Specifications

Figure 1 Principle of optical oxygen detection using fluorescent dye

The dye fluorescence is quenched by the presence of oxygen. The oxygen concentration can be calculated by measuring the decay time of the fluorescence intensity as shown by Figure 2 left. The higher the oxygen concentration is, the shorter the decay time will be. By modulating the excitation, the decay time is transformed into a phase-shift of the modulated fluorescence signal, which is independent of fluorescent intensity and thus of potential aging (Figure 2 right).

Figure 2 Fluorescence decay time (left) and modulated signals (right)

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Specifications

The oxygen partial pressure (pO2) is then linked to the corresponding phase-shift measurement (Φ) to build the sensor calibration curve (shown right in Figure 3). This curve is described by the Stern-Volmer equation (shown left in Figure 3) where K

-1

mbar

) representing the quenching efficiency of the oxygen and thus the sensor sensitivity, f0 is

a constant and Φ

is the phase-shift at zero oxygen representing the unquenched fluorescence

is the indicator quenching constant (in

decay time of the dye. The calibration curve thus relies on two parameters: the phase-shift at zero oxygen and the luminescent spot sensitivity, K

. The dissolved oxygen concentration is

then calculated with Henry’s law using the water solubility curve as a function of the temperature.

2.4 Hardware description

The instrument hardware is made of one main board, and one measurement board for the measurement channel (= the sensor).

The main board includes the controls for power, display, the touch screen, the barometric sensor, the alarms, and communication ports. The measurement board performs measurements and executes commands from the main board. It holds the "Analog output" and "Relays" that send information to external systems.

A hardware watchdog is activated at program start up, to check that the system is not frozen (i.e. infinite loop, system crash, etc.). If the watchdog is not refreshed by the software every minute, the measurement display, the relays and the analog output are frozen up to 2 minutes. Then the reset shuts down the instrument for 10 seconds and the start-up procedure is performed. At the same time all the hardware (sensor, measurement board) are reset.

Figure 3 Stern-Volmer equation and calibration curve

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2.5 Security level table

Main 01234View 01234

iew XXXXX Numeric

Measurement XXXXX Graphic

Calibration X X X Statistical XXXXX Inputs/outputs X X X Event Communication X X Diagnostic Securit

X X Configure Products X X X Global config X X Measurement 01234

Services X X Config instrument

Config channel Measurement file

Gas senso

01234

Calibration

Calibration 01234

erification

Gas senso

Configuration

Baromete

Reports

Reports 0 1234

Inputs/Outputs 01234 Senso

Snooze

Baromete

iew Relays Analog outputs

Communication 01234

RS 485 RS 485 simple Profibus DP USB-

HTTP / TCPIP

Securit

01234

Configuration Access tabl

iew log file

Products 01234

Select product Modify produc

Global config 01234

Save config Select config

Services 01234

Diagnostic Language Clock Screen Buzzer Boards info Batteries Soft download More

Security level : 01234

vailable

Optional

Not available today

Diagram Legend:

A cross means that the user who has this user security level can access this function or setting (see User management on page 88).

Note: When not shown, the sub-levels carry the same security level as the level above.

Specifications

Note: For the USB-A option in the Communication Menu, level 4 access is required to import the access table data.

XXXXX

XX XX XX

XXX

XX XX

XX XX XX XX XX

tXX

XXX

XX XX

XX XX XX XX XX XX XX

X X

XXX

XX XX

XXX XXX

XXX

Page 20

Specifications

2.6 Default parameters

The table below indicates the factory default configurations. The instrument has these settings when started for the first time.

Parameter Default settings Customer settings Security Disabled Measurement

Measurement mode Continuous Measurement interval 2 seconds Data filter Disabled Medium Liquid Gas unit type Dissolved Gas unit ppm-ppb

Liquid

Display resolution XXX.X Storage mode Rolling buffer User offset Disabled Out of range protection Enabled

Temp unit °C

K1100 low and high range - Water M1100 low range - Beer M1100 high range - Water

Pressure unit bar Calibration

Mode Zero calibration Hold Enabled Auto-end Enabled Interferences Disabled

Analog outputs

Range 4-20 mA Outputs Gas measurement Extended mode Disabled Characteristics Monolinear mode

Alarm relays Disabled Thermal cutoff Enabled

Thermal cutoff temp

Calibration timer Disabled Service timer Disabled Buzzer

Screen tap Enabled Alarm sound Disabled

Display

K1100 - 40°C M1100 - 30°C

Minigraph Enabled Temperature Disabled

Page 21

2.7 M1100 EHEDG Certification

Specifications

Page 22

Specifications

Page 23

Section 3 Installation

This section provides necessary information to install and connect the analyzer. The installation of the analyzer should be performed in accordance with relevant local regulations.

Electrocution Hazard. Do not connect AC power to a 5 VDC powered model.

Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical connections.

Potential Electrocution Hazard. If this equipment is used outdoors or in potentially wet locations a Ground Fault Interrupt device must be used for connecting the equipment to its main power source.

DANGER

WARNING

Personal Injury Hazard. Only qualified personnel should conduct the tasks described in this section of the manual.

Install the device in a location and position that gives easy access to the disconnect device and its operation.

3.1 Unpacking

Remove carefully the instrument and its accessories from the box and packing material, referring to the packing list included to confirm that everything has been delivered.

Potential Electrocution Hazard. A protective earth (PE) ground connection is required for both 100-240 VAC and 5 VDC wiring applications. Failure to connect a good PE ground connection can result in shock hazards and poor performance due to electromagnetic interferences. ALWAYS connect a good PE ground to the controller terminal.

CAUTION

NOTICE

Potential Instrument Damage. Delicate internal electronic components can be damaged by static electricity, resulting in degraded performance or eventual failure.

Please visually inspect the instrument for shipping damage. If anything is missing or damaged, contact the manufacturer or your dealer immediately.

You may want to retain the box and other packing material in case later you need to ship the instrument (see Storage, handling and transportation on page 99). Please dispose safely and ecologically of the box and packing material (if not stored for future use).

Please read through this manual thoroughly before carrying out the installation.

Page 24

Installation

3.2 Installation check list

For a complete installation, proceed to the following actions following the instructions in this manual very carefully:

1. Install the 410 analyzer (section 3.3 on page 23 through section 3.8 on page 34).

2. Install the sensor in the sample pipe or flow chamber and connect it to the instrument

(section 3.9 on page 35).

3. Turn the instrument on and set the operating language (section 13.2 on page 95).

4. Set the security levels, users ID’s and passwords (Section 10 on page 87).

5. Verify that the sensor cap selected (i.e. low or high range: K/M1100-L or K/M1100-H)

corresponds to the sensor in use (section 6.2 on page 52).

6. The measurement liquid is set by default to water for the K1100 and M1100 high range

sensors, and beer for the M1100 low range sensor. For the M1100 low range sensor, change this to water if the sample being measured is not beer (section 6.2 on page 52).

7. Enable thermal cutoff and set it to the minimum possible value (e.g. 10°C if the liquid in the

sample line is at 0-5°C). This is critical to ensure long-term stability (section 6.2 on

page 52).

8. Set the measurement interval according to your response time needs (section 6.2 on

page 52).

9. Enable the calibration timer and set the number of days to 180 days (6 months) or

according to your quality needs (section 13.2 on page 95), to ensure a regular sensor calibration.

10. Enable the service timer and set the number of days to 360 days (1 year) or according to

your quality needs (Service timer on page 95), to ensure a regular sensor service.

11. If required, program the relay and analog outputs to ensure an event is set when a

calibration or service is required. These can be programmed for each as custom events (Section 8 on page 61). Note that when a calibration or service timer has expired, the instrument will automatically display this information as a warning message (see the table entitled List of Events on page 101).

As the system is factory calibrated and does not require an initial calibration (refer to Calibration

Menu on page 55 for more details), the instrument and sensor should now be ready for

operation. If a problem should arise, please refer initially to Troubleshooting on page 99. If the difficulty cannot be overcome, please contact your Hach Lange representative who will be happy to assist you.

Page 25

3.3 Wall mount and pipe mount instruments

3.3.1 Instrument dimensions

Installation

Figure 4 Wall/Pipe mount instrument dimensions (in millimeters)

Page 26

Installation

3.3.2 Wall mounting

Attach the U bracket (provided) to the wall with two screws (not provided).

Tilt the instrument slightly backwards to align the bracket pins and the insertion slots, and slide the instrument onto the bracket as shown.

Insert the 2 locking screws with washers through the side slots.

Adjust instrument angle for better screen vision, and lock both side screws.

Figure 5 Wall mount bracket

3.3.3 Pipe mounting

Assemble the pipe mount bracket to the U-bracket, using the two screws provided

Attach this assembly to the pipe using two clamps (not provided) as shown on the left

The rest of the procedure is similar to the wall mount version, pictured above.

Slide the instrument onto the bracket.

Insert the 2 locking screws with washers through the side slots.

Adjust the instrument angle for better screen vision, and lock both side screws.

Figure 6 Pipe mount diagram

Page 27

3.3.4 Connections (bottom of instrument)

A square key is provided to open the instrument front panel locks. The two locks are located on the right side of the instrument on the top and bottom panels (bottom panel indicated with the number 9 in Figure 7 below).

The front panel can be easily pivoted to the left as shown below. To retain the instrument waterproof tightness, make sure the seal is clean and in good condition before closing the front panel.

Installation

Figure 7 Wall and pipe mount connection

panel

1 - Power cable 6 - External pressure sensor connection 2 - USB-B client 4 pin connector 7 - Input/Output 2 cable gland 3 - Ethernet cable gland 8 - Input/Output 1 cable gland 4 - Sensor connection 9 - Keylock 5 - USB-A host connector for mass storage device

Note: The type of power cable connection will vary depending on the instrument specification.

Page 28

Installation

3.4 Panel mount instrument

3.4.1 Instrument dimensions

Figure 8 Panel mount instrument dimensions (in millimeters)

Page 29

3.4.2 Mounting

Figure 9 Panel mount bracket frame

Installation

1. Cut an opening in the panel to accommodate

the bracket frame provided (this is the same size as previous generations of ORBISPHERE type 3600 instruments).

Figure 10 Opening dimensions

2. Install the provided frame in the opening.

3. Fold the 6 tabs over the panel lips, using

adjustable joint pliers.

4. Slide the instrument in the bracket frame. The

instrument should go over the four “T” pins. Rotate the 4 fast locking screws on both sides of the front panel and slide it in.

5. Rotate the 4 fast locking screws 1/4 turn twice in

the lock direction as indicated on the side of the front panel. This locks the instrument in place on the four “T” pins.

6. To access the connections inside the

instrument, remove the instrument housing (six screws on the back panel, and slide the housing back out)

7. Pass the cables through the housing, then

through the cable gland (if applicable) and then perform the connections as detailed below.

Note: Do not forget to pass the cable through the housing before passing it through the cable gland on the back panel.

Page 30

Installation

Alternative Instrument Mounting Procedure

When it is not convenient to work from the back of the panel, the instrument can be connected before fitting in the panel.

1. Install the panel support frame in the panel opening

2. Slip the cables through the panel opening

3. Remove the instrument cover

4. Slip the cables through the instrument cover

5. Slip the cables through the instrument back panel cable glands

6. Connect the cables to the instrument electronic boards

7. Tighten the cable glands

8. Reinstall the instrument cover

9. Install the instrument in the panel opening

3.4.3 Connections (bottom of instrument)

Figure 11 Panel mount connection panel

1 - Power cable 5 - Input/Output 1 cable gland 2 - Ethernet cable gland 6 - Sensor connection 3 - USB-A host connector for mass storage device 7 - External pressure sensor connection 4 - USB-B client 4 pin connector 8 - Input/Output 2 cable gland

Note: The type of power cable connection will vary depending on the instrument specification.

Page 31

3.5 Connectors assembly instructions

Potential Electrocution Hazard. In order to maintain the NEMA/IP environmental ratings of the enclosure, use only conduit fittings and cable glands rated for at least NEMA 4X/IP65 to route cables into the instrument.

3.5.1 Cable gland wiring instructions

A waterproof cable gland is provided each time a cable must be connected inside the instrument. The nickel-plated brass cable glands are EMC-types, designed so that the cable shields attach directly to the instrument housing as a ground. Typical cable wiring instructions are detailed below.

Installation

WARNING

Gland parts (washers not shown):

1. Nut

2. Rubber gasket (seal)

3. Gland fitting with O-ring (attached to

instrument housing)

1. Unscrew the cable gland nut. Inside, the assembly is composed of a rubber gasket, and two

metal washers. Note that the ethernet gland on panel and wall mount instruments does not have washers and the gasket is cut.

2. If wiring a sensor cable, the cable has already been prepared so simply remove the piece of

plastic protection from the exposed shielding. For other cables, strip off external insulation as required, and 25 mm of shielding. Strip the

wires about 8 mm from their ends (see illustration below).

3. Pass the cable through the nut, the rubber gasket, and the two washers

4. Pinch the shield so that its entire circumference is pressed between the two washers and

pass the cable into the housing, blocking the cable gland

NOTICE

It is vitally important to ensure the shielding is pinched and secured between the two washers to ensure the shielding attaches directly to the instrument housing as a ground. Failure to do this could cause damage to the instrument, and for sensor cables give incorrect readings.

5. Reattach and tighten the cable gland nut

6. Attach the wires to the corresponding terminal block connections

Page 32

Installation

3.5.2 USB-B client adapter cable

This supplied cable can be used to connect the instrument to a PC.

Connect to the instrument, and connect the USB connector to the USB outlet on the user’s PC.

Figure 12 USB-B adapter cable

3.6 Connection to mains power supply

3.6.1 Power supply connection (low voltage instruments)

For low voltage instruments (10-30 VDC), connection to the mains power supply is with a 7-pin BINDER connector (supplied).

Note: The connectors are grooved to avoid an incorrect fitting to the instrument.

Connect the power cable to the connector as follows:

Pin Connections:

Figure 13 BINDER connector

2) Power 10-30 VDC

5) Ground

7) Earth

1 + 3 + 4 + 6) Unused

Page 33

3.6.2 Power supply connection (high voltage instruments)

High voltage instruments (100-240 VAC) have a 4-pin male connector pre-wired internally with a male BINDER connector ready for mains connection. A compatible female connector is supplied with the instrument.

If this female connector was supplied with a mains power plug already pre-attached (cable part numbers 33031, 33032, 33033 and 33034) then the female connector can be plugged directly into the instrument power connector. The two connectors are grooved to avoid an incorrect fitting. Tighten the female connector to the instrument power connector finger-tight.

If no power cable was ordered with the equipment, a mains power plug must be connected to the supplied female connector as described in the following procedure.

CAUTION

Personal Injury Hazard. Only qualified personnel should conduct the tasks described in this section of the manual.

User-supplied power cable specifications:

• 3-wire (live, neutral and earth)

• cable

• wire selection ≥ 1mm

ø ≥ 7mm; ≤ 9.5mm

, AWG18; ≤ 2.5mm2, AWG14

Installation

WARNING

Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical connections.

Prepare the user-supplied power cable as follows:

Strip off 23 mm (0.9 ins.) of shielding from the power cable. Cut back the live and neutral wires to 15 mm (0.6 ins.) in length but leave the earth wire as is. Then strip off a small amount of external insulation from the three wires as required:

Page 34

Installation

Wire the female connector as follows:

1. Take the narrow end of the connector (4) in one hand and the main body (2) in the other

and unscrew the two. Pull away the cable clamp (3) and unscrew the end plug (1) to reveal the four parts that make up the connector.

2. Loosen the screws on the cable clamp (3) to allow enough room to pass the power cable

through.

3. Pass the power cable through the end plug (1), the main body (2), and the cable clamp (3),

and then connect the three wires (live, neutral and earth) to the connector (4) as follows:

1) Live (brown)

2) Neutral (blue)

3) Not used

Note: The numbers and earth symbol are stamped on the end of the connector. Ensure it is connected correctly.

Earth (green and yellow)

4. Slide the cable clamp (3) back onto the connector (4) and tighten the screws on the clamp

to secure the cable.

5. Screw the two parts (4) and (2) back together.

6. Secure the power cable by screwing the end plug (1) back in place.

7. The female connector can now be plugged directly into the instrument power connector. The

two connectors are grooved to avoid an incorrect fitting. Tighten the female connector to the instrument power connector finger-tight.

Page 35

3.7 Connections to electronic boards

Potential Instrument Damage. Delicate internal electronic components can be damaged by static electricity, resulting in degraded performance or eventual failure.

Note: Any loose connection wires should be bundled tightly together with the use of nylon cable ties.

3.7.1 Electronic boards connectors

Connectors P8 on the main board (Figure 14) and J7 on the measurement board (Figure 17) are made of two parts. Push down carefully the black levers on either side of the connector and pull it out securely. Perform all connections with these connectors unplugged. Once finished, attach the connectors to the boards by pushing them firmly in place (levers up).

3.7.2 Main board connections

Installation

NOTICE

Figure 14 Main board

Connector P8:

1. RS-485 (signal A)

2. RS-485 (signal B)

3. PROFIBUS-DP (GND)

4. PROFIBUS-DP (+ 5 V)

5. PROFIBUS-DP (signal -)

6. PROFIBUS-DP (signal +)

Connector P3:

Figure 15 Connector P8

Figure 16 Connector P3

7. PROFIBUS-DP (signal RTS)

8. Not used

9. Not used

10. Not used

11. System alarm relay (N.O.)

12. System alarm relay (N:C.)

13. System alarm relay (Common)

Ethernet RJ 45. Connect the instrument to the local network by passing an ethernet cable through the ethernet cable gland (gland location illustrated in Figure 7 on page 25 for the wall mount and Figure 11 on page 28 for the panel mount) and connecting to the P3 connector illustrated above.

Page 36

Installation

3.7.3 Measurement board

Figure 17 Measurement board

Connector J7 (inputs & outputs)

Figure 18 Connector J7

Measurement alarms relays:

1. Common

2. Output relay 1

3. Output relay 2

4. Output relay 3

Digital inputs:

9. to 16. Not used

3.8 Measurement alarm relays

Analog current outputs:

5. GND

6. Output 1

7. Output 2

8. Output 3

The three output relays are located on the measurement board.

They can be individually configured to Normally Open (NO) or to Normally Closed (NC) by physically moving the jumper on each relay. On the picture example on the left:

• Upper relay is set to NC

• Middle relay is set to NO

• Lower relay is shown with no jumper

Note: J14 (upper relay) is relay 1 J18 (middle relay) is relay 2 J19 (lower relay) is relay 3

Figure 19 Output relays

Page 37

3.9 Sensor installation

3.9.1 Sensor positioning information

The sensor must be installed in a socket or flow chamber that allows contact with the sample fluid to be analyzed.

The sensor and measuring instrument are connected by a cable. The standard sensor cable lengths are 3, 5, 10, 15 and 20 meters.

Ensure that the sensor will be mounted:

• perpendicular to the pipe

• horizontal

• on a horizontal pipe section (or on flow-ascending vertical pipe)

• minimum of 15 meters away from the pump's discharge side

• in a place where the sample flow is stable and rapid, and as far as possible from:

• valves

• pipe bends

• the suction side of any pumps

• a CO

Note: There may be situations where not all the above conditions can be met. If this is the case, or you have any concerns, please consult your Hach Lange representative to appraise the situation and define the best applicable solution.

injection system or similar

Installation

3.9.2 Recommended sample flow rate

For optimal response time, the recommended sample flow rate for both the K1100 and M1100 sensors is 150 mL/min.

Control the flow with the outlet valve on the flow meter (No. 3 in Figure 20 below) to avoid foam developing inside the flow chamber which could lead to erroneous oxygen measurement values.

Figure 20 Typical measurement schematic

1. Valve to redirect sample for measurement 3. Flow meter with outlet valve

2. Sensor and flow chamber combination 4. Drain

3.9.3 Sensor insertion

• Insert the sensor straight into the flow chamber or socket. Do not twist the sensor.

• Hand tighten the attaching collar.

• Connect the sensor cable.

• Check for leaks; replace O-rings if product leaks are visible.

Page 38

Installation

3.9.4 Sensor removal

• If not using the ORBISPHERE 32003 insertion/extraction valve (see details in The 32003

insertion/extraction valve on page 37) you will need to shut off the sample flow and drain the

sampling circuit of liquid.

• Remove the sensor cable connected at the sensor end.

• Hold the sensor body in one hand to avoid rotation, and unscrew the collar with the other

hand.

• Pull the sensor straight out of the socket or flow chamber.

• Install sensor storage cap and sensor base (to protect the connection).

3.9.5 Weld-on stainless steel socket

The ORBISPHERE 29501 weld-on sensor socket can be used to install a sensor into a stainless steel pipe (min.Ø 50 mm or 2”). When welding the socket to the pipe, check that setback between the pipe’s inner diameter and the sensor tip does not exceed 4 mm (see diagram).

Figure 21 Weld-on sensor socket

Note: Be sure to remove the two O-rings from the socket before welding and leave the sensor’s stainless steel cap screwed on during welding to prevent thread distortion.

Recommendation:

To facilitate sensor removal and installation, we suggest installing the socket in a location where the liquid can be drained quickly and easily. By creating a one meter long piece of pipe (see

Figure 22) with shut off valves at both ends, just a small volume of liquid needs to be drained to

enable sensor removal.

Also, a precise sensor and socket installation can be performed in the workshop, and this assembly can be placed in the production line with minimal down time.

Figure 22 Installation in-line

Page 39

3.9.6 The 32003 insertion/extraction valve

The ORBISPHERE 32003 insertion/extraction valve (illustrated below) allows for sensor removal and installation without having to drain the fluid in the line. It can withstand a pressure of up to 20 bars, with the sensor in place or not.

Sensor insertion is made by inserting the sensor into the housing and tightening the retaining collar until it stops. As the retaining collar is tightened, the valve will open to allow the sample to flow past the sensor head. Remove the sensor by unscrewing the collar and pulling the sensor out. As the collar is unscrewed, the valve will automatically close to avoid any sample spillage.

Installation

Figure 23 ORBISPHERE model 32003 insertion/extraction valve

The diagram above right, shows the sensor in a sample line with the valve open.

Note: This insertion/extraction valve is only available for the M1100-S00 sensor and cannot be used with the M1100-S10 sensor.

3.9.7 The 33095 and 33096 sensor housing

Two other types of sensor housing are available for use with the M1100 sensor but require that the sample flow be turned off prior to insertion or removal of the sensor.

These are the ORBISPHERE 33095 housing (for use with the M1100-S00 sensor) and the ORBISPHERE 33096 housing (for use with the M1100-S10 sensor).

Sensor insertion is made by inserting the sensor into the housing and tightening the retaining collar until it stops. Removal is made by unscrewing the collar and pulling the sensor out. Be sure that the sample flow has been turned off before inserting or removing the sensor.

Note: The M1100-S10 sensor has a PG-13.5 12 mm diameter fitting and can be inserted directly into any existing compatible fitting.

3.9.8 Tuchenhagen Varivent® in-line access unit

The following illustration shows the Tuchenhagen Varivent® In-Line Access Unit.

Figure 24 Tuchenhagen Varivent® in-line access unit

Purchasing a Tuchenhagen Varivent® in-line access unit, or an equivalent fitting with a 68 mm flange diameter from the fitting manufacturer, is required to make use of the ORBISPHERE model 32003, 33095 or 33096 sensor housing devices detailed above.

Page 40

Installation

3.9.9 Instrument connections

The sensor is supplied with a cable having a LEMO connector at both ends. One end is attached to the sensor and the other to the instrument. An illustration of the M1100-S10 sensor with the cable attached is illustrated below:

A red dot can be seen on each LEMO connector and on both the sensor and instrument sockets. Be sure to line up these red dots when connecting the cable to the sensor and instrument. The LEMO connector can then simply be pushed into place.

Refer to the illustration of the connector panels for the correct instrument socket to attach the cable (see Figure 7 on page 25 for the wall and pipe mount instruments and Figure 11 on page

28 for panel instruments).

3.10 Calibration devices

3.10.1 Portable calibration device

Figure 25 Portable calibration device

The portable calibration device (part number 33088 illustrated above) is ideal for calibrating the sensor close to its location in the sample. For calibrating a M1100-S10 sensor, insert the supplied adapter (No. 1 in Figure 25) into the sensor holder on top of the device.

The device is designed to hold a 1 liter gas cylinder (as shown above), but is fully compatible for use with other kinds of gas cylinders. When using other types of gas cylinders, simply connect the gas supply to the Swagelok™ connector (No. 2 in Figure 25), and make sure that the inlet gas pressure does not exceed 2 bars absolute.

Page 41

The gas bottle is not supplied and must be purchased locally. To ensure the calibration works correctly, the calibration gas bottles must be of 99.999% (50) quality or better. Bottles containing 34 liters of compressed gas, with a 5/8-18 UNF (C10) fitting are compatible with the hand-held calibration device and recommended for this purpose.

Empty gas bottles are easily removed from the device. Simply unscrew the small black screw (No. 3 in Figure 25) a few turns, slide the bottle out of the black plastic holder, and unscrew the bottle from the pressure reducer. Follow this same procedure in reverse order to install a new bottle.

3.10.2 ORBISPHERE flow chambers

Note: This is the recommended option for the K1100 sensors.

The ORBISPHERE flow chambers are used to draw the calibration sample past the sensor.

They connect to 6-mm or ¼" stainless steel tubing by means of two Swagelok™ fittings. If necessary, copper or plastic tubing with low permeability can be substituted.

Installation

Dimensions of sensor and flow chamber assembly :

• Width: 50 mm

• Height: 210 mm

(add 100 mm for connection length)

Page 42

Installation

Page 43

Section 4 User Interface

4.1 Instrument

The instrument front panel provides these user interfaces:

• Touch screen acting as display, touch pad and keyboard. Contrast can be adjusted.

• LED, showing when the instrument is on.

• A buzzer which sounds each time the screen is touched, and when an event alarm is set.

Turning Instrument On and Off

There is no power switch on the instrument. The mains must be disconnected to turn the instrument off. The LED indicates when the instrument is on.

Measurement window

The main (numeric) measurement window continuously displays:

• Sensor numeric values

• Measured sensor trends (for the last 10 minutes to last hour)

• Measured sensor data alarm limits and other events

• Temperature

4.2 Touch screen

The user interface on the front panel is a 320x240 pixels display with touch screen. To make navigation user friendly, the interface software is Windows CE based, providing easy selection through menus.

Figure 26 Numeric view

Touching some items on the display calls a related function, similar to a shortcut.

All the measurement, configuration, calibration and "standard service" routines can be called by pressing buttons and menu bars on screen.

Measurement display shows one measurement slope.

Display can be configured to only show a sensor measurement, or to show a parametrized graphic representation of the last measurements.

Page 44

User Interface

4.2.1 Function keys on the header bar

Shortcut to the user login window. Pressing this button for more than 2 seconds calls the ID and password window (see Identification and

authorization level on page 44).

• Closed padlock indicates that the touch screen is locked.

• Open padlock indicates that the instrument is in view mode only,

• When a user is logged in, this box show the authorization level of

This icon is used for adjusting the display brightness to improve visibility. It is available all the time to any user, regardless of the user security level. This icon is a shortcut to the backlight adjustment window. See Screen on page 96.

Short cut to the data storage window. Number shows the number of measurement currently stored in volatile memory.

but no user is logged in (level 0).

this user as 1, 2, 3 or 4 (4 being the highest, see User

management on page 88).

normal (top) - snooze

(bottom)

• No storage

• Store at once: When the buffer is full (1,000 positions), the

recording of measurement stops.

• Rolling buffer: When the buffer is full, the latest measurement set

replaces the oldest one (first-in, first-out)

In the event of an alarm, the “snooze” button stops the instrument buzzer and returns all the relays in the instrument to their normal state during the "snooze time". The icon indicates if the alarms is on “snooze” or not. This "snooze" is configurable (see Configure

snooze on page 62).

Current date and time. This is also a shortcut to the date and time setting window.

Call the contextual menu. This menu is in the header bar and its content is related to the view displayed.

Opens the main menu page for easy navigation through all available menus.

Page 45

4.2.2 Menu navigation

Figure 27 Main menu window

User Interface

Pressing the “menu” button in the header bar calls the main menu. The display is made of three columns:

• The left column is the menus, or submenus (greyed out

options are not available)

• The center column shows a tree view of actual position

inside the menu structure

• The right column has the generic controls detailed below.

Return to previous menu (one step back)

Jump directly to main menu

Close the menu and go back to measurement view display. If the menu button is pressed again, the menu returns to its previous state (tree structure is saved)

4.2.3 Rolling list

Figure 28 Rolling list

4.2.4 Virtual keyboard

Help topics concerning current menu

For convenience, selection through a possible large list of items has been designed with a rolling list, like in this example. Use the up and down arrow to navigate, or select directly one item and press OK.

example

When a text box (alphanumeric field) has to be edited and is pressed, a virtual keyboard appears on screen. It can be used as a PC keyboard (pressing CAP gives access to special keys).

Figure 29 Virtual editing

keyboard

Once values have been entered, press the “ENTER” key to confirm and exit the virtual keyboard.

During the editing, the edited field name is displayed, along with units where applicable.

Page 46

User Interface

4.2.5 Identification and authorization level

Once the access rights have been set, (see User

management on page 88) it is necessary to log in as an

authorized user to get access to the instrument functionalities and settings.

Press the closed padlock for two seconds to open the identification window. The user identification and password must be entered to access functionalities authorized by the security level of the given user (5 levels available, see User

management on page 88).

Figure 30 Identification

window

Note: To get to level 0, press the unlock button and OK, without entering any ID or password.

For security, when the session inactivity delay period has expired (adjustable, via Configure security on page 88), the user is logged off automatically.

4.2.6 Warning windows

Figure 31 Warnings

At various stages, a warning message may be displayed to request confirmation from the operator that his last action(s) must really be saved or cleared, or that there is a problem that did not enable the requested action, such as during instrument calibration (example shown left).

Page 47

4.3 Main menu structure

This is the structure of the main menu which is used to control every functionality of the instrument. These submenus are detailed in the following sections of this Operator Manual.

User Interface

Figure 32 Main menu structure

Page 48

User Interface

Page 49

Section 5 View Menu

Figure 33 View menu

Page 50

View Menu

5.1 Selection of the view style

Numeric view

This is the default view. Display shows the numeric measurement value identified for the gas measurement channel, a graphic showing measurement value evolution during the set time frame, and sample temperature.

The display is refreshed after each measurement cycle (2 seconds). This display can be configured to suit individual conditions and convenience. Both the K1100 and M1100 low range sensors measure dissolved oxygen up to a maximum value of

2,000 ppb. Should the measured concentration go above this value a warning screen will be displayed and the measurement cycle increased from 2 to 60 seconds.

The “> 2.0 ppm” value will blink alternately with an “Out of range” message. An arrow symbol to the right indicates if the value is increasing, decreasing or remaining constant.

Once the value falls below the 2,000 ppb value, then the measurement cycle returns to a 2 second interval.

For K1100 and M1100 high range sensors, the above also applies but the maximum value measured is 40 ppm. Therefore the out of range message will display “> 40 ppm” which is suppressed when the measured value falls below 40 ppm.

Diagnostic view

The diagnostic view contains useful information for troubleshooting purposes.

Statistic view

This feature offers statistical data that matches with Total Quality management tools. Statistics is a tool to better analyze how a process behave. The 410 statistics window gives some useful information.

The statistics are calculated from the data in the measurement file. The values are updated each time a new value is added to this file. Therefore the changes made in the configuration window are considered only once a new value is added.

Cp process capability

Cp is an index used to assess the width of the process spread in comparison to the width of the specification. It is calculated by dividing the allowable spread by the actual spread.

• A Cp of one indicates that the width of the process and the width of the specification are the

same.

• A Cp of less than one indicates that the process spread is greater than the specification. This

means that some of the data lies outside the specification.

• A Cp of greater than one indicates that the process spread is less than the width of the

specification. Potentially this means that the process can fit inside the specification limits

CPk process variability

Cpk takes into account the center of the data relative to the specifications, as well as the variation in the process.

• A Cpk value of one indicates that the tail of the distribution and the specification are an equal

distance from the overall average.

• A Cpk of less than one means that some of the data is beyond the specification limit.

• A Cpk greater than one indicates that the data is within the specification.

• The larger the Cpk, the more central and within specification the data.

CPm process repeatability

Capability index that takes into account variation between the process average and the target. If the process average and the target are the same value, Cpm will be the same as Cpk. If the average drifts from the target, Cpm will be less than Cpk.

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Skewness

View Menu

negative

positive

Figure 34 Skewness

Kurtosis

Figure 35 Kurtosis

An asymmetric frequency distribution is skewed to the left if the lower tail is longer than the upper tail, and skewed to the right if the upper tail is longer than the lower tail. Distributions of positive-valued random variables values are often skewed right.

Kurtosis is a parameter that describes the shape of a random variable’s probability distribution.

The graphs on the left illustrate the notion of kurtosis. The lower curve has higher kurtosis than the upper curve. It is more peaked at the center, and it has fatter tails

5.2 Configuration of the view styles

Numeric view configuration

List of parameters that can be adjusted to customize the numeric view display:

• Display temperature: no, channel temperature

• Display mini graph: yes/no

• Display time base: yes/no

• Upper bound: Adjust graph upper limit

• Lower boun d: Adjust graph lower limit

• Time base: Adjust graph time span

• Grid button: Set up the graph to display the x or y axes, the grid, or the thresholds

• Auto Scale update: Automatically set the graph upper and lower bounds to best fit the actual values

displayed.

• Clean button: Clear the slope displayed. The slope restarts from the left side. Statistic view configuration

Scope:

• Number of values: Statistic calculation range (from 10 to 1,000 values). Number of value taken in

consideration in the log file since last value stored. The recorded values with alarms are not considered for calculation, but are part of the log file.

Histogram:

• Upper limit: Select High or High High alarm value, or a custom value.

•Lower limit: Select Low or Low Low alarm value, or a custom value. Capability:

• Upper limit: Select High or High High alarm value, or a custom value.

•Lower limit: Select Low or Low Low alarm value, or a custom value.

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View Menu

Page 53

Section 6 Measurement Menu

6.1 Instrument configuration

Continuous mode description

Continuous mode is typically used for process measurement.

Continuous mode cycle

• Every 2 sec. measurements are refreshed on the display

• The relays and the analog outputs are updated

• Measurements are continuously stored in memory (volatile and non volatile memory) according to

individual settings

Measurement mode is locked on Continuous. Select the units for barometric pressure and temperature.

Figure 36 Measurement menu

Page 54

Measurement Menu

6.2 Measurement configuration

Measurement configuration

• Sensor: Sensor model.

•Medium: Liquid or gas phase.

• Gas unit type: Partial, Fraction, Dissolved.

• Gas unit: The list of available units depends on unit type selected above.

Note: This is the gas concentration measured by the sensor. When a composite unit is selected (e.g. ppm-ppb) the unit will change depending on the range of the value to display.

•Liquid: For the K1100 sensor this option is locked on water. For the M1100 low range sensor, choose

between water and beer. For the M1100 high range sensor, choose between water, beer, wort, wine and carbonated drink.

• Display resolution: Maximum resolution depends on gas, membrane and unit. A maximum of 5

digits can be displayed. Decimals can be limited to 0, 1, 2 or 3 decimals for easier reading. That does not affect the actual resolution of data measured and stored, but only the data displayed.

• Thermal cutoff: To protect the sensor, the thermal cutoff function allows for setting a sample high

temperature limit. If exceeded (during a Cleaning In Place cycle for example) the electrical signal to the sensor is cut off, the measurement session is suspended and the system displays a “HOT” alarm message. The system resumes when temperature drops to 90% of the specified cutoff temperature.

• Thermal cut off: It is recommended to enable this feature to maximize sensor life and system

performance.

• Thermal cut off temperature: Set to 5°C above sample temperature e.g. if sample temperature

is 2°C, set thermal cut-off to 7°C.

Measurement advanced configuration

Important Note: The offset feature described below should be used for minor measurement adjustments only, and not as an alternative to a sensor calibration. Make sure your sensor has been correctly calibrated before applying this feature.

• Offset enabled: Check this box to enable the user measurement offset option. If checked enter an

offset value or a target value:

• Offset value: Enter an offset value to manually adjust (increase or decrease) the current

measurement value. If the gas unit type or gas unit (defined in the main measurement configuration screen) are changed, the offset value is automatically reset to zero.

• Measurement: This field cannot be updated. It shows the current measurement value with the

offset value applied.

• Target value: Enter a target measurement value. The offset value is then automatically

computed so that the displayed measurement value will be equal to the target value.

• Compute offset: Use this button to recompute the offset value at any time during the

measurement process. The offset value will be computed based on the current and target measurement values.

• Out of range protection: Enabled by default. When enabled and the measured value exceeds the

instrument specification, the measurement interval will be increased to 1minute to protect the lifetime of the sensor spot. If disabled, the lifetime of the spot can be negatively impacted if the sensor is exposed to high oxygen concentrations for long periods of time.

• Measurement interval: This parameter defines the interval for refreshing the measurement value on

the display. Set the value to between 2 and 60 seconds, according to your response time requirements.

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Measurement Menu

Measurement alarms configuration

Set the thresholds for the low/high concentration levels, according to the application. Each alarm type can be individually enabled or disabled without losing its settings.

These events can activate the relays and can be displayed.

•Low-low: 2nd stage for too low concentration

•Low: 1st stage for too low concentration

•High: 1st stage for too high concentration

• High-high: 2nd stage for too high concentration

• Hysteresis: A percentage of the above concentration values. The hysteresis is used to prevent relay

“flickering” when the measurement is just at the alarm levels. Set this to a minimum, but enough to eliminate flickering.

As an example, if the High Alarm is set to 40 units and the Hysteresis is set to 10%, then the High Alarm is activated once the measurement reaches 40 units, but only deactivated once the measurement drops below 36 units. With the Low Alarm the opposite is true, in that if the Low Alarm is set to 20 units and the Hysteresis set to 10%, then the Low Alarm is activated when the measurement drops below 20 units, and deactivated when the measurement rises above 22 units.

• Delay: The delay in seconds, before alarms go on whenever concentration values go above ”High

alarms” or below “Low alarms”. Set this to a minimum value, but enough to avoid alarms for non-representative peaks beyond the set level.

Figure 37 Alarms system diagram

Measurement filter configuration

The filters are aimed at “flattening” the measurement curve in situations where the process shows atypical peak values that could otherwise hamper the interpretation of measurement readings. The filter is applied on the last set of measurements each time a measurement is taken.

• Mean: Mathematical average of the last set (depth) of measurement values.

• Median filter: Allows for eliminating atypical peak measurement values, and average the remaining

ones. The calculation sorts the last measurements set (depth) by values, then delete the highest and lowest values, and averages the remaining values (central depth).

Example for depth 7, central depth 5: Sorted values, both ends eliminated, the average of the center five is then 3.88.

0.7 - 1.1 - 4.0 - 4.3 - 4.4 - 5.6 - 7.0

Example for depth 5, central depth 3: Sorted values, both ends eliminated, the average of the center three is then 4.23.

1.1 - 4.0 - 4.3 - 4.4 - 5.6

Example for depth 8, central depth 4: Sorted values, both ends eliminated, the average of the center four is then 4.43.

0.7 - 1.1 - 4.0 - 4.3 - 4.4 - 5.0 - 5.6 - 7.0

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Measurement Menu

Oxygen interference configuration

These options are available to take into account the influence of some components or gases in the sample during measurement. All available interference corrections are disabled by default.

• Select Chlorinity, Salt or disabled. For chlorinity or salt, it is required to enter the actual concentration

in sample.

6.3 Measured data storage

Measured data storage

There is one measurement file which contains the data generated by the measurement cycle. The measurement files are updated in volatile memory, and regularly copied in non-volatile memory (file back-up). At start up, the measurement files in volatile memory are updated with the files from the non-volatile memory.

Note: When the measurement file is full, it is managed as a First in-First out buffer.

This dialog box allows adjustment of the parameters for recording and storing measurements.

Storage modes:

• No storage

•Store once: When the volatile memory is full (1,000 positions), the recording of measurement stops

• Rolling buffer: When the volatile memory is full, the latest measurement set replaces the oldest one

continuously (first-in, first-out)

Note: Data stored in volatile memory are lost when instrument is off, non-volatile memory is permanent. In case of an accidental power off event, the instrument resumes measurement storage after the last measurement stored in flash.

• RAM time (volatile memory): Delay in seconds between two recordings of measured data.

• FLASH time (non-volatile memory): Delay in seconds between two data file transfers from volatile

memory into non-volatile memory. The last data file erases the previous one. This field is only available if the Auto save in flash box is checked.

• Save in flash now: Press this button to store measurement data in flash (non-volatile memory)

immediately. After pressing this button, press OK to initiate the process. A warning screen appears informing you that the operation can take up to 30 seconds. Press Yes to continue with the process, or No to abort.

• Auto save in flash: Check this box to save measurements in flash (non-volatile memory)

automatically. Measurements are saved at regular time intervals as defined in the FLASH time box.

• Start logging measurement: Store once mode. Starts and stops the measurement recording

session. Measurement recording is stopped when the buffer is full.

• Purge data: Clear all data for all channels in the volatile and non-volatile memories.

• Open data: Opens a table showing the measured values which are stored in the volatile memory

(RAM). Use the scroll bar at the right to move to another data range (the id range will be shown in the title bar). The page number being viewed and the total number of pages are shown at the bottom.

Use the keys at the bottom to move directly to the first page, previous page, next page or last page.

Page 57

Section 7 Calibration Menu

Figure 38 Calibration menu

Calibrations can only be performed once the instrument has been installed, configured, and the channel has been set up. You must also ensure that you have the correct access rights to access the calibration menu.

It is recommended to calibrate the sensor every 6 months for beverage applications with multiple CIP. The temperature sensor is factory calibrated and can only be changed by a Hach Lange representative.

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Calibration Menu

7.1 Sensor calibration

Sensor calibration

The sensor can be calibrated manually on an ad hoc basis. By default, the mode is set to zero calibration with auto-end (see Calibration configuration on page 57 for more details), but these parameters can be changed.

For higher level concentrations (above 1% oxygen which corresponds to about 400 ppb dissolved O high level adjustment can be performed using a gas mixture containing more than 1% oxygen, or a known line sample. However, this should not be done without first ensuring the zero point is accurate. This can be achieved by performing a zero calibration first.

Low range sensors: (K1100-L and M1100-L spots)

There are two calibration modes available - zero or high level adjustment. The sensor is factory calibrated at zero. During use, the zero calibration is the best calibration to guarantee the sensor specifications. After a spot replacement, a zero calibration is recommended.

High range sensors: (K1100-H and M1100-H spots)

There are three calibration modes available - zero, high level adjustment or in 100% humid air.

The sensor is factory calibrated at zero and in 100% humid air. During use, humid air calibration is the best calibration to guarantee the sensor specifications. After a spot replacement, a zero calibration and a 100% humid air calibration are recommended.

) a

Initial sensor calibration

The sensor has been calibrated at the factory prior to shipment and is ready for use upon delivery. However, if the sensor has not been used for a period of more than six months since delivery, or if the sensor spot has been replaced or changed in any way, then a sensor calibration will be required.

Select the Configuration option from the Gas sensor calibration menu to check the calibration parameters.

Ensure the parameters are set up as follows:

• Auto-calibration: This option is not available for the K1100 and M1100 sensors.

• Manual-calibration Auto-End: On by default.

• Hold during c alibration or verification: On by default.

• Interferences enabled during cal: Ensure this is disabled by unchecking the box.

• Zero calibration bottle: Ensure this is disabled by unchecking the box as it is not relevant for the

K1100 and M1100 sensors.

Exit from the configuration screen by pressing on OK. Then select Calibration from the Gas sensor calibration menu and perform a manual zero calibration as described in Zero calibration on page 58. For high range sensors perform an additional 100% humid air calibration as described in 100% humid air

calibration (high range sensors only) on page 58.

Manual calibration

Manual calibrations can be made at any time. Perform a calibration by following these steps:

1. Remove the sensor from the sample line.

2. Rinse the sensor head with clean water.

3. Wipe the sensor head with a clean soft tissue to remove any excess moisture.

4. If using the supplied calibration device (see Portable calibration device on page 38), insert the

sensor into the sensor holder on top of the calibration device. If not using the calibration device, insert the sensor into the flow chamber.

5. Flow the calibration sample through the calibration device or flow chamber as applicable. If using the

calibration device, fully open the valve on the pressure reducer to give a gas flow rate of 0.1 L/min. If you are not using the supplied calibration device with pressure reducer, the maximum allowable inlet pressure must be no more than 2 bar absolute.

6. Configure the calibration as described in Calibration configuration on page 57.

7. Start the calibration as described in Zero calibration on page 58, 100% humid air calibration (high

range sensors only) on page 58, or High level adjustment on page 58 depending on the preferred

calibration method.

Page 59

7.2 Calibration configuration

Calibration configuration

This option can be invoked directly from the main calibration menu by selecting the Configuration option, or by pressing the Modify button in either the zero calibration or high level adjustment screens. The process sets all the parameters used for sensor calibration.

• Auto-calibration: This option is not available for the K1100 and M1100 sensors.

• Manual-calibration Auto-End: On by default. When enabled, a manual calibration will complete

automatically when the parameters defined in Stop parameters are reached. Press on Configure to set the manual calibration parameters (see Configure manual calibration on page 57 for details). If the calibration fails, the previous calibration parameters remain unchanged and a warning message displayed.

• Hold during calibration or verification: On by default. This keeps the last measured value and

stops updating the outputs during the calibration or verification process. This avoids sending invalid information to any connected device. At the end of a calibration, this hold remains for a further 10 minutes to allow the system to stabilize.

• Interferences enabled during cal: Off by default. This option enables the Chlorine or Salt

interference during calibration and verification. This option must be used if there is chlorine in the calibration solution and if the chlorine interference correction is enabled during measurement.

• Zero calibration bottle: Ensure this is disabled by unchecking the box as it is not relevant for the

K1100 and M1100 sensors.

If the Stop parameters button is pressed on the main configuration screen, you can view or change the existing values, or restore the default values.

It is highly recommended to leave these parameters at their default values and not change them. These values apply to manual calibrations with the Auto-End parameter set.

•Start period: is the minimum time period that must elapse before measurements are considered

valid.

• Number of points: is the minimum number of measurements that must be taken.

• Stop criteria: is the maximum allowable signal standard deviation value to ensure an accurate

calibration.

Calibration Menu

Configure manual calibration

This option sets the parameters required for manual sensor calibration.

• Calibration mode:

• Zero calibration

• High level adjustment

• In 100% humid air calibration (available for high range sensors only)

If zero calibration or 100% humid air calibration is selected, no other parameters are required to be set. However, the following parameters must be set if high level adjustment has been selected.

• Calibration sample: Set to In line sample, Gas bottle or Factory parameters. If factory

parameters is selected, the Ksv value is displayed but can be changed.

These additional parameters are required if in line sample or gas bottle has been selected as the calibration sample.

•Medium: This is automatically set to liquid if in line sample has been selected as the calibration sample, or gas if gas bottle has been selected.

• Gas unit type: Either partial or dissolved are available for an in line sample. If gas bottle was selected this is set to fraction.

• Gas unit: The list of available units depends on unit type selected above.

•Liquid: This defaults to water for K1100 sensors and to beer for M1100 sensors.

• Reference value: Enter the reference value for calibration

Press OK to return to the main calibration screen.

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Calibration Menu

7.3 Zero calibration

Zero calibration

With this method, the sensor should be removed from the sample and exposed to pure N2 gas. It is recommended to use the specially designed portable calibration device for this purpose (see also

Calibration devices on page 38).

Press Start to start the calibration. A screen is displayed showing the measured values and length of time the sensor has been under

calibration. These values are continually refreshed. The value % last calibration displayed in the top box is an informational message showing the

difference between the current and previous sensor calibrations. The Signal within range and Stability reached boxes in the top right corner indicate whether the

calibration is within acceptable limits. When both boxes indicate YES, press Finish to accept the new calibration. A confirmation screen then asks to accept and store the new parameters.

If one or both boxes show NO, you can still perform a calibration but it is not recommended, and the calibration should be aborted by pressing the Cancel button.

In the case of a calibration failure, attempt a second calibration after about 5 minutes. If the second attempt also fails, then refer to your Hach Lange representative for advice.

Note: If the Auto-End parameter is set (see Calibration configuration on page 57), then the calibration will be deemed successful when the parameters defined in Stop parameters are met. You will then be asked to confirm the calibration.

If you have not accepted or cancelled the calibration after an elapsed time of 10 minutes then the process will time-out, and a warning message will be displayed.

7.4 100% humid air calibration (high range sensors only)

In 100% humid air calibration

With this method, the sensor should be removed from the sample and exposed to air saturated with humidity. Do this by putting a drop of water in the calibration cap before installing the cap on the sensor.

Press Start to start the calibration. The process is then the same as for the zero calibration described previously.

7.5 High level adjustment

High level adjustment

Note: Before using this option, ensure a zero calibration has been successfully completed first.

This calibration exposes the sensor to a gas or a liquid sample with a known gas concentration. You also have the option to reset the sensor’s calibration parameters to factory settings (from drop-down list for Cal. sample).

Press Start to start the calibration. The process is then the same as for the zero calibration described previously.

7.6 Sensor verification

Sensor verification

Similar to the calibration procedure, but used for verifying the calibration values. The results of the measurements made during the verification are not stored and the calibration data is not modified.

Page 61

7.7 Barometric pressure calibration

Barometric pressure calibration

Note: The barometric sensor has been factory calibrated but should be periodically verified with a precision certified barometer. This is only necessary if measuring in gas phase with fraction units (%, ppm).

Upper box shows the barometric pressure measured by the instrument. Using a precision certified barometer, measure barometric pressure in the location where the measuring

instrument is used. Compare the values, if values are the same press Cancel, otherwise enter the new barometric value in the lower box and Validate the new setting.

On completion a calibration report is created.

7.8 Calibration reports

Calibration reports

Once a calibration is completed (for a gas or pressure sensor), the calibration report is updated with the new details. The calibration report contains data for the last 10 calibrations.

For full details on the data displayed for all the different type of calibration reports, refer to the examples listed under Data available on page 73.

Each calibration record will contain parameters useful for traceability. For instance, it will contain:

• the date and time

• the calibration mode (zero, 100% humid air, or high level adjustment)

• the calibration type (manual or automatic)

• the operator name and ID

• all the measurements which influence the calibration (temperature, barometric pressure, current,

etc.)

Calibration Menu

Page 62

Calibration Menu

Page 63

Section 8 Inputs/Outputs Menu

Figure 39 Inputs/Outputs menu

Page 64

Inputs/Outputs Menu

8.1 Configure snooze

Configure snooze

In the event of an alarm, the “snooze” button stops the instrument buzzer and returns all the relays in the instrument to their normal state during a "snooze time".

Enter the snooze time in seconds and press OK.

8.2 View inputs/outputs

View inputs/outputs

This view option displays the state of the 3 alarm relays (on or off), and the analog output current value for each.

8.3 Relays

Relays

There are three measurement alarm relays and one system alarm relay for the instrument. These relays are configurable as either standard or custom events through the instrument menu.

• An alarm relay can be activated or deactivated

• When the alarm is OFF, it is activated,

• When the alarm is ON, it is deactivated

All the relays are activated as soon as the instrument is ON (but alarms are OFF). When the instrument is OFF, the relays are deactivated, thus in this state, all alarms are ON. The logic "Relay deactivated = Alarm ON" has been chosen for this safety reason.

When the main board does not communicate with the measurement board for more than 30 seconds, the measurement board switches all the alarm relays and the analog output to the alarm state.

Relays configuration The three relays can be triggered by several standard events, or a

Test channel relays The three measurement alarm relays can be manually activated for testing

Test system relay Similarly, the system alarm relay can be manually activated for testing

Note: In both the Test Channel Relays and Test System Relay options above, once the tests have been completed press Cancel to exit the screen. At the same time, this will reset all relays (including the system relay) back to a status of “Not under test”.

combination of events (custom). The relays output can be used to turn on a beacon, horn or PLC (see Connections to electronic boards on page 33)

Note: Relays can be set to Normally Open [NO] or Normally Closed [NC] by changing the jumper positions on the measurement board (see

Measurement alarm relays on page 34).

• Select a standard event in the rolling list

• If “Custom event” has been selected, it has to be configured by touching the configure button

• Press on the text box to open the selection menu (rolling menu). Select

the events that must trigger the relay, and press OK.

Proceed in the same manner for other events that should trigger the relay.

purposes:

• Select Relay On, Off or Not under test.

See note regarding the relays below. “Not under test” means the relay is in operating mode, and it will be triggered normally.

Note: A relay set to NO will close when activated (On), but a relay set to NC will open. See Measurement alarm relays on page 34.

purpose.

• Select Relay On, Off or Not under test.

Page 65

8.4 Analog outputs

Inputs/Outputs Menu

Figure 40 Analog outputs menu

Page 66

Inputs/Outputs Menu

Analog outputs

There are three analog outputs available. These outputs are configurable in terms of function, content, and behavior through the instrument menus. Analog outputs are used to output a current which is a function (e.g. a linear characteristic) of a measurement: AOut = f (M). The analog outputs can be typically connected to a PLC. Knowing the function (f), the PLC can compute the value of the measurement.

Instrument configuration

Standard event indication

Extended event indication

• Select analog output range of current:

4-20 mA or 0-20 mA

• The 4-20 mA range (recommended) allows for an extended event indication mode that can be selected and configured (default = standard mode)

For some events (sensor out, purge failure, etc.) the actual measurement is not significant, but the PLC needs to know how the analog output behaves in these cases. Two "Event indication modes" are available:

• Standard mode (default)

• Extended mode

Refer to Table 1 Standard event indication below.

The "Extended event indication" mode is only available when the 4-20 mA output is selected. In this mode, the range between 0 mA and 4 mA is used to indicate selected events. The events are defined using the channel configuration option (see Channel configuration on page 65).

Table 1 Standard event indication

Event output range

Analog output

0-20 mA 4-20 mA

Gas concentration 20 mA 20 mA

Temperature 20 mA 20 mA

Event

• Channel out

• Sensor out

• Thermal cut-off

• Interfering gas error

• Channel out

• Sensor out

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Inputs/Outputs Menu

Analog outputs (continued) Channel configuration Set the type of measurement that will be transmitted through each output

channel, and the output characteristics.

• Meas. type: Select between the type of measurements available in the

rolling list.

• Characteristics: Select either Linear, Tri-linear or None (see Analog

output characteristics on page 67).

• Limits: Press the configure button to adjust the analog output set points

for each output. Enter values in the appropriate text boxes. In Linear mode, only the ML and MH values can be adjusted. Tri-linear mode allows all limits to be adjusted, and the None mode denies access to this screen.

The authorized user may define a maximum of 12 customized events for each analog output and change the order of priority of all events.

Note: This only applies to Tri-linear and Linear outputs. It is not available if the output characteristic is set to None.

Configure the events that should be signaled at the corresponding current shown in the right column.

• Only one event signal at a time can be sent via the current output. As

there is a possibility to have several events at the same time, an order of priority must be set. This order has been set by default, but it can be modified to suit particular needs and conditions. Touch the priority number in the left column and edit it.

• The shaded events in the list have preset outputs and only the priority

can be changed. The other events can be customized by the user. Touch a white text box to call up the rolling list. Select an event from this list and press OK. Then adjust the priority as required.

Note: When an event occurs, measurement information is superseded by the event information on the output.

The following table lists the default configuration. The first two events on the list are pre-set and only the priority can be changed:

Table 2 Extended Event Table

Priority Event I [mA]

Sensor out 0.25

0 1

Interfering gas error 0.50 2 Custom Event 1 0.75 3 Custom Event 2 1.00 4 Custom Event 3 1.25 5 Custom Event 4 1.50 6 Custom Event 5 1.75 7 Custom Event 6 2.00 8 Custom Event 7 2.25 9 Custom Event 8 2.50

10 Custom Event 9 2.75 11 Custom Event 10 3.00 12 Custom Event 11 3.25 13 Custom Event 12 3.50 14 Custom Event 13 3.75

Page 68

Inputs/Outputs Menu

Analog outputs (continued) Calibration of the analog

output

Direct test Test to check the calibration of the analog outputs. A precision amperometer

Characteristics test This is a test for the correct operation of the peripherals connected to each

The calibration of the analog output is aimed at aligning the internally calculated current to the real current output. This was performed at factory, but could become necessary again because of electronic tolerances. A precision amperometer connected at the corresponding analog output connection point is required. See Measurement board on page 34.

• Select the analog output channel to calibrate and press the Start button.

• Measure with the amperometer the current value for point 1. It should be

below 4 mA

• Edit point 1 and enter the same value as read on the amperometer, then

press the Continue button.

• Measure with the amperometer the current value for point 2. It should be

above 20 mA.

• Edit point 2 and enter the same value as read on the amperometer,

before pressing the Continue button.

Calibration of the selected analog output channel is completed.

connected at the analog output connection point is required.

• Select a value (4, 12, 20 mA available) for each channel and compare

this value (+ 0.02 mA) with what the amperometer shows.

A calibration is required if the value on the amperometer differs from the current selected +

Note: It is possible to test one analog output without interfering with the others. During the test, the other analog outputs will continue to indicate the measurement.

analog output, by verifying that the PLC computes the correct value. The analog output will send the current corresponding to the value entered

in the text boxes.

• Type in a test value for each analog output, and check for the related

action on the peripheral.

0.02 mA).

Page 69

8.5 Analog output characteristics

Analog output characteristics “Linear” analog output The "Linear" output is the default setting for the analog output. It is

illustrated below (4-20 mA output is shown, 0-20 mA settings are similar).

The goal of this setting is to use all the points available on the slope from

4 mA to 20 mA to show the range of measurements that are usual in the

measured process. Setting the output this way allows for the highest signal

resolution for the actual conditions.

The downside is that any measures below the set range will have the same

analog signal locked at 4 mA. Similarly, any measure over the set range will

have the same analog signal locked at 20 mA. Settings must be made in

balancing these aspects.

Settings

For the output, set ML and MH in the current measuring unit (e.g. °C for a

temperature output). When a compound unit is selected the smallest unit will

be used (e.g. ppb for a "ppm-ppb" compound unit).

These points should be set keeping in balance the following conditions (see

illustration above):

• The smaller is Range 1, the better is the analog signal resolution within

• In Range 0 the analog output only shows that measurement is below the

The formula to compute the measurement knowing the current I and the

resolution R is given in the following table:

Inputs/Outputs Menu

the expected range of measure.

ML value. Similarly in Range 2 the analog output only shows that measurement is over the MH value.

Linear Range Measurement M Resolution R

4-20 mA 20 > I > 4 M = ML + (MH - ML)

0-20 mA 20 > I > 0 M = ML + (MH - ML)

(I - 4) / 16 R = (MH-ML) / 808

I / 20 R = (MH-ML) / 1010

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Inputs/Outputs Menu

Analog output characteristics (continued) “Tri-linear” analog

output

The "Tri-linear" output brings benefits over the “Linear output” discussed before. It is illustrated below (4-20 mA output is shown, 0-20 mA settings are similar).

Compared to the “Linear” mode, the expected range of measure is Range 2. A Range 1 and 3 are available to show the measures falling out of this Range 2, but normally at a lower resolution. Expected measurements for the measured process are supposed to be in Range 2 most of the time, and in Range 1 or 3 occasionally (problems, calibration, line stop, etc.). The benefits are:

• The PLC can compute the measurement over a large range (1, 2 and 3).

• The PLC can compute a higher resolution signal for the expected

measuring range (Range 2: MH > M > ML).

• Carefully selecting the set points allows for an individual resolution for

each range, so a different resolution can be applied to Range 1, 2 and 3, allowing to tailor the analog output to the actual conditions.

As before, the downside is that any measure below or over the Range 1, 2 and 3 will have the same signal locked at 4 mA and 20 mA respectively, but Range 1, 2 and 3 should cover a larger range than in the “Linear” mode. Settings must made in balancing these aspects.

Settings

For each output, set MLL, ML, MH, and MHH in the current measuring unit (e.g. °C for a temperature output). When a compound unit is selected, the smallest unit will be used (e.g. ppb for a "ppm-ppb" compound unit). Also set AOL (Analog Output Low) and AOH (High) in mA.

These points should be set keeping in balance the following conditions (see illustration above):

• The smaller is Range 2, the better is the analog signal resolution within

the expected range of measure.

• Size of Range 1 and 3 should be set to deliver an adequate level of

resolution for the measures falling out of the expected range of measure.

• In Range 0 the analog outputs only shows that measurement is below

the MLL value. Similarly in Range 4 the analog output only shows that measurement is over the MHH value.

The formula to compute the measurement knowing the current and the resolution R is given in the following table:

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Inputs/Outputs Menu

Tri-linear Range Measuremen t M Resolution R

1: AOL >

4-20 mA

0-20 mA

Analog output characteristics (continued) None This is the default value.

2: AOH > I > AOL M=ML+(MH-ML)*(I-AOL)/ (AOH-AOL) R=(MH-ML)*20/((AOH-AOL)*1010)

3: 20 > I > AOH M=MH+(MHH-MH)

1: AOL >

2: AOH >

3: 20 > I > AOH M=MH+(MHH-MH)*(I-AOH)/(20-AOH) R=(MHH-MH)*20/((20-AOH)*1010)

I > 4 M=MLL+(ML-MLL)*(I-4)/(AOL-4) R=(ML-MLL)*20/((AOL-4)*1010)

I > 0 M=MLL+(ML-MLL)*I/AOL R=(ML-MLL)*20/(AOL*1010)

I > AOL M=ML+(MH-ML)*(I-AOL)/ (AOH-AOL) R=(MH-ML)*20/((AOH-AOL)*1010)

Setting the analog output to “None” means that the output value will always

be zero and importantly ensures that no current is emitted on that output, so

reducing power consumption as well as reducing heat within the instrument.

(I-AOH) / (20-AOH) R=(MHH-MH)*20/((20-AOH)*1010)

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Inputs/Outputs Menu

Page 73

Section 9 Communication Menu

Figure 41 Communication menu

The external RS-485 port of the main board is directly connected to a RS-485 bus (single twisted pair). Optionally it can be connected to a fieldbus module (gateway).

The RS 485 menu allows to select between RS485 simple or Profibus DP communication protocol, depending on application.

• Click on the text box to select either the RS-485 simple or the PROFIBUS-DP

communication protocol.

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Communication Menu

9.1 RS-485 simple mode configuration

This protocol allows the instrument to output data to an external device (PLC, SCADA, PC, etc.). The communication is unidirectional. The data are output on the RS-485 link as simple ASCII text. If for instance you use a PC, the data can be easily visualized and saved in a file using the "Hyperterminal" software.

To use this communications mode, on the instrument:

• Select the RS-485 option from the Communication menu

• Choose the protocol Simple (default configuration) and press on OK

• Then select the RS-485 Simple option from the Communication menu:

• "Baud rate", "Parity", "No of stop bits", "Byte size" Standard parameters of the RS-485

link.

• "Enable" The measurements can be sent continuously (approximately every 2 sec.).

This field allows enabling or disabling this feature.

• "Mode" This is the format of the measurements sent continuously (see Cyclic

measurements on page 73 of this document). In "Expert" mode, more data are sent.

These additional data can be useful for diagnostic purpose.

Note: In case of problem verify first that jumper J3 is not installed on the mother board (default configuration).

Send data

This dialog box is used to send text files to an external device. The possible files are the following:

• Calibration reports

• User actions log file

• Instrument configuration

• Measurements stored in the instrument memory

The button "Stop Cyclic meas." allows to stop and to restart the cyclic transmission of measurements. It is advised to stop the cyclic transmission in order not to mix cyclic measurements and data of the file being transmitted. This button has the same effect as the "Enable" checkbox of the "Communication/RS-485 Simple/Configuration" window.

After stopping the cyclic measurements, select the "Calibration Reports", "User Actions", "Configuration", "Measurements" button to send the corresponding file, or the "All files" button to send all these files in one shot.

Once the button is pressed, the file is sent immediately. The field "Current file status" shows “Sending” alongside the file transmission progress bar. On completion this changes to “Sent”.

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9.1.1 Data available

All individual data are separated by at least one tabulation character (ASCII code=0x09).

For the cyclic measurements, the data format is detailed. For the files, only one example for each file is given to explain the data format.

Cyclic measurements

1. If the option "Mode = standard" is chosen, the following message is sent:

CHn\t Gas\t Gas Unit\t Temperature\t Temperature Unit\t Barometric Pressure\t Barometric Pressure Unit\t\ Event\t\r\n

with:

\t ................................................the ASCII tab character: code=0x09

\r ................................................the ASCII Carriage Return character: code=0x0D

\n ..............................................the ASCII Line Feed character: code=0x0A

CHn ..........................................the 2 ASCII characters "CH" + the channel no.

Gas............................................the gas concentration.

Gas Unit ....................................the gas unit.

Temperature..............................the temperature.

Temperature Unit.......................the temperature unit.

Barometric Pressure..................the barometric pressure.

Barometric Pressure Unit ..........the barometric pressure unit.

Event .........................................the event bit mask in hexadecimal format.

Communication Menu

The values are not described here (see List of events and alarms on page 101).

• Example of one measurement:

CH1 697.176 ppb 20.1 °C 0.982 bar C00

2. If the option "Mode = expert" is chosen, the following message is sent:

CHn\t Gas\t Gas Unit\t Temperature\t Temperature Unit\t BarometricPressure\t Barometric Pressure Unit\t

Event\t Phase Shift\t °\t Partial Pressure\t bar\t Reference Phase\t °\t

Fluorescent Phase\t °\t Reference Amp\t V\t Fluorescent Amp\t V\t

Tinst\t Tinst Unit\t Offset\t Time\t Index\r\n

with:

Phase shift.................................The fluorescence phase shift in [°].

Partial pressure .........................The partial pressure in [bar].

Time ..........................................The time of the measurement. Format "hh:mm:ss."

Index..........................................This is the index of the last measurement.

This number starts at 0 at power up of the program. The following is an example of one measurement:

CH1 697.173 ppb 20.1 °C 0.982 bar 03000000 26.045 ° 0.69700 bar -21.409 ° -64.991 ° 2.349 V 2.499 V 25.531 °C 45.000 22:59:42 5923

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Communication Menu

Gas sensor calibration report example

Calibration report nb 1

Calibration mode . . . . . . . . . . . .Manual high level adjustment

Date (yy.mm.dd - hh:mm) . . . . .05.02.17 - 18:40

Operator . . . . . . . . . . . . . . . . . .jp

Operator ID . . . . . . . . . . . . . . . .3

Cal. sample . . . . . . . . . . . . . . . .In line sample

Medium . . . . . . . . . . . . . . . . . . .Liquid

Gas unit. . . . . . . . . . . . . . . . . . .ppb

Liquid. . . . . . . . . . . . . . . . . . . . .Beer

Ref. value . . . . . . . . . . . . . . . . . 1.500000

Cal. coefficient Phi0(Tcal) . . . . .25.974°

Cal. coefficient Tcal. . . . . . . . . .24.41°C

Cal. coefficient Ksv(25°C) . . . . .-0.1312 mbar-1

Cal. coefficient Tcal.Inst . . . . . .25.20°C

Standard deviation . . . . . . . . . .0.003 mbar

Fluor. amplitude. . . . . . . . . . . . .0.834 V

Interferences . . . . . . . . . . . . . . .Disable

Temperature . . . . . . . . . . . . . . .20.1 °C

Calibration duration . . . . . . . . . .3 mn

Barometric sensor calibration report example

Calibration report nb 1

Date (yy.mm.dd - hh:mm) . . . . .05.02.16 - 20:38

Operator . . . . . . . . . . . . . . . . . .jp

Operator ID . . . . . . . . . . . . . . . .3

Previous barometric pressure . .0.956 bar

New Barometric pressure . . . . .0.976 bar

Calibration offset . . . . . . . . . . . .3.73 [kPa]

Interfering gas calibration report example

Calibration report nb 1

Date (yy.mm.dd - hh:mm) . . . . .05.02.17 - 20:03

Operator . . . . . . . . . . . . . . . . . .jp

Operator ID . . . . . . . . . . . . . . . .3

Calibration Coefficient . . . . . . . .366.127661

Chlorinity/Salinity. . . . . . . . . . . .19.000000 [g/l]

Ratio with last calibration . . . . .99.990075 %

% of ideal current . . . . . . . . . . .111.624287 %

Stability . . . . . . . . . . . . . . . . . . .0.000000 %

Temperature . . . . . . . . . . . . . . .20.1 °C

Barometric pressure . . . . . . . . .1.020 bar

External pressure . . . . . . . . . . .0.977 bar

Sensor current. . . . . . . . . . . . . .7.990 µA

User action log file example

The "User action log file" below contains 3 user actions.

Nr mm/dd hh:mm:ss User ID User Name Action ID Description

1 1/21 15:13:44 1007 Armstrong 139 Change Time/Date 0 1/21 15:13:27 1007 Armstrong 501 Cal. parameters 2 1/21 15:12:15 1007 Armstrong 132 Identification

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Communication Menu

Measurement file example

6 measurements are illustrated below:

Nr mm/dd hh:mm:ss Gas Temp Mask Barom Ext.P Phase T.inst Offset Index [ppb] [°C] [bar] [bar] [deg] [°C] [ppb]

0 2/17 21:15:37 75.05 20.1 03000000 1.005 0.000 26.39 22.5 35.0 2271 1 2/17 21:15:27 74.95 20.1 03000000 1.005 0.000 26.45 22.5 35.0 2266 2 2/17 21:15:17 75.15 20.1 03000000 1.005 0.000 26.52 22.5 35.0 2261 3 2/17 21:15:57 75.05 20.1 03000000 1.005 0.000 26.41 22.5 35.0 2256 4 2/17 21:15:47 75.00 20.1 03000000 1.005 0.000 26.38 22.5 35.0 2251 5 2/17 21:15:37 74.95 20.1 03000000 1.005 0.000 26.54 22.5 35.0 2246

Configuration report example

GENERAL CONFIGURATION

Measurement mode . . . . . . . . .Continuous mode

Pressure unit. . . . . . . . . . . . . . . bar

Temperature unit. . . . . . . . . . . . °C

Storage mode . . . . . . . . . . . . . . Rolling buffer

Storage RAM time. . . . . . . . . . . 10 [s]

Storage FLASH time . . . . . . . . . 3600 [s]

Autosave in FLASH. . . . . . . . . . Disabled

Channel 1

Sensor. . . . . . . . . . . . . . . . . . . . M1100-L

Medium . . . . . . . . . . . . . . . . . . . Liquid

Gas unit. . . . . . . . . . . . . . . . . . . ppm->ppb

Liquid . . . . . . . . . . . . . . . . . . . . Beer

Resolution displayed. . . . . . . . . 1

Thermal alarm. . . . . . . . . . . . . .Enabled 90.0 [°C]

Measurement interval . . . . . . . . 5 [s]

Out of range protection . . . . . . . Enabled

User offset. . . . . . . . . . . . . . . . . Enabled

User offset value . . . . . . . . . . . . 45

Alarms

Low Low . . . . . . . . . . . . . . . . . . Enabled 100.000000 [ppb]

Low . . . . . . . . . . . . . . . . . . . . . . Enabled 200.000000 [ppb]

High. . . . . . . . . . . . . . . . . . . . . . Enabled 9000.000000 [ppb]

High High . . . . . . . . . . . . . . . . .Enabled 10000.000000 [ppb]

Hysteresis . . . . . . . . . . . . . . . . .5 [%]

Delay. . . . . . . . . . . . . . . . . . . . . 15 [s]

Filter

State . . . . . . . . . . . . . . . . . . . . . Disabled

Type . . . . . . . . . . . . . . . . . . . . . Median

Depth . . . . . . . . . . . . . . . . . . . .5

Central depth . . . . . . . . . . . . . . 0

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Communication Menu

9.1.2 Example of use

In this example we use:

• One PC with a RS232 port.

• One "RS-485<->RS232 converter"

Procedure:

1. Connect both RS-485 wires of the instrument to the "RS-485<->RS232 converter".

2. Connect the "RS-485<->RS232 converter" to the PC RS232 port using a standard cable

(RS232 DB9 straight cable).

On the PC:

1. Run "Hyperterminal" on the PC.

2. Configure the PC COM port used (e.g. COM2). Menu "File/Properties/Configure".

3. Configure the parameters "Baud rate", "Parity", "Nb of stop bits", "Byte size" (Menu

"File/Properties/Configure"). Use the same parameters for the instrument and the PC.

4. Configure the "Font = Courier 10" (Menu "View/Font").

5. Connect "Hyperterminal" (Menu "Call/Call").

6. Save the data received in the file of your choice (Menu "Transfer/Capture Text/Start").

On the instrument:

1. Use the menu "Communication/RS-485 Simple/Send files" and the button "All files". When the transfer is finished, close the file with "Hyperterminal" (Menu "Transfer/Capture

Text/Stop"). Now, all the reports are saved in a text file on your PC.

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9.2 PROFIBUS-DP communication (optional)

9.2.1 Installation

On the ORBISPHERE CD, there is an “Orbi3218.gsd” and an “Orbi3218.bmp” file available in the “Profibus DP” folder to help configure the PROFIBUS-DP. The GSD file contains the following elements:

• The module Gateway Version >= 2.0 - 1 channel for receiving data from the instrument.

Note: Gateway version >= 2.0 and user software version >= 2.15 are mandatory

• The module Gateway Version < 2.0 for receiving data from an instrument equipped with a

profibus gateway version < 2.0 or user software version < 2.15

Communication Menu

WARNING

Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical connections.

CAUTION

Personal Injury Hazard. Only qualified personnel should conduct the tasks described in this section of the manual.

NOTICE

Potential Instrument Damage. Proper ESD (electrostatic discharge) protocols must be followed to prevent damage to the product. All fittings must be properly seated and tightened to prevent any water and dust ingress.

1. Install the PROFIBUS-DP module and the jumper J3 on the main board (location highlighted

in the illustration below).

2. Select the menu "Configuration/RS-485" and choose "PROFIBUS-DP" as the protocol.

3. Select the menu "Configuration/PROFIBUS-DP", choose the slave address and restart the

instrument.

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Communication Menu

9.2.2 Input/Output data

The main board:

• Writes the latest measurement data to the Profibus Input Buffer.

• Checks if a command written by the Profibus Master must be executed (Profibus Output

Buffer). If a command is to be executed, the instrument executes it and writes the result (status, data, etc.) in the Profibus Input Buffer.

All numbers are coded in “Big Endian” format, and float values are coded according to IEEE Standards. The field types “Byte” and “Double Word” are unsigned.

Measurements

Measurements are formatted in the Profibus Input Buffer as follows:

Barometric pressure Input float 32 bits 0 Barometric pressure unit Input byte 8 bits 4 Channel 1 gas concentration Input float 32 bits 5 Channel 1 gas unit Input byte 8 bits 9 Channel 1 temperature Input float 32 bits 10 Channel 1 temperature unit Input byte 8 bits 14 Channel 1 external pressure Input float 32 bits 15 Channel 1 external pressure unit Input byte 8 bits 19 Channel 1 events Input double word 32 bits 20 Channel 1 measurement index Input double word 32 bits 24

Name Type Size Offset

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Communication Menu

The gas, temperature and barometric pressure unit values are coded as defined in the following tables:

Gas Unit Value Temperature Unit Value

bar 0 K 0 bar 0 mbar 1 °C 1 mbar 1 Pa 2 °F 2 psia 2 kPa 3 atm. 3 hPa 4 Pa 4 psia 5 kPa 5 atm. 6 hPa 6 mbar->bar 9 Pa->KPa 10 %Vbar 12 ppm Vbar 13 %Vext 14 ppm Vext 15 ppm Vbar->%Vbar 16 ppm Vext->%Vext 17 ppm 18 ppb 19 g/l 20 mg/l 21 µg/l 22 %O

%Air 24 Note: For the field “Event”, please see the column “Bit mask g/kg 25 V/V 26 %W 27 cc/kg 28 ml/l 29

value” in Table 4 on page 101.

Barometric

Pressure Unit

Value

Note: If the instrument stops sending measurement data to the module, then after 30 seconds the module sets the event mask to the value PROFIBUS-DP value not updated (0x80000000) bit mask.

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Communication Menu

Commands

The “Command Output Buffer” is formatted as follows:

Output command toggle (OCT) Output byte 8 bits 0 Output command ID (OCI) Output byte 8 bits 1 Output command data byte 1 (OCD1) Output byte 8 bits 2 Output command data byte 2 (OCD2) Output byte 8 bits 3 Output command data byte 3 (OCD3) Output byte 8 bits 4 Output command data byte 4 (OCD4) Output byte 8 bits 5

The “Command Input Buffer” is located just after the measurement data and is formatted as follows:

Input command toggle (ICT) Input byte 8 bits 74 Input command status (ICS) Input byte 8 bits 75 Input command data byte 1 (ICD1) Input byte 8 bits 76 Input command data byte 2 (ICD2) Input byte 8 bits 77 Input command data byte 3 (ICD3) Input byte 8 bits 78 Input command data byte 4 (ICD4) Input byte 8 bits 79

Name Type Size Offset

The following commands are available:

• Change product

• Activate sensor (valid for EC sensors only)

Change product command - output

Name Value Comment

OCT 1-2

OCI 1

OCD1 0

OCD2 0-99 Product number

OCD3 0-1

OCD4 Not used

Channel number: 0 = Channel 1

Erase measurement files: 0 = Never erase the measurement files. 1 = Erase measurement file if necessary (e.g. gas unit changes)

Change product command - input

Name Value Comment

ICT 1-2

0 = OK

ICS 0-3

ICD1 Not used ICD2 Not used ICD3 Not used ICD4 Not used

1 = Unknown command ID 2 = Invalid parameter (e.g. invalid channel no or product number) 3 = Execution failure

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Activate sensor command - output

Name Value Comment

OCT 1-2

OCI 2

OCD1 0

OCD2 0-1

OCD3 Not used OCD4 Not used

Channel number: 0 = Channel 1

Sensor activation: 0 = Deactivate the EC sensor 1 = Activate the EC sensor

Activate sensor command - input

Name Value Comment

ICT 1-2

0 = OK

ICS 0-3

ICD1 Not used ICD2 Not used ICD3 Not used ICD4 Not used

1 = Unknown command ID 2 = Invalid parameter (e.g. invalid channel no) 3 = Execution failure

Communication Menu

9.3 USB-A port (host)

This option allows the export or import of data from an external mass storage device. The device must first be connected to the instrument through the USB-A port.

Select one of the two import options (product list or access table) to import data from the storage device. This is useful for transferring these files to additional instruments without the need of having to re-enter the data individually on each instrument.

Note: The imported data will override any current settings on the instrument.

Select the export option to export data from the instrument to the storage device. For information regarding the uploaded files, refer to Uploaded Files on page 85.

For both import and export options, the progress bar is updated to give an indication of the progress of the selected option.

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Communication Menu

9.4 HTTP/TCP-IP

9.4.1 Overview

When activated this option downloads data from the instrument directly to a web page that can be accessed from a PC. To be able to use this option, the instrument must be connected to the network (specifically Connector P3 - see details in Main board connections on page 33) and the network must have a DHCP server installed.

• Check the Enable server box to enable the web server communication link.

• Enter the Server name for the instrument. This is free format text and should typically be

used to identify the instrument.

• Check the Enable security box if you require a password to be entered on the PC to access

the web page.

If any of the details on the previous screen have been changed, a warning message will be displayed as illustrated left.

The changes must be confirmed, after which the instrument must be powered down and powered up again for the changes to take effect.

Note: The IP Diagnostics button at the bottom of the screen is for use by experienced IT personnel only to help resolve any communications problems.

9.4.2 PC interface

Once the server has been enabled and the interface information set up, access the information by launching an internet browser and typing “http://” followed by the server name that has been assigned to the instrument, in the address box as illustrated below:

If the enable security option has been checked on the instrument, you will be required to enter a username and password on your PC to gain access to the web page.

The username and password must be a valid username/password combination that has been set up on the instrument (see also User management on

page 88 on how to set up users on the instrument).

Domain information is not required.

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Communication Menu

Once a valid username/password combination has been entered, the initial web page will be displayed giving a list of options:

Click on any of these options and the data will be displayed on the PC screen. The following shows an example of the screen when selecting the Current Measurement option:

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Communication Menu

9.5 Data file transfer through the USB-B port (client)

The USB port allows you to copy data files from the instrument to a PC using Microsoft synchronization software. The files in the instrument are coded in a binary format, so they must be converted to a readable format on your PC to make them suitable for viewing. This is done automatically using the software supplied on the ORBISPHERE CD (see PC software

installation below and Upload report files on page 84 for details).

Check that the instrument and PC are powered, then connect them with the USB cable that was supplied with the instrument. Follow the instructions below:

9.5.1 PC software installation

Insert the ORBISPHERE CD inside the PC drive. If the auto executable installation does not start, browse the CD with Windows Explorer and double click on the setup.exe file to start the installation. Follow the step by step instructions appearing on the screen.

Once the installation is complete, two icons are installed on the PC Desktop:

• Orbisphere 410, 51x USB upload is used to upload and convert report files from the

instrument to the PC (see Upload report files on page 84).

• Orbisphere 410, 51x Setup is software used by the Hach Lange after sales technicians to

upload new software versions. To avoid an accidental software modification, a key is required.

9.5.2 Microsoft synchronization software

• Windows XP - A copy of the synchronization software is available on the ORBISPHERE CD. Inside the ActiveSync folder double click on ActiveSync.exe to install on the PC.

• Windows Vista and Windows 7 - Download and install the Windows Mobile Device Center application which contains the synchronization software.

Once installed, the synchronization software starts automatically when the instrument is connected to the PC and an icon will appear in the task bar at the bottom of the screen.

Note: By default the software proposes to set up a partnership with the instrument. This is not required, so make sure this is set to NO before continuing.

9.5.3 Upload report files

Double click on the Orbisphere 410, 51x USB upload icon on the PC desktop (created during the process described previously in PC software installation on page 84) to start the upload and convert process.

When the main screen is displayed, click on the Wizard button in the top left corner.

• Check that the USB connection from the instrument to PC has been made, and that the synchronization software has been activated and the link recognized (the icon in the task bar should be colored green). Click on Next.

• Choose the directory where the files are to be stored. If the directory path does not exist it will be automatically created. Click on Next.

• A warning message appears to warn that all files currently in the directory (if any exist) will be

deleted prior to upload. Click on Yes to continue with the process or No to abort. If Yes is selected, a progress bar of the upload is displayed.

• Should any of the files be missing (e.g. a calibration file will be missing if no calibration has been performed), a warning message is displayed, but no action is required. Click on OK. Once the upload is complete, the files are converted and stored in the folder defined above.

• Click on Finish to terminate the process, or on either of the other two buttons to open the folder or view the text files.

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Communication Menu

Uploaded Files

There are a number of files that are uploaded to the PC during this process. However, only the text files (with a .txt file extension) are in a readable format on the PC. Most document editors (Word, Notepad, etc.) can be used to open these files, as well as spreadsheet and other reporting tools (e.g. Excel).

There are four reports available:

• Instrument Configuration

• Calibration Reports

• Measurements

• Product Lists

• User Actions

The reports show information for the channel. Below is an example of the Instrument Configuration report as viewed using the Notepad utility.

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Communication Menu

9.6 Printer

This menu provides the facility to print a number of reports directly to a printer. The printer must be connected to the instrument through the instrument USB-B 4-pin port.

The following information is available for printing:

• Calibration reports

• User action log files

• Instrument configuration details

• Measurements stored in the instrument memory

• Cyclic measurements for continuous printing

Configuration Printer configuration Currently only the USB port is a valid printer connection.

Report configuration

Calibration - Choose the channel(s) for which calibration reports are

required. Choose to print the last report or all reports for the selected channel(s).

User actions - Define the date and time criteria for which user action logs are required.

Configuration - Choose the channel(s) for which instrument configuration details are required.

Measurements - Choose the channel(s) for which measurement reports are required. Define the start and end times for the measurement reports.

Cyclic measurements - Check the enable continuous mode checkbox and choose the channel(s) for which cyclic measurements are required.

Cancel - Exit the configuration option.

Send files

Choose the report (or All) to print the reports that match the configuration criteria. A status bar at the top of the screen shows printing progress.

Push the Cancel button to cancel a print job.

9.6.1 Printer error messages

Error message Meaning

Printer not available

Paper out

Unknown error

Note: Cyclic measurement mode is automatically disabled when an error occurs. After the error is corrected, reactivate the cyclic mode in the report configuration option if cyclic measurements are required.

Indicates that no printer has been detected. Check that the printer is connected to the USB-B port and is powered on.

Indicates that the printer is out of paper. In cyclic mode, it is necessary to activate cyclic printing after reloading paper in the printer. In other modes, printing can be restarted directly.

An unidentified error has been detected that prevents printing. If this error occurs, refer to the printer User Manual to identify the cause of the problem.

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Section 10 Security Menu

Note: When the instrument is started for the very first time, security is disabled by default. It is highly recommended that each user be entered into the system and given appropriate access rights as soon as possible to avoid any unauthorized access. Details of this process are described in this section.

10.1 Access rights management

Access rights management

Each user has a unique ID and user password. The ID and password are used by the software to:

• Allow or deny a user to perform specific actions.

• To trace this action with his "ID" in a log file.

Once the ID and password are entered, the user is allowed to perform actions according to the "Access level" that has been attributed to his ID by the Manager. See Security level table on page 17.

Level Typical rights Comments

0 View parameters, change views Press the unlock button and OK to access

1 + Start / Stop measurements

2 + Calibration

Figure 42 Security menu

Table 3 Access levels

3 + Modify parameters

+ Modify table "User ÅÆ Access level"

+ Enable/Disable "Access right" features

Note: At startup, all the menus are locked. The user has to identify himself to get access beyond the different views (see Function keys on the header bar on page 42).

There is at least one ID having the level 4

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Security Menu

10.2 Configure security

Configure security

This enables defining the users with their access level when the software starts for the first time. It is possible to configure several parameters related to confidentiality. This requires a user access level 4.

Note: Access rights are disabled by default.

• Access rights: When enabled, it is required to log in as a registered user (see User management on

page 88) to access the menus. When disabled (default), all menu are access free, and the effect of

leaving the text box blank in user login window is that there will be no name recorded for the action in the log file.

• Enter a maximum session time in minutes for improved confidentiality. The user is logged out

automatically when the set delay for inactivity is over.

• User action logging: When enabled, every action from a logged on user is recorded in a user log file

for traceability.

• Clear all user actions log file. Confirm to clear the log file. This functionality is aimed at clearing demo

or test logs for example. The log file is a rolling buffer recording the past 100 actions.

10.3 User management

User management

This window shows the list of registered users for the instrument. They are listed by name, ID, password and access level.

Note: The "User password" must be at least 4 characters long.

Pressing on an empty line, or pressing the Add button brings a window to add a new user. Name, ID, password and access level (from 1 to 4) must be entered.

Pressing on a registered user line brings a window for editing or deleting the user data in the list.

Note: The list can contain up to 99 users

10.4 User action log file

User action log file

Each time the user performs an important action, a record is written in the "User action log file". It is a rolling buffer which contains the last 1000 user actions. The "User Interface" will allow viewing this log file (Menu Security / View log file). This log file contains the following data:

• line number

• the action name

• the user name and ID

• the current date and time.

Note: Unsuccessful attempts to register are recorded in the log file without a user ID.

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Section 11 Products Menu

Figure 43 Products menu

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Products Menu

Products

This option allows users to save and/or use previously saved product configurations. A maximum of 100 different product configurations can be stored in the instrument. The basic measurement configuration (gas to analyze, gas unit, alarm limits, analog outputs, etc.) can be set up for a product and will be automatically used by the instrument when that product is selected.

Product configurations can be moved from instrument to instrument if required. However, as the sensor only analyzes oxygen, only products configured to analyze oxygen can be selected on this instrument. Products configured to analyze other gases can, however, be set up on this instrument and easily transferred to other 410 or 51x instruments analyzing gases other than oxygen.

For ease of use, where product configurations are identical or similar, a Copy facility exists on the modify product screen. This enables copying a stored configuration and storing it in one or more additional locations. Then use the modify product option to identify and/or modify the duplicate configurations.

Select product Note: If the PROFIBUS-DP communications protocol has been enabled,

products can be selected for analysis using that facility (see Input/Output

data on page 78 and specifically Change product command - output on page 80 for details).

• Select the product (0-99) to be analyzed, or use the Next and Previous

buttons to scroll sequentially through the existing product list. Alternatively, use the Search facility to search for a product. Enter a full

or partial search criteria. If only one match is found, this product is automatically selected. If a number of products match the search criteria, then a list of matches will be displayed. Select a product directly from the list of matching products.

• Press OK to select the product or Cancel to exit.

Modify product • Select the product (index 0-99) to modify, or use the Next and Previous

buttons to scroll sequentially through the existing product list. Alternatively, use the Search facility to search for a product. Enter a full

• Select the gas to analyze (up to three can be selected) from the drop

down list.

• After selecting a product and gas, press Configure to configure the

product. Configure the product as required (refer to Measurement

configuration on page 52 for additional information).

• Press Analog out to configure the analog outputs. Configure the analog

output as required (refer to Channel configuration on page 65 for additional information).

• Press OK to accept the configuration, or Cancel to exit.

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Section 12 Global Configuration Menu

Figure 44 Global configuration menu

Global configuration

The global configuration option allows users to save, and use previously saved, instrument configurations. A maximum of 10 configurations can be saved, with configuration 0 (zero) the instrument default.

Once all the instrument parameters have been set up, use this option to save the configuration. Selecting pre-defined configurations avoids the need to re-enter all the parameters when using the instrument for a different application.

Save • Define the index (1-9) to save the current configuration. Use the Next

and Previous buttons to scroll sequentially through existing configurations, to overwrite an existing configuration or save as a new one.

• Enter a name to define the current configuration.

• Enter any comments to associate with this configuration.

Select • Select the configuration (index 0-9) to use on the instrument.

Confirmation will be required for the selected configuration. The instrument must then be restarted (powered off and then back on) in order for the new configuration to take effect.

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Global Configuration Menu

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Section 13 Services Menu

Figure 45 Services menu - part 1

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Services Menu

Figure 46 Services menu - part 2

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13.1 Sensor diagnostics

Sensor diagnostics Calibration timer The instrument can automatically remind the user when the next sensor

Service timer The instrument can automatically remind the user when the next sensor

Sensor Select either General or Zero diagnostic from the menu.

Services Menu

calibration is due.

• Select enable and enter a delay in days.

• The display shows the current instrument date and time, next calibration

due date and time, and the remaining days.

The next calibration date is updated when the sensor is calibrated. The event “Cal. required” is generated when the delay has elapsed.

service is due.

• Select enable and enter a delay in days. This should be validated by a

level 3 user.

The display shows the current instrument date and time, the next sensor service due date and time, and the remaining days.

The next service date is updated when the button Service done is pressed after a service. The event “Service required” is generated when the delay has elapsed.

The sensor attached to your instrument will require periodic servicing and maintenance. For more information on this, please refer to the manual delivered with the sensor.

General will display values for the measurements in the sample, while Zero is used to display values when the gas concentration is at zero (e.g. during a zero calibration using pure nitrogen as the calibration medium).

The screen layouts are identical for both diagnostic options, and show useful information for troubleshooting purposes.

The first screen displays measurement information, with a status (OK or NOK) alongside. A status of NOK indicates the value is outside of the acceptable minimum or maximum value. To view the acceptable range limits press the Show criteria button.

The criteria screen displays the acceptable range limits (minimum and maximum values) for more in-depth troubleshooting.

Note: If Zero diagnostic is selected, a warning message appears. Ensure the sensor has been calibrated in pure N

before selecting this option.

13.2 Language selection

Language selection

Check the language as required and restart the instrument to apply the change. The instrument will restart in the language selected.

13.3 Clock

Clock

Type in each appropriate box the actual time and date, and select the display format for them.

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Services Menu

13.4Screen

13.5 Buzzer

Screen Screen calibration This screen allows you to adjust the click position corresponding to the

displayed buttons. Use it if ever the sensitive areas are no longer properly aligned with the buttons on display.

Place the stylus right on the cross when asked and proceed. User will be asked to press on the screen to accept the new setting. If not, the new setting is not recorded and no change is made.

Screen brightness Press the up or down arrow to increase or decrease the screen brightness.

Four levels are pre-set: Max, Comfortable, Standard (default setting) and Economy. Press OK when finished.

Note: This can also be called through the brightness icon on the main display.

Buzzer

Adjust the sounds available on the instrument. When “screen tap” is enabled, a click sound is heard each time the screen is touched. The instrument alarm sound can be enabled or disabled to suit the application. The sound type can also

be adjusted. Press the Test button to test the adjustment made. Press again to stop.

13.6 Boards info

Boards info Main board info For reference, this display gives information on the instrument model,

Measurement board info For reference, this display gives information on the sensor measurement

Sensor parameters For reference this display gives information on the sensor model and type,

13.7 Batteries

Batteries

On all instruments this display gives the real time clock battery charge level and voltage.

Note: A warning message (and icon) is displayed if the battery level becomes too low and needs to be replaced.

13.8Software download

software version and instrument ID.

board hardware and software. Pressing the Analog outputs corr. button displays the correction factor that

is applied to the analog outputs. Pressing the Amplifiers corr. button displays the value of the actual

correction factor on the amplifiers.

last calibration, settings and behavior.

Software download

For Hach Lange technician use only. Used when reloading the software for new versions. This ends the application. User must stop and restart the instrument to restart the program.

13.9 End application

End application

This ends the application. User must stop and restart the instrument to restart the program.

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Section 14 Maintenance and Troubleshooting

14.1 Instrument maintenance

CAUTION

Personal Injury Hazard. Any instrument maintenance should be carried out by a qualified Hach Lange Service Technician. Please contact your local representative should you feel any maintenance or instrument adjustments are required

14.2 Sensor maintenance

The sensor spot needs to be replaced about once a year, though for M1100 sensors this will also depend on the CIP frequency. The procedure is very simple and takes no more than a couple of minutes.

Important Note: The shelf-life of the K1100/M1100 LDO spot is 2 years prior to first use.

14.2.1 Equipment required

A replacement sensor spot (No. 1) and O-ring (No. 3) supplied with the sensor spot.

The maintenance tool (No. 2) which is delivered with the sensor.

14.2.2 Sensor spot removal

1. Push the maintenance tool (square sides upmost)

as far down as possible over the old sensor spot. Continue to push down on the tool and turn gently until the square sides of the tool and the square slots of the sensor spot engage. The tool should then drop into position.

2. Turn the tool counter clockwise to unscrew the old

sensor spot.

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Maintenance and Troubleshooting

3. When unscrewed completely simply lift out the old

sensor spot. Pull off the maintenance tool and discard the old sensor spot.

4. Check the red O-ring (position indicated right). If it

appears damaged in any way, then using a pair of tweezers, remove and replace it with the new O-ring from the maintenance kit.

14.2.3 Sensor spot replacement

Avoid scratching or damaging the sensor spot (the black surface on the sensor head) during this process.

NOTICE

1. Push the maintenance tool (square sides upmost)

as far down as possible over the new sensor spot. Continue to push down on the tool and turn gently until the square sides of the tool and the square slots of the sensor spot engage. The tool should then drop into position.

2. Make sure the sensor collar is as far down as it will

go, so that the top of the collar is aligned with the base of the sensor head.

3. Take the combined maintenance tool and sensor

spot and place it in the end of the sensor.