Sektion 6 Så här beställer man ................................................................. 147
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Section 1General information
1.1Safety information
Please read this entire application instruction and the POCKET COLORIMETERTM II
instruction manual before unpacking, setting up, or operating this equipment. Pay
attention to all danger and caution statements. Failure to do so could result in serious
injury to the operator or damage to the equipment.
To ensure that the protection provided by this equipment is not impaired, do not use
or install this equipment in any manner other than that specified in this manual.
1.1.1Use of hazard information
DANGER
Indicates a potentially or imminently hazardous situation which, if not
avoided, could result in death or serious injury.
Important Note: Information that requires special emphasis.
Note: Information that supplements points in the main text.
1.2General product information
This application instruction describes how to evaluate LANGE Cuvette Tests on a
single-wavelength POCKET COLORIMETER II.
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Section 2Installation
Important Note: This application instruction is only valid in conjunction with the
POCKET COLORIMETERTM II instruction manual and the applied LCK working
procedure. Please read this entire application instruction and the entire POCKET
COLORIMETER II instruction manual before unpacking, setting up or operating the
instrument.
2.1Packing list
2.1.1COD (high range LCK 014/114)
•POCKET COLORIMETER II 600 nm, Cat. No. 5870060
•Instrument cap with HACH LANGE label, Cat. No. LZV 759
•Cuvette adapter 1 cm, Cat. No. 5954600
•Application instruction DOC027.98.00799
2.1.2COD (low range LCK 314/614)
•POCKET COLORIMETER II 450 nm, Cat. No. 5870045
•Instrument cap with HACH LANGE label, Cat. No. LZV 759
•Cuvette adapter 1 cm, Cat. No. 5954600
•Application instruction DOC027.98.00799
2.2Insert the adapter
Remove the instrument cap and carefully position the cuvette adapter into the cell
holder with the arrow pointing downward. Fix it by pressing it down.
2.3Replace the instrument cap
Use the instrument cap with the HACH LANGE label when evaluating LANGE
cuvettes.
ZERO/SCROLL (BLUE key) : In measurement mode, sets the instrument to zero. In
menu mode, scrolls through menu options. Also scrolls numbers when entering or
editing a value.
READ/ENTER (GREEN key) : In measurement mode, initializes sample
measurement. In menu mode, selects a menu option. When entering numbers,
moves one space to the right. Confirm the function when the entry is complete.
3.2Enter calibration data of LANGE Cuvette Tests
3.2.1Overview
Each POCKET COLORIMETER II has two channels in which measurements can be
made. Each channel (measuring range) will accept user-defined calibration data.
This application instruction contains the calibration data of the LANGE Cuvette Tests
for COD:
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System start up
•high range with POCKET COLORIMETER II 600 nm
•LCK 014: 1000-10000 mg/l COD
•LCK 114: 150-1000 mg/l COD
•low range with POCKET COLORIMETER II 450 nm
•LCK 314: 15-150 mg/l COD
•LCK 614: 50-300 mg/l COD
Each programming procedure has only to be followed once prior to the first test
evaluation.
For detailed information please read the POCKET COLORIMETER II instruction manual.
3.2.2Data table
3.2.2.1Evaluation COD (high range) with POCKET COLORIMETER II 600 nm
Table 1 Evaluation COD (high range) with POCKET COLORIMETER II 600 nm
LCK 014LCK 114
RES (resolution)
S0 (standard 0)
A0 (absorbance 0)
S1 (standard 1)
A1 (absorbance 1)
--------
10000150
0.1770.075
99991000
1.6500.505
3.2.2.2Evaluation COD (low range) with POCKET COLORIMETER II 450 nm
Table 2 Evaluation COD (low range) with POCKET COLORIMETER II 450 nm
LCK 314LCK 614
RES (resolution)
S0 (standard 0)
A0 (absorbance 0)
S1 (standard 1)
A1 (absorbance 1)
---.----.-
015.0050.0
-0.062-0.195
150.0300.0
-0.593-1.15
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System start up
3.3Programming procedure
Note: Each programming procedure has only to be followed once prior to the first test
evaluation.
Note: After programming the calibration data, it could be helpful to mark the channel(s) 1
and/or 2 accordingly with a label.
3.3.1COD (high range LCK 014/114) with
POCKET COLORIMETER II 600 nm
3.3.1.1LCK 014 COD
1.Press POWER to switch on the instrument.
2.Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2).
3.Select measuring range 1 or 2 for LCK 014 (1000-10000 mg/l COD).
Note: Press GREEN key to toggle between measuring ranges.
4.Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
5.Press BLUE key until "Edit" is displayed. Press GREEN key. " RES" is
displayed.
6.Press GREEN key. "-.---" is displayed.
7.Press BLUE key until "----" is displayed. Press GREEN key. "S0" is displayed.
8.Press GREEN keyuntil "A0" is displayed.
9.Press GREEN key until "S1" is displayed.
10. Press GREEN key. Enter "9999" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A1" is
displayed.
11. Press GREEN key. Enter "1.650" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "Add" is
displayed.
12. Press MENU until "Edit" is displayed. Press GREEN key until „S0“ is displayed.
13. Press GREEN key. Enter "1000" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A0" is
displayed.
14. Press GREEN key. Enter "0.177" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until „S1“ is
displayed.
15. Press MENU until "Edit" is displayed to check the entered data. Press GREEN
key. „RES“ is displayed.
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System start up
16. Press BLUE key to scroll through the entries. Compare the entries with the data
shown in the table below.
Table 3 Calibration data of LCK 014 COD
RES--.--
S01000
A00.177
S19999
A11.650
17. After comparing the entries press MENU two times to enter the measuring
mode. See 4.3 Evaluate LANGE COD Cuvette Tests on page 29.
Note: In case of any mistake retrieve the factory calibration first. See 3.5.1 Retrieve the factory
calibration on page 28. After retrieving the factory calibration, start the programming procedure
again. If the instrument is shut-off or loses power during data entry, all edits will be lost.
Automatic shut-off is 60 minutes.
3.3.1.2LCK 114 COD
1.Press POWER to switch on the instrument.
2.Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2).
3.Select measuring range 1 or 2 for LCK 114 (150-1000 mg/l COD).
Note: Press GREEN key to toggle between measuring ranges.
4.Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
5.Press BLUE key until "Edit" is displayed. Press GREEN key. " RES" is
displayed.
6.Press GREEN key. "-.---" is displayed.
7.Press BLUE key until "----" is displayed. Press GREEN key. "S0" is displayed.
8.Press GREEN keyuntil "A0" is displayed.
9.Press GREEN key until "S1" is displayed.
10. Press GREEN key. Enter "1000" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A1" is
displayed.
11. Press GREEN key. Enter "0.505" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "Add" is
displayed.
12. Press MENU until "Edit" is displayed. Press GREEN key until „S0“ is displayed.
13. Press GREEN key. Enter "0150" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A0" is
displayed.
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System start up
14. Press GREEN key. Enter "0.075" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until „S1“ is
displayed.
15. Press MENU until "Edit" is displayed to check the entered data. Press GREEN
key. „RES“ is displayed.
16. Press BLUE key to scroll through the entries. Compare the entries with the data
shown in the table below.
Table 4 Calibration data of LCK 114 COD
RES----
S0150
A00.075
S11000
A10.505
17. After comparing the entries press MENU two times to enter the measuring
mode. See 4.3 Evaluate LANGE COD Cuvette Tests on page 29.
Note: In case of any mistake retrieve the factory calibration first. See 3.5.1 Retrieve the factory
calibration on page 28. After retrieving the factory calibration, start the programming procedure
again. If the instrument is shut-off or loses power during data entry, all edits will be lost.
Automatic shut-off is 60 minutes.
3.3.2COD (low range LCK 314/614) with
POCKET COLORIMETER II 450 nm
3.3.2.1LCK 314 COD
1.Press POWER to switch on the instrument.
2.Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2).
3.Select measuring range 1 or 2 for LCK 314 (15-150 mg/l COD).
Note: Press GREEN key to toggle between measuring ranges.
4.Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
5.Press BLUE key until "Edit" is displayed. Press GREEN key. " RES" is
displayed.
6.Press GREEN key. "-.---" is displayed.
7.Press BLUE key until "---.-" is displayed. Press GREEN key until "S0" is
displayed.
8.Press GREEN keyuntil "A0" is displayed.
9.Press GREEN key until "S1" is displayed.
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System start up
10. Press GREEN key. Enter "150.0" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A1" is
displayed.
Note: If the pre-decimal place of a negative number is zero it will not be displayed. For
example: "-.593".
11. Press GREEN key. Enter "-.593" by using BLUE key to change value (and/or
the sign) and GREEN key to move to the next space. Press GREEN key until
"Add" is displayed.
12. Press MENU until "Edit" is displayed. Press GREEN key until „S0“ is displayed.
13. Press GREEN key. Enter "015.0" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A0" is
displayed.
Note: If the pre-decimal place of a negative number is zero it will not be displayed. For
example: "-.062".
14. Press GREEN key. Enter "-.062" by using BLUE key to change value (and/or
the sign) and GREEN key to move to the next space. Press GREEN key until
„S1“ is displayed.
15. Press MENU until "Edit" is displayed to check the entered data. Press GREEN
key. „RES“ is displayed.
16. Press BLUE key to scroll through the entries. Compare the entries with the data
shown in the table below.
Table 5 Calibration data of LCK 314 COD
RES---.-
S015.0
A0-.062
S1150.0
A1-.593
17. After comparing the entries press MENU two times to enter the measuring
mode. See 4.3 Evaluate LANGE COD Cuvette Tests on page 29.
Note: In case of any mistake retrieve the factory calibration first. See 3.5.1 Retrieve the factory
calibration on page 28. After retrieving the factory calibration, start the programming procedure
again. If the instrument is shut-off or loses power during data entry, all edits will be lost.
Automatic shut-off is 60 minutes.
3.3.2.2LCK 614 COD
1.Press POWER to switch on the instrument.
2.Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2).
3.Select measuring range 1 or 2 for LCK 614 (50-300 mg/l COD).
Note: Press GREEN key to toggle between measuring ranges.
4.Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
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System start up
5.Press BLUE key until "Edit" is displayed. Press GREEN key. " RES" is
displayed.
6.Press GREEN key. "-.---" is displayed.
7.Press BLUE key until "---.-" is displayed. Press GREEN key until "S0" is
displayed.
8.Press GREEN keyuntil "A0" is displayed.
9.Press GREEN key until "S1" is displayed.
10. Press GREEN key. Enter "300.0" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A1" is
displayed.
11. Press GREEN key. Enter "-1.15" by using BLUE key to change value (and/or
the sign) and GREEN key to move to the next space. Press GREEN key until
„Add“ is displayed.
12. Press MENU until "Edit" is displayed. Press GREEN key until „S0“ is displayed.
13. Press GREEN key. Enter "050.0" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A0" is
displayed.
Note: If the pre-decimal place of a negative number is zero it will not be displayed. For
example: "-.195".
14. Press GREEN key. Enter "-.195" by using BLUE key to change value (and/or
the sign) and GREEN key to move to the next space. Press GREEN key until
„S1“ is displayed.
15. Press MENU until "Edit" is displayed to check the entered data. Press GREEN
key. „RES“ is displayed.
16. Press BLUE key to scroll through the entries. Compare the entries with the data
shown in the table below.
Table 6 Calibration data of LCK 614 COD
RES---.-
S050.0
A0-.195
S1300.0
A1-1.15
17. After comparing the entries press MENU two times to enter the measuring
mode. See 4.3 Evaluate LANGE COD Cuvette Tests on page 29.
In case of any mistake retrieve the factory calibration first. See 3.5.1 Retrieve the factory
calibration on page 28. After retrieving the factory calibration, start the programming procedure
again. If the instrument is shut-off or loses power during data entry, all edits will be lost.
Automatic shut-off is 60 minutes.
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System start up
3.4Check entered data
To avoid erroneous measurements it is recommended to check the data after
completing the programme procedure.
1.Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
2.Press BLUE key to scroll to "Edit". Press GREEN key.
3."RES" is displayed. Press BLUE key to scroll through the entries. Compare the
entries with the figures in the 3.2.2 Data table on page 22.
In case a value was not stored correctly, retrieve the factory calibration first. See 3.5.1
Retrieve the factory calibration on page 28. After retrieving the factory calibration,
start the programming procedure again.
3.5Overwrite stored calibration data
With the POCKET COLORIMETER II it is possible to overwrite stored calibration
data. Before overwriting calibration data it is recommended to retrieve the factory
calibration first. After retrieving the factory calibration, you can program new
calibration data.
In case of any mistake retrieve the factory calibration first.
3.5.1Retrieve the factory calibration
1.Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2). Press GREEN key to toggle between measuring
ranges. Select measuring range retrieving the factory calibration.
1.Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
2.Press BLUE key to scroll to "dFL". Press GREEN key.
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