GF Signet 3719 User Manual

Signet 3719 pH/ORP Wet-Tap
*3-3719.090*
3-3719.090 Rev L 12/11 English
English
Do not exceed maximum temperature/pressure specifi cations.
Wear safety goggles or face shield during installation/service.
Do not attempt to disassemble the retraction housing and the electrode piston.
Do not alter product construction.
Failure to follow safety instructions may result in severe personal injury.
1. Description
2. Specifi cations
3. Dimensions
4. 3719 System Overview
5. Installation
6. Maintenance & Cleaning
7. Troubleshooting
8. Ordering Information
1. Description
The Signet 3719 pH/ORP Wet-Tap allows installation and removal of pH or ORP electrodes without the need for process shutdown during routine electrode maintenance and calibration. Process isolation is achieved with a double O-ring seal on a unique and compact retraction assembly; no separate valve is required. A cam-activated automatic locking mechanism, SafeLoc™, and the short stroke design help to assure operator safety.
2. Specifi cations
General
• Compatible sensors: 2716-WT Twist-Lock pH Electrode 2717-WT Twist-Lock ORP Electrode 2756-WT DryLoc® pH Electrode 2756-WT-1 DryLoc® pH Electrode 2756 -WTP DryLoc® plastic pH electrode 2756-WTP-1 DryLoc® plastic pH electrode 2757-WT DryLoc® ORP Electrode 2757-WTP DryLoc® plastic ORP electrode
• Shipping Weight: Wet-tap assembly: 1.2 kg (2.7 lbs.) Electrode: 0.13 kg (0.3 lb)
Process Connection: 3-3719-11: 1½ in. NPT 3-3719-21: 2 in. NPT 3-3719-12: ISO 7/1-R1½ 3-3719-22: ISO 7/1-R2
Wetted materials
• Retraction Housing: CPVC
• O-rings: FPM
Electrode Body: Glass OR Plastic
Electrode junctions: Porous PTFE
Electrode sensing surface:
Glass Membrane (pH) Platinum (ORP)
• Electrode O-rings: FPM
Other Materials
• Locking Shroud: PVC
Hardware: 316 stainless steel
Performance
Maximum Flow Velocity: 3 m/s (10 ft/s)
• Effi ciency: > 97% @ 25 °C (77 °F)
Response Time: pH: <5s for 95% of signal change ORP: Application dependent
Drift: < 2 mV per week
Operating Range: pH: 0 to 14 pH ORP: –2000 to +2000 mV
Reference Junctions: Porous PTFE
• Electrolyte: 3.5M KCl
• Elements: Ag/AgCl
Temp. Sensor (pH): 3K Balco (3-2716-WT, 3-2756-WT-1, WTP-1)
PT1000 (3-2756-WT, -WTP)
Temp. response time ( 438 s
Sodium Ion Error: < 0.05 pH in 0.1 molar Na+ ion at 12.8 pH
Impedance (pH): <150 MΩ @ 25 °C
Storage Temperature:
Wet-tap assembly: -15 to 120 °C (5 to 248 °F)
Electrode: 0 to 50 °C (32 to 122 °F)
WARNING!
If used in conditions that exceed recommended pressure ratings, this product can pose a serious hazard. We urge customers to read the specifi cations carefully before installing and operating this product. Improper use can cause components and process liquids to be expelled at high speeds and cause serious personal injury.
Standards and Approvals
Manufactured under ISO 9001 and 14001
25
China RoHS (Go to www.gfsignet.com for details)
76 mm (3.0 in.)
130 mm (5.13 in.)
49 mm (1.94 in.)
45 mm (1.75 in.)
39 mm (1.52 in.)
20 mm (0.8 in.)
75 mm (2.94 in.)
Pipe thread 1
1
/2 in. NPT
or
ISO 7-R1
1
/
2
76 mm (3.0 in.)
39 mm (1.52 in.)
20 mm (0.8 in.)
Pipe thread
2 in. NPT
or
ISO 7-R2
34 mm
(1.32 in.)
41 mm
(1.62 in.)
25 mm
(1.00 in.)
3. Dimensions
12 mm
(0.47 in.)
30,5 mm
(1.2 in.)
218 mm
(8.57 in.)
35 mm
(1.4 in.)
3719-1 Wet-tap
11/2 in. outlet for 21/2 to 4 in. pipe
3719-2 Wet-tap
2 in. outlet for
6 to 12 in. pipe
CAUTION!
When using clamp-on saddle fi ttings (customer-supplied), the system temperature and pressure is limited by the saddle specifi cations. The process temperature is limited to 40 °C (104 °F) maximum when using saddles.
2716-WT pH electrode
2717-WT ORP electrode
2756-WT(-1) pH electrode, glass
2756-WTP(-1) pH electrode, plastic
2757-WT ORP electrode, glass
2757-WTP ORP electrode, plastic
2 Signet 3719 pH/ORP Wet-Tap
4. 3719 System Overview
a
b
c
d
e
d
a) 3719 pH/ORP Wet-Tap b) Customer-supplied Low-Profi le Clamp-on Saddle Fitting
(ASTM sizes 2½ to 12 in.)
c) DryLoc® pH or ORP Electrode (6 versions available; see
ordering infomation on page 8.) ("DryLoc®" refers to the electrode connector style) d) 2750 or 2760 DryLoc® pH/ORP Preamplifi er/Sensor
electronics e) Output signal options: 2750:
- Digital (S3L)
- 4 to 20 mA 2760:
- Analog mV Output- Digital (S3L)
All components (items a–d) are sold separately.
5. Installation
5.1 Notes on Location, Orientation and Required Clearance
The 3719-1 is designed for use in pipes up to 4 in.
The 3719-2 is designed for use in pipes from 6 to 12 in.
Select a location that will provide suffi cient clearance to remove and insert the electrode.
The 3719 can be mounted in any orientation, including horizontal and inverted. Avoid the 12 o'clock position. In the presence of sediment, avoid the 6 o'clock position.
If inverted, use caution when removing the sensor.
Residual fl uid may be present in the retraction housing.
Keep electrode connector clean and dry at all times.
Any angle OK
Provide 20 inches (minimum) clearance from the top of the pipe for electrode removal..
218 mm (8.57 in.)
250 mm (9.9 in.)
115 mm (4.5 in.)
OR
89.4 mm (3.5 in.)
45 mm (1.75 in.)
3Signet 3719 pH/ORP Wet-Tap
5.2 Installation in Pipe Sizes 2.5 to 12 Inches
3-3719-11 pH/ORP Wet-Tap (Fully Inserted)
For reliable in-line measurements of pH and ORP, it is imperative to position the electrode tip into the process stream.
Because of its compact “short stroke” design, the 3719 requires low-profi le fi ttings to ensure proper positioning in pipe sizes DN65 to DN300 (2.5 to 12 inches).
It is strongly recommended to use low-pro le PP clamp-
on saddle fi ttings (customer-supplied).
Choose the 3719 version (-11 or -21) appropriate to the size of the branch connection of the required fi tting:
Use -11 for sizes DN65 to DN100 (2.5 to 4 in), and -21 for
sizes DN150 to DN300 (6 to 12 in.)
5.3 Installation in Pipe Sizes less than 2.5 Inches
It is possible to install the 3719 into pipe sizes below
2.5 inches by creating a “fl ow cell” with standard piping components.
One simple solution, using a tee fi tting and reducer bushings, is shown in the example below.
3-3719-11 pH/ORP Wet-Tap
1½ in. NPT Threads
2 in. Tee (S x S x S)
Flush Style Reducer Bushing (Spg x FT) 2 in. x 1½ in.
Flush Style Reducer Bushings (Spg x S) 2 in. x ½ in. 2 in. x ¾ in. 2 in. x 1 in. 2 in. x 1¼ in. 2 in. x 1½ in.
5.4 Installation (Wet-Tap Into Fitting)
The 3719 is packaged with no electrode installed, and with the electrode piston in the fully inserted position.
Examine the female threads at the top of the electrode piston. Do not install electrode if threads are damaged.
Examine the two O-rings at the lower end of the assembly. Do not install if O-rings are missing or there are any signs of damage.
Lubricate O-rings with a non-petroleum based, viscous lubricant (grease) compatible with the system.
The pipe can be pressurized after completion of step 4.
DO NOT ATTEMPT TO REMOVE THE RETRACTION HOUSING FROM A PRESSURIZED PIPING SYSTEM!
Many similar confi gurations are conceivable in a wide variety of materials, but be very careful to verify dimensional compatibility.
Select an appropriate installation orientation to avoid the entrapment of air inside the fl ow cell.
Contact your local Georg Fischer Sales and Support offi ce for assistance.
Grasp the retraction housing below the locking shroud; turn the locking shroud 1/4-turn clockwise.
1 2
Pull the locking shroud straight up until both O-rings are fully seated inside the retraction housing.
Locking Shroud
Retraction Housing
Lubricated O-rings
4 Signet 3719 pH/ORP Wet-Tap
1
2
3
4
OR
OR
Lubricate O-Rings
Lubricate O-Rings
3 4
Turn the shroud 1/4-turn counterclockwise and lift it completely away from the electrode piston.
Electrode Piston
The electrode piston is locked in position by SS locking pins.
DO NOT tamper with the locking pins! If the piston is depressed with no electrode installed, the pipe contents are exposed.
Thread the Wet-Tap into the pipe fi tting.
Smaller pipes may require bracing to support the Wet-Tap
weight and the longitudinal forces required for operation.
Use an appropriate thread sealant to prevent leaks.
The piping system can now be safely pressurized.
Inspect the installation for leaks.
5.5 Electrode Installation
Before installation, lubricate O-rings with a non-petroleum based, viscous lubricant (grease) compatible with the system.
1. Remove the safety plug from top of
2. Place the Locking Shroud over electrode;
3. Turn the shroud 1/4-turn counterclockwise to
4. Install the matching electronics assembly or
electrode piston. Slide electrode straight down into electrode piston. Thread electrode into place until connector shoulder is fl ush with top of electrode piston. Hand tighten only.
WARNING:
Do not fl ex the electrode when inserting into the Wet-Tap assembly. The electrode can be permanently damaged if it is fl exed during installation.
turn ¼-turn clockwise to unlock the piston, then press down fi rmly on the locking shroud to lower the electrode piston into the pipe.
lock the piston.
preamplifi er onto the electrode connector.
2750 2760
DO NOT ATTEMPT TO REMOVE THE
RETRACTION HOUSING FROM A PRESSURIZED PIPING SYSTEM!
5Signet 3719 pH/ORP Wet-Tap
5.6 Electrode Removal
The electrode in any pH or ORP system requires periodic service, calibration or replacement. When removing the electrode from the wet-tap assembly, it is very important to exercise caution and follow the instructions carefully.
1. Remove the preamplifi er from the top of
the wet-tap assembly.
2. Turn the locking shroud
to unlock the piston.
3. Pull up on the locking shroud to retract the
electrode piston into the pipe.
DANGER!
The piston should retract easily from a pressurized pipe. If the piston offers resistance, there is a danger that the piston is coated with deposits from the process.
STOP! DO NOT FORCE THE PISTON UP!
It may damage the O-rings or break off the piston tip.
Return the locking shroud to the LOCKED position and follow the steps in the box below.
4. Turn the locking shroud ¼-turn counterclockwise and lift up to remove it from the wet-tap assembly.
5. Remove the electrode by turning it counterclockwise.
For safety, keep your body clear of the top of the wet-tap assembly while removing the electrode.
1
/4-turn clockwise
1
2
3 4
3
5
5
DANGER!
If any fl uid is observed leaking from the electrode threads, STOP! DO NOT REMOVE THE ELECTRODE. There is a danger that the piston tip has been damaged.
Tighten the electrode back down to reseal the assembly and follow the steps in the box below.
If the piston does not retract easily, or if any fl uid is observed leaking from the electrode threads, the pipe must be drained before the 3719 can be safely removed.
Stop the fl ow and depressurize the pipe.
Remove the entire 3719 assembly from the pipe.
Remove the electrode from the assembly
Clean any scaling and debris found on or in the piston tip and surrounding area.
6. Electrode Maintenance and Cleaning
Cleaning
Cleaning techniques vary depending on the type of coating present on the glass electrode surface or reference junction.
Remove soft coatings by vigorous stirring, or with directed spray of a suitable detergent or solvent onto the glass electrode surface.
Use chlorine bleach or mild detergent to remove soft coatings. Rinse electrode tip in clean water after cleaning.
Use the least harsh chemical available to remove hard coatings without attacking the materials of construction. (For example, remove calcium carbonate with a 5% HCL (muriatic acid) solution.
Remove oily or organic coatings with detergents or an appropriate solvent that does not attack the materials of construction.
ORP electrode surface (platinum) can be gently sanded with 600 grit wet and dry silicone or carbide sandpaper, jewelers rouge, crocus cloth, or very fi ne steel wool.
Never scrape or sand the glass electrode surface.
Treat glass electrode surfaces with appropriate care to avoid breakage.
Lubricate O-rings with a non-petroleum based, viscous lubricant (grease) compatible with the system.
Wet-Tap Maintenance
The Wet-Tap assembly should be operated (retracted) on a monthly basis
The O-rings on the piston tip should be inspected and lubricated annually, and whenever the system is off line for maintenance.
Lubricate O-rings with a non-petroleum based, viscous, lubricant (grease) compatible with the system.
6 Signet 3719 pH/ORP Wet-Tap
7. Troubleshooting
Offset in pH Electrodes
Electrode offsets occur due to:
Clogged reference junction
Aged or contaminated reference solution/wire
A constant output near 0 mV in all buffer solutions indicates a shorted electrode that must
be replaced.
Check offsets in a pH 7 buffer @ 25 °C. The theoretical output is 0 mV. Any deviation from 0 mV is the pH electrode offset. The mV offset will track across the entire pH range. The slope is usually not affected by offset changes. (i.e., pH 7= +10 mV, pH 4= +187 mV); slope = 59 mV.
pH Electrode Offset pH 7 buffer @ 25 °C Theoretical: pH 7.0 (0.0 mV) New electrode: pH 7 ± 0.25 pH (±15 mV) Reliable: pH 7 ± 0.85 pH (± 50 mV)
Electrode offsets greater than 0.85 pH (50 mV) indicate the electrode requires cleaning or replacement. See Maintenance and Cleaning section.
Offset in ORP Electrodes
ORP electrode offsets are usually caused by clogged reference junctions or by an aged or contaminated reference solution/wire.
Offsets should be checked in pH 7 buffer saturated with quinhydrone @ 25 °C. The theoretical output is +86 mV. Any deviation from +86 mV is the ORP electrode offset (e.g., +90 mV).
Quinhydrone is the oxidizer measured by the ORP electrode and is required for calibration. To measure ORP electrode offset, saturate 50 mL of pH 4 and pH 7 buffers with g quinhydrone.
A new ORP electrode measures these values ±15 mV. The electrode continues to be functional until the offset from these values exceeds 50 mV. Electrodes with offset greater than 50 mV should be cleaned and replaced if necessary.
Theoretical mV Values @ 25 °C
pH mV
2 +296 mV
3 +237 mV
4 +177 mV
5 +118 mV
6 +59 mV
7 0 mV
8 -59 mV
9 -118 mV
10 -177 mV
11 -237 mV
12 -296 mV
4 pH w/Quinhydrone 7 pH w/Quinhydrone Temp: 20 °C 25 °C 30 °C 20 °C 25 °C 30 °C ORP: 268 mV 263 mV 258 mV 92 mV 86 mV 79 mV
Slope in pH electrodes
Electrode slope is the mV output per pH unit. At 25C the theoretical slope is 59.16 mV per pH. The graph below illustrates potential pH error when a temperature-compensated instrument is not used.
Coatings on the glass may affect sensor slopes. See Maintenance and Cleaning section.
Temperature affects electrode slope. Calibrate temperature before calibrating the standard and slope.
°C
23456789101112
pH
15 0.15 0.12 0.09 0.06 0.03 0 0.03 0.06 0.09 0.12 0.15
2500000000000
35 0.15 0.12 0.09 0.06 0.03 0 0.03 0.06 0.09 0.12 0.15
45 0.3 0.24 0.18 0.12 0.06 0 0.06 0.12 0.18 0.24 0.3
55 0.45 0.36 0.27 0.18 0.09 0 0.09 0.18 0.27 0.36 0.45
Slope in ORP electrodes
ORP slope errors are caused by contamination of the platinum electrode surface. Cleaning the electrode surface will usually restore proper values, response time, and stability. Many systems require both pH and ORP calibration. To conserve calibration reference solutions, use pH 7 and 4 buffers for pH calibration fi rst. ORP calibration can be performed with the same buffers after adding quinhydrone.
Response Time/Stability
Response time and stability are affected by the condition of the glass surface (ORP electrode - Platinum surface), reference junction, and reference solution. Restoration to acceptable levels can often be accomplished by cleaning the electrode's glass surface (ORP electrode - platinum surface) and reference junction.
pH and ORP electrodes are similar to batteries; they age with time and usage. The following information will help maximize electrode life:
High temperatures or concentrated acids/caustics will accelerate electrode aging.
Never store the electrode tip in deionized (DI) water.
Never expose electrode to temperatures below –12 °C (10 °F) or allow it to dehydrate. These conditions will damage the electrode.
7Signet 3719 pH/ORP Wet-Tap
8. Ordering Information
Mfr. Part No. Code Description
3-3719-11 159 000 804 pH/ORP Wet-Tap, 11/2 in. NPT 3-3719-21 159 000 805 pH/ORP Wet-Tap, 2 in. NPT 3-3719-12 159 000 806 pH/ORP Wet-Tap, ISO 7/1-R 1.5 3-3719-22 159 000 807 Wet-Tap Assembly, ISO 7/1-R 2
Parts and accessories
3-2716-WT 159 000 809 Electrode, pH, twist-lock, bulb, 3 KΩ, wet-tap 3-2717-WT 159 000 811 Electrode, ORP, twist-lock, bulb, 10 KΩ ID, wet-tap
®
3-2756-WT 159 000 834 Electrode, pH, DryLoc 3-2756-WT-1 159 001 383 Electrode, pH, DryLoc®, bulb, 3 KΩ, wet-tap 3-2756-WTP 159 001 390 Electrode, pH, DryLoc®, plastic bulb, PT1000, wet-tap 3-2756-WTP-1 159 001 384 Electrode, pH, DryLoc®, plastic bulb, 3 KΩ, wet-tap 3-2757-WT 159 000 835 Electrode, ORP, DryLoc®, bulb, 10 KΩ ID, wet-tap 3-2757-WTP 159 001 391 Electrode, ORP, DryLoc
3-2750-1 159 000 744 In-line DryLoc® pH/ORP Sensor with J-Box 3-2750-2 159 000 745 In-line DryLoc® pH/ORP Sensor with J-Box and EasyCal
3-2760-11 159 001 367 In-line Preamplifi er with ¾ in. NPT threads and 4.6 m (15 ft) cable 3-2760-21 159 001 368 In-line Preamplifi er with ¾ in. ISO threads and 4.6 m (15 ft) cable 3-2760-31 159 001 369 In-line Connector with 4.6 m (15 ft) cable and ¾ in. NPT threads 3-2760-41 159 001 370 In-line Connector with 4.6 m (15 ft) cable and ISO 7/1R ¾ threads
, bulb, PT1000, wet-tap
®
, plastic bulb, 10 KΩ ID, wet-tap
3-3719.390 159 000 855 3719 Locking Shroud 1220-0114 159 000 854 3719 O-ring, FPM, Piston Tip 3-2700.395 159 001 605 pH Calibration Kit: includes 3 Polypropylene cups, box used as stand, 1 pint pH 4.01, 1 pint pH 7.00 3-0700.390 198 864 403 pH buffer kit (1 each 4,7,10 pH buffer in powder form, makes 50 ml of each) 3822-7115 157 001 606 20 gm bottle Quinhydrone for ORP calibration (must use ph 4.01 and/or pH 7.00 buffer solutions)
3-3719.390 Locking shroud
3-2756-WT Dry-Loc pH electrode 3-2756-WT-1 Dry-Loc pH electrode 3-2756-WTP Dry-Loc pH electrode 3-2756-WTP-1 Dry-Loc pH electrode 3-2757-WT Dry-Loc pH electrode 3-2757-WTP Dry-Loc ORP electrode
1220-0114
O-rings
3-2716-WT pH electrode 3-2717-WT ORP electrode
Georg Fischer Signet LLC, 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057 For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090 For the most up-to-date information, please refer to our website at www.gfsignet.com
3-3719.090 Rev L 12/11 English © Georg Fischer Signet LLC 2011
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