High-pressure liquids and gases are potentially hazardous. Energy stored in these liquids and gases
can be released unexpectedly and with extreme force. High-pressure systems should be assembled and
operated only by personnel who have been instructed in proper safety practices.
Information in this document is subject to change without notice. No part of this document may be reproduced or transmitted in any
form or by any means, electronic or mechanical, for any purpose, without the express written permission of DH Instruments, a
Fluke Company. 4765 East Beautiful Lane Phoenix Arizona 85044-5318 USA.
DH Instruments makes sincere efforts to ensure the accuracy and quality of its published materials; however, no warranty,
expressed or implied, is provided. DH Instruments disclaims any responsibility or liability for any direct or indirect damages
resulting from the use of the information in this manual or products described in it. Mention of any product or brand does not
constitute an endorsement by DH Instruments of that product or brand. This manual was originally composed in English and was
subsequently translated into other languages. The fidelity of the translation cannot be guaranteed. In case of conflict between the
English version and other language versions, the English version predominates.
DH Instruments, DH, DHI, PG7601-AF, PG7601, PPPC3, CalTool and COMPASS are trademarks, registered and otherwise, of
DH Instruments, a Fluke Company.
Swagelok is a registered trademark of the Swagelok Company.
Krytox is a registered trademark of the Dupont de Nemours Company.
Products described in this manual are manufactured under international patents and one or more of the following U.S.
patents: 6,701,791, 5,142,483, 5,257,640, 5,331,838, 5,445,035. Other U.S. and international patents pending.
1.1.4 MASS SET (MS-7001-35-AF)........................................................................................................................6
4.2.1.1 KEYPAD LAYOUT AND PROTOCOL......................................................................................................45
4.2.1.2 MAIN RUN SCREEN................................................................................................................................46
4.2.1.3 GENERAL FUNCTION/MENU FLOW CHART........................................................................................48
4.2.2.1 KEYPAD LAYOUT AND PROTOCOL......................................................................................................49
4.2.2.2 DIRECT PRESSURE CONTROL KEYS..................................................................................................50
4.2.2.3 MAIN RUN SCREEN................................................................................................................................51
4.5.1.5 SELECT THE ACTIVE PISTON-CYLINDER MODULE...........................................................................87
4.5.1.6 ADD MASS SET.......................................................................................................................................87
4.5.1.7 EDIT MASS SET......................................................................................................................................91
4.5.1.8 VIEW MASS SET.....................................................................................................................................91
4.5.1.9 DELETE MASS SET................................................................................................................................91
4.5.1.10 SELECT MASS SET................................................................................................................................92
4.5.1.11 ADD MASS LOADING BELL....................................................................................................................92
4.5.1.12 EDIT MASS LOADING BELL...................................................................................................................93
4.5.1.13 VIEW MASS LOADING BELL..................................................................................................................94
4.5.1.14 DELETE MASS LOADING BELL.............................................................................................................94
4.5.1.15 SELECT MASS LOADING BELL.............................................................................................................94
4.5.2 <2PRESU>, CUSTOMIZE UNIT FUNCTION SELECTIONS.......................................................................94
4.5.3 <3HEAD>, CUSTOMIZE FLUID HEAD FUNCTIONS .................................................................................96
5.2.1.2 COM2 AND COM3.................................................................................................................................116
6.6.1 CHECK/TOP OFF OIL LEVEL...................................................................................................................191
6.6.2 DRAIN AND REFILL OIL...........................................................................................................................191
6.7 RELOADING EMBEDDED SOFTWARE INTO PLATFORM OR PRESSURE CONTROLLER FLASH
6.8.2.2 MASS SET.............................................................................................................................................193
This manual provides the user with the information necessary to operate and maintain a PG7601-SYS-AF
gas operated piston gauge system.
Before using the manual, take a moment to familiarize yourself with the Table of Contents structure.
All first time PG7601-AF users should read Section 2 and 4. Section 5 covers remote communication
with an external computer. Sections 6 and 7 provide maintenance and calibration information. Section 1
is a quick troubleshooting guide. Use the information in Section 1 to troubleshoot unexpected PG7601AF behavior based on the symptoms of that behavior.
Certain words and expressions have specific meaning as they pertain to PG7601-AFs. The
(see Section 9.3)
they are used in this manual.
The PG7601-SYS-AF system includes a PPC3-7M-AF pressure controller. This manual covers the
pressure controller to the extent necessary for normal operation of the PG7601-AF system. The PPC3-7M-AF
has a complete, independent manual that is included on the PG7601-SYS-AF Support Disc.
FOR THOSE OF YOU WHO “DON’T READ MANUALS”, GO DIRECTLY TO SECTION 3.3 TO SET UP
YOUR PG7601-AF. THEN GO TO SECTION 3.5. THIS WILL GET YOU RUNNING QUICKLY WITH MINIMAL RISK OF
CAUSING DAMAGE TO YOURSELF OR YOUR PG7601-AF. THEN… WHEN YOU HAVE QUESTIONS OR START TO
WONDER ABOUT ALL THE GREAT FEATURES YOU MIGHT BE MISSING, GET INTO THE MANUAL!
T
HHIISS
T
is useful as a quick reference for the definition of specific words and expressions as
M
AANNUUAAL
M
L
Glossary
Manual Conventions
(CAUTION) is used throughout the manual to identify user warnings and cautions.
(NOTE) is used throughout the manual to identify operating and applications advice and
additional explanations.
[ ] indicates direct function keys (e.g., [UNIT]).
PG7601-SYS-AF is a very high performance pressure calibration system for the validation and calibration
of pressure measuring devices using gas as the pressurized medium. It operates on the piston gauge
principle. Pressure is defined by balancing it against the force exerted by a known mass accelerated by
gravity on the effective area of a piston-cylinder.
PG7601-SYS-AF covers the pressure range of 7 to 7000 kPa (1 to 1 000 psi) in absolute and gauge
modes with semi-automated operation and state of the art measurement uncertainty.
A PG7601-SYS-AF is made up of:
PG7601-BAS-AF, p/n 402351, the “base” system, including the piston gauge platform, pressure
controller, vacuum pump and interconnecting hardware (everything except the piston-cylinder modules
and masses).
PG7601-EXC-AF, p/n 402350, the “exchange package”, including the piston gauge’s three different size
piston-cylinder modules and the mass set.
I
NNTTRROODDUUCCTTIIOON
I
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1.1 SPECIFICATIONS
1.1.1 OVERALL SYSTEM SPECIFICATIONS
Power requirements
Instruments
Reference vacuum pump (D16B)
Operating temperature range
Storage temperature range
Operating humidity range
Storage humidity range
Dimensions
Bench space needed for installation
Weight (shipping)
PG7601-AF platform in case
PG7601-AF vacuum bell jar
PPC3-7M-AF pressure controller
D16B vacuum pump
Base system accessories
35 kg mass set, main masses case
35 kg mass set, fractional masses case
(3) piston-cylinder modules in case
Exchange pack accessories
System external communication ports
Overall pressure ranges
Actual range depends on piston-cylinder
installed
Operating media
85 to 264 VAC, 50/60 Hz, 52 VA max. consumption
100 to 120 VAC, 50/60 Hz, 1430 VA max. consumption, full load 9.4
to 13 A
15 to 35 °C
5 to 90 °C (vacuum pump), -40 to 100 °C (other components)
5 to 95% R.H., non-condensing
5 to 95% R.H., non-condensing
65 cm x 56 cm (65 in. x 22 in.)
36 kg (79 lb)
5 kg (11 lb)
18 kg (40 lb)
40 kg (88 lb)
12 kg (26 lb)
35 kg (77 lb)
20 kg (44 lb)
10 kg (22 lb)
6 kg (13 lb)
RS 232 (COM1), IEEE-488
7 kPa to 7 MPa (1 to 1000 psi), gauge and absolute
The pressure measurement specifications of the PG7601-AF depend upon the
piston-cylinder module used.
PC-7100/7600-10-L (10 kPa/kg)
PC-7100/7600-50 (50 kPa/kg)
PC-7100/7600-200 (200 kPa/kg)
1. Sensitivity: The smallest variation in input detectable in output.
2. Reproducibility: Combined long term stability of piston-cylinder effective area and masses predicted for 30
months.
3. Measurement uncertainty:
gauge and absolute measurement modes, at the PG7601-AF reference level including precision, predicted 30 month stability,
temperature effect and calibration uncertainty, combined and expanded (k=2) following the ISO “Guide to the Expression of
Uncertainty in Measurement. Assumes the PG7601-AF platform sensors are properly adjusted, use of MS-7001-35-AF mass
set with measurement uncertainty of ± 5 ppm, uncertainty of not more than ± 2 ppm in the value of local acceleration due to
gravity entered into the PG7601-AF Terminal.
Swagelok
stems of 1/4 in. NPT F, 1/8 in. NPT F, AN4 M, 1/4 in. Swage
1/8 in. NPT F
1/8 in. NPT F
Sensitivity
Reproducibility
Measurement uncertainty
Sensitivity
Reproducibility
Measurement uncertainty
Sensitivity
Reproducibility
Measurement uncertainty
Maximum deviation of the PG7601-AF indicatied pressure from the true value of pressure, in
®
SS-QC4-B1-400 quick connector with quick connector
1
0.02 Pa + 0.5 ppm
2
± 4 ppm
3
± (0.2 Pa + 15 ppm)
1
0.1 Pa + 0.5 ppm
2
± 4 ppm
3
± (0.5 Pa + 20 ppm)
1
0.4 Pa + 0.5 ppm
2
± 6 ppm
3
± (2 Pa + 25 ppm)
1.1.2PISTON GAUGE PLATFORM (PG7601-AF)
Power requirements
Operating temperature range
Weight
Instrument platform
PG Terminal
Dimensions
Instrument platform
PG Terminal
Microprocessors
Instrument platform
PG Terminal
Communication ports
RS232
IEEE-488
85 to 264 VAC, 50/60 Hz, 22 VA max. consumption.
15 to 25 °C
17 kg (37 lb)
1.4 kg (3 lb)
36 cm H (top of bell jar) x 40 cm W x 35 cm D (14.5 in. x 15.8 in. x
13.8 in.)
12 cm H x 15 cm W x 20 cm D (4.7 in. H x 5.9 in. W x 7.9 in. D)
Motorola 68302
Hitachi 64180
COM1: Host computer communications
COM2: Not used (may be used for optional external barometer or
vacuum gauge)
COM3: PPC3 pressure controller communications
Operating media
Mass load range
Pressure connections
TEST port
Bell jar vent (VACUUM) port
Refe r e n c e v a c u u m pump down port
CE Conformance
7 kPa to 7 MPa (1 to 1000 psi), gauge and absolute (actual range
depends on piston-cylinder selected)
air, helium, nitrogen
0.7 to 36.2 kg
DH200 (for 1/4 in. OD tube, equivalent to AE SF250C, HIP LF4)
DH200
KF25
Available, must be specified.
1.1.2.1 EMBEDDED FEATURES
• Local control with 2 x 20 vacuum fluorescent display and 4 x 4 function
driven keypad.
• Real time (1 second update rate) display and measurement of ambient
(pressure, temperature, humidity) and instrument (piston-cylinder
temperature, piston position, piston drop rate, piston rotation rate, piston
rotation decay rate, reference vacuum) conditions.
• Real time (1 second update rate) mass-to-pressure and pressure-to-mass
calculations taking into consideration all environmental and operational
variables.
• Full gas and liquid fluid head corrections including DUT head correction and
piston position head correction.
• Adjustable mass loading resolution (0.01 g to 0.1 kg).
• Audible prompts of instrument status (piston movement, Ready/Not Ready indication)
with override capability.
• Integrated automated mass handling (optional).
• Interfacing and automatic exploitation of optional external barometer via
RS232 (optional).
• Interfacing and automatic exploitation of external vacuum gauge via RS232
(optional).
•Storage and one step activation of metrological data digital IDs on up to 18 piston-
cylinder modules, (3) mass sets and (3) mass loading bells.
• Continuous pressure Ready/Not Ready indication based on measured
conditions.
• Motorized, intelligent piston drive system based measured rotation rate with
operator alert and manual override.
• Integrated automated pressure control with PPC3-7M-AF pressure controller.
• Full RS232 and IEEE-488 communications with multi-level commands to set
1 x 4.5 kg disc(makeup mass)
5 x 5 kg disc
2 x 2 kg disc
1 x 1 kg disc
1 x 0.5 kg puck
2 x 0.2 kg puck
1 x 0.1 kg puck
1 x 0.3 kg mass loading bell
Trim mass set of 50 g to 0.01 g (total 100 g)
85 to 264 VAC, 50/60 Hz, 30 VA max consumption
15 to 35 °C
12.7 kg (28.2 lb) approx
Motorola 68302, 16 MHz
RS232 (COM1), RS232 (COM2), IEEE-488.2
1 A, 250 VAC fuse, 5 x 20 mm, time lag type fuse
Internal power supply fuse not replaceable by operator: 2A, 250 V (UV 440-2
power supply), 3.15A, 250 V (NFS40-7612 power supply)
7 kPa to 7 MPa (1 to 1000 psi), gauge and absolute
Any clean, dry, non-corrosive gas
SUPPLY: 1/8 in. NPT F
TEST(+): 1/8 in. NPT F
TEST(-): 1/8 in. NPT F
ATM (Vent):10-32 UNF
EXHAUST:1/4 in. NPT F
7.7 MPa (1100 psi)
Ultimate pressure lower than 2 kPa (0.3 psia); capacity 85 slm (3 cfm) min
7.03 MPa (1020 psi)
9.6 MPa (1 400 psi)
The pressure measurements made by the PPC3-7M-AF utility sensor are used only for
pressure control and indication. They have no metrological function therefore they do not require
traceable calibration. Adjustment of the PPC3 utility sensor is performed only for operational
reasons (see Section 6.5).
1.1.6REFERENCE VACUUM PUMP (D16B)
Power requirements
Operating temperature range
Weight
Oil capacity
Nominal pumping speed
Pumping speed
Ultimate total pressure
Pressure connections (intake
and exhauts)
100 to 120 VAC, 50/60 Hz, 1430 W max consumption, full load 9.4 to 13 A
12 to 40 °C
26 kg (57 lb) approx
PG7601-SYS-AF is a very high performance pressure calibration system for the validation and calibration of
pressure measuring devices using gas as the pressurized medium in the range of 7 to 7000 kPa (1 to 1 000 psi).
A PG7601-SYS-AF is made up of:
PG7601-BAS-AF, the “base system”. The base system is the operational piston gauge
system, not including the piston-cylinder modules and mass set. The base system includes:
- PG7601-AF piston gauge platform with PG Terminal and vacuum bell jar
- PPC3-7M-AF pressure controller
- D16B reference vacuum pump
- Pressure and vacuum interconnecting hardware packages
PG7601-EXC-AF, the “exchange package”. The exchange package is the system’s
metrological elements: the piston-cylinder modules and mass set. The exchange package
includes:
D
EESSCCRRIIPPTTIIOON
D
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- (3) piston-cylinder modules, PC-7100/7600-10-L, -50 and -200.
- MS-7001-35-AF 35 kg mass set
The following figures in this section describe the PG7601-SYS-AF system:
Figure 1. System, PG7601-SYS-AF, standard installation
Figure 2. System, PG7601-SYS-AF, system pneumatic schematic
Figure 3. System, PG7601-SYS-AF, electrical and communications schematic
The heart of the PG7601-SYS-AF is the PG7601-AF gas operated piston gauge and its piston-cylinder
modules and mass set.
The PG7601-AF operates on the principle of the piston gauge in which pressure is defined by balancing it
against a known force on a known area (see Figure 4). The known area is defined by a vertically
mounted piston rotating in a cylinder and the known force is applied
mass subjected to acceleration due to gravity. When the force applied by the pressure and the force
appl ied by t he ma ss accelerated by gravity are in equilibrium, the piston floats and the pressure under the
piston remains constant. The pressure can be calculated following the equation in Figure 4. The
pressurized gas under the piston also lubricates the gap between the piston and the cylinder.
floating, the piston must be rotating to keep it well centered in the cylinder and perfectly mobile.
The system includes three piston cylinder modules and a 35 kg mass set. The combination provides
three ranges of 7 to 350 kPa (1 to 50 psi), 25 to 1750 kPa (3.6 to 260 psi) and 100 to 7 000 kPa (14.5 to
1000 psi). The PG7601-AF platform includes a bell jar that can be evacuated using the supplied
reference vacuum pump so that pressure can be defined against vacuum (absolute mode) or atmosphere
(gauge mode). The PPC3-7M-AF pressure controller adjusts pressure automatically or manually to float
the piston (see Section 4.1.2).
The PG7601-AF platform is the instrument base into which the piston-cylinder modules are
mounted and onto which the masses are loaded. The platform also includes the electronic
measurement system.
The PG7601-AF platform rear panel provides the connection to the PG Terminal, remote
communication connections and pressure connection ports.
1. COM2 (RS232) for external barometer (optional), external
vacuum gauge (optional), pass through communications
2. COM3 (RS232) – for PPC3-7M-AF pressure controller,
AMH-38 automated mass handler (optional)
The piston-cylinder module is mounted in the PG7601-AF platform. The piston-cylinder precisely
converts pressure to a proportional force (see Section 4.1.1). There are three piston-cylinder modules for
three different pressure ranges.
Combinations of masses from the 35 kg mass set are loaded onto in the piston-cylinder, as needed, to result
in the set pressure desired.
The mass set is made up of (1) mass loading bell of 0.3 kg, (1) 4.5 kg makeup mass disc, (5) 5 kg mass
discs, (2) 2 kg discs, (1) 1 kg disc, (1) 0.5 kg puck, (2) 0.2 kg puck, (1) 0.1 kg puck, 50 g to 0.01 g trim mass
set in 1-2-2-1 progression.
Figure 9. Mass set, MS-7100-35-AF
2.5 PRESSURE CONTROLLER (PPC3-7M-AF)
The PPC3-7M-AF pressure controller is used to set and adjust pressure in the PG7601-SYS-AF system.
Its operation can be fully automated to float the PG7601-AF’s piston under control of the PG7601-AF
platform’s AutoGen function (see Section 4.1.2). It can also be used manually under direct operator
control using its front panel direct pressure control keys.
The PPC3-7M-AF pressure controller is a component of the PG7601-SYS-AF system. It can also act as
a stand alone component. For information on use of PPC3-7M-AF outside of the PG7601-SYS-AF system, see
the PPC3 Operation and Maintenance Manual.
The pressure measurements made by the PPC3-7M-AF utility sensor are used only for pressure control
and indication. They have no metrological function therefore they do not require traceable calibration.
Adjustment of the PPC3 utility sensor is performed only for operational reasons (see Section 6.5).