Hach-Lange 5341 User Manual [en, de, es, fr, it]

pH
53 41
pH
53 41
1
2
3
4
5
pH@20ºC F- limit (ppm)
5 no limit
2
6
7
8
9
KCl 3M
Key points. Hauptteile. Puntos clave. Points clé. Punti chiave. Pontos chaves.
Protective cap.
1
Schutzkappe.
Tapón protector.
Bouchon protecteur.
Tappo protettore.
Tampa protetora.
S8 connector.
2
S8-Stecker.
Conector S8.
Connecteur S8.
Connettore S8.
Conector S8.
PG 13.5 thread.
3
Montagegewinde PG 13,5.
Rosca de sujeción PG 13,5.
Filetage PG 13,5.
Filettatura PG 13,5.
Rosca de fixação PG 13,5.
Reference element.
4
Referenzelement.
Elemento de referencia.
Élément de référence.
Elemento di riferimento.
Elemento de referência.
Internal diaphragm.
5
Internes Diaphragma.
Diafragma interno.
Diaphragme interne.
Diaframma interno.
Diafragma interno.
Gel electrolyte.
6
Elektrolytgel.
Electrolito gel.
Électrolyte gel.
Elettrolita gel.
Eletrólito gel.
Diaphragm: ceramic.
7
Diaphragma: Keramik.
Diafragma: cerámico.
Diaphragme: céramique.
Diaframma: ceramico.
Diafragma: cerâmico
Sensitive glass membrane.
8
Sensitive Glasmembran.
Membrana sensible.
Membrane sensible.
Membrana sensibile.
Membrana sensível de vidro.
Storage protector.
9
Lagerungsschutz.
Protector de almacenamiento.
Tube protecteur de stockage.
Protettore per la conservazione.
Protetor para armazenamento.
(EU Directive 2002/96/EC)
3
pH electrode 53 41
Introduction
The 53 41 is a low maintenance pH elec- trode for samples containing HF.
SAFETY NOTE Before use with hazardous substanc­es, find out about the relevant haz­ards, protective measures, and what to do in an emergency.
Electrode preparation
• Remove the storage protector
• Verify that there are not air bubbles
inside the membrane removed by shaking the electrode as a clinical thermometer.
Installation
In immersion, insertion, flotation housings, etc. with PG 13,5 thread.
See Housing instruction manual.
In some cases the electrode is installed, with the help of sockets and adapters, directly onto pipes. Cable. They are connected to coaxial cables with an AS9 connector.
Calibration
See pH-meter instruction manual.
Measurements. Recommendations
See pH-meter instruction manual. Ensure that the electrode’s specifications are adapted to the process. Sample must cover the diaphragm
Maintenance
• Deposits forming on the electrodes,
caused by continual exposure of the sen­sors to a dirty or contaminated medium, is one of the most frequent causes of prob­lems when measuring pH. When possible it’s recommended to use a housing with automatic sensor cleaning system.
• When an electrode gets contaminated,
the simple rinsing with distilled water is not suffi cient. The most suitable clean­ing solution is one which acts in a more selective way over the contamination (look for regeneration solutions).
Re-hydration. A “dry” electrode re-
covers by immersing it in diluted HCl solution for several hours. It is recom­mended to read the information sup­plied with the electrode’s regenerating solutions.
.
. They can be
.
Troubleshooting
... the meter always shows the same pH
value. Short circuit in the electrode or cable.
Substitute the cable or the elec­trode.
... shifting of pH values.
Reference system contamination.
Replace the electrode
... unstable reading.
Diaphragm blockage.
Clean, regenerate, replace the elec­trode.
4
GB
... impossible to perform calibration. ... very slow response.
Dirt on the diaphragm or the mem­brane. De-hydrated membrane. Electrode ageing or wear.
Clean, regenerate, replace the elec­trode.
Storage
The connector should be protected from humidity by the protective cap . Place the electrode in the storage protec­tor with KCl 3M.
Specifications
Measuring range 0 to 14 pH Operating temp. 0 to 80 °C Max. pressure 6 bar Reference element cartridge Diaphragm ceramic Electrolyte gel Body material glass Thread PG 13,5 Connector S8 Min. immersion depth 17 mm
Applications
Water containing fluoride.
Warning. The resistance of the membrane is directly related to the HF concentration and the pH of the sample (see ).
Limitations
Viscous solutions or samples with colloids. Distilled water.
CERTIFICATE OF QUALITY
The attached electrode 53 41 has passed the quality test and follows the next speci­fications:
• Asymmetry potential < ± 15 mV.
• Sensitivity, pH 4 to 7 (at 25 ˚C) > 98%.
• Response time, pH 4 to 7 < 20 s.
5
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