Fluke 7103 Operating Manual

7103
Micro-Bath
User’s Guide
PN 3729337 December 2013
© 2013 Fluke Corporation. All rights reserved. Specifications are subject to change without notice. All product names are trademarks of their respective companies.
LIMITED WARRANTY AND LIMITATION OF LIABILITY
Fluke authorized resellers shall extend this warranty on new and unused products to end-user customers only but have no authority to extend a greater or different warranty on behalf of Fluke. Warranty support is available only if product is purchased through a Fluke authorized sales outlet or Buyer has paid the applicable international price. Fluke reserves the right to invoice Buyer for importation costs of repair/replacement parts when product purchased in one country is submitted for repair in another country.
Fluke's warranty obligation is limited, at Fluke's option, to refund of the purchase price, free of charge repair, or replacement of a defective product which is returned to a Fluke authorized service center within the warranty period.
To obtain warranty service, contact your nearest Fluke authorized service center to obtain return authorization information, then send the product to that service center, with a description of the difficulty, postage and insurance prepaid (FOB Destination). Fluke assumes no risk for damage in transit. Following warranty repair, the product will be returned to Buyer, transportation prepaid (FOB Destination). If Fluke determines that failure was caused by neglect, misuse, contamination, alteration, accident, or abnormal condition of operation or handling, including overvoltage failures caused by use outside the product’s specified rating, or normal wear and tear of mechanical components, Fluke will provide an estimate of repair costs and obtain authorization before commencing the work. Following repair, the product will be returned to the Buyer transportation prepaid and the Buyer will be billed for the repair and return transportation charges (FOB Shipping Point).
THIS WARRANTY IS BUYER'S SOLE AND EXCLUSIVE REMEDY AND IS IN LIEU OF ALL OTHER WARRANTIES, EXPRESS OR IMPLIED, INCLUDING BUT NOT LIMITED TO ANY IMPLIED WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE. FLUKE SHALL NOT BE LIABLE FOR ANY SPECIAL, INDIRECT, INCIDENTAL, OR CONSEQUENTIAL DAMAGES OR LOSSES, INCLUDING LOSS OF DATA, ARISING FROM ANY CAUSE OR THEORY.
Since some countries or states do not allow limitation of the term of an implied warranty, or exclusion or limitation of incidental or consequential damages, the limitations and exclusions of this warranty may not apply to every buyer. If any provision of this Warranty is held invalid or unenforceable by a court or other decision-maker of competent jurisdiction, such holding will not affect the validity or enforceability of any other provision.
Fluke Corporation P.O. Box 9090 Everett, WA 98206-9090 U.S.A.
Fluke Europe B.V. P.O. Box 1186 5602 BD Eindhoven The Netherlands
11/99
To register your product online, visit register.fluke.com
Table of Contents
1 Before You Start .......................................................................1
1.1 Symbols Used ........................................................................................... 1
1.2 Safety Information .................................................................................... 2
1.2.1 Warnings ...................................................................................................2
1.2.2
1.3 Authorized Service Centers ..................................................................... 5
Cautions ....................................................................................................4
2 Introduction .............................................................................7
3 Specications and Environmental Conditions ......................9
3.1 Specifications ........................................................................................... 9
3.2 Environmental Conditions ........................................................................ 9
4 Quick Start ..............................................................................11
4.1 Unpacking .............................................................................................. 11
4.2 Setup ...................................................................................................... 11
4.3 Power ..................................................................................................... 12
4.4 Setting the Temperature ......................................................................... 12
5 Installation .............................................................................13
5.1 Bath Environment .................................................................................... 13
5.2 “Dry-out” Period ...................................................................................... 13
5.3 Bath Preparation and Filling ................................................................... 13
5.4 Power ..................................................................................................... 14
6 Bath Use .................................................................................15
6.1 General .................................................................................................. 15
6.2 Comparison Calibration ......................................................................... 15
6.3 Calibration of Multiple Probes ................................................................. 16
7 Parts and Controls ................................................................17
7.1 Back Panel ............................................................................................. 17
7.2 Front Panel ............................................................................................. 18
7.3 Accessories ........................................................................................... 19
7.3.1 Transport/Pour Access Lid ...........................................................................19
iii
7.3.2 Access Cover ...............................................................................................19
7.3.3 Probe Basket ................................................................................................20
7.3.4 Stir Bar ..........................................................................................................20
8 General Operation ..................................................................21
8.1 Changing Display Units .......................................................................... 21
8.2 Switching to 230V Operation .................................................................. 21
8.3 Bath Fluid ............................................................................................... 21
8.3.1 Temperature Range .......................................................................................21
8.3.2 Viscosity ........................................................................................................ 22
8.3.3 Specific Heat ................................................................................................. 22
8.3.4 Thermal Conductivity ....................................................................................22
8.3.5 Thermal Expansion........................................................................................22
8.3.6 Electrical Resistivity .......................................................................................22
8.3.7 Fluid Lifetime ................................................................................................. 23
8.3.8 Safety ............................................................................................................23
8.3.9 Cost ...............................................................................................................23
8.3.10 Commonly Used Fluids .................................................................................23
8.3.10.1 Water (Distilled) ................................................................................................... 24
8.3.10.2 Mineral Oil ............................................................................................................ 24
8.3.10.3 Silicone Oil (Dow Corning 200.05, 200.10, 200.20) ............................................. 24
8.3.11 Fluid Characteristics Charts ..........................................................................24
8.3.11.1 Limitations and Disclaimer .................................................................................. 25
8.3.11.2 About the Graph .................................................................................................. 26
8.4 Stirring .................................................................................................... 27
8.5 Power ..................................................................................................... 28
8.6 Thermal Electric Devices (TED) ............................................................. 28
8.7 Fluid Drain .............................................................................................. 28
8.8 Temperature Controller .......................................................................... 28
9 Controller Operation .............................................................31
9.1 Well Temperature ................................................................................... 31
9.2 Temperature Set-point ........................................................................... 31
9.2.1 Programmable Set-points ............................................................................31
9.2.2 Set-point Value .............................................................................................33
9.2.3 Temperature Scale Units ..............................................................................33
9.3 Scan ....................................................................................................... 34
9.3.1 Scan Control ................................................................................................. 34
9.3.2 Scan Rate .....................................................................................................34
9.4 Temperature Display Hold ..................................................................... 35
iv
9.4.1 Hold Temperature Display ............................................................................35
9.4.2 Mode Setting ................................................................................................35
9.4.3 Switch Wiring ................................................................................................ 36
9.4.4 Switch Test Example ....................................................................................36
9.5 Secondary Menu .................................................................................... 36
9.6 Thermal Electric Device (TED) ............................................................... 36
9.7 Proportional Band .................................................................................. 37
9.8 Controller Configuration .......................................................................... 38
9.8.1 Operating Parameters ...................................................................................38
9.8.1.1 High Limit ............................................................................................................39
9.8.1.2 Stir Speed ............................................................................................................39
9.8.2 Serial Interface Parameters .......................................................................... 39
9.8.2.1 Baud Rate ............................................................................................................. 40
9.8.2.2 Sample Period ...................................................................................................... 40
9.8.2.3 Duplex Mode ........................................................................................................ 40
9.8.2.4 Linefeed ............................................................................................................... 41
9.8.3 Calibration Parameters ..................................................................................41
9.8.3.1 Hard Cutout ......................................................................................................... 42
9.8.3.2 R0 ........................................................................................................................ 42
9.8.3.3 ALPHA .................................................................................................................42
9.8.3.4 DELTA .................................................................................................................. 42
9.8.3.5 BETA .................................................................................................................... 42
10 Digital Communication Interface ..........................................43
10.1 Serial Communications .......................................................................... 43
10.1.1 Wiring ...........................................................................................................43
10.1.2 Setup ............................................................................................................43
10.1.2.1 Baud Rate ........................................................................................................... 44
10.1.2.2 Sample Period ...................................................................................................... 44
10.1.2.3 Duplex Mode ........................................................................................................ 44
10.1.2.4 Linefeed ................................................................................................................ 44
10.1.3 Serial Operation ............................................................................................ 44
10.2 Interface Commands .............................................................................. 45
11 Test Probe Calibration ...........................................................47
11.1 Calibrating a Single Probe ..................................................................... 47
11.2 Stabilization and Accuracy .................................................................... 47
12 Calibration Procedure ...........................................................49
12.1 Calibration Points ................................................................................... 49
v
12.2 Calibration Procedure ............................................................................ 49
12.2.1 Compute DELTA ...........................................................................................49
12.2.2 Compute R0 & ALPHA ..................................................................................50
12.2.3 Compute BETA ..............................................................................................50
12.2.4 Accuracy & Repeatability ............................................................................. 51
13 Maintenance ..........................................................................53
14 Troubleshooting .....................................................................55
14.1 Troubleshooting Problems, Possible Causes, and Solutions ................. 55
14.2 Comments ............................................................................................... 56
14.2.1 EMC Directive ............................................................................................... 56
14.2.2 Low Voltage Directive (Safety) ......................................................................56
vi
Tables
Table 1 International Electrical Symbols ........................................................... 1
Table 2 Specifications ....................................................................................... 9
Table 3 Table of Various Bath Fluids ............................................................... 25
Table 4 Nominal Stirrer Motor Settings With Different Liquids ........................ 27
Table 5 Controller Communications Commands ............................................. 46
vii
Figures
Figure 1 7103 Back Panel and Bottom ............................................................ 17
Figure 2 7103 Front Panel ................................................................................ 18
Figure 3 Bath Lids and Lid Parts ..................................................................... 19
Figure 4 Probe Basket ..................................................................................... 20
Figure 5 Stir Bar .............................................................................................. 20
Figure 6 Chart of Various Bath Fluids ............................................................. 26
Figure 7 Controller Operation Flowchart ......................................................... 32
Figure 8 Serial Cable Wiring ........................................................................... 43
viii
Before You Start
Symbols Used
Before You Start1
Symbols Used1.1
Table 1 lists the International Electrical Symbols. Some or all of these symbols may be used on the instrument or in this manual.
Table 1 International Electrical Symbols
Symbol Description
AC (Alternating Current)
AC-DC
Battery
CE Complies with European Union directives
DC
Double Insulated
Electric Shock
Fuse
PE Ground
Hot Surface (Burn Hazard)
Read the User’s Guide (Important Information)
Off
On
Canadian Standards Association
1
7103 Micro-Bath User’s Guide
Safety Information
Symbol Description
OVERVOLTAGE (Installation) CATEGORY II, Pollution Degree 2 per IEC1010-1 re fers to the level of Impulse Withstand Voltage protection provided. Equipment of OVERVOLTAGE CATEGORY II is energy-consuming equipment to be supplied from the xed installation. Examples include household, office, and laboratory appliances.
C-TICK Australian EMC mark
The European Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/ EC) mark.
Safety Information 1.2
Use this instrument only as specied in this manual. Otherwise, the protection provided by the instrument may be impaired.
The following denitions apply to the terms “Warning” and “Caution”.
L
“Warning” identies conditions and actions that may pose hazards to the user.
L
“Caution” identies conditions and actions that may damage the instru ment being used.
1.2.1 Warnings
Disclaimer: Hart Scientific manufactures instruments for the purpose of temperature calibration. Instruments used for applications other than
calibration are used at the discretion and sole responsibility of the customer. Hart Scientific cannot accept any responsibility for the use of instruments for any application other than temperature calibration.
GENERAL DO NOT use the instrument for any application other than calibration work.
The instrument was designed for temperature calibration. Any other use of the unit may cause unknown hazards to the user.
DO NOT use the unit in environments other than those listed in the user’s guide. Completely unattended operation in not recommended. DO NOT install access cover without holes onto a bath that is energized. Dangerous
pressures may result from uids vaporizing. Follow all safety guidelines listed in the user’s manual.
2
Before You Start
Safety Information
Calibration Equipment should only be used by Trained Personnel. If this equipment is used in a manner not specied by the manufacturer, the protection
provided by the equipment may be impaired or safety hazards may arise. Inspect the instrument for damage before each use. DO NOT use the instru ment if it
appears damaged or operates abnormally. Before initial use, or after transport, or after storage in humid or semi-humid
environments, or anytime the instrument has not been energized for more than 10 days, the instrument needs to be energized for a “dry-out” period of 2 hours before it can be assumed to meet all of the safety requirements of the IEC 61010-1. If the product is wet or has been in a wet environment, take necessary measures to remove moisture prior to applying power such as storage in a low humidity temperature chamber operating at 50°C for 4 hours or more.
The instrument is intended for indoor use only. Lift the instrument by the handle provided to move the instrument. DO NOT move
the instrument until the display reads less than 25°C (77°F) and the unit has been drained or the Transport Lid installed.
BURN HAZARD ALWAYS ensure the instrument is COOL before closing the instrument for storage.
DO NOT mix water and oil when exceeding temperatures of 90°C (194°F). DO NOT touch the well access surface of the unit. The temperature of the well access is the same as the actual temperature shown on
the display, e.g. if the unit is set at 125°C and the display reads 125°C, the well is at 125°C.
Ensure the power cord is positioned in such a way as it cannot contact hot sur faces or temperature probes. Always inspect power cord before use for any damage to the insulation due to contact with hot surfaces, cuts or abrasions.
The top sheet metal of the instrument may exhibit extreme temperatures for ar eas close to the well access.
DO NOT turn off the unit at temperatures higher than 100°C. This could create a hazardous situation. Select a set-point less than 100°C and allow the unit to cool before turning it off.
DO NOT remove the fluid at high temperatures. The uid will be the same temperature as the display temperature.
DO NOT operate near ammable materials. Extreme temperatures could ignite the ammable material.
Use of this instrument at HIGH TEMPERATURES for extended periods of time requires caution.
3
7103 Micro-Bath User’s Guide
Safety Information
ELECTRICAL HAZARD
These guidelines must be followed to ensure that the safety mechanisms in this instrument will operate properly. This instrument must be plugged into a 115 VAC (± 10%) or 230 VAC (± 10%) 50/60 Hz only electric outlet as indicated on the back panel. The power cord of the instrument is equipped with a three-pronged grounding plug for your protection against electrical shock haz ards. It must be plugged directly into a properly grounded three-prong recepta cle. The receptacle must be installed in accordance with local codes and ordinances or adapter plug. DO NOT use an extension cord. Consult a qualied electrician. Always inspect the power cord before use for any damage to the in sulation due to contact with hot surfaces, cuts or abrasions.
The instrument is equipped with operator accessible fuses. If a fuse blows, it may be due to a power surge or failure of a component. Replace the fuse once. If the fuse blows a second time, it is likely caused by failure of a component part. If this occurs, contact a Hart Scientic Authorized Service Center. Always replace the fuse with one of the same rating, voltage, and type. Never replace the fuse with one of a higher current rating.
Always replace the power cord with an approved cord of the correct rating and type. If you have questions, contact a Hart Scientific Authorized Service Center (see Section
1.3). High voltage is used in the operation of this equipment. Severe injury or death may
result if personnel fail to observe the safety precautions.
1.2.2 Cautions
Always operate this instrument at room temperatures listed in Section 3.2, Environmental Conditions. Allow sufcient air circulation by leaving at least 6 inches (15 cm) of clearance around the instrument.
Overhead clearance is required. DO NOT place this instrument under a cabinet or other structure.
Never introduce any foreign material into the well. DO NOT change the values of the calibration constants from the factory set values.
The correct setting of these parameters is important to the safety and proper operation of the unit.
DO NOT slam the probe stems into the well. This type of action can cause a shock to the sensor and affect the calibration.
DO use a ground fault interrupt device. DO NOT operate this instrument in an excessively wet, oily, dusty, or dirty
environment.
4
Before You Start
Authorized Service Centers
The unit is a precision instrument. Although it has been designed for optimum durability and trouble free operation, it must be handled with care.
Most probes have handle temperature limits. Be sure that the probe handle tem perature limit is not exceeded in the air above the instrument.
The instrument and any thermometer probes used with it are sensitive instru ments that can be easily damaged. Always handle these devices with care. Do not allow them to be dropped, struck, stressed, or overheated.
When calibrating PRTs always follow correct calibration procedure and cali brate from high temperatures to low temperatures with the appropriate triple point of water checks.
Components and heater lifetimes can be shortened by continuous high tempera ture operation.
If a mains supply power uctuation occurs, immediately turn off the bath. Power bumps from brown-outs and black-outs can damage the instrument. Wait until the power has stabilized before re-energizing the bath.
Fluids may expand at different rates. Allow for uid expansion inside the well as the instrument heats. Otherwise, the uid may overow the well and leak into the instrument.
1.3 Authorized Service Centers
Please contact one of the following authorized Service Centers to coordinate service on your Hart product:
Fluke Corporation
Hart Scientic Division
799 E. Utah Valley Drive American Fork, UT 84003-9775 USA
Phone: +1.801.763.1600 Telefax: +1.801.763.1010 E-mail: support@hartscientic.com
5
7103 Micro-Bath User’s Guide
Authorized Service Centers
Fluke Nederland B.V.
Customer Support Services Science Park Eindhoven 5108 5692 EC Son NETHERLANDS
Phone: +31-402-675300 Telefax: +31-402-675321 E-mail: ServiceDesk@fluke.nl
Fluke Int’l Corporation
Service Center - Instrimpex Room 2301 Sciteck Tower 22 Jianguomenwai Dajie Chao Yang District Beijing 100004, PRC CHINA
Phone: +86-10-6-512-3436 Telefax: +86-10-6-512-3437 E-mail: xingye.han@uke.com.cn
Fluke South East Asia Pte Ltd.
Fluke ASEAN Regional Ofce Service Center 60 Alexandra Terrace #03-16 The Comtech (Lobby D) 118502 SINGAPORE
Phone: +65-6799-5588 Telefax: +65-6799-5589 E-mail: anthony.ng@uke.com
When contacting these Service Centers for support, please have the following information available:
L
Model Number
L
Serial Number
L
Voltage
L
Complete description of the problem
6
Introduction
Introduction 2
The Hart Scientic 7103 Micro-Bath may be used as a portable instrument or bench top temperature calibrator for calibrating thermocouple and RTD temper ature probes. The 7103 is small enough to use in the eld, and accurate enough to use in the lab. With an ambient temperature of 23°C (74°F), calibrations may be done over a range of -30°C to 125°C (-22°F to 257°F). The resolution of the 7103 temperature display is
0.01 degrees. The Micro-Bath calibrator features:
L
Convenient handle
L
RS-232 interface
L
Switchable AC Input (115 VAC or 230 VAC)
Built in programmable features include:
L
Temperature scan rate control
L
Temperature switch hold
L
Eight Set-point memory
L
Adjustable readout in °C or °F
The temperature is accurately controlled by Hart’s hybrid analog/digital con troller. The controller uses a precision platinum RTD as a sensor and controls the well temperature with thermal electric devices (TED).
The LED front panel continuously shows the current well temperature. The temperature may be easily set with the control buttons to any desired tempera ture within the specied range. The calibrator’s multiple fault protection de vices insure user and instrument safety and protection.
The 7103 Micro-Bath was designed for portability, low cost, and ease of opera tion. Through proper use, the instrument will continuously provide accurate calibration of temperature sensors and devices. The user should be familiar with the safety guidelines and operating procedures of the calibrator as de scribed in the instruction manual.
7
Specications and Environmental Conditions3
3.1 Specications
Table 2 Specifications
Range -30 to 125°C (-22 to 257°F)
Accuracy ±0.25°C
Stability ±0.03°C at -25°C (oil, 5010)
Uniformity ±0.02°C
Resolution 0.01°C/F
Operating Temperature 5 to 45°C (41 to 113°F)
Heating Time 25°C to 100°C: 35 minutes
Cooling Time 25°C to –25°C: 45 minutes
Well Size 2.5" dia. x 5.5" deep (64 x 139 mm)
Size 9" W x 13.2" H x 10.5" D (23 x 34 x 26 cm)
Weight 22 lb. (10 kg) with uid
Display LED, Switchable °C or °F
Cooling Fan and Thermal Electric Devices (TED)
Fault Protection Sensor burnout and short protection
Power 94 – 234 VAC (±10%), 50/60 Hz, 400 W
Safety Overvoltage (Installation) Category II, Pollution Degree 2 per IEC 61010-01
Fuse Rating 250 V 5 A F(fast acting) NO USER SERVICEABLE PARTS
Specications and Environmental Conditions
Specications
±0.05°C at 125°C (oil, 5010)
(access opening is 1.9" [48 mm] in diameter)
3.2 Environmental Conditions
Although the instrument has been designed for optimum durability and trou ble-free operation, it must be handled with care. The instrument should not be operated in an excessively dusty or dirty environment. Maintenance and clean ing recommendations can be found in the Maintenance Section of this manual.
The instrument operates safely under the following conditions:
L
ambient temperature range: 5 – 45°C (41 – 113°F)
L
ambient relative humidity: maximum 80% for temperature <31°C, de creasing linearly to 50% at 40°C
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mains voltage within ± 10% of nominal
L
vibrations in the calibration environment should be minimized
L
altitudes less than 2,000 meters
9
Quick Start4
Caution: READ SECTION 6 ENTITLED BATH USE before placing the bath in service. Incorrect handling can damage the bath and void the war ranty.
4.1 Unpacking
Unpack the Micro-Bath carefully and inspect it for any damage that may have occurred during shipment. If there is shipping damage, notify the carrier immediately.
Verify that the following components are present:
L
7103 Micro-Bath
L
Transport/Pour Access Lid
L
Probe Basket
L
Stir Bar
L
Power Cord
L
Manual
Access Cover, if purchasedL
Quick Start
Unpacking
Setup 4.2
Caution: DO NOT operate the instrument without fluid.
Place the calibrator on a at surface with at least 6 inches of free space around the instrument. Plug the power cord into a grounded mains outlet. Observe that the nominal voltage corresponds to that indicated on the back of the calibrator.
Carefully insert the probe basket into the well. Fill the well with the appropriate fluid. The set-point temperature and the number of and size of probes deter mine the uid level. Be sure to keep the uid level an adequate distance below the top of the well to prevent overowing the fluid when the probes are in serted. For example, placing
200.05 oil at room temperature (25°C) into the bath and heating the unit to 126°C, causes a 1-inch (2.54 cm) expansion of the uid inside the well.
Keep the uid level at least 1.9 cm (0.75 inches) below the top of the well at all times. With the probe (probes) in the well ll the tank 3/4 full. Heat to the maximum
temperature of the fluid. Slowly fill the well to 2.54 cm (1 inch) be low the top of the basket at the maximum temperature of the fluid, or to the second ring on the basket.
11
7103 Micro-Bath User’s Guide
Power
Turn on the power to the calibrator by toggling the switch on the power entry module. The fan should begin blowing air through the instrument and the con troller display should illuminate after 3 seconds. After a brief self test the con troller should begin normal operation. If the unit fails to operate please check the power connection.
The display shows the well temperature and the well TEDs start operating to bring the temperature of the well to the set-point temperature. Insure that the fluid is being stirred.
Power 4.3
Plug the Micro-Bath power cord into a mains outlet of the proper voltage, fre quency, and current capability. Refer to Section 3.1, Specifications, for power details.
Turn the bath on using the rear panel “POWER” switch. The Micro-Bath will turn on and begin to heat to the previously programmed temperature set-point. The front panel LED display will indicate the actual bath temperature.
Setting the Temperature 4.4
Section 9.2 explains in detail how to set the temperature set-point on the cali brator using the front panel keys. The procedure is summarized here.
Press “SET” twice to access the set-point value. 1.
Press “UP” or “DOWN” to change the set-point value. 2.
Press “SET” to store the new set-point. 3.
Press “EXIT” to return to the temperature display. 4.
When the set-point temperature is changed the controller switchs the well heater on or off to raise or lower the temperature. The displayed well tempera ture gradually changes until it reaches the set-point temperature. The well may require 90 minutes to reach the set-point depending on the span. Another 10 to 15 minutes is required to stabilize within ±0.04°C of the set-point. Ultimate sta bility may take 20 to 30 minutes more of stabilization time.
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