Hach-Lange LDO10130 User Manual

DOC022.52.80021
User Manual
Luminescent Dissolved Oxygen Probe: Model LDO10101, LDO10103, LDO10105, LDO10110, LDO10115 or LDO10130

Safety information

Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol on the instrument is referenced in the manual with a precautionary statement.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of-life equipment to the Producer for disposal at no charge to the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return end-of-life equipment, producer-supplied electrical accessories, and all auxiliary items for proper disposal.

Specifications

Note: Specifications are subject to change without notice.
Specifications Details
Probe type Luminescent dissolved oxygen (LDO) probe
Dissolved oxygen range 0.1 to 20.0 mg/L (ppm) 1 to 200% saturation
Dissolved oxygen accuracy ±0.1 mg/L for 0 to 8 mg/L
±0.2 mg/L for greater than 8 mg/L
% saturation resolution 0.1%
Stabilization time T90% at 10 seconds (when stirred)
Temperature resolution 0.1 °C (0.18 °F)
Temperature accuracy ±0.3 °C (±0.54 °F)
Pressure resolution 1 hPa
Pressure accuracy ±0.8%
Operating temperature range 0 to 50 °C (32 to 122 °F)
Storage temperature range 0 to 40 °C (32 to 104 °F)
Minimum sample depth 25 mm (0.984 in.)
Dimensions (standard) Diameter: 29 mm (1.14 in.)
Length: 191 mm (7.52 in.)
Cable length: 1 or 3 m (3.28 or 9.84 ft)
Dimensions (rugged) Diameter: 46 mm (1.81 in.)
Length: 223 mm (8.73 in.)
Cable length: 5, 10, 15 or 30 meter (16.40, 32.81, 49.21 or 98.42 ft)
Cable connection M12 digital output and connector compatible with HQd meters

Product overview

The LDO101 series probe is a luminescent dissolved oxygen probe (Figure 1). The LDO10105, LDO10110, LDO10115 or LDO10130 rugged probe is available with a 5, 10, 15 or 30 m (16.40, 32.81, 49.21 or 98.42 ft) cable. The LDO10101 or LDO10103 standard
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probe is available with a 1 or 3 m (3.28 or 9.84 ft) cable and is intended for laboratory use. The probe measures the dissolved oxygen concentration in wastewater, drinking water and general applications.
Note: For BOD applications, use the LBOD10101 probe which has LDO technology and a stirrer.
Figure 1 Probe overview
1 LDO probe cap 5 Pressure sensor module
2 Rugged probe (5, 10, 15 or 30 meter cable) 6 iButton® compartment
3 Standard probe (1 or 3 meter cable) 7 Pressure sensor module cap
4 Probe cable
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iButton is a registered trademark of Maxim Integrated Products, Inc.
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Preparation for use

Note: Do not touch the probe cap with a hand, fingers or any surface that can scratch the cap.
Prepare the probe for use before calibration or sample measurement.
1. Make sure that the probe cap and iButton are installed correctly. The iButton label should be up.
2. Make sure that the probe cap and iButton have the same lot code.
3. If a rugged probe, make sure that the shroud is installed before field use (refer to
Install the shroud on page
Note: Damage to the sensing elements can occur if the shroud is not installed during field use. Damage under these conditions is not covered by the product warranty.
4. Rinse the probe cap with deionized water. Blot dry with a lint-free cloth.
5. If dissolved oxygen monitoring periods are longer than 6 hours, condition the probe
cap for 72 hours. Calibrate the probe once every 8 hours.
Note: After 72 hours, the probe cap will reach a fully hydrated state.
9).
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Calibration

Before calibration:
The probe must have the correct service-life time stamp. Set the date and time in the meter before the probe is attached.
It is not necessary to recalibrate when moving a calibrated probe from one HQd meter to another if the additional meter is configured to use the same calibration options.
To view the current calibration, push , select View Probe Data, then select View Current Calibration.
If any two probes are connected, push the UP or DOWN arrow to change to the single display mode in order to show the Calibrate option.
Prepare the probe for use (refer to Preparation for use on page 2.
If a rugged probe, remove the shroud from the probe (refer to Remove the shroud on page 9).
Calibration notes:
% saturation or mg/L calibration methods are available in the Modify Current Settings menu.
The slope value is the comparison between the latest calibration and the factory calibration shown as a percentage.
An additional zero point calibration can be added to the calibration routine. Refer to
Change calibration options on page 8.
The calibration is recorded in the probe and the data log. The calibration is also sent to a PC, printer or flash memory stick if connected.
Air bubbles under the sensor tip when submerged can cause slow response or error in measurement. If bubbles are present, gently shake the probe until bubbles are removed.
If a calibration error occurs, refer to Troubleshooting on page 10.

Water-saturated air (100%) calibration procedure:

1. Connect the
probe to the meter. Make sure that the cable locking nut is securely connected to the meter. Turn on the meter.
2. Push Calibrate.
3. Push Methods. Select
User Cal - 100%. Push OK.
4. Rinse the probe cap with deionized water. Blot dry with a lint­free cloth.
5. Add approximately ¼ inch (6.4 mm) of reagent water to a narrow-neck bottle, such as a BOD bottle.
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6. Put a stopper
in the bottle and shake the bottle vigorously for approximately 30 seconds to saturate the entrapped air with water. Allow up to 30 minutes for contents to equilibrate to room temperature.
7. Remove the stopper. Carefully dry the probe cap with a non­abrasive cloth. Put the probe in the bottle.
8. Push Read. The display shows "Stabilizing" and a progress bar as the probe stabilizes. The display shows the standard value when the reading is stable.
9. Push Done to view the calibration summary.
10. Push Store to accept the calibration and return to the measurement mode. If a rugged probe, install the shroud on the probe (refer to
Install the shroud
on page 9).

Sample measurement

Before measurement:
The probe must have the correct service-life time stamp. Set the date and time in the meter before the probe is attached.
If complete traceability is necessary, enter a sample ID and operator ID before measurement. Refer to the HQd meter manual for more information.
Regular calibration is required for the best measurement accuracy (refer to Calibration on page 3). Calibrate the probe if accuracy better than ±0.50 mg/L is necessary for the application.
Prepare the probe for use (refer to Preparation for use on page 2).
To deploy a rugged probe at a distance, toss the probe body with a gentle underhand throw. Do not swing the probe by the cable as this may cause injury to the user, will cause severe strain on the cable and will shorten the service life of the cell. Damage under these conditions is not covered by the product warranty.
Do not submerge the pressure sensor module.
Measurement notes:
Stabilization times with smaller concentration changes generally will be longer and can be minimized by correct stirring and conditioning. Experiment to determine the correct stir rate if necessary.
Salinity affects the concentration of dissolved oxygen in the sample. To correct for salinity effects, refer to Advanced operation on page 6 or do the Auto salinity
correction on page 5.
Data is automatically stored in the data log when Press to Read or Interval is selected in the Measurement Mode. When Continuous is selected, data will only be stored when Store is selected.
Air bubbles under the sensor tip when submerged can cause slow response or error in measurement. If bubbles are present, gently shake the probe until bubbles are removed.
If a measurement error occurs, refer to Troubleshooting on page 10.
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