Fluke 6102 Operating Manual

6102
Micro-Bath
User’s Guide
PN 3729224 January 2013
© 2013 Fluke Corporation. All rights reserved. Specifications are subject to change without notice. All product names are trademarks of their respective companies.
LIMITED WARRANTY AND LIMITATION OF LIABILITY
Fluke authorized resellers shall extend this warranty on new and unused products to end-user customers only but have no authority to extend a greater or different warranty on behalf of Fluke. Warranty support is available only if product is purchased through a Fluke authorized sales outlet or Buyer has paid the applicable international price. Fluke reserves the right to invoice Buyer for importation costs of repair/replacement parts when product purchased in one country is submitted for repair in another country.
Fluke's warranty obligation is limited, at Fluke's option, to refund of the purchase price, free of charge repair, or replacement of a defective product which is returned to a Fluke authorized service center within the warranty period.
To obtain warranty service, contact your nearest Fluke authorized service center to obtain return authorization information, then send the product to that service center, with a description of the difficulty, postage and insurance prepaid (FOB Destination). Fluke assumes no risk for damage in transit. Following warranty repair, the product will be returned to Buyer, transportation prepaid (FOB Destination). If Fluke determines that failure was caused by neglect, misuse, contamination, alteration, accident, or abnormal condition of operation or handling, including overvoltage failures caused by use outside the product’s specified rating, or normal wear and tear of mechanical components, Fluke will provide an estimate of repair costs and obtain authorization before commencing the work. Following repair, the product will be returned to the Buyer transportation prepaid and the Buyer will be billed for the repair and return transportation charges (FOB Shipping Point).
THIS WARRANTY IS BUYER'S SOLE AND EXCLUSIVE REMEDY AND IS IN LIEU OF ALL OTHER WARRANTIES, EXPRESS OR IMPLIED, INCLUDING BUT NOT LIMITED TO ANY IMPLIED WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE. FLUKE SHALL NOT BE LIABLE FOR ANY SPECIAL, INDIRECT, INCIDENTAL, OR CONSEQUENTIAL DAMAGES OR LOSSES, INCLUDING LOSS OF DATA, ARISING FROM ANY CAUSE OR THEORY.
Since some countries or states do not allow limitation of the term of an implied warranty, or exclusion or limitation of incidental or consequential damages, the limitations and exclusions of this warranty may not apply to every buyer. If any provision of this Warranty is held invalid or unenforceable by a court or other decision-maker of competent jurisdiction, such holding will not affect the validity or enforceability of any other provision.
Fluke Corporation P.O. Box 9090 Everett, WA 98206-9090 U.S.A.
Fluke Europe B.V. P.O. Box 1186 5602 BD Eindhoven The Netherlands
11/99
To register your product online, visit register.fluke.com

Table of Contents

1 Before You Start .......................................................................1
1.1 Symbols Used ........................................................................................... 1
1.2 Safety Information .................................................................................... 2
1.2.1 Warnings .........................................................................................................2
1.2.2 Cautions ..........................................................................................................4
1.3 Authorized Service Centers ..................................................................... 5
2 Introduction .............................................................................7
3 Specications and Environmental Conditions ......................9
3.1 Specifications ........................................................................................... 9
3.2 Environmental Conditions ......................................................................... 9
4 Quick Start ..............................................................................11
4.1 Unpacking .............................................................................................. 11
4.2 Setup ...................................................................................................... 11
4.3 Power ..................................................................................................... 12
4.4 Setting the Temperature ......................................................................... 12
5 Installation .............................................................................13
5.1 Bath Environment ................................................................................... 13
5.2 “Dry-out” Period ..................................................................................... 13
5.3 Bath Preparation and Filling ................................................................... 13
5.4 Power ..................................................................................................... 14
6 Bath Use .................................................................................15
6.1 General .................................................................................................. 15
6.2 Comparison Calibration ......................................................................... 15
6.3 Calibration of Multiple Probes ................................................................. 16
7 Parts and Controls ................................................................17
7.1 Back and Bottom Panel .......................................................................... 17
7.2 Front Panel .............................................................................................. 18
7.3 Accessories ........................................................................................... 19
7.3.1 Transport/Pour Lid ........................................................................................19
iii
7.3.2 Access Cover (Optional) .............................................................................. 19
7.3.3 Probe Basket ................................................................................................19
7.3.4 Stir Bar ..........................................................................................................20
7.3.5 Tank Extender (Optional) ..............................................................................20
8 General Operation ..................................................................21
8.1 Switching to 230V Operation .................................................................. 21
8.2 Bath Fluid ............................................................................................... 21
8.2.1 Temperature Range .......................................................................................21
8.2.2 Viscosity ........................................................................................................22
8.2.3 Specific Heat ................................................................................................. 22
8.2.4 Thermal Conductivity ....................................................................................22
8.2.5 Thermal Expansion........................................................................................22
8.2.6 Electrical Resistivity .......................................................................................22
8.2.7 Fluid Lifetime .................................................................................................23
8.2.8 Safety ............................................................................................................ 23
8.2.9 Cost ...............................................................................................................23
8.2.10 Commonly Used Fluids .................................................................................23
8.2.10.1 Water (Distilled) ................................................................................................... 24
8.2.10.2 Mineral Oil ............................................................................................................ 24
8.2.10.3 Silicone Oil (Dow Corning 200.10, 200.20) .......................................................... 24
8.2.11 Fluid Characteristics Charts ..........................................................................24
8.2.11.1 Limitations and Disclaimer .................................................................................. 25
8.2.11.2 About the Graph .................................................................................................. 26
8.3 Stirring .................................................................................................... 27
8.4 Power ...................................................................................................... 28
8.5 Heater ..................................................................................................... 28
8.6 Fluid Drain ............................................................................................... 28
8.7 Temperature Controller .......................................................................... 28
9 Controller Operation ..............................................................31
9.1 Well Temperature ................................................................................... 31
9.2 Temperature Set-point ........................................................................... 31
9.2.1 Programmable Set-points ............................................................................31
9.2.2 Set-point Value .............................................................................................33
9.2.3 Temperature Scale Units ..............................................................................33
9.3 Scan ....................................................................................................... 34
9.3.1 Scan Control .................................................................................................34
9.3.2 Scan Rate .....................................................................................................34
9.4 Temperature Display Hold ..................................................................... 35
iv
9.4.1 Hold Temperature Display ............................................................................35
9.4.2 Mode Setting ................................................................................................35
9.4.3 Switch Wiring ................................................................................................36
9.4.4 Switch Test Example ....................................................................................36
9.5 Secondary Menu .................................................................................... 36
9.6 Heater Power .......................................................................................... 37
9.7 Proportional Band .................................................................................. 37
9.8 Cutout .................................................................................................... 38
9.9 Controller Configuration .......................................................................... 39
9.10 Operating Parameters ............................................................................ 39
9.10.1 Stir Speed ......................................................................................................39
9.10.2 High Limit .....................................................................................................40
9.10.3 Cutout Reset Mode .......................................................................................40
9.11 Serial Interface Parameters ................................................................... 41
9.11.1 BAUD Rate ....................................................................................................41
9.11.2 Sample Period ............................................................................................... 41
9.11.3 Duplex Mode ................................................................................................. 42
9.11.4 Linefeed ....................................................................................................... 42
9.12 Calibration Parameters ........................................................................... 43
9.12.1 R0 .................................................................................................................43
9.12.2 ALPHA .......................................................................................................... 43
9.12.3 DELTA ...........................................................................................................43
9.12.4 C0 and CG ....................................................................................................44
9.12.5 rCAL ..............................................................................................................44
10 Digital Communication Interface ..........................................45
10.1 Serial Communications .......................................................................... 45
10.1.1 Wiring ...........................................................................................................45
10.1.2 Setup ............................................................................................................45
10.1.2.1 Baud Rate ........................................................................................................... 46
10.1.2.2 Sample Period ...................................................................................................... 46
10.1.2.3 Duplex Mode ........................................................................................................ 46
10.1.2.4 Linefeed ................................................................................................................ 46
10.1.3 Serial Operation ............................................................................................ 46
10.2 Interface Commands .............................................................................. 47
11 Test Probe Calibration ...........................................................49
11.1 Calibrating a Single Probe ..................................................................... 49
11.2 Stabilization and Accuracy .................................................................... 49
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11.3 Multiple Probe Calibration ..................................................................... 49
12 Calibration Procedure ...........................................................51
12.1 Calibration Points ................................................................................... 51
12.2 Calibration Procedure ............................................................................ 51
12.2.1 Compute DELTA ...........................................................................................52
12.2.2 Compute R0 & ALPHA ..................................................................................52
12.2.3 Accuracy & Repeatability ............................................................................. 53
13 Maintenance ...........................................................................55
14 Troubleshooting .....................................................................57
14.1 Troubleshooting Problems, Possible Causes, and Solutions ................. 57
14.2 CE Comments ......................................................................................... 58
14.2.1 EMC Directive ............................................................................................... 58
14.2.2 Low Voltage Directive (Safety) ......................................................................58
vi

Tables

Table 1 International Electrical Symbols ........................................................... 1
Table 2 Specifications ....................................................................................... 9
Table 3 Table of Various Bath Fluids ............................................................... 25
Table 4 Nominal Stirrer Motor Settings With Different Liquids ........................ 28
Table 5 Controller Communications Commands ............................................. 48
vii

Figures

Figure 1 6102 Back Panel and Bottom ............................................................ 17
Figure 2 6102 Front Panel ................................................................................ 18
Figure 3 Bath Lids and Lid Parts ..................................................................... 19
Figure 4 Probe Basket ..................................................................................... 20
Figure 5 Stir Bar ............................................................................................... 20
Figure 6 Chart of Various Bath Fluids ............................................................. 26
Figure 7 Controller Operation Flowchart ......................................................... 32
Figure 8 Serial Cable Wiring ........................................................................... 45
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Before You Start

Symbols Used

Before You Start1
Symbols Used1.1
Table 1 lists the International Electrical Symbols. Some or all of these symbols may be used on the instrument or in this manual.
Table 1 International Electrical Symbols
Symbol Description
AC (Alternating Current)
AC-DC
Battery
CE
DC
Double Insulated
Electric Shock
Fuse
PE Ground
Hot Surface (Burn Hazard)
Read the User’s Guide (Important Information)
Off
On
Canadian Standards Association
1
6102 Micro-Bath User’s Guide

Safety Information

Symbol Description
C-TICK Australian EMC mark
The European Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/ EC) mark.
OVERVOLTAGE (Installation) CATEGORY II, Pollution Degree 2 per IEC1010-1 re fers to the level of Impulse Withstand Voltage protection provided. Equipment of OVERVOLTAGE CATEGORY II is energy-consuming equipment to be supplied from the xed installation. Examples include household, office, and laboratory appliances.
Safety Information 1.2
Use this instrument only as specied in this manual. Otherwise, the protection provided by the instrument may be impaired.
The following denitions apply to the terms “Warning” and “Caution”.
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“Warning” identies conditions and actions that may pose hazards to the user.
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“Caution” identies conditions and actions that may damage the instru ment being used.

Warnings1.2.1

To avoid personal injury, follow these guidelines.
GENERAL DO NOT use the instrument for any application other than calibration work. The
instrument was designed for temperature calibration. Any other use of the unit may cause unknown hazards to the user.
DO NOT overll the bath. Overowing extremely cold or hot uid may be harmful to the operator. See Section 5.3, Bath Preparation and Filling, for specic instructions.
DO NOT install access cover without holes onto a bath that is energized. Dangerous pressures may result from uids vaporizing.
Calibration Equipment should only be used by Trained Personnel. If this equipment is used in a manner not specied by the manufacturer, the protection
provided by the equipment may be impaired. Before initial use, or after transport, or after storage in humid or semi-humid
environments, or anytime the instrument has not been energized for more than 10 days, the instrument needs to be energized for a “dry-out” period of 2 hours before it can be assumed to meet all of the safety requirements of the IEC 61010-1. If the product is wet or has been in a wet environment, take necessary measures to remove moisture prior to applying power such as storage in a low humidity temperature chamber operating at 50°C for 4 hours or more.
2
Before You Start
Safety Information
Overhead clearance is required. Do not place the instrument under a cabi net or other structure. Always leave enough clearance to allow for safe and easy insertion and removal of probes.
The instrument is intended for indoor use only.
DO NOT use the unit in environments other than those listed in the user’s guide. DO NOT carry the unit without the transport lid in place and properly se cured.
Thoroughly wipe the inside of the well dry when changing fluids as some high temperature uids react violently to water or other liquid mediums.
Use of this instrument at HIGH TEMPERATURES for extended periods of time requires caution.
Completely unattended high temperature operation in not recommended.
BURN HAZARD
High temperatures may be present in this equipment. Fires and severe burns may result if personnel fail to observe safety precautions.
DO NOT mix water and oil when exceeding temperatures of 90°C (194°F).
ELECTRICAL HAZARD
These guidelines must be followed to ensure that the safety mechanisms in this instrument will operate properly. This instrument must be plugged into an AC only electric outlet as listed in Section 3.1, Specications. The power cord of the instrument is equipped with a three-pronged grounding plug for your protection against electrical shock haz ards. It must be plugged directly into a properly grounded three-prong receptacle. The receptacle must be installed in accordance with local codes and ordinances. DO NOT use an extension cord or adapter plug.
DO use a ground fault interrupt device. This unit contains a liquid. A ground fault device is advised in case liquid is present in the electrical system and could cause an electrical shock.
Always replace the power cord with an approved cord of the correct rating and type. If you have questions, contact an Authorized Service Center (see Section 1.3).
High voltage is used in the operation of this equipment. Severe injury or death may result if personnel fail to observe the safety precautions. Before working inside the equipment, turn off the power and disconnect the power cord.
DO NOT connect this unit to a non-grounded, non-polarized outlet. Always replace the fuse with one of the same rating, voltage, and type.
3
6102 Micro-Bath User’s Guide
Safety Information
BATH FLUIDS
Fluids used in this unit may produce noxious or toxic fumes under certain circumstances. Consult the uid manufacturer’s MSDS (Material Safety Data Sheet). Proper ventilation and safety precautions must be observed.
The unit is equipped with a soft cutout (user settable rmware) and a hard cutout. Check the ash point, boiling point, or other uid characteristic applicable to the circumstances of the unit operation. Ensure that the soft cutout is adjusted to the uid characteristics of the application. DO NOT exceed the boiling or ash temperatures of the fluid being used.

Cautions1.2.2

DO NOT overll the bath. Overowing liquid may damage the electrical system. Be sure to allow for thermal expansion of the uid as the bath temperature increases. See Section 5.3, Bath Preparation and Filling, for specic instructions.
Read Section 6, Bath Use, before placing the unit into service. DO NOT change the values of the bath calibration constants from the fac tory set
values. The correct setting of these parameters is important to the safety and proper operation of the unit.
The Factory Reset Sequence should be performed only by authorized personnel if no other action is successful in correcting a malfunction. You must have a copy of the most recent Report of Test to restore the test pa rameters.
Most probes have handle temperature limits. Be sure that the probe handle temperature limit is not exceeded in the air above the instrument.
The instrument and any thermometer probes used with it are sensitive in struments that can be easily damaged. Always handle these devices with care. Do not allow them to be dropped, struck, stressed, or overheated.
Operate the instrument in room temperatures as listed in Section 3.2, Environmental Conditions. Allow sufcient air circulation by leaving at least 6 inches of space be­tween the instrument and nearby objects.
Overhead clearance needs to al low for safe and easy insertion and removal of probes for calibration.
Use only clean uid with the instrument. The Micro-Bath is a precision instrument. Although it has been designed for optimum
durability and trouble free operation, it must be handled with care. Always carry the unit in an upright position to prevent the liquid from spilling out. The convenient fold-up handle allows one hand carry ing. The instrument should not be operated in excessively wet, oily, dusty, or dirty environments. It is important to keep the well of the instrument clean and clear of any foreign matter. Do not operate near flammable ma terials.
4
If a mains supply power uctuation occurs, immediately turn off the in strument. Power bumps from brown-outs and black-outs could damage the instrument. Wait until the power has stabilized before re-energizing the instrument.
Components and heater lifetime can be shortened by continuous high temperature operation.
DO NOT operate the instrument without fluid. The input voltage and heater voltage switch settings must always be set to the same
value.

1.3 Authorized Service Centers

Please contact one of the following authorized Service Centers to coordinate service on your Hart product:
Fluke Corporation
Hart Scientic Division
799 E. Utah Valley Drive American Fork, UT 84003-9775 USA
Before You Start
Authorized Service Centers
Phone: +1.801.763.1600 Telefax: +1.801.763.1010 E-mail: support@hartscientic.com
Fluke Nederland B.V.
Customer Support Services Science Park Eindhoven 5108 5692 EC Son NETHERLANDS
Phone: +31-402-675300 Telefax: +31-402-675321 E-mail: ServiceDesk@fluke.nl
5
6102 Micro-Bath User’s Guide
Authorized Service Centers
Fluke Int’l Corporation
Service Center - Instrimpex Room 2301 Sciteck Tower 22 Jianguomenwai Dajie Chao Yang District Beijing 100004, PRC CHINA
Phone: +86-10-6-512-3436 Telefax: +86-10-6-512-3437 E-mail: xingye.han@uke.com.cn
Fluke South East Asia Pte Ltd.
Fluke ASEAN Regional Ofce Service Center 60 Alexandra Terrace #03-16 The Comtech (Lobby D) 118502 SINGAPORE
Phone: +65-6799-5588 Telefax: +65-6799-5589 E-mail: anthony.ng@uke.com
When contacting these Service Centers for support, please have the following information available:
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Model Number
L
Serial Number
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Voltage
L
Complete description of the problem
6

Introduction

Introduction 2
The Hart Scientic 6102 Micro-Bath may be used as a portable instrument or bench top temperature calibrator for calibrating thermocouple and RTD temper ature probes. The 6102 is small enough to use in the eld, and accurate enough to use in the lab. Calibrations may be done over a range of 35°C to 200°C (95°F to 392°F). The resolution of the 6102 temperature display is 0.01 degrees.
The Micro-Bath calibrator features:
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Convenient handle
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RS-232 interface
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Switchable AC Input (115 VAC or 230 VAC)
Built in programmable features include:
L
Temperature scan rate control
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Temperature switch hold
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Eight Set-point memory
L
Adjustable readout in °C or °F
The temperature is accurately controlled by Hart’s digital con troller. The controller uses a precision platinum RTD as a sensor and controls the well temperature with a solid state relay (triac) driven heater.
The LED front panel continuously shows the current well temperature. The temperature may be easily set with the control buttons to any desired tempera ture within the specied range. The calibrator’s multiple fault protection de vices insure user and instrument safety and protection.
The 6102 Micro-Bath was designed for portability, low cost, and ease of opera tion. Through proper use, the instrument will continuously provide accurate calibration of temperature sensors and devices. The user should be familiar with the safety guidelines and operating procedures of the calibrator as de scribed in the instruction manual.
7
Specications and Environmental Conditions3
3.1 Specications
The 6102 may not meet the specication published if a different fluid is used other than distilled water or Dow Corning (200.10, 200.20) oil.
Do not exceed the boiling point or ash point temperatures of the uid. To ensure that the boiling and ash point temperatures are not exceeded adjust the High Limit and Cutout parameters. To set these parameters, refer to Section 9, Controller Operation.
Specifications Table 2
Range 35 to 200°C (95 to 392°F)
Accuracy ±0.25°C
Stability ±0.02°C at 100°C
Uniformity ±0.02°C
Resolution 0.01°C/F
Operating Temperature 5 to 45°C (41 to 113°F)
Heating Time 25°C to 200°C: 40 minutes
Cooling Time 200°C to 100°C: 35 minutes
Well Size 1.9" dia. x 5.5" deep (48 x 139 mm)
Size 5.5" W x 10.38" H x 8" D (14 x 26 x 20 cm)
Weight 10 lb. (4.5 kg) with uid
Power 115 VAC (±10%), 12.3 A, or 230 VAC (±10%), 1.1 A, switchable, 50/60 Hz,
System Fuse 115 V: 250 V, 3A, F
Safety Overvoltage (Installation) Category II, Pollution Degree 2 per IEC 61010-01
Specications and Environmental Conditions
Specications
±0.03°C at 200°C
270 W
230 V: 250 V, 1.6A, F

3.2 Environmental Conditions

Although the instrument has been designed for optimum durability and trou ble-free operation, it must be handled with care. The instrument should not be operated in an excessively dusty or dirty environment. Maintenance and clean ing recommendations can be found in the Maintenance Section of this manual.
The instrument operates safely under the following conditions:
L
ambient temperature range: 5 – 45°C (41 – 113°F)
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ambient relative humidity: maximum 80% for temperature <31°C, de creasing linearly to 50% at 40°C
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mains voltage within ± 10% of nominal
L
vibrations in the calibration environment should be minimized
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altitudes less than 2,000 meters
9
Quick Start4
Caution: READ SECTION 6 ENTITLED BATH USE before placing the bath in service. Incorrect handling can damage the bath and void the war ranty.

4.1 Unpacking

Unpack the Micro-Bath carefully and inspect it for any damage that may have occurred during shipment. If there is shipping damage, notify the carrier immediately.
Verify that the following components are present:
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6102 Micro-Bath
L
Transport/Pour Lid
L
Probe Basket
L
Stir Bar
L
Power Cord
L
User’s Guide
L
Report of Calibration
L
Calibration Label
L
RS-232 Cable

Quick Start

Unpacking
9930 Interface-Lit Software
L
Access Cover (optional)
L
Extender, perf-cage, wrench (optional)

Setup 4.2

Place the calibrator on a at surface with at least 6 inches of free space around the instrument. Plug the power cord into a grounded mains outlet. Observe that the nominal voltage corresponds to that indicated on the back of the calibrator.
Carefully insert the probe basket into the tank. Fill the tank with the appropriate fluid. The set-point temperature and the number of and size of probes deter mine the fluid level. Be sure to keep the uid level an adequate distance below the top of the well to prevent overowing the fluid when the probes are in serted. For example, placing
200.20 oil at room temperature (25°C) into the bath and heating the unit to 200°C, causes a 1-inch (2.54 cm) expansion of the uid inside the well.
Keep the uid level at least 0.64 cm (0.25 inches) below the top of the probe basket at all times. With the probe (probes) in the tank ll the tank 3/4 full. Heat to the
maximum temperature of the fluid. Slowly fill the well to 1.3 cm (.5 inch) be low the top of the probe basket at the maximum temperature of the fluid.
11
6102 Micro-Bath User’s Guide

Power

Turn on the power to the calibrator by toggling the switch on the power entry module. The fan should begin blowing air through the instrument and the con troller display should illuminate after 3 seconds. After a brief self test the con troller should begin normal operation. If the unit fails to operate please check the power connection.
The display will begin to show the uid temperature and the tank heater will start operating to bring the temperature of the uid to the set-point temperature. Insure that
the uid is being stirred.
Power 4.3
Plug the Micro-Bath power cord into a mains outlet of the proper voltage, fre quency, and current capability. Refer to Section 3.1, Specications, for power details. Turn the bath on using the rear panel “POWER” switch. The Micro-Bath will turn on and begin to heat to the previously programmed temperature set-point. The front panel LED display will indicate the actual bath temperature.

Setting the Temperature 4.4

Section 9.2 explains in detail how to set the temperature set-point on the cali brator using the front panel keys. The procedure is summarized here.
Press “SET” twice to access the set-point value. 1.
Press “UP” or “DOWN” to change the set-point value. 2.
Press “SET” to store the new set-point. 3.
Press and hold “EXIT” to return to the temperature display. 4.
When the set-point temperature is changed the controller switches the tank heater on or off to raise or lower the temperature. The displayed tempera ture gradually changes until it reaches the set-point temperature. The 6102 may require 25 minutes to reach the set-point depending on the span. Another 10 to 15 minutes is required to stabilize within ±0.03°C of the set-point. Ultimate sta bility may take 20 to 30 minutes more of stabilization time.
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