DOC022.98.90030
POCKET COLORIMETER
TM
Zinc/Zink/Cinc/Zinco
LCK 360
APPLICATION INSTRUCTION
PROGRAMMIERANLEITUNG
INSTRUCTIONS DE FONCTIONNEMENT
INSTRUCCIONES DE APLICACIÓN
ISTRUZIONI APPLICATIVE
GEBRUIKSAANWIJZING
INSTRUKTIONSHANDBOK
January 2008, Edition 1
Januar 2008, Ausgabe 1
Janvier 2008, édition 1
Enero 2008, Edición 1
Gennaio 2008, edizione 1
Jan 2008, Editie 1
Januari 2008, Utgåva 1
II -
Table of contents
Section 1 General information .....................................................................17
1.1 Safety information .....................................................................................17
1.1.1 Use of hazard information .............................................................. 17
1.2 General product information ..................................................................... 17
Section 2 Installation ......................................................................................19
2.1 Packing list ................................................................................................ 19
2.2 Insert the adapter ...................................................................................... 19
2.3 Replace the instrument cap ......................................................................19
Section 3 System start up .............................................................................21
3.1 Instrumen t keys and display ..................................................................... 21
3.1.1 Key-Functions .................................................................................21
3.2 Ente r calibration data of LANGE Cuvette Test .........................................21
3.2.1 Overview .........................................................................................21
3.2.2 Data table .......................................................................................22
3.3 Programming procedure ...........................................................................22
3.3.1 LCK 360 solved Zink Zn ................................................................. 22
3.3.2 LCK 360 total Zi nc Zn .....................................................................23
3.4 Check entered data ..................................................................................24
3.5 Overwrite stored calibration data ..............................................................25
3.5.1 Retrieve the factory calibration ....................................................... 25
Section 4 Operation ........................................................................................ 27
4.1 Analyse Zinc with LANGE Cuvette Test ...................................................27
4.2 Quality assurance ............................................ ... ... ...................................27
4.3 Evaluate LANGE Zinc Cuvette Test ......................................................... 27
Section 5 Replacement Parts and Accessories ....................................29
5.1 Replacement Parts ................................................................................... 29
5.2 Accessories .............................................................................................. 29
Section 6 Warranty, liability and complaints ........................................... 31
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Inhalt
Abschnitt 1 Allgemeine Informationen ......................................................33
1.1 Sicherheitsinformationen .......................................................................... 33
1.1.1 Bedeutung der Hinweise ................................................................33
1.2 Allgemeine Produktinformationen ......................................................... .... 33
Abschnitt 2 Installation ................................................................................... 35
2.1 Verpackungsliste ...................................................................................... 35
2.2 Küvettenadapter einsetzen .......................................................................35
2.3 Austa usch der Instrumentenkappe ...........................................................35
Abschnitt 3 Inbetriebnahme .........................................................................37
3.1 Gerätetasten und Display ......................................................................... 37
3.1.1 Tasten-Funktionen .......................................................................... 37
3.2 Einga be der Kalibrierdaten für LANGE Küvetten-Test ..............................38
3.2.1 Überblick .........................................................................................38
3.2.2 Datentabelle ...................................................................................38
3.3 Programmierung ....................................................................................... 38
3.3.1 LCK 360 freies Zink Zn ................................................................... 39
3.3.2 LCK 360 Gesamt-Zink Zn ............................................................... 40
3.4 Dateneingabe kontrollieren ....................................................................... 41
3.5 Überschreiben gespeicherter Kalibrierdaten .............................................41
3.5.1 Grundeinstellung wieder herstellen ................................................41
Abschnitt 4 Betrieb .......................................................................................... 43
4.1 Analyse von Zink mit dem LANGE Küvetten-Test .................................... 43
4.2 Qualitätssicherung .................................................................................... 43
4.3 Auswertung des LANGE Zink Küvetten-Tests ..........................................43
Abschnitt 5 Ersatzteile und Zubehör ......................................................... 45
5.1 Ersatzteile ................................................................................................. 45
5.2 Zubehör ....................................................................................................45
Abschnitt 6 Gewährleistung, Haftung und Reklamationen ................47
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Sommaire
Section 1 Informations générales ...............................................................49
1.1 Consi gnes de sécurité ..............................................................................49
1.1.1 Uti lisation des informations relatives aux risques .................... ... .. ..49
1.2 Informations générales relatives au produit ..............................................49
Section 2 Installation ......................................................................................51
2.1 Liste d’expédition ......................................................................................51
2.2 Insertion de l’adaptateur ...........................................................................51
2.3 Réinstallation du capuchon de l’instrument ..............................................51
Section 3 Démarrage du système ..............................................................53
3.1 Écran et touch es de l’instrument ............................................................... 53
3.1.1 Fonctions des touches ....................................................................53
3.2 Saisie des données d'étalonnage de test en cuve LANGE ...................... 54
3.2.1 Vue d’ensemble ..............................................................................54
3.2.2 Tableau de données ....................................................................... 54
3.3 Procédure de programmation ...................................................................54
3.3.1 LCK 360 dissous zinc Zn ................................................................ 54
3.3.2 LCK 360 total zinc Zn ..................................................................... 56
3.4 Vérification des données saisies ...............................................................57
3.5 Écra s ement des donn ées d'étalonnage stockées ....................................57
3.5.1 Récup ération de l'étalonnage usine ...............................................57
Section 4 Fonctionnement ............................................................................59
4.1 Analyse de zinc à l’aide de test en cuve LANGE ......................................59
4.2 Assurance qualité .....................................................................................59
4.3 Évaluation de test en cuve zinc LANGE ..................................................59
Section 5 Pièces de remplacement et accessoires ..............................61
5.1 Pièces de remplacement .......................................................................... 61
5.2 Accessoires .............................................................................................. 61
Section 6 Garantie, responsabilité et réclamations ..............................63
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Índice de contenido
Sección 1 Información general ...................................................................65
1.1 Indicaciones de seguridad ........................................................................65
1.1.1 Utilización de las indicaciones de peligro .......................................65
1.2 Información general del producto .............................................................65
Sección 2 Instalación .....................................................................................67
2.1 Lista de embalaje ......................................................................................67
2.2 In ser tar el adaptador .................................................................................67
2.3 Reempl azar la tapa del instrumento .........................................................67
Sección 3 Arranque del sistema ................................................................. 69
3.1 Teclas y pantalla del instrumento .............................................................69
3.1.1 Funciones de tecla .........................................................................69
3.2 Introd uzca los datos de calibración de la cubeta test de LANGE .............70
3.2.1 Vista general ...................................................................................70
3.2.2 Tabla de datos ................................................................................70
3.3 Pro cedimientos de programación .............................................................70
3.3.1 LCK 360 disuelto cinc Zn ................................................................71
3.3.2 LCK 360 total de cinc Zn ................................................................ 72
3.4 Controlar los datos introducidos. ..............................................................73
3.5 Sobree scribir los datos de calibración almacenados. ...............................73
3.5.1 Recuperación de calibración por defecto .......................................74
Sección 4 Operación ......................................................................................75
4.1 Análisis de cinc con la cubeta test de LANGE ..........................................75
4.2 Aseguramiento de calidad ........................................................................ 75
4.3 Evaluación de cinc de LANGE Cubeta test .............................................75
Sección 5 Piezas de repuesto y accesorios ........................................... 77
5.1 Piezas de repuesto ...................................................................................77
5.2 Accesorios ................................................................................................77
Sección 6 Garantía, responsabilidad y reclamaciones .......................79
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Indice
Capitolo 1 Informazioni generali .................................................................81
1.1 Istruzioni di sicurezza ................................................................................81
1.1.1 Uti lizzo delle informazioni di sicurezza ........................................... 81
1.2 Informazioni generali sul prodotto .............................................................81
Capitolo 2 Installazione .................................................................................83
2.1 Distinta di imballaggio ...............................................................................83
2.2 Inserimento dell’adattatore ........................................................................83
2.3 Inserimento del coperchio Hach Lange ....................................................83
Capitolo 3 Messa in esercizio del sistema ..............................................85
3.1 Tasti e display dello strumento ................................................................. 85
3.1.1 Funzioni dei tasti .............................................................................85
3.2 Inserimento dei dati di calibrazione dei test in cuvetta LANGE ................85
3.2.1 Panoramica strumentale .................................................................85
3.2.2 Tabella dati di calib razione .............................................................86
3.3 Procedura di programmazione ..................................................................86
3.3.1 LCK 360 zinco disciolto Zn .............................................................86
3.3.2 LCK 360 zinco totale Zn ................................................................. 87
3.4 Controllo dei dati inseriti ............................................................................ 89
3.5 Come sovrascrivere i dati di calibrazione memorizzati ............................. 89
3.5.1 Come richia mare la calibrazione di fabbrica ...................................89
Capitolo 4 Esercizio ........................................................................................ 91
4.1 Analisi zinco con test in cuvetta LANGE ...................................................91
4.2 Garanzia di qualità ....................................................................................91
4.3 Test in cuvetta LANGE zinco ...................................................................91
Capitolo 5 Parti di ricambio e accessori ...................................................93
5.1 Parti di ricambio ............................................ ............................................93
5.2 Accessori .................................................................................................. 93
Capitolo 6 Garanzia, responsabilità e reclami .......................................95
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12
Inhoud
Deel 1 Algemene informatie .........................................................................97
1.1 Veili gheidsinformatie .................................................................................97
1.1.1 Gebruik van geva renin formatie .......................................................97
1.2 Algemene productinformatie .....................................................................97
Deel 2 Installatie ..............................................................................................99
2.1 Paklijst ......................................................................................................99
2.2 De adapter insteken ..................................................................................99
2.3 De kap van het instrument terug aanbrengen. ..........................................99
Deel 3 Het systeem opstarten ...................................................................101
3.1 Instrumenttoetsen en display ............................................... ... .. .............. 101
3.1.1 Toets-functies ............................................................................... 101
3.2 De kalibratiedata van LANGE kuvettentesten invoeren ..........................101
3.2.1 Overzicht ......................................................................................101
3.2.2 Datatabel ......................................................................................102
3.3 Pro grammeerprocedure ..........................................................................102
3.3.1 LCK 360 opgelost zink Zn ............................................................102
3.3.2 LCK 360 total zink Zn ................................................................... 103
3.4 De ing evoerde data co ntroleren ..............................................................105
3.5 Opgeslagen kalibratiedata overschrijven ................................................ 105
3.5.1 De fabriekskalibratie herstellen ..................................................... 105
Deel 4 Bedrijf ..................................................................................................107
4.1 Zink met Lange kuvette ntest an alyseren ................................................107
4.2 Kwaliteitsborging .....................................................................................107
4.3 LANGE zink kuvettentest .......................................................................107
Deel 5 Reservedelen en toebehoren ......................................................109
5.1 Reservedelen ..........................................................................................109
5.2 Accessoires ............................................................................................ 109
Deel 6 Garantie, aansprakelijkheid en klachten .................................. 111
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Innehåll
Sektion 1 Allmän information .....................................................................113
1.1 Säkerhetsinformation ..............................................................................113
1.1.1 Så här används säkerhetsinformationen ......................................113
1.2 Allmän produktinformation ......................................................................113
Sektion 2 Installation ....................................................................................115
2.1 Packlista ................................................................................................. 115
2.2 Installera adaptern ..................................................................................115
2.3 Byta ut instrumentlocket .......................................................................... 115
Sektion 3 Systemstart ..................................................................................117
3.1 Instrumenttan genter och display .............................................................117
3.1.1 Funktio nstangenter ....................................................................... 117
3.2 Mata in kalibreringsdata för LANGE kyvett-tester ................................... 117
3.2.1 Översikt ........................................................................................117
3.2.2 Datatabell .....................................................................................118
3.3 Programmeringsprocedur ....................................................................... 118
3.3.1 LCK 360 löst zink Zn ....................................................................118
3.3.2 LCK 360 total zink Zn ................................................................... 119
3.4 Kontrollera indata ....................................................................................120
3.5 Skriv över sparade kalibreringsdata ........................................................ 120
3.5.1 Återgå till först fabrikskalibreringen ............................................... 121
Sektion 4 Användning ..................................................................................123
4.1 Analysera zink med LANGE kyvett-test .................................................. 123
4.2 Kvalitetssäkring .......................................................................................123
4.3 Utvärdering LANGE zink kyvett-test ...................................................... 123
Sektion 5 Reservdelar och tillbehör ......................................................... 125
5.1 Reservdelar ............................................................................................125
5.2 Tillbehör .................................................................................................. 125
Sektion 6 Garanti, ansvar och reklamationer ....................................... 127
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Section 1 General information
1.1 Safety information
Please read this entire application instruction and the POCKET COLORIMETERTM II
instruction manual before unpacking, setting up, or operating this equipment. Pay
attention to all danger and caution statements. Failure to do so could result in serious
injury to the operator or damage to the equipment.
To ensure that the protection provided by this equipment is not impaired, do not use
or install this equipment in any manner other than that specified in this manual.
1.1.1 Use of hazard information
DANGER
Indicates a potentially or imminently hazardo us situation which, if not
avoided, could result in death or serious injury.
Important Note: Information that requires special emphasis.
Note: Information that supplements points in the main text.
1.2 General product information
This application instruction describes how to evaluate LANGE Cuvette Tests on a
single-wavelength POCKET COLORIMETER II.
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18
Section 2 Installation
Important Note: This application instruction is only valid in conjunction with the
POCKET COLORIMETERTM II instruction manual and the applied LCK working
procedure. Please read this entire application instruction and the entire POCKET
COLORIMETER II instruction manual bef or e un packing, setting up or operating the
instrument.
2.1 Packing list
• POCKET COLORIMETER II 500 nm, Cat. No. 5870050
• Instrument cap with HACH LANGE label, Cat. No. LZV 759
• Cuvette adapter 1 cm, Cat. No. 5954600
• Application instruction DOC022.98.90030
2.2 Insert the adapter
Remove the instrument cap and carefully position the cuvette adapter into the cell
holder with the arrow pointing downward. Fix it by pressing it down.
2.3 Replace the instrument cap
Use the instrument cap with the HACH LANGE label when evaluating LANGE
cuvettes.
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Section 3 System start up
3.1 Instrument keys and display
Figure 1 Instrument keys and display
1 POWER/BACKLIGHT 6 Measuring range indicator (2)
2 ZERO/SCROLL (BLUE key)7Menu indicator
3MENU 8Calibration adjusted indicator
4 Numeric display 9 Battery low indicator
5 Measuring range indicator (1) 10 READ/ENTER (GREEN key)
3.1.1 Key-Functions
ZERO/SCROLL (BLUE key) : In measurement mode, sets the instrument to zero. In
menu mode, scrolls through menu options. Also scrolls numbers when entering or
editing a value.
READ/ENTER (GREEN key) : In measurement mode, initiali ze s sample
measurement. In menu mode, selects a menu option. When entering numbers,
moves one space to the right. Confirm the function when the entry is complete.
3.2 Enter calibration data of LANGE Cuvette Test
3.2.1 Overview
Each POCKET COLORIMETER II has two channels in which measurements can be
made. Each channel (measuring range) will accept user-defined calibration data.
This application instruction contains the calibration data of the LANGE Cuvette Test
for Zinc:
21
System start up
• LCK 360: 0.2-6 mg/l solved Zinc
• LCK 304: 0.24-7.2 mg/l total Zinc after digestion with Crack-Set LCW 902
Each programming procedure has only to be followed once prior to the first test
evaluation.
For detailed information please read the POCKET COLORIMETER II instruction
manual.
3.2.2 Data table
3.2.2.1 Evaluation as Zinc
Table 1 Evaluation as solved Zinc and total Zinc
RES (resolution)
S0 (standard 0)
A0 (absorbance 0)
S1 (standard 1)
A1 (absorbance 1)
LCK 360
solved Zinc
--.-- --.--
00.20 00.24
0.035 0.035
06.00 07.20
0.610 0.610
LCK 360
total Zinc
3.3 Programming procedure
Note: Each programming procedure has only to be followed once prior to the first test
evaluation.
Note: After programming the calibration data, it could be helpful to mark the channel(s) 1
and/or 2 accordingly with a label.
3.3.1 LCK 360 solved Zink Zn
1. Press POWER to switch on the instrument.
2. Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2).
3. Select measuring range 1 for LCK 360 (0.2-6 mg/l Zn).
Note: Press GREEN key to toggle between measuring ranges.
4. Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
5. Press BLUE key until "Edit" is displayed. Press GREEN key. " RES" is
displayed.
6. Press GREEN key. "-.---" is displayed.
7. Press BLUE key until "--.--" is displayed. Press GREEN key. "S0" is displayed.
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System start up
8. Press GREEN key until "A0" is displayed.
9. Press GREEN key until "S1" is displayed.
10. Press GREEN key. Enter "06.00" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A1" is
displayed.
11. Press GREEN key. Enter "0.610" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "Add" is
displayed.
12. Press MENU until "Edit" is displayed. Press GREEN key until „S0“ is displayed.
13. Press GREEN key. Enter "00.20" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A0" is
displayed.
14. Press GREEN key. Enter "0.035" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until „S1“ is
displayed.
15. Press MENU until "Edit" is displayed to check the entered data. Press GREEN
key. „RES“ is displayed.
16. Press BLUE key to scroll through the entries. Compare the entries with the data
shown in the table below.
Table 2 Calibration data of LCK 360 solved Zn
RES --.--
S0 0.20
A0 0.035
S1 6.00
A1 0.610
17. After comparing the entries press MENU two times to enter the measuring
mode. See 4.3 Evaluate LANGE Zinc Cuvette Test on page 27.
Note: In case of any mistake retrieve the factory calibration first. See 3.5.1 Retrieve the factory
calibration on page 25. After retrieving the factory calibration, start the programming procedure
again. If the instrument is shut-off or loses power during data entry, all edits will be lost.
Automatic shut-off is 60 minutes.
3.3.2 LCK 360 total Zinc Zn
1. Press POWER to switch on the instrument.
2. Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2).
3. Select measuring range 2 for LCK 360 (0.24-7.2 mg/l Zn).
Note: Press GREEN key to toggle between measuring ranges.
4. Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
5. Press BLUE key until "Edit" is displayed. Press GREEN key. " RES" is
displayed.
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System start up
6. Press GREEN key. "-.---" is displayed.
7. Press BLUE key until "--.--" is displayed. Press GREEN key. "S0" is displayed.
8. Press GREEN key until "A0" is displayed.
9. Press GREEN key until "S1" is displayed.
10. Press GREEN key. Enter "07.20" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A1" is
displayed.
11. Press GREEN key. Enter "0.610" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "Add" is
displayed.
12. Press MENU until "Edit" is displayed. Press GREEN key until „S0“ is displayed.
13. Press GREEN key. Enter "00.24" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until "A0" is
displayed.
14. Press GREEN key. Enter "0.035" by using BLUE key to change value and
GREEN key to move to the next space. Press GREEN key until „S1“ is
displayed.
15. Press MENU until "Edit" is displayed to check the entered data. Press GREEN
key. „RES“ is displayed.
16. Press BLUE key to scroll through the entries. Compare the entries with the data
shown in the table below.
Table 3 Calibration data of LCK 360 total Zn
RES --.--
S0 0.24
A0 0.035
S1 7.20
A1 0.610
17. After comparing the entries press MENU two times to enter the measuring
mode. See 4.3 Evaluate LANGE Zinc Cuvette Test on page 27.
Note: In case of any mistake retrieve the factory calibration first. See 3.5.1 Retrieve the factory
calibration on page 25. After retrieving the factory calibration, start the programming procedure
again. If the instrument is shut-off or loses power during data entry, all edits will be lost.
Automatic shut-off is 60 minutes.
3.4 Check entered data
To avoid erroneous measurements it is recommended to check the data after
completing the programme procedure.
1. Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
2. Press BLUE key to scroll to "Edit". Press GREEN key.
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System start up
3. "RES" is displayed. Press BLUE key to scroll through the entries. Compare the
entries with the figures in the 3.2.2.1 Evaluation as Zinc on page 22.
In case a value was not stored correctly, retrieve the factory calibration first. See 3.5.1
Retrieve the factory calibration on page 25. After retrieving the factory calibration,
start the programming procedure again.
3.5 Overwrite stored calibration data
With the POCKET COLORIMETER II it is possible to overwrite stored calibration
data. Before overwriting calibration data it is recommended to retrieve the factory
calibration first. After retrieving the factory calibration, you can program new
calibration data.
In case of any mistake retrieve the factory calibration first.
3.5.1 Retrieve the factory calibration
1. Press MENU. "SEL" is displayed. A flashing arrow indicates the current
measuring range (1 or 2). Press GREEN key to toggle between measur ing
ranges. Select measuring range retrieving the factory calibration.
2. Press MENU for about five seconds until "USER" followed by "CAL" is
displayed.
3. Press BLUE key to scroll to "dFL". Press GREEN key.
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Section 4 Operation
4.1 Analyse Zinc with LANGE Cuvette Test
DANGER
Handling chemical samples, standards and reagents can be dangerous. Users
of this product are advised to familiarize themselves with safety procedures
and the correct use of chemicals, and to carefully read all relevant material
safety data sheets.
T o analyse zinc follow the working procedure enclosed in the according Cuvette Test
LCK 360.
4.2 Quality assurance
The measurement results must be subjected to plausibility checks (dilute and/or
spike the sample).
Regular checks with corresponding standard solutions (see Section 5 Replacement
Parts and Accessories on page 29) ensure that your measurement system is
functioning properly and is being correctly operated.
4.3 Evaluate LANGE Zinc Cuvette Test
Note: Make sure that the instrument is programmed with the corresponding calibration data,
see 3.4 Check entered data on page 24.
1. Press POWER to switch on the instrument.
2. Make sure that the correct measuring range is selected!
Otherwise press MENU. "SEL" is displayed. A flashing arrow indicates the
current measuring range (1 or 2). Press GREEN key to select measuring range.
Press MENU to get back to the measuring mode.
3. Insert the zero-solution into the cell holder equipped with the cuvette adapter
1cm.
Note: Make sure that the cuvette adapter is positioned correctly.
4. Place the instrument cap with the HACH LANGE label over the cell holder to
cover the cuvette.
5. Press BLUE key. "0.00" is displayed.
6. Remove the instrument cap and insert the sample cuvette.
7. Place the instrument cap over the cell holder to cover the cuvette.
8. Press GREEN key.
9. The result is displayed in mg/l Zinc.
Note: In case the zinc concentration is out of the selected measuring range the value for
the lowest or highest concentration is displayed and flashes. Repeat the test using the
appropriate measuring range or dilute your sample.
Note: A new zero measurement should be performed prior to each individual test series.
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Section 5 Replacement Parts and
Accessories
5.1 Replacement Parts
Description Quantity Cat. Number
POCKET COLORIMETERTM II 500 nm 1 5870050
Instrument cap with HACH LANGE label 1 LZV 759
Cuvette adapter 1 cm 1 5954600
5.2 Accessories
Description Quantity Cat. Number
Zinc Cuvette Test (0.2-6 mg/l Zn) 1 pk/24 pc LCK 360
Crack-Set 50 dig. LCW 902
Standard and Ring Test solution for LCK 360 1 LCA 701
Pipette 0.2-1 ml 1 BBP 078
Pipette tips for BBP 078 1 pk/100 pc BBP 079
Pipette 1-5 ml 1 BBP 065
Pipette tips for BBP 065 1 pk/75 pc BBP 068
Cuvette Stand for LANGE cuvettes 1 LYW 915
Thermostat LT 200 1 LTV082.99.51002
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