Emerson MicroCEM User Manual

Instruction Manual
748467-A January 2002
Model MicroCEM
Continuous Emissions Monitor
http://www.processanalytic.com

ESSENTIAL INSTRUCTIONS

READ THIS PAGE BEFORE PROCEEDING!
Rosemount Analytical designs, manufactures and tests its products to meet many national and international standards. Because these instruments are sophisticated technical products, you MUST properly install, use, and maintain them to ensure they continue to operate within their normal specifications. The following instructions MUST be adhered to and integrated into your safety program when installing, using, and maintaining Rosemount Analytical products. Failure to follow the proper instructions may cause any one of the following situations to occur: Loss of life; personal injury; property damage; damage to this instrument; and warranty invalidation.
Read all instructions prior to installing, operating, and servicing the product.
If you do not understand any of the instructions, contact your Rosemount Analytical repre-
sentative for clarification.
Follow all warnings, cautions, and instructions marked on and supplied with the product.
Inform and educate your personnel in the proper installation, operation, and maintenance of the
product.
Install your equipment as specified in the Installation Instructions of the appropriate Instruction
Manual and per applicable local and national codes. Connect all products to the proper electri­cal and pressure sources.
To ensure proper performance, use qualified personnel to install, operate, update, program,
and maintain the product.
When replacement parts are required, ensure that qualified people use replacement parts speci-
fied by Rosemount. Unauthorized parts and procedures can affect the product’s performance, place the safe operation of your process at risk, and VOID YOUR WARRANTY. Look-alike substitutions may result in fire, electrical hazards, or improper operation.
Ensure that all equipment doors are closed and protective covers are in place, except
when maintenance is being performed by qualified persons, to prevent electrical shock and personal injury.
The information contained in this document is subject to change without notice.
Logos, trademarks and copyrights are property of their respective owners.
Emerson Process Management
Rosemount Analytical Inc. Process Analytic Division
1201 North Main Street Orrville, Ohio 44667-09012 T (330) 682-9010 F (330) 684-4434 e-mail: gas.csc@EmersonProcess.com
http://www.processanalytic.com
Model MicroCEM
PREFACE...........................................................................................................................................P-1
Definitions ...........................................................................................................................................P-1
Intended Use Statement.....................................................................................................................P-2
Safety Summary .................................................................................................................................P-2
General Precautions For Handling And Storing High Pressure Gas Cylinders .................................P-5
Documentation....................................................................................................................................P-6
Compliances .......................................................................................................................................P-6
1-0 DESCRIPTION AND SPECIFICATIONS..............................................................................1-1
1-1 Overview................................................................................................................................1-1
1-2 Typical Applications...............................................................................................................1-1
1-3 Theory Of Operation..............................................................................................................1-1
a. Chemiluminescense NOX................................................................................................1-1
b. Non-Dispersive Infrared (NDIR) CO ...............................................................................1-1
c. Paramagnetic O2.............................................................................................................1-2
1-4 Detector Methodologies.........................................................................................................1-2
a. Non-Dispersive Infrared (NDIR)......................................................................................1-2
b. Paramagnetic Oxygen Method .......................................................................................1-6
c. Electrochemical Oxygen Method ....................................................................................1-7
1-5 Central Processing Unit.........................................................................................................1-9
a. Embedded Enhanced Bios .............................................................................................1-9
b. Specifications ..................................................................................................................1-9
1-6 Analog/Digital I/O Board ........................................................................................................1-10
a. Automatic Calibration......................................................................................................1-10
b. Analog Inputs ..................................................................................................................1-10
c. Programmable Input Ranges ..........................................................................................1-11
d. Enhanced Trigger and Sampling Control Signals...........................................................1-11
e. Analog Outputs ...............................................................................................................1-11
f. FIFO and 16-Bit Bus Interface ........................................................................................1-11
g. Specifications ..................................................................................................................1-13
1-7 PCMCIA Adapter ...................................................................................................................1-14
a. Features ..........................................................................................................................1-14
b. Software ..........................................................................................................................1-14
1-8 Modem...................................................................................................................................1-15
a. Features ..........................................................................................................................1-15
1-9 Flash Drive.............................................................................................................................1-16
a. Specifications ..................................................................................................................1-16
1-10 Pocket PC..............................................................................................................................1-18
a. Specifications ..................................................................................................................1-18
1-11 Wireless LAN Adapter ...........................................................................................................1-19
a. Specifications ..................................................................................................................1-19
1-12 500 Watts Power Supply .......................................................................................................1-20
a. Features ..........................................................................................................................1-20
1-13 MicroCEM Specifications.......................................................................................................1-21
a. Analyzer ..........................................................................................................................1-21
b. Probe/Sample Handling ..................................................................................................1-22
Instruction Manual
748467-A
January 2002

TABLE OF CONTENTS

Rosemount Analytical Inc. A Division of Emerson Process Management Contents i
Instruction Manual
748467-A January 2002
2-0 INSTALLATION ....................................................................................................................2-1
2-1 Overview................................................................................................................................2-1
a. Limitations .......................................................................................................................2-1
b. Mounting Options ............................................................................................................2-1
2-2 Location .................................................................................................................................2-1
2-3 Gases ....................................................................................................................................2-3
a. Connection ......................................................................................................................2-3
b. Conditioning ....................................................................................................................2-3
2-4 Electrical Connections ...........................................................................................................2-6
a. AC Power ........................................................................................................................2-8
b. Circular Connector Assembly Instructions......................................................................2-8
c. Interface Connections .....................................................................................................2-11
2-5 Analytical Leak Check ...........................................................................................................2-14
a. Flow Indicator Method.....................................................................................................2-14
b. Manometer Method.........................................................................................................2-15
3-0 OPERATION .........................................................................................................................3-1
3-1 Startup Procedure .................................................................................................................3-1
3-2 Pocket PC User Interface ......................................................................................................3-1
a. Connecting Pocket PC to MicroCEM ..............................................................................3-1
b. Main Display....................................................................................................................3-3
c. MicroCEM Menu .............................................................................................................3-4
d. MicroCEM Alarms ...........................................................................................................3-4
e. MicroCEM Login..............................................................................................................3-6
f. MicroCEM Login-Current User Indication .......................................................................3-6
3-3 MicroCEM Settings................................................................................................................3-7
a. Range..............................................................................................................................3-7
b. Auto Calibration...............................................................................................................3-8
c. Auto Calibration Time and Frequency ............................................................................3-8
d. Manual Calibration ..........................................................................................................3-9
e. Limits...............................................................................................................................3-10
f. Calibration Gas ...............................................................................................................3-10
g. Maintenance Mode .........................................................................................................3-11
3-4 MicroCEM Factory Settings...................................................................................................3-12
a. PID Control Loop Factory Settings .................................................................................3-15
3-5 MicroCEM Administration ......................................................................................................3-17
a. User Settings...................................................................................................................3-17
b. Auto Logoff......................................................................................................................3-17
3-6 MicroCEM Data Logs ............................................................................................................3-18
a. Maximum Log File Size...................................................................................................3-18
b. Maximum Number of Log Files .......................................................................................3-18
c. Log File Name Format ....................................................................................................3-18
d. Measurement Log File Format........................................................................................3-18
e. Calibration Log File Format.............................................................................................3-19
f. Alarm Log File Format ....................................................................................................3-20
3-7 View Data Logs .....................................................................................................................3-21
3-8 Viewing MicroCEM Data with a Web Browser ......................................................................3-23
a. Real-Time Page ..............................................................................................................3-23
b. Emissions Page ..............................................................................................................3-24
c. Download Page ...............................................................................................................3-26
3-9 Viewing MicroCEM Data with MS Excel................................................................................3-27
3-10 Auto Calibration .....................................................................................................................3-28
Model MicroCEM
ii Contents Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
4-0 SOFTWARE ..........................................................................................................................4-1
4-1 Overview................................................................................................................................4-1
4-2 MicroCEM User Interface Software .......................................................................................4-1
4-3 MicroCEM Web Server Software ..........................................................................................4-1
4-4 Software Development Management ....................................................................................4-2
5-0 MAINTENANCE AND SERVICE ..........................................................................................5-1
5-1 Overview................................................................................................................................5-1
5-2 Converter ...............................................................................................................................5-3
5-3 Ozone Generator...................................................................................................................5-4
5-4 Personality Modules ..............................................................................................................5-4
5-5 Chemiluminescense Detector Assembly...............................................................................5-5
a. Reaction Chamber ..........................................................................................................5-5
b. Photodiode ......................................................................................................................5-5
6-0 TROUBLESHOOTING ..........................................................................................................6-1
6-1 Troubleshooting Leaks ..........................................................................................................6-1
6-2 Pocket PC Connection Failure ..............................................................................................6-1
6-3 Trouble LED ..........................................................................................................................6-1
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7-0 REPLACEMENT PARTS ......................................................................................................7-1
8-0 RETURN OF MATERIAL ......................................................................................................8-1
8-1 Return Of Material .................................................................................................................8-1
8-2 Customer Service ..................................................................................................................8-1
8-3 Training..................................................................................................................................8-1
Rosemount Analytical Inc. A Division of Emerson Process Management Contents iii
Instruction Manual
748467-A January 2002
Figure 1-1. Absorption Bands of Sample Gas and Transmittance of Interference Filters ....... 1-3
Figure 1-2. Opto-Pneumatic Gas Detector............................................................................... 1-4
Figure 1-3. Overall NDIR Method............................................................................................. 1-5
Figure 1-4. Paramagnetic Oxygen Analysis............................................................................. 1-6
Figure 1-5. Reaction of Galvanic Cell ...................................................................................... 1-7
Figure 1-6. Electrochemical Oxygen Sensor............................................................................ 1-8
Figure 1-7. CPU ....................................................................................................................... 1-9
Figure 1-8. ADIO Board.......................................................................................................... 1-10
Figure 1-9. ADIO Block Diagram............................................................................................ 1-12
Figure 1-10. PCMCIA Interface................................................................................................ 1-14
Figure 1-11. Modem................................................................................................................. 1-15
Figure 1-12. 128MB Flash Drive .............................................................................................. 1-16
Figure 1-13. Pocket PC............................................................................................................ 1-18
Figure 1-14. Wireless LAN adapter.......................................................................................... 1-19
Figure 1-15. 500 Watts Power Supply ..................................................................................... 1-20
Figure 2-1. MicroCEM Outline and Mounting Dimensions....................................................... 2-2
Figure 2-2. MicroCEM Gas Connections ................................................................................. 2-4
Figure 2-3. MicroCEM Flow Diagram....................................................................................... 2-4
Figure 2-4. MicroCEM Installation and Test Setup Configuration............................................ 2-5
Figure 2-5. MicroCEM Electrical Connections ......................................................................... 2-6
Figure 2-6. MicroCEM Wiring Diagram .................................................................................... 2-7
Figure 2-7. Leak Test Flow Method ....................................................................................... 2-14
Figure 2-8. Leak Test Manometer Method............................................................................. 2-15
Figure 3-1. Pocket PC .............................................................................................................. 3-1
Figure 3-2. MicroCEM Front Panel .......................................................................................... 3-2
Figure 3-3. MicroCEM Pocket PC Display (Main Display Shown) ........................................... 3-3
Figure 3-4. MicroCEM Menu .................................................................................................... 3-4
Figure 3-5. Pocket PC Alarms Screen ..................................................................................... 3-4
Figure 3-6. MicroCEM Login .................................................................................................... 3-6
Figure 3-7. Current User Indication.......................................................................................... 3-6
Figure 3-8. Range Settings ...................................................................................................... 3-7
Figure 3-9. Auto Calibration Settings ....................................................................................... 3-8
Figure 3-10. Auto Calibration Time and Frequency ................................................................... 3-8
Figure 3-11. Manual Calibration................................................................................................. 3-9
Figure 3-12. Manual Calibration Results.................................................................................... 3-9
Figure 3-13. Limit Settings ....................................................................................................... 3-10
Figure 3-14. Calibration Gas Settings...................................................................................... 3-10
Figure 3-15. Maintenance Mode Settings ................................................................................ 3-11
Figure 3-16. User Settings .......................................................................................................3-17
Figure 3-17. Auto Logoff........................................................................................................... 3-17
Figure 3-18. View Data Logs.................................................................................................... 3-21
Figure 3-19. View Data Logs Table.......................................................................................... 3-22
Figure 3-20. Real-Time Web Page .......................................................................................... 3-23
Figure 3-21. Emissions Selection............................................................................................. 3-24
Figure 3-22. Emissions Table .................................................................................................. 3-24
Figure 3-23. Calibration Table.................................................................................................. 3-25
Figure 3-24. Download Web Page ........................................................................................... 3-26
Figure 3-25. New Web Query .................................................................................................. 3-27
Figure 3-26. Auto Calibration ................................................................................................... 3-28
Figure 4-1. MicroCEM Software Block Diagram ...................................................................... 4-1
Figure 5-1. MicroCEM Component Location............................................................................ 5-2
Model MicroCEM

LIST OF ILLUSTRATIONS

iv Contents Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Figure 5-2. Converter Assembly .............................................................................................. 5-3
Figure 5-3. Personality Modules and Backplane. .................................................................... 5-4
Figure 5-4. Chemiluminescense Detector Assembly ............................................................... 5-6
Figure 5-5. Chemiluminescense Detector Assembly – Exploded View ................................... 5-7
Table 2-1. Interface Connections.......................................................................................... 2-11
Table 2-2. AC Power Connection Terminal Assignments..................................................... 2-11
Table 2-3. Analog Output Terminal Assignments ................................................................. 2-11
Table 2-4. Digital Output Terminal Assignments .................................................................. 2-12
Table 2-5. RS-232 Interface Terminal Assignments............................................................. 2-13
Table 2-6. RS-485 Terminal Assignments............................................................................ 2-13
Table 2-7. LAN Interface Terminal Assignments .................................................................. 2-13
Table 2-8. Phone Line (Modem) Terminal Assignments ...................................................... 2-13
Table 2-9. Antenna (Peltier Power) Connection Terminal Assignments .............................. 2-14
Table 3-1. Status Values.........................................................................................................3-3
Table 3-2. Alarm Summary ..................................................................................................... 3-5
Table 3-3. Factory Settings – Calibration.............................................................................. 3-13
Table 3-4. Factory Settings - General................................................................................... 3-14
Table 3-5. PID Settings – Section Names ............................................................................ 3-15
Table 3-6. PID Settings – Sections Descriptions .................................................................. 3-16
Table 3-7. Measurement Log File Format............................................................................. 3-18
Table 3-8. Calibration Log File Format ................................................................................. 3-19
Table 3-9. Alarm Log File Format ......................................................................................... 3-20
Table 3-10. Average Period Selection .................................................................................... 3-21
Instruction Manual
748467-A
January 2002

LIST OF TABLES

Rosemount Analytical Inc. A Division of Emerson Process Management Contents v
Instruction Manual
748467-A January 2002
Model MicroCEM
vi Contents Rosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
Model MicroCEM

PREFACE

The purpose of this manual is to provide information concerning the components, functions, in­stallation and maintenance of the MicroCEM.
Some sections may describe equipment not used in your configuration. The user should become thoroughly familiar with the operation of this module before operating it. Read this instruction manual completely.

DEFINITIONS

The following definitions apply to DANGERS, WARNINGS, CAUTIONS and NOTES found throughout this publication.
DANGER .
Highlights the presence of a hazard which will cause severe personal injury, death, or substantial property damage if the warning is ignored.
748467-A
January 2002
WARNING .
Highlights an operation or maintenance procedure, practice, condition, statement, etc. If not
strictly observed, could result in injury, death, or long-term health hazards of personnel.
CAUTION.
Highlights an operation or maintenance procedure, practice, condition, statement, etc. If not strictly observed, could result in damage to or destruction of equipment, or loss of effectiveness.
NOTE
Highlights an essential operating procedure, condition or statement.
Rosemount Analytical Inc. A Division of Emerson Process Management Preface P-1
Instruction Manual
748467-A January 2002
Model MicroCEM

INTENDED USE STATEMENT

The MicroCEM Continuous Emissions Monitor is intended for use as an industrial process meas­urement device only. It is not intended for use in medical, diagnostic, or life support applications, and no independent agency certifications or approvals are to be implied as covering such applica­tions.

SAFETY SUMMARY

If this equipment is used in a manner not specified in these instructions, protective systems may be impaired.
AUTHORIZED PERSONNEL
To avoid explosion, loss of life, personal injury and damage to this equipment and on-site property, do not operate or service this instrument before reading and understanding this instruction manual and receiving appropriate training. Save these instructions.
DANGER.
ELECTRICAL SHOCK HAZARD
Do not open while energized. Installation requires access to live parts which can cause death or serious injury.
For safety and proper performance this instrument must be connected to a properly grounded three-wire source of power.
DANGER.
POSSIBLE EXPLOSION HAZARD
Do not operate without covers secure. Ensure that all gas connections are made as labeled and are leak free. Improper gas connections could result in explosion and death.
P-2 Preface Rosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
Model MicroCEM
DANGER.
TOXIC GAS
This device may contain explosive, toxic or unhealthy gas components. Before cleaning or chang­ing parts in the gas paths, purge the gas lines with ambient air or nitrogen.
This unit’s exhaust may contain hydrocarbons and other toxic gases such as carbon monoxide. Carbon monoxide is highly toxic and can cause headache, nausea, loss of consciousness, and death.
WARNING: TOXIC GAS
Avoid inhalation of the exhaust gases at the exhaust fitting.
Connect exhaust outlet to a safe vent using stainless steel or Teflon line. Check vent line and con­nections for leakage.
Keep all tube fittings tight to avoid leaks. See Sections 2-5 for leak check information.
WARNING.
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January 2002
DEVICE HAZARDOUS AREA CERTIFICATION(S)
Any addition, substitution, or replacement of components installed on or in this device, must be certified to meet the hazardous area classification that the device was certified to prior to any such component addition, substitution, or replacement. In addition, the installation of such device or devices must meet the requirements specified and defined by the hazardous area classification of the unmodified device. Any modifications to the device not meeting these requirements, will void the product certification(s).
WARNING.
PARTS INTEGRITY AND UPGRADES
Tampering with or unauthorized substitution of components may adversely affect the safety of this instrument. Use only factory approved components for repair.
Because of the danger of introducing additional hazards, do not perform any unauthorized modifi­cation to this instrument.
Return the instrument to Rosemount Analytical Customer Service Center. See Section 8.
CAUTION.
PRESSURIZED GAS
This unit requires periodic calibration with a known standard gas. It also may utilizes a pressur­ized carrier gas, such as helium, hydrogen, or nitrogen. See General Precautions for Handling and Storing High Pressure Gas Cylinders, page P-5.
Rosemount Analytical Inc. A Division of Emerson Process Management Preface P-3
Instruction Manual
748467-A January 2002
CAUTION.
HEAVY WEIGHT
Use two persons or a suitable lifting device to move or carry the instrument.
Model MicroCEM
P-4 Preface Rosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
748467-A
Model MicroCEM
January 2002
GENERAL PRECAUTIONS FOR HANDLING AND STORING HIGH
PRESSURE GAS CYLINDERS
Edited from selected paragraphs of the Compressed Gas Association's "Handbook of Compressed Gases" published in 1981
Compressed Gas Association 1235 Jefferson Davis Highway Arlington, Virginia 22202 Used by Permission
1. Never drop cylinders or permit them to strike each other violently.
2. Cylinders may be stored in the open, but in such cases, should be protected against extremes of weather and, to prevent rusting, from the dampness of the ground. Cylinders should be stored in the shade when located in areas where extreme temperatures are prevalent.
3. The valve protection cap should be left on each cylinder until it has been secured against a wall or bench, or placed in a cylinder stand, and is ready to be used.
4. Avoid dragging, rolling, or sliding cylinders, even for a short distance; they should be moved by using a suitable hand-truck.
5. Never tamper with safety devices in valves or cylinders.
6. Do not store full and empty cylinders together. Serious suckback can occur when an empty cylinder is attached to a pressurized system.
7. No part of cylinder should be subjected to a temperature higher than 125°F (52°C). A flame should never be permitted to come in contact with any part of a compressed gas cylinder.
8. Do not place cylinders where they may become part of an electric circuit. When electric arc welding, precautions must be taken to prevent striking an arc against the cylinder.
Rosemount Analytical Inc. A Division of Emerson Process Management Preface P-5
Instruction Manual
748467-A January 2002
Model MicroCEM

DOCUMENTATION

The following MicroCEM instruction materials are available. Contact Customer Service Center or the lo­cal representative to order (See Section 8).
748467 Instruction Manual (this document) 748468 Instruction Manual, MicroCEM Sample Handling System

COMPLIANCES

This product may carry approvals from several certifying agencies. The certification marks appear on the product name-rating plate.
CSA (Pending)
P-6 Preface Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM

DESCRIPTION AND SPECIFICATIONS

1-1 OVERVIEW

The MicroCEM Analyzer Module is designed to continuously determine the concentration of
, CO, and NOx in a flowing gaseous mix-
O
2
ture. The concentration is expressed in per­cent (%) or parts-per-million (PPM).
SECTION 1
Instruction Manual
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January 2002
and oxygen (O2). Some of the NO
NO
2
molecules produced are in an electroni­cally excited state (NO
* where the * re-
2
fers to the excitation). These revert to the ground state, with emission of photons (essentially, red light). The reactions in­volved are:
2
The sampled gas is collected from the stack and prepared by the Probe/Sample Handling System for analysis and processing by the Analysis Enclosure. The Analysis Enclosure shall be a standalone, computer-controlled unit, utilizing PC/104 as the system bus.
The MicroCEM is enclosed in a rugged NEMA 4X, IP65 type enclosure, for harsh environ­ment. The analysis enclosure utilizes convec­tion cooling with no air intake and air vents. The analysis enclosure is modular, general purpose and easily expandable. It utilizes in­dustry standard components such as PC/104 boards, and modular signal conditioning mod­ules.

1-2 TYPICAL APPLICATIONS

SCR Emission Compliance per EPA 40 CFR Part 60 Gas Turbines Natural Gas Fired Boilers Process Heaters
NO2 + O3 NO2* + O
2
NO2* NO2 + red light
The sample is continuously passed through a heated bed of vitreous carbon, in which NO
is reduced to NO. Any NO
2
initially present in the sample passes through the converter unchanged, and any NO
is converted to an approximately
2
equivalent (95%) amount of NO.
The NO is quantitatively converted to NO by gas-phase oxidation with molecular ozone produced within the analyzer form air supplied by an external source. During the reaction, approximately 10% of the NO
molecules are elevated to an elec-
2
tronically excited state, followed by imme­diate decay to the non-excited state, accompanied by emission of photons. These photons are detected by a photo­multiplier tube which produces an output proportional to the concentration of NOx in the sample.
2

1-3 THEORY OF OPERATION

To minimize system response time, an internal sample bypass feature provides
a. Chemiluminescense NO
X
high-velocity sample flow through the
analyzer. The NOx analyzer continuously analyzes a flowing gas sample for NOx [nitric oxide (NO) plus nitrogen dioxide (NO
)]. The
2
sum of the concentrations is continuously reported as NOx.

b. Non-Dispersive Infrared (NDIR) CO

The optical bench can selectively meas-
ure multiple components in a compact
design by using a unique dual optical The MicroCEM NOx Analyzer Module uses the chemiluminescense method of detection. This technology is based on NO’s reaction with ozone (O
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-1
) to produce
3
bench design. Depending on the applica-
tion, any two combinations of NDIR chan-
nels can be combined on a single
chopper motor/dual source assembly.
Instruction Manual
748467-A January 2002
Model MicroCEM
Other application-dependent options in­clude a wide range of sample cell materi­als, optical filters and solid state detectors. The NDIR Microflow detector consists of two chambers, measurement and reference with an interconnected path in which an ultra low flow filament sensor is mounted. During operation, a pulsating flow occurs between the two chambers which is dependent upon: sample gas ab­sorption, modulation by the chopper mo­tor and the fill gas of the detector chambers. The gas flow/sensor output is proportional to the measured gas con­centration. The optical bench is further enhanced by a novel “Look-through” de­tector technique. This design allows two detectors to be arranged in series --- ena­bling two different components to be measured on a single optical bench. The optical bench contains a unique eddy cur­rent drive chopper motor and source as­sembly. This design incorporates on board “intelligence” to provide continuous “self test” diagnostics.

c. Paramagnetic O2

measured. The gas-specific wavelengths
of the absorption bands characterize the
type of gas while the strength of the ab-
sorption gives a measure of the concen-
tration of the gas component being
measured.
An optical bench is employed comprising
an infrared light source, two analysis cells
(reference and measurement), a chopper
wheel to alternate the radiation intensity
between the reference and measurement
side, and a photometer detector. The de-
tector signal thus alternates between con-
centration dependent and concentration
independent values. The difference be-
tween the two is a reliable measure of the
concentration of the absorbing gas com-
ponent.
Depending on the gas being measured
and its concentration, one of two different
measuring methods may be used as fol-
lows:
Interference Filter Correlation (IFC)
Method
The determination of oxygen is based on the measurement of the magnetic sus­ceptibility of the sample gas. Oxygen is strongly paramagnetic, while other com­mon gases are not. The detector used is compact, has fast response and a wide dynamic range. The long life cell is corro­sion resistant, heated and may be easily cleaned. It has rugged self-tensioning suspension and is of welded non-glued construction.

1-4 DETECTOR METHODOLOGIES

The MicroCEM can employ up to three differ­ent measuring methods depending on the configuration chosen. The methods are: NDIR, Paramagnetic O and Chemiluminescense.

a. Non-Dispersive Infrared (NDIR)

The non-dispersive infrared method is based on the principle of absorption of in­frared radiation by the sample gas being
, Electrochemical O2,
2
With the IFC method the analysis cell is
alternately illuminated with filtered infrared
concentrated in one of two spectrally
separated wavelength ranges. One of
these two wavelength bands is chosen to
coincide with an absorption band of the
sample gas and the other is chosen such
that none of the gas constituents ex-
pected to be encountered in practice ab-
sorbs anywhere within the band.
The spectral transmittance curves of the
interference filters used in the MicroCEM
analyzer and the spectral absorption of
the gases CO and CO
ure 1-1. It can be seen that the absorption
bands of these gases each coincide with
the passbands of one of the interference
filters. The forth interference filter, used
for generating a reference signal, has its
passband in a spectral region where none
of these gases absorb. Most of the other
gases of interest also do not absorb within
the passband of this reference filter.
are shown in Fig-
2
1-2 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
The signal generation is accomplished with a pyroelectrical (solid-state) detector. The detector records the incoming infra­red radiation. This radiation is reduced by the absorption of the gas at the corre­sponding wavelengths. By comparing the measurement and reference wavelength, an alternating voltage signal is produced. This signal results from the cooling and heating of the pyroelectric detector mate­rial.
Instruction Manual
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January 2002
CO
2
Transmittance (%)
0 15 30 54 60 75 90
Transmittance (%)
0 18 36 54 72 90
3000 3200 3400 3600 3800 4000 4200 4400 4600 4800 5000 5200 5400 5600
HC CO2 CO
Reference
Wave Length (nm)
CO
Absorption Band
Figure 1-1. Absorption Bands of Sample Gas and Transmittance of Interference Filters
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-3
Instruction Manual
748467-A January 2002
Opto-Pneumatic Method
Model MicroCEM
In the opto-pneumatic method, a thermal radiator generates the infrared radiation which passes through the chopper wheel. This radiation alternately passes through the filter cell and reaches the measuring and reference side of the analysis cell with equal intensity. After passing another filter cell, the radiation reaches the pneu­matic detector.
The pneumatic detector compares and evaluates the radiation from the measur­ing and reference sides of the analysis cell and converts them into voltage sig­nals proportional to their respective inten­sity.
The pneumatic detector consists of a gas­filled absorption chamber and a compen­sation chamber which are connected by a flow channel in which a Microflow filament sensor is mounted. This is shown in Fig­ure 1-2.
In principle the detector is filled with the infrared active gas to be measured and is only sensitive to this distinct gas with its characteristic absorption spectrum. The absorption chamber is sealed with a win­dow which is transparent for infrared ra­diation. The window is usually Calcium Fluoride (CaF
).
2
When the infrared radiation passes
through the reference side of the analysis
cell into the detector, no pre-absorption
occurs. Thus, the gas inside the absorp-
tion chamber is heated, expands and
some of it passes through the flow chan-
nel into the compensation chamber.
When the infrared radiation passes
through the open measurement side of
the analysis cell into the detector, a part
of it is absorbed depending on the gas
concentration. The gas in the absorption
chamber is, therefore, heated less than in
the case of radiation coming from the ref-
erence side. Absorption chamber gas be-
comes cooler, gas pressure in the
absorption chamber is reduced and some
gas from the compensation chamber
passes through the flow channel into the
absorption chamber.
The flow channel geometry is designed in
such a way that it hardly impedes the gas
flow by restriction. Due to the radiation of
the chopper wheel, the different radiation
intensities lead to periodically repeated
flow pulses within the detector.
The Microflow sensor evaluates these
flow pulses and converts them into elec-
trical pulses which are processed into the
corresponding analyzer output.
Absorption chamber
Flow channel with Microflow sensor
CaF2 Window
Compensation chamber
Figure 1-2. Opto-Pneumatic Gas Detector
1-4 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
Overall NDIR Method
In the case of dual-channel analyzers, the broadband emission from two infrared sources pass through the chopper wheel. In the case of the Interference Filter Cor­relation (IFC) method, the infrared radia­tion then passes through combinations of interference filters. In the case of the opto-pneumatic method, the infrared ra­diation passes through an optical filter
Light Source
Chopper Blade
MOTOR
depending on the application and need for
reduction of influences. Then the infrared
radiation enters the analysis cells from
which it is focused by filter cells onto the
corresponding detector. The preamplifier
detector output signal is then converted
into the analytical results expressed di-
rectly in the appropriate physical concen-
tration units such as percent volume,
ppm, mg/Nm
3
, etc. This is shown in Fig-
ure 1-3.
Duplex Filter Disc
Adapter Cell (high measuring range)
Analysis Cell
(measuring side)
Analysis Cell
(reference side)
Filter Cell
Gas Detector
Analysis Cell (undivided)
Filter Cell
Preamplifier
Pyroelectric Detector (solid-state detector)
Preamplifier
Chopper Blade
Figure 1-3. Overall NDIR Method
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-5
Instruction Manual
748467-A January 2002
Model MicroCEM

b. Paramagnetic Oxygen Method

The paramagnetic principle refers to the induction of a weak magnetic field, paral­lel and proportional to the intensity of a stronger magnetizing field.
The paramagnetic method of determina­tion of oxygen concentration utilizes nitro­gen filled quartz spheres arranged at opposite ends of a bar, the center of which is suspended by and free to rotate on a thin platinum wire ribbon in a cell. Nitrogen (N
) is used because it is dia-
2
magnetic or repelled by a magnet.
A small mirror that reflects a light beam coming from a light source to a photode­tector, is mounted on the platinum ribbon. A strong permanent magnet specifically shaped to produce a strong, highly inho­mogeneous magnetic field inside the analysis cell, is mounted outside the wall of the cell.
When oxygen molecules enter the cell, their paramagnetism will cause them to
be drawn towards the region of greatest
magnetic field strength. The oxygen
molecules thus exert different forces on
the two suspended nitrogen filled quartz
spheres, producing a torque which
causes the mirror to rotate away from its
equilibrium position.
The rotated mirror deflects the incident
light onto the photodetector creating an
electrical signal which is amplified and fed
back to a coil attached to the bar holding
the quartz spheres, forcing the suspended
spheres back to the equilibrium position.
The current required to generate the re-
storing torque to return the quartz bar to
its equilibrium position is a direct measure
of the O
concentration in the sample gas.
2
The complete paramagnetic analysis cell
consists of an analysis chamber, perma-
nent magnet, processing electronics, and
a temperature sensor. The temperature
sensor is used to control a heat ex-
changer to warm the measuring gas to
about 55 °C. Refer to Figure 1-4.
Light
Source
Display
Permanent Magnet
Platinum Wire
Mirror
Quartz Sphere(s)
Wire Loop
Photodetector
Amplifier
Figure 1-4. Paramagnetic Oxygen Analysis
1-6 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002

c. Electrochemical Oxygen Method

The electrochemical method of determin­ing oxygen concentration is based on the galvanic cell principle shown in Figure 1-5.
The electrochemical oxygen sensor (Fig­ure 1-6) incorporates a lead and gold gal­vanic process with a lead anode and a gold cathode, using an acid electrolyte.
Oxygen molecules diffuse through a non­porous Teflon membrane into the electro­chemical cell and are reduced at the gold cathode. Water is the byproduct of this reaction.
On the anode, lead oxide is formed which is transferred into the electrolyte. The lead anode is continuously regenerated and, therefore, the electrode potential remains unchanged for a long time. The rate of diffusion and corresponding response time (t90) of the sensor is dependent on the thickness of the Teflon membrane.
The electric current between the elec-
trodes is proportional to the O
concentra-
2
tion in the sample gas being measured.
The resultant signal is measured as a
voltage across the resistor and thermistor,
the latter of which is used for temperature
compensation. A change in the output
voltage (mV) represents oxygen concen-
tration.
NOTE
The electrochemical O2 cell requires a
minimum internal consumption of
oxygen. Sample gases with an oxygen
concentration of less than 2% could
result in a reversible detuning of sensi-
tivity and the output will become un-
stable. The recommended practice is
to purge the cell with conditioned am-
bient air between periods of measure-
ment. If the oxygen concentration is
below 2% for several hours or days,
the cell must be regenerated for about
one day with ambient air. Temporary
flushing with nitrogen (N
) for less than
2
one hour (analyzer zeroing) will have
no effect on the sensitivity or stability.
(Red) V out (Black)
Thermistor (5) Resistor (6)
(-) (+)
Gold Lead
Cathode (2) Anode (1)
O2 + 4 H + 4 e → 2 H2O2 Pb + 2 H
Electrolyte (3)
(ph 6)
Summary reaction O
+ 2 Pb → 2 PbO
2
O → 2PbO + 4 H + 4 e
2
Figure 1-5. Reaction of Galvanic Cell
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-7
Instruction Manual
748467-A January 2002
Lead Wire (Anode)
Lead Wire (Cathode)
Anode (Lead)
O-Ring
Plastic Disc
Model MicroCEM
Black
Red
Plastic Disk
Resistor
Thermistor
Acid Electrolyte
Sponge Disc
Cathode (Gold Film)
Teflon Membrane
Figure 1-6. Electrochemical Oxygen Sensor
1-8 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002

1-5 CENTRAL PROCESSING UNIT

The CPU is an Embedded Pentium-like AT Computer in 5.75” x 8” form factor. The pe­ripherals integrated on board are: SVGA, 4 serial ports and one parallel port, Fast Ethernet ctrl., IDE, Keyboard, Mouse, 2 USB. The module is built around the Intel Tillamook processor and is equipped with 64MB SDRAM. The module also integrates one socket for SSD that performs like an HDD unit and can be used to store the operating sys­tem, the user’s programs and the data files. Other peripherals available on board are the Floppy disk controller, the parallel port. The CPU is shown in Figure 1-7.

a. Embedded Enhanced Bios

Award, 256KB Flash Bios.The Bios is
immediately activated when you first turn
on the system. The Bios reads system
configuratio information in CMOS RAM
and begins the process of checking out
the system.
Figure 1-7. CPU

b. Specifications

Architecture: ................................. PC/AT Compatible
Dimensions: .................................. 5.75” x 8”
Processor: .................................... Intel Tillamook processor - 266MHz
Memory: ........................................ 64 MB SDRAM
Ram/Rom disk: ............................. 1 x 32 pin socket (max. 288MB)
Operating System: ........................ WinNT
BIOS: ............................................ Standard with embedded extensions
Interfaces: ..................................... IDE ctrl
Floppy ctrl SVGA-CRT 10/100 Mbps Fast Ethernet 2 USB ports 4 RS232 serial ports (one can be 485) Parallel port (bi-directional EPP-ECP) Keyboard PS/2 Mouse PS/2
Bus: .............................................. AT bus according to PC/104 spec.
Power Supply: .............................. AT/ATX
Connectors: .................................. COM1-4, SVGA, USB 1 and 2, PS/2 Mouse/Keyboard, ATX Power,
Parallel, IDE, Floppy, and Fast Ethernet
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-9
Instruction Manual
748467-A January 2002

1-6 ANALOG/DIGITAL I/O BOARD

The Analog/Digital IO (ADIO) Board is an off­the-shelf, complete data acquisition system in a compact PC/104 packaging. The analog section contains 32 input channels, multi­plexed A/D converter with 16 bit resolution and 10uS conversion time. Input ranges are +/-5v or +/- 10V. It also includes on-board DMA support. The analog output section in­cludes two 12 bit D/A converters. Both sec­tions features simplified calibration using on board programmable digital potentiometer. The digital I/O section provides 24 digital I/O lines, which feature high current TTL drivers. The board requires only +5V from the system power supply and generates its own +/-15V analog supplies on board. The board operates over the Extended Temperatures range of -25 to +85C. Figure 1-8 depicts the ADIO board and Figure 1-9 depicts the ADIO block dia­gram.
Model MicroCEM

a. Automatic Calibration

The ADIO board features automatic cali-
bration of both analog inputs and outputs
for enhanced accuracy and reliability. The
potentiometers, which are subject to tam-
pering and vibration, have been elimi-
nated. Instead, all A/D calibration
adjustments are performed using an octal
8-bit DAC. The DAC values are stored in
an EEPROM and are recalled automati-
cally on power up. The board includes
three precision voltage references for
negative full scale, zero, and positive full-
scale. A calibration utility program pro-
vided with the board allows you to recali-
brate the board anytime, in both unipolar
and bipolar modes, and store the new
settings in EEPROM.
Autocalibration applies to the 4 D/A chan-
nels as well. The full-scale D/A range is
selected with a jumper block. The analog
outputs are fed back to the A/D converter
so they can be calibrated without user in-
tervention. Again, calibration settings are
stored in EEPROM and automatically re-
called on power-up.
Figure 1-8. ADIO Board

b. Analog Inputs

The ADIO board provides split configura-
tion capability, with more total input chan-
nels than any other PC/104 analog I/O
board. The board can be user-configured
in any of three ways:
Channels Format
32 32 single-ended 24 8 differential, 16 single-ended 16 16 differential
1-10 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002

c. Programmable Input Ranges

A programmable gain amplifier, pro­grammable unipolar/bipolar range, and programmable 5V/10V full-scale range combine to give the ADIO board a total of 10 different possible analog input ranges. All range settings are controlled in soft­ware for maximum flexibility.
Mode
Unipolar 10V 1 0-10V 0.153mV Unipolar 5V 1 0-5V 0.076mV Unipolar 5V 2 0-2.5V 0.038mV Unipolar 5V 4 0-1.25V 0.019mV Unipolar 5V 8 0-0.625V 0.0096mV Bipolar 10V 1 ±10V 0.305mV Bipolar 5V 1 ±5V 0.153mV Bipolar 5V 2 ±2.5V 0.076mV Bipolar 5V 4 ±1.25V 0.038mV Bipolar 5V 8 ±0.625V 0.019mV
d. Enhanced Trigger and Sampling Con-
Full-
scale
trol Signals
The ADIO board has an extra A/D trigger and sample control signals in the design. Seven auxiliary digital I/O lines on the analog I/O connector provide a sam­ple/hold output signal, A/D trigger in and out lines (to enable synchronization of multiple boards) and external A/D clock­ing.
Gain
Input
Range
Resolution

e. Analog Outputs

The ADIO board contains 4 12-bit analog
outputs with autocalibration capability. Up
to 5mA of output current per channel can
be drawn from all channels simultane-
ously. Both unipolar and bipolar output
ranges are supported with jumper con-
figuration. And on power up, all outputs
are reset to 0V automatically.
Mode
Unipolar 10V 0-10V 2.44mV Unipolar 5V 0-5V 1.22mV
Bipolar 10V ±10V 4.88mV
Bipolar 5V ±5V 2.44mV

f. FIFO and 16-Bit Bus Interface

An on-board 1024-byte FIFO enables the
ADIO board to work with Windows 95 and
NT by dramatically reducing the interrupt
overhead. Each interrupt transfers 256 2-
byte samples, or half the buffer, so the
interrupt rate is 1/256 the sample rate.
FIFO operation can be disabled at slow
sample rates, so there is no lag time be-
tween sampling and data availability. The
16-bit interface further reduces software
overhead by enabling all 16 A/D bits to be
read in a single instruction, instead of re-
quiring 2 8-bit read operations. The net
result of this streamlined design is that the
ADIO board supports gap-free A/D sam-
pling at rates up to 200,000 samples per
second, twice as fast as our previous
boards.
Full-
scale
Output
Range
Resolution
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-11
Instruction Manual
748467-A January 2002
Model MicroCEM
+15V -15V
DC/DC
+15V
ADDR
CTRL
16-BIT DATA
AUTOCALIBRATION
CIRCUIT
1K X8
FIFO
MASTER
CONTROLLER
8255 CIRCUIT
16-BIT A/D
CONVERTER
X1,2,4,8
PROGRAMMABLE GAIN AMP
12-BIT A/D
CONVERTERS
82C54
COUNTER/TIMER
10 MHZ
OSCILLATOR
INPUT MUX
HIGH CURRENT
DRIVE
ANALOG
INPUTS
0-31 SE 0-15 DI
ANALOG OUTPUTS 0-3
TIMING AND CONTROL SIGNALS
24 DIGITAL I/O
PC/104
BUS
Figure 1-9. ADIO Block Diagram
BUFFER
BUFFER
BUFFER
BUFFER
PORT A
PORT B
PORT CH
PORT CL
ACK/STROBE
1-12 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM

g. Specifications

Analog Inputs
Number of inputs ................... 32 single-ended, 16 differential, or 16 SE + 8 DI; user selectable
A/D resolution ........................ 16 bits (1/65,536 of full scale)
Bipolar ranges ....................... ±10V, ±5V, ±2.5V, ±1.25V, ±0.625V
Unipolar ranges ..................... 0-10V, 0-5V, 0-2.5V, 0-1.25V, 0-.625V,
Input bias current................... 100pA max
Overvoltage protection .......... ±35V on any analog input without damage
Nonlinearity............................ ±3LSB, no missing codes
Conversion rate ..................... 200,000 samples/sec.max
On-board FIFO ...................... 1K x 8(512 16-bit samples)
Calibration.............................. Automatic;values stored in EEPROM
Analog Outputs
Number of outputs ................. 4
D/A resolution ........................ 12 bits (1/4096 of full scale)
Output ranges........................ ±5, ±10, 0-5, 0-10
Output current........................ ±5mA max per channel
Settling time........................... 6µS max to 0.01%
Relative accuracy .................. ±1 LSB
Nonlinearity............................ ±1 LSB, monotonic
Reset ..................................... All channels reset to OV
Calibration.............................. Automatic; values stored in EEPROM
Digital I/O
Main I/O ................................. 24 programmable I/O
Input current........................... ±1µA max
Output current........................
Logic 0 ................................... 64mA max per line
Logic 1 ................................... -15mA max per line
Auxilary I/O ............................ 4 inputs, 4 outputs, optional use as trigger/control lines
Instruction Manual
748467-A
January 2002
Counter/Timers
A/D Pacer clock ..................... 32-bit down counter
(2 82C54 counters cascaded)
Clock source.......................... 10MHz on-board clock or external signal
General purpose.................... 16-bit down counter (1 82C54 counter)
General
Power supply ......................... +5VD±10%@200mA typ
Operating temperature .......... -25 to +85°C
Weight.................................... 3.4oz/96g
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-13
Instruction Manual
748467-A January 2002
Model MicroCEM

1-7 PCMCIA ADAPTER

The PCMCIA adapter board (Figure 1-10) supports Type I, II and III PCMCIA cards. The board is in full compliance with Microsoft FFS­II, PCMCIA V.2 and JEIDA 4.1 specifications. The PCMCIA socket accepts The following PCMCIA cards:
Type I Memory, Flash/SRAM/ROM
Type II Fax, Modem, LAN, Wireless LAN,
and SCSI
Type III ATA mass storage

a. Features

Dimensions
Compliant with the PC/104 standard Compatible with AT PC/104 CPU mod­ules
Functions on board
2 PCMCIA slots
Optional remote socket
PCMCIA features
Supports PCMCIA V.1.0 and V.2.0 Supports PCMCIA types I, II and III Supports both I/O and Memory Card Supports Hot insertion
Operating Systems
DOS and Windows and any other RTOS that supports PCMCIA
Connectors
J1 : PCMCIA 2 slots connector J3: PC/104 8 bit connector (XT compati­ble) J4 : PC/104 16 bit extension (AT exten­sion compatible).
Figure 1-10. PCMCIA Interface

b. Software

Software mappable memory windows and one I/O window.
Jumperless interrupt steering from PC Card to system.
Complete set of device drivers complying with PCMCIA V2.1 /JEIDA V4.1, running under MS-DOS or MS-WINDOWS:
PCMCIA socket & card services drivers
Flash File System
1-14 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM

1-8 MODEM

Instruction Manual
748467-A
January 2002
The PC/104 Modular Modem is a self­contained modem module that provides the flexibility to include modem functionality into embedded system, with minimal engineering resources. The PC/104 Modular Modem is full featured including high-speed data and fax transmission. The PC/104 Modular Modems support both dial-up and 2-wire leased-line. Figure 1-11 depicts the Modem.

a. Features

V.90, 56 kbps data (560PC/104) V.34, 33.6 kbps data (336PC/104)
14.4 kbps fax Voice playback and record DTMF decode
-40oC to 85oC operation
3.775" x 3.550" x 0.568" (with modular phone jack)
3.775" x 3.550" x 0.435" (without modular phone jack)
8 bit PC/104 bus type V.42 and MNP 2-4 error correction V.42bis, and MNP-5 data compression FCC Part 68 registered FCC Part 15 compliant 2 wire leased-line and dial up support Industry Canada CS-03 certified
Figure 1-11. Modem
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-15
Instruction Manual
748467-A January 2002

1-9 FLASH DRIVE

Model MicroCEM
Figure 1-12. 128MB Flash Drive

a. Specifications

System Performance
All values quoted are typical at ambient temperature and nominal supply voltage unless otherwise stated.
All performance timing assumes the controller is in the default (i.e., fastest) mode.
Start-up Time
Sleep to Write................................ 2.5 msec max.
Sleep To Read .............................. 2.5 msec max.
Reset to Ready.............................. 50 msec typical, 400 msec max.
Data Transfer Rate
to/from host............................ 16.0 MB/sec burst
Active to Sleep Delay .................... Programmable
Controller Overhead
Command to DRQ ................. <1.25 msec
Power Requirements
All values quoted are typical at ambient temperature and nominal supply voltage unless otherwise stated.
DC Input Voltage
Commercial ................................... 3.3 V ± 5%, 5 V ± 10%
Industrial ........................................ 3.3 V ± 5%, 5 V ± 5%
1-16 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Power Dissipation
Sleep mode currently is specified under the condition that all card inputs are static CMOS levels and in a "Not Busy" operating state.
The currents specified show the bounds of programmability of the product.
Sleep ............................................. 200 µA @3.3 V 500 µA @5.0 V
Read .............................................. 35 mA RMS @3.3 V 50 mA RMS @5.0 V
Write .............................................. 35 mA RMS @3.3 V 50 mA RMS @5.0 V
Environmental Specifications
Temperature
Operating Commercial .......... 0°C to 60°C
Operating Industrial .............. -40°C to 85°C
Non-Operating Commercial .. -25°C to 85°C
Non-Operating Industrial ...... -50°C to 100°C
Humidity
Operating............................... 8% to 95%, non-condensing
Non-Operating ...................... 8% to 95%, non-condensing
Acoustic Noise ...................... 0dB
Vibration
Operating............................... 15 G peak to peak max.
Non-Operating ...................... 15 G peak to peak max.
Shock
Operating............................... 1,000 G max.
Non-Operating ....................... 1,000 G max.
Instruction Manual
748467-A
January 2002
Altitude (relative to sea level)
Operating/Non-Operating ..... 80,000 feet max.
System Reliability and Maintenance
MTBF1 ................................... >1,000,000 hours
Preventive Maintenance ....... None
Data Reliability ...................... <1 non-recoverable error in 10
(14)
bits read
Physical Specifications
Length............................................ 100.2mm ± 0.51mm
Width ............................................. 69.85mm ± 0.51mm
Thickness (Body) .......................... 9.6mm ± 5.0mm
Thickness (Removable Edge) ....... N/A
Weight ........................................... 160 g. max
1
Mean Time Between Failures
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-17
Instruction Manual
748467-A January 2002

1-10 POCKET PC

The Pocket PC acts as an Graphic User Interface to the MicroCEM unit.

a. Specifications

Processor ..................................... 133MHz 32-bit Hitachi SH3 processor
Memory ......................................... 32MB RAM, 16MB ROM
Display .......................................... 240 x 320 pixels LCD, Rich-color CSTN, backlit
User Interface ............................... Pen-and-touch interface (stylus included)
Handwriting recognition software On-screen keyboard 4 user-configurable quick launch screen icons 2 quick keys (Record and Scroll/Action) Notification LED
Power ........................................... Built-in Lithium-Ion rechargeable battery
8 hours of battery life 1 Worldwide auto-voltage AC adapter
Input/Output .................................. IrDA infrared port
RS232 serial port USB port
Compact Flash Type I card slot
AC input jack Stereo earphone jack
Sound ........................................... Audio speaker and microphone
Built-in voice recorder Digital audio player compatible
Other Standard Features............... USB cradle
Serial cable
Earphones Removable metal cover Password protected and DMI compatible
Dimensions ................................... 5.2 × 3.1 × 0.6 in (13 × 7.8 × 1.6 cm)
Weight .......................................... 9.1 oz (260 g) with battery
Operating Temperature ................. 32–104° F (0–40° C)
Storage Temperature ................... 32–140° F (0–60° C)
Humidity......................................... 90% relative humidity at 104° F (40° C)
Model MicroCEM
Figure 1-13. Pocket PC
1-18 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
Model MicroCEM

1-11 WIRELESS LAN ADAPTER

Wireless LAN adapter is an option to allow the user to remove the Pocket PC from the enclosure and to operate the MicroCEM from a distance up to 1000 feet. Figure 1-14 depicts the wireless LAN adapter.
Figure 1-14. Wireless LAN Adapter

a. Specifications

Data Rate ...................................... 11 Mbps send/receive with automatic fallback for extended range
Useful Range................................. Up to 1000 feet (300 meters) open field; 300 feet (90 meters) typi-
cal indoor installations (intervening metal and thick concrete struc­tures degrade performance and range)
Security.......................................... Supports Wired Equivalent Privacy (WEP) which provides 64-bit
and 128-bit data encryption; additional security through the use of a 32-character network system ID
Standard Support .......................... Interoperable with 2 Mbps IEEE 802.11 Direct Sequence Spread
Spectrum (DSSS) and 802.11b (11 and 5.5 Mbps) extension
OS Support.................................... NDIS drivers included for Windows 95, 98, ME and NT and 2000
Channels ....................................... Supports 11 US/Canada and 13 ETSI selectable, fully-independent
channels
Transmit Power ............................. 25mW typical
Radio Frequency ........................... 2.4 to 2.4835 GHz
748467-A
January 2002
Power Requirement....................... PC Card: 5 VDC @ 217 mA average with 338 mA maximum on
transmit; 215 mA continuous receive, 17 mA standby
PCI: 5VDC @ 247 mA average with 368 mA maximum on transmit;
245 mA continuous receive, 47 mA standby
Status lights ................................... 1 (Reports: Link, Power)
Regulatory Approval...................... US - FCC part 15B and 15C, IC RSS-210
ETSI - FCC part 15B, CE, ETS 300 328, ETS 300 826, C-Tick
(Australia)
Physical Specification.................... PC Card: PCMCIA Type II PC Card
PCI: 32-bit, 5V Key, Full Plug-N-Play
Antenna(s) ..................................... Integrated: Printed dual diversity
External: 2.2dBi dipole; additional options for specific installation
needs
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-19
Instruction Manual
748467-A January 2002

1-12 500 WATTS POWER SUPPLY

The 500 Watts power supply combine high performance midrange power with high power density (4.4
3
watts/in cial and industrial systems. Providing tightly regulated DC power, the power supply delivers full output per­formance with only 300 Linear Feet per Minute (LFM) forced air-cooling by utilizing a factory installed fan. Other features include remote sense, power fail, logic level inhibit, DC power good. Main channel current sharing is provided for redundant applications. The power supply is approved to the latest international regulatory standards, and displays the CE Mark.
),active Power Factor Correction (PFC) and high reliability to meet the requirements of commer-
Model MicroCEM
Figure 1-15. 500 Watts Power Supply

a. Features

Power Factor Correction (PFC) Meets EN61000-3-2
Fully Regulated Outputs
Remote Sense
Current Share, Power Fail, and Power Good Signals
Overtemperature, Overvoltage, and Overcurrent Protected
Available with Metric or SAE Mountings
Input Transient & ESD Compliance to EN61000-4-2/-3/-4/-5
Fan Output Voltage and Optional Fan
Optional Isolation Diodes for Parallel or Redundant Operation
1-20 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM

1-13 MicroCEM SPECIFICATIONS

a. Analyzer

Power ............................................ Universal Power Supply 85 – 264 VAC, 50 – 60 Hz, + 10%, 500
Microprocessor.............................. Intel Pentium processor, 266MHz, 64MB RAM, PC/104 architec-
Pocket PC...................................... 133MHz, 21 bit Hitachi SH3 processor, 32MB RAM 16MB ROM,
Detectors//Number ........................ NDIR, Paramagnetic, Electrochemical, Chemiluminescense// Up to
Mounting........................................ Wall Mount
Area Classification......................... General Purpose / NEMA 4X (IP65) Fiberglass Enclosure
Ambient Range
Temperature ......................... -30° to 50° Celsius.
Relative Humidity................... 5 to 99%
Instruction Manual
748467-A
January 2002
Watts Maximum at Start Up. 250 Watts Nominal
ture, Windows NT embedded Platform
240 X 320 pixels LCD, Riuch color, backlit, Wireless LAN optional
three in one analyzer
Inputs/Outputs
Digital..................................... RS-485 Serial Port. (Multi-Drop Network)
RS-232 Serial Port.
LAN, Ethernet 10/100-BaseT
Modem.
Connectivity Protocols ........... HTML (Web Browser) – Status, file transfer Modem/Webrowser
TCP/IP..Modbus (In Process)
Foundation Fieldbus (In Process)
Analog Current Outputs......... 3 Isolated 4-20 mA DC, 500 ohms Max Load (O2, CO, NOX)
Analog Inputs:MW, Fuel Flow
Digital OutputsTrouble Alarm, Sample Pump on/off, Drain Pump on/off, Purge on/off, Calibrate on/off – 110VAC @ 1amp Dry Con­tact
O2 Limit Exceed, CO Limit Exceed, NOx Limit Exceed, O2 Low
Range, CO Low Range, NO rent 20 mA
Digital Inputs.......................... Process on/off, Initiate Auto Calibration
Instrument Weight ......................... 62 lbs. Typical
Dimensions.................................... 24“ x 20“ x 12“ (HxWxD)
Ranges .......................................... O2: 0 –25%
CO: 0 –100ppm Selectable to 1000ppm
NOX: 0 – 10ppm Selectable to 1000ppm
Sample Temperature..................... 0° C to 55° C
Sample Flow Rate ......................... .5 to 1.5 liters/min
Warm Up Time .............................. Max 25 minutes @ low ambient temperatures
Low Range. - TTL: 5 VDC Max Cur-
X
Rosemount Analytical Inc. A Division of Emerson Process Management Description and Specifications 1-21
Instruction Manual
748467-A January 2002
Model MicroCEM
Electro-
Chemical
O
2
NDIR
CO
Chemiluminescense
Linearity
Zero Drift Span Drift Repeatability Response Time (t90)
Paramagnetic
O2
< ± 1% < ± 1% < ± 1% < ± 1%
< ± 1% /day < ± 1% /day < ± 1% /day < ± 1% /day < ± 1% /day < ± 1% /day < ± 1% /day < ± 1% /day < ± 1% < ± 1% < ± 1% < ± 1%/day
10< ± t90< ±-15 10< ± t90< ± 15 15s< ± t90< ± 20s 15s< ±-t90< ± 20s Influence of Ambient Temperature
(-20°C to 45°C) On Zero On Span
< ± 1% < ± 1%
< ± 1% < ± 1%
< ±-2% < ±-2%

b. Probe/Sample Handling

Power ............................................ Universal Power Supply 85 – 264 VAC, 50 – 60 Hz, + 10%
500 Watts Maximum at Start Up. 250 Watts Nominal
Mounting........................................ Wall Mount
Area Classification......................... General Purpose / NEMA 4X (IP65) Fiberglass Enclosure
Ambient Range
Temperature .......................... -30° to 50° Celsius
Relative Humidity................... 5 to 99%
NO
1
< ±-2% < ±-2%
X
1
1
1
Instrument Weight ......................... 75 lbs. Typical
Dimensions.................................... 24“ x 24“ x 12“ (HxWxD)
Stack Sample Moisture ................. Up to 25%
Sample Cooler............................... Thermo Electric dual pass Chiller.
Max. Stack Temperature ............... 500° F (Higher temperatures available by utilizing elongated
Stack Pressure .............................. -5 to 15 inches H2O
Sample Flow Rate ......................... 1 L/min from sample handling enclosure to Analysis enclosure
Response Time (Max distance between Analysis Enclosure and Sample Conditioning/Probe)
Probe Length................................. 48" length 316 SS Probe with .5 micron sintered filter. (Customer
Mounting Flange............................ Optional 4“ 150#
Sample Pump................................ 316 SS diaphragm type
Instrument Air Requirements......... Instrument grade air required. 15 SCFM @ 60 -100 PSIG (30 sec-
1
0-10ppm NOx range is <± 3%.
Permeation Tube (-30° C) dewpoint. Customer instrument air required @ 5 L/M, -40° C dewpoint
spools)
Enclosure is 300'. (Response time is 20 seconds/100' w/1/4" tub-
ing).
to cut to length in field.)
onds 2 times per day). (Pressure Regulation by Customer.)
1-22 Description and Specifications Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
SECTION 2

INSTALLATION

WARNING
ELECTRICAL SHOCK HAZARD
POSSIBLE EXPLOSION HAZARD
Do not open while energized. Do not op­erate without doors and covers secure. Installation requires access to live parts which can cause death or serious injury.
DANGER.
ELECTRICAL SHOCK HAZARD
Installation and servicing of this device re­quires access to components that may present electrical shock and/or mechanical hazards. Refer installation and servicing to qualified service personnel.
CAUTION.
CODE COMPLIANCE
Installation of this device must be made in accordance with all applicable national and/or local codes. See specific refer­ences on the installation drawing located in the rear of this manual.
CAUTION.

2-1 OVERVIEW

a. Limitations

Ambient Temperature:-30° to 50° Celsius (-4° to 122° F)
Relative Humidity:5% to 99%

b. Mounting Options

Although the MicroCEM is enclosed in an environmentally sealed enclosure, it should be protected from direct sunlight. In areas subjected to harsh winter cli­mates, protection should be provided from sun, rain and snow. A corrugated awning or other suitable means can be provided to meet these conditions.

2-2 LOCATION

The MicroCEM is designed to be installed in an outdoor environmental location. It is rec­ommended that the analyzer be located out of direct sunlight and direct rain/snow to the ex­tent possible.
The MicroCEM analysis enclosure should be installed as near as possible to the probe/sample handling enclosure, in order to avoid low response time caused by long sam­ple gas lines.
PRESSURIZED GAS
This unit requires periodic calibration with a known standard gas. It also may utilizes a pressurized carrier gas, such as helium, hydrogen, or nitrogen. See General Pre­cautions for Handling and Storing High Pressure Gas Cylinders, page P-5.
Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-1
Instruction Manual
748467-A January 2002
Model MicroCEM
4.3
109.2
SAMPLE
CALIBRATION
GAS 3
GAS 2
GAS 1
OZONE / AIR
VENT
11.6
295.3
4.9
124.5
1.5 TYP
38.1
KEY LOCK
1.1
27.9
17.9
456.9 MOUNTING DIMENSION
20.2
513.1
25.2
640.1
1.1
27.9
HINGE
TYP
24.6
624.8
25.5
647.7 MOUNTING DIMENSION
CLEARANCE HOLE FOR 3/8 BOLT (4 PLACES)
7.1
180.3
4.9
124.5
AC POWER
INPUT
ANALOG
INTERFACE
1.5
38.1
DIGITAL
INTERFACE
TYP
RS232
INTERFACE
LAN
INTERFACE
RS485
INTERFACE
PHONE
ANTENNA
LINE
Figure 2-1. MicroCEM Outline and Mounting Dimensions
2-2 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002

2-3 GASES

NOTE
For external gas lines, the use of new tub­ing throughout is strongly recommended. The preferred type is teflon or stainless steel, sealed at both ends.

a. Connection

Besides sample gas, the MicroCEM re­quires other gases for operation. In most cases, one or more Calibration Standards must be provided. These should be cylin­ders of gas which closely resemble the expected sample, both in species and concentrations. These calibration gases are normally introduced into the system as an input to the Sample Conditioning Plate Option or sample conditioning may be provided by others.
Each gas cylinder should be equipped with a clean, hydrocarbon free two-stage pressure regulator with indicating gauges of approximately 0 to 3000 psig (0 to 20.7 bar) for cylinder pressure and 0 to 100 psig (0 to 6.7 bar) for delivery pressure. Pressure regulators should have a metal­lic as opposed to elastomeric diaphragm, and provide for ¼ inch compression fitting outlet and should be LOX clean.
NOTE
All connections specified in the In­stallation Drawing, in conjunction with the Application Data Sheet, should be made.

b. Conditioning

system is used with corrosive gases, it must be verified that there are no gas components which may damage the gas path components.
The gas conditioning must meet the fol­lowing conditions:
Free of condensable constituents
Free of dust above 2 µm
Free of aggressive constituents which
may damage the gas paths
Temperature and pressure in accor-
dance with the specifications
When analyzing vapors, the dewpoint of the sample gas must be at least 10 °C below the ambient temperature in order to avoid the precipitation of condensate in the gas paths.
An optional barometric pressure compen­sation feature can be supplied. This re­quires a pressure sensor with a range of 800 – 1,100 hPa. The concentration val­ues computer by the detectors will then be corrected to eliminate erroneous measurements due to changes in baro­metric pressure.
The gas flow rate must be in the range of
0.2 l/min to a maximum of 1.5 l/min. A
constant flow rate of 1 l/min is recom­mended.
NOTE
The maximum gas flow rate for par­amagnetic oxygen detectors is 1.0 l/min!
All gases must be supplied to the ana­lyzer as conditioned gases! When the
Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-3
Instruction Manual
748467-A January 2002
Model MicroCEM
SAMPLE
CAL
CAL GAS 3
CAL GAS 2
CAL GAS 1
OZONE AIR
EXHAUST
3-WAY VALVE
2-WAY VALVE
MANIFOLD
ASSEMBLY
Figure 2-2. MicroCEM Gas Connections
IN
FLOWMETER
W/VALVE
GAUGE
638614
REGULATOR 904017
OZONE GENERATOR
659494
NDIR DETECTOR
90003225
PARAMAGNETIC
DETECTOR
90003311
CAPILLARY
VENT
634398
OUT
CONVERTER
656715
DETECTOR
659754
Figure 2-3. MicroCEM Flow Diagram
2-4 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Sample Inlet ½” FPT
Stack
Sample
Sample Handling System
Power In 115 VAC 60Hz 5A
Instruction Manual
748467-A
January 2002
MicroCEM Analyzer
Instrument Air
¼” Teflon tubing. Customer supplied.
3
Drain to safe location.
2
Customer supplied.
1
3
2
Atmospheric Pressure
Calibration Line to Analyzer
3
Sample From Analyzer
Dry Contact Initiate Auto Calibration
O2 / NO
Mid Range
1
High Range
O2 / NO
1
Nitrogen
Electrical connections. See Section 2-4 and Figure 2-5.
Figure 2-4. MicroCEM Installation and Test Setup Configuration
Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-5
Instruction Manual
748467-A January 2002

2-4 ELECTRICAL CONNECTIONS

NOTE
The enclosure is a NEMA 4. All entry loca­tions must be sealed.
Connect all required signal cables to the con­nections at the bottom of the MicroCEM. The cable locations are indicated on the inside bottom cover of the MicroCEM box. The ac-
Model MicroCEM
tual electrical connections will be specified in the Application Data package. All connections are not necessary for every application.
Cable length for these signals should not ex­ceed 3,000 feet (914 meters), to avoid exces­sive capacitance and corresponding signal distortion.
All electrical connections are made through the bottom of the MicroCEM enclosure using circular connectors.
AC POWER
INPUT
ANALOG
INTERFACE
DIGITAL
INTERFACE
RS232
INTERFACE
LAN
INTERFACE
RS485
INTERFACE
PHONE
LINE
AC POWER INPUT – J1 LAN INTERFACE – J5 ANALOG INTERFACE – J2 RS485 INTERFACE – J6 DIGITAL INTERFACE – J3 PHONE LINE – J7 RS232 INTERFACE - J4 ANTENNA – J8
Figure 2-5. MicroCEM Electrical Connections
ANTENNA
2-6 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
(
(
(
(
(
(
5
A
/O
Instruction Manual
748467-A
January 2002
EXTERNAL
CONNECTIONS
A21
INTERNAL PANEL
CONNECTIONS
AND FUNCTIONS
A20
DIGITAL
ANALOG
ANTENN
RS232
LAN
RS485
PHONE
AC IN
CIRCUIT
BREAKER
6A
+5V
RS232
TROUBLE
HEARTBEAT
J3
J2
J8
J4
J5
J6
J7
J1
CB1
PRIMARY
POWER
SUPPLY A1
J17 POCKET PC
J11
DS1 (RED)
DS2 (GRN)
24VDC
MODEM
A5
J9
PC-104
CN8
CPU
A4
CN16C
CN15
CN16B
PC-104
POWER
CN16A
EXIO
A22
J2
J3
2
O
CO
ADIO
BACKPLANE
A3
J3
J4
DIGITAL
ANALOG
I
A2
P5
P4
P1
P2
P3
NOx
2
O
CO NOx
2
O CO NOx
4-20mA CURR LOOP 1 4-20mA CURR LOOP 2
SAMPLE PUMP DRAIN PUMP PURGE VALVE CALIBRATION VALVE
AUX
A23
J28
J38
PELTIER POWER J1
J18
FAN POWER J2
J5
TEMP SENSOR
J2
TEMP SENSOR
J1
J48
SPAN VALVE MID VALVE ZERO VALVE
J3
SAMPLE VALVE
PMD
A24
J1
2
INPUT SENSOR P1
O
TEMP SENSOR P1
J2
NDIR
A25
J3
STEPPER MOTOR P 5
LIGHT BARRIER SYNC P2
J18
CO SIGNAL P1
J2
LIGHT SOURCE P4
J28
TEMP SENSOR P3
J4
PDD A2
SAMPLE PRESS LIMIT
OZONE PRESSURE
PHOTODIODE J1
J1
THERMAL SWITCH J8
J28
TEMP SENSOR/HTR J8
J2
J3
CONVERTER HTR J4
J38
TEMP SENSOR J9
J4
THERMAL SWITCH
J38
INT) J3 EXT) J4
SV3) J3
SV2) J2
SV1) J1
SV4) J1
J10
AXX
DIAGNOSTIC OUTPUT
VOLTAGE
AXX
4-20 mA
CURRENT LOOPS
AXX
LOW RANGE
READING
AXX
OVER LIMIT
INDICATOR
AXX
PLC
AXX
TROUBLE
AXX
EXTERNAL SWITCH -
INITIATE CALIBRATION
AXX
EXTERNAL PROCESS
FROM CUSTOMER
AXX
PUMP CONTROL
A17
MOISTURE DE TECTOR
A17
BAROMETRIC
PRESSURE
A9
ZONE HEATER
(PELTIER)
A10
SYSTEM HEARTBEAT
INDICATOR
A11
VALVES
MANIFOLD
ASSEMBLY
A12
CALIBRATION VALVE
ASSEMBLY
A8
ELECTROCHEMICAL
DETECTOR
(PMD OPTION)
A8
NDIR
DETECTOR
CO
A18
SAMPLE PRESSURE
SENSOR
A16
OZONE PRESSURE
SENSOR
A7
PHOTODIODE
DETECTOR
A14
HI VOLTAG E
PWR SUP -1.7KV
A15
CONVERTER
ASSEMBLY
A13
OZONATOR
Figure 2-6. MicroCEM Wiring Diagram
Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-7
Instruction Manual
 
748467-A January 2002
Model MicroCEM

a. AC Power

Connect AC power through a 10A circuit breaker that is to be located close to the MicroCEM. The circuit breaker will pro­vide over current protection as well as a means of disconnecting the power.
Maximum power requirements will be 380 watts, with most applications requiring less than this amount.
b. Circular Connector Assembly Instruc-
tions
Wire Stripping
Strip insulation from end of wire to be crimped. Do not cut or damage wire strands. Refer to table for proper strip­ping dimensions.
A
2. Using correct crimp tool and locator, cycle the tool once to be sure the in­dentors are open. Insert contact and wire into locator. Squeeze tool han­dles firmly and completely to insure a proper crimp. The tool will not re­lease unless the crimp indentors in the tool head have been fully actu­ated.
Wire Size Dim. A
22O or 22M* .125 (3.18)
20 .188 (4.77) 16 .188 (4.77)
12 .188 (4.77) *Inactive. Not recommended for new design, replacement only.
Contact Crimping
1. Insert stripped wire into contact crimp pot. Wire must be visible through in­spection hole.
Visual Inspection Hole
3. Release crimped contact and wire from tool. Be certain the wire is visi­ble through inspection hole in contact.
2-8 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
Contact Insertion
1. Remove hardware from plug or re­ceptacle and slip over wire bundle in proper order for reassembly.
2. Using proper plastic or metal insertion tool for corresponding contact, posi­tion wire in tip of the tool so that the tool tip butts up against the contact shoulder.
3. Press tool against contact shoulder and, with firm and even pressure, in­sert wired contact and tool tip into center contact cavity. A slight click may be heard as metal retaining tines snap into place behind contact shoul­der.
4. Remove tool and pull back lightly on wire to make sure contact is properly seated. Repeat operation with re­mainder of contacts to be inserted, beginning with the center cavity and working outward in alternating rows.
5. After all contacts are inserted, fill any empty cavities with wire sealing plugs. Reassemble plug or receptacle hard­ware.
Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-9
Instruction Manual
748467-A January 2002
Contact Extraction
1. Remove hardware from plug or re­ceptacle and slide hardware back along wire bundle.
Model MicroCEM
4. Hold wire firmly in tool and extract wired contact and tool. Repeat op­eration for all contacts to be ex­tracted.
2. Using plastic or metal extraction tool with proper color code corresponding to contact size, place wire in tool.
3. Insert tool into contact cavity until tool tip bottoms against the contact shoul­der, expanding clip retaining tines.
5. Fill any empty wire cavities with wire sealing plugs.
6. Reassembly plug or receptacle.
2-10 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM

c. Interface Connections

Instruction Manual
748467-A
January 2002
Connection Designator
AC Power J1 12 3 16 Table 2-2
Analog Interface J2 12 22 26, 24, 22 Table 2-3
Digital Interface J3 14 37 26, 24, 22 Table 2-4
RS232 J4 10 13 28, 26, 24 Table 2-5
LAN Interface J5 8 6 28, 26, 24, 22 Table 2-7
RS485 J6 8 3 24, 22, 20 Table 2-6
Phone Line (Modem) J7 8 3 24, 22, 20 Table 2-8
Antenna (Peltier Power) J8 16 3 14, 12 Table 2-9
Table 2-1. Interface Connections
SIGNAL NAME DEFINITION PIN
L1 A L2 GND AC Ground B
Table 2-2. AC Power Connection Terminal Assignments
85-264 VAC, 47-440 Hz
Shell
Size
No.
Contacts
AWG Table
C
SIGNAL NAME DEFINITION PIN
O2CL+ 1
O2CL-
COCL+ 3
COCL-
NOX+ 5
NOX-
EXP1CL+ 7
EXP1CL-
EXP2CL+ 9
EXP2CL­BAROP+ 11
BAROP-

Table 2-3. Analog Output Terminal Assignments

O2 Reading, 4-20 mA Output
CO Reading, 4-20 mA Output
NOX Reading, 4-20 mA Output
External process No. 1, Current Loop input, 4-20 mA
External process No. 2, Current Loop input, 4-20 mA
Barometric pressure Compensator 0-10V input
2
4
6
8
10
12
Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-11
Instruction Manual
748467-A January 2002
SIGNAL NAME DEFINITION PIN
SPUMPNO 1 SPUMPC 2 SPUMPNC DPUMPNO 4 DPUMPC 5 DPUMPNC PURGNO 7 PURGC 8 PURGNC CALNO 10 CALC 11 CALNC TRBLNO 13 TRBLC 14 TRBLNC O2LR+ 16 O2LR­COLR+ 18 COLR­NOxLR+ 20 NOxLR­EXTDIG1+ 22 EXTDIG1­INCAL+ 24 INCAL­O2OL+ 26 O2OL­COOL+ 28 COOL­NOxOL+ 30 NOxOL-
Model MicroCEM
Sample Pump Control, Dry contact, 110V 1A Rating
Drain Pump Control, Dry contact, 110V 1A Rating
Purge Valve Control, Dry contact, 110V 1A Rating
Calibration Valve Control, Dry contact, 110V 1A Rating
Trouble Indicator, Dry contact, 110V 1A Rating
O2 Low Reading Digital output (0=LR)
CO Low Reading Digital output (0=LR)
NOx Low Reading Digital output (0=LR)
Digital Input from External process
Initiate Calibration Switch Input
O2 Over Limit Indicator
CO Over Limit Indicator
NOx Over Limit Indicator
Not Used
3
6
9
12
15
17
19
21
23
25
27
29
31
32-37
Table 2-4. Digital Output Terminal Assignments
2-12 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
SIGNAL NAME DEFINITION PIN
DCD (pin 1) DSR (pin 6) RxD (pin 2) RTS (pin 7) TxD (pin 3) CTS (pin 8) DTR (pin 4) RI (pin 9) GND (pin 5) Signal Ground 9
SIGNAL NAME DEFINITION PIN
TxD/RxD+ (pin 2) A TxD/RxD- (pin 7) GND (pin 3)
Data Carrier Detect Input Data Set Ready Input Receive Data Input Request to Send Output Transmit Data Output Clear To Send Input Data Terminal Ready Output Ring Indicator Input
Not Used
Table 2-5. RS-232 Interface Terminal Assignments
Bi-directional Data
Ground
Instruction Manual
748467-A
January 2002
1 2 3 4 5 6 7 8
10-13
B
C
Table 2-6. RS-485 Terminal Assignments
SIGNAL NAME DEFINITION PIN
TxD+ (pin 1) 1 TxD- (pin 2) RxD+ (pin 3) 3 RxD- (Pin 6)

Table 2-7. LAN Interface Terminal Assignments

SIGNAL NAME DEFINITION PIN
TIP (pin T) A RING (pin R)

Table 2-8. Phone Line (Modem) Terminal Assignments

SIGNAL NAME DEFINITION PIN
Vbb Vbb_rtn Gnd
Transmit Data
Receive Data
Not Used
Modem Interface to Phone Line
Not Used
+24VDC +24V Return GND
5-6
2
4
B
C
A B
C

Table 2-9. Antenna (Peltier Power) Connection Terminal Assignments

Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-13
Instruction Manual
748467-A January 2002
Model MicroCEM

2-5 ANALYTICAL LEAK CHECK

If explosive or hazardous gas samples are being measured with the MicroCEM, it is rec­ommended that gas line fittings and compo­nents be thoroughly leak-checked prior to initial application of electrical power, bimonthly intervals thereafter, and after any mainte­nance which involves breaking the integrity of the sample containment system.

a. Flow Indicator Method

Supply air or inert gas such as nitrogen, at 10 psig (689 hPa), to the analyzer through a flow indicator with a range of 0 to 250 cc/min. Install a shut-off valve at the sample gas outlet. Set the flow rate to 125 cc/min.
Close the outlet shut-off valve and notice that the flow reading drops to zero. If the flow reading does not drop to zero, the system is leaking and must be corrected before the introduction of any flammable sample gas or application of power.
MicroCEM Analyzer
N
2
10 psig
(69 kPa)
Inlet Outlet
Flow Meter
Gas Outlet
Figure 2-7. Leak Test Flow Method
2-14 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002

b. Manometer Method

Install a water-filled U-tube manometer at the sample gas outlet. Install a shut-off valve at the sample gas inlet. Admit air or inert gas to the inlet shut-off valve until the analyzer is pressurized to approxi­mately 50 hPa. The water column will be about 500 mm.
MicroCEM Analyzer
Inlet Outlet
Close the inlet shut-off valve and, follow­ing a brief period for pressure equilibrium, verify that the height of the water column does not drop over a period of about 5 minutes. If the water column height drops, the system is leaking and must be cor­rected before the introduction of any flammable sample gas or application of power.
N
2
Water
Figure 2-8. Leak Test Manometer Method
Overpressure Approx. 50 hPa
Rosemount Analytical Inc. A Division of Emerson Process Management Installation 2-15
Instruction Manual
748467-A January 2002
Model MicroCEM
2-16 Installation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
CAUTION.
Instruction Manual
748467-A
January 2002
SECTION 3

OPERATION

Do not operate or service this instru­ment before reading and understanding this instruction manual and receiving appropriate training.
Refer to installation drawing supplied with the application data package.

3-1 STARTUP PROCEDURE

Once the MicroCEM has been correctly as­sembled and installed in accordance with the instructions in Section 2, the analyzer is ready for operation.
Before operating the system, verify that the leak checks have been performed and that the sample handling unit is performing cor­rectly.
Apply power to the system and verify that sample gas is flowing.
NOTE
A warm-up time of from 15 to 50 minutes is required depending on the installed detector(s).

a. Connecting Pocket PC to MicroCEM

1. Open MicroCEM door. Refer to Figure 3-2.
2. Plug RS232 plug into adapter lo­cated on front panel.
3. Plug power supply cable into 5V adapter
4. Turn Pocket PC on
5. In order to assure no other win­dows are open press the reset button. Reset button is located on the back of the pocket PC.
6. Using the MicroCEM menu click on “programs”
7. Click on “Connection” icon
8. Click on “uCEM” icon.
9. Go to tools menu and click on Mi­croCEM .
10. Unit will display data in 3 to 5 sec­onds.
Analyzer operation can be confirmed on the screen of the pocket PC through the glass window on the door. Upon power up, the analyzer will perform a self-test routine. This test will last approximately 60 sec­onds.

3-2 POCKET PC USER INTERFACE

The MicroCEM User Interface runs on a Pocket-PC with Windows CE operating system. It communicates with the Micro­CEM via serial communication port. All in­put to the Pocket-PC is done using a pointing device that comes with the Pocket­PC.
Rosemount Analytical Inc. A Division of Emerson Process Management Operation 3-1
Figure 3-1. Pocket PC
Instruction Manual
748467-A January 2002
Printer Connector
5V Connector
VGA Connector
RS232 Connector
Model MicroCEM
Flowmeter
Heartbeat LED
Keyboard Connector
Mouse Connector
USB Connector
Reset Button
Floppy Connector
IDE Connector
Figure 3-2. MicroCEM Front Panel
Trouble LED
Power Switch
3-2 Operation Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002

b. Main Display

The MicroCEM Main Display (Figure 3-3) provides the status of the three emissions channels. The status in­cludes the current reading (updated approximately every 2 seconds), the
Drag the edge of the column to resize.
last 1-minute average, and the last 15­minute average. The status column (Sts) indicates the status of the meas­urement and can be any of the values in listed in Table 3-1. (“Status” shown in order of precedence. Maintenance mode status takes highest prece­dence.)
S. = Status See Table 3-1.
Use the scrollbar to see full set of data.
Tools Menu
Provides access to all functionality.
Note: Exit is only be available when current user has administrative access.
Toolbar Buttons About
Data Logs MicroCEM Admin MicroCEM Settings Alarms
Figure 3-3. MicroCEM Pocket PC Display (Main Display Shown)
STATUS DESCRIPTION
M Indicates that maintenance mode is active. C Calibration in process
I Invalid Reading. Indicates that the reading is invalid due to calibration failure or sensor failure. V Valid Reading P Customer Process Off Line (Dry contact by customer)
O MicroCEM System Off
Table 3-1. Status Values
Rosemount Analytical Inc. A Division of Emerson Process Management Operation 3-3
Instruction Manual
748467-A January 2002
Model MicroCEM

c. MicroCEM Menu

Clicking on the Tools text in the lower left corner of the display activates the MicroCEM menu. From this menu, all of the MicroCEM user-interface func­tions can be accessed.

d. MicroCEM Alarms

The MicroCEM Alarms dialog shows all the current alarms. A current alarm is one with an Active status of 1 (active) or an Acknowledged state of 0 (not ac­knowledged).. If the Show Historical Alarms checkbox is checked, all non­current alarms are also shown (non­active acknowledged alarms). Up to 100 alarms will be shown. To see more than the last 100 alarms, the web based MicroCEM interface must be used. If one or more alarms are cur­rent, the most recent of them will be displayed on the main display. If more than one alarm is current “(more)” will be displayed after the name of the most recent alarm on the main window to in­dicate that more than one alarm is ac­tive. Horizontal scroll bar is be used to see Date and Time of the Alarms.
On-screen keyboard is available at any time by clicking on the keyboard button.
Figure 3-4. MicroCEM Menu
Figure 3-5. Pocket PC Alarms Screen
Alarms with a critical level will cause the System trouble output to become active when the alarm is active. When all active critical alarms are acknowl­edged, the System trouble output will become inactive.
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ALARM NAME LEVEL DESCRIPTION
O2 Calibration Failed Critical O2 Calibration Failed to meet the maximum Drift requirements
CO Calibration Failed Critical CO Calibration Failed to meet the maximum Drift requirements
January 2002
NOx Calibration Failed Critical
O2 High Limit Critical O2 Sensor reading is above the minimal acceptable limit
O2 Low Limit Critical O2 Sensor reading is below the minimal acceptable limit
CO High Limit Critical CO Sensor reading is above the minimal acceptable limit
CO Low Limit Critical CO Sensor reading is below the minimal acceptable limit
NOx High Limit Critical NOx Sensor reading is above the minimal acceptable limit
NOx Low Limit Critical NOx Sensor reading is below the minimal acceptable limit
24V Over Max Critical 24V diagnostic input exceeds the specified maximum
24 Low Min Critical 24V diagnostic input is below the specified minimum
O2 Emission Limit Warning O2 reading is over the specified Limit
CO Emission Limit Warning CO reading is over the specified Limit
NOx Emission Limit Warning NOx reading is over the specified Limit
Converter Over Temp Critical
Converter Low Temp Critical Converter temperature reading is below the specified minimum
Zone Over Temp Critical Zone temperature reading exceeds the specified maximum
NOx Calibration Failed to meet the maximum Drift require­ments
Converter temperature reading exceeds the specified maxi­mum
Zone Low Temp Critical Zone temperature reading is below the specified minimum
PDT Over Temp Critical
PDT Low Temp Critical
PMT Over Temp Critical
PMT Low Temp Critical
Warm-up Time Limit Critical System Warm-up process exceeded the specified time limit
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Peltier Cooler (PDT) temperature reading exceeds the speci­fied maximum
Peltier Cooler (PDT) temperature reading is below the specified minimum
PDD Chamber temperature reading exceeds the specified maximum
PDD Chamber temperature reading is below the specified minimum

Table 3-2. Alarm Summary

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e. MicroCEM Login

The login dialog appears (Figure 3-6) when first requesting the MicroCEM Settings or MicroCEM Admin. If a valid user name and password are entered, the user logging in will have permission to use the MicroCEM Settings and/or the MicroCEM Administration (Refer to the User Settings page of the Micro­CEM Settings dialog). After logging in the first time, it is not required again until the user logs out, or is logged out automatically because of a period of in­activity (Refer to the Auto Logout page of the MicroCEM Administration dialog).
f. MicroCEM Login-Current User Indi-
cation
When a user is logged in, the Micro­CEM main display will indicate the user name of the logged in user as shown in Figure 3-7. When the user logs off, the current user and the Logoff button will not be shown.
Current User
Logoff Button
Figure 3-7. Current User Indication
Figure 3-6. MicroCEM Login
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3-3 MicroCEM SETTINGS

The MicroCEM Settings dialog is only available to users with MicroCEM Settings permission. If a user is not currently logged in, the login dialog will be displayed. If the current user doesn’t have MicroCEM Set­tings permission, a message will be dis­played which reads “Permission denied”. When the MicroCEM Settings are invoked from the Tools menu or the MicroCEM Set­tings button, the MicroCEM Settings tabbed dialog is displayed. The Range page (tab) is displayed initially.

a. Range

The Range Settings page is used to set the range of the Emissions analog out­puts. The outputs support dual range mode. When the emission is below the Range 1 value, the output switches to Range 1 mode and the Range 1 value becomes the full-scale value of the out­put. The range indication digital output will change to the Range 1 state. When the emission is above the Range 1 value, the output switches to Range 2 mode and the Range 2 value becomes the full-scale value of the output. The range indication digital output will change to the Range 2 state. The Range 2 settings cannot be changed and are factory-set.
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Tabs allow selection of the MicroCEM Settings pages
Figure 3-8. Range Settings
NOTE
If only one range is needed, set the Range 1 values to the range 2 value. This will disable the dual range fea­ture.
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b. Auto Calibration

The Auto-Calibration settings are set on the Auto-Calibration page of the Micro­CEM settings. If auto calibration is turned to the on position, then the user can select time and/or frequency of the auto calibration in the Auto Calibration Frequency tab (Section 3-3c).
c. Auto Calibration Time and Fre-
quency
The Auto-Calibration Time and Fre­quency tab allows specifying time and frequency of the auto-calibration. Time field requires military time format.
Figure 3-9. Auto Calibration Settings
Figure 3-10. Auto Calibration Time and
Frequency
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d. Manual Calibration

A dry-run Calibration may be initiated from the Manual Calibration page of the MicroCEM Settings. The results of the calibration will not be applied and only provide a dry run of the calibration. If desired a partial calibration may be in­voked for one or more of the emission types. While the manual calibration is in process, a calibration progress dialog will be displayed as shown in Figure 3-26. When the manual calibration is completed, the results are displayed in the Manual Calibration Results dialog as shown in Figure 3-12. If the Local Calibration checkbox is checked, the Local Calibration valve will be used during the calibration rather than the probe Calibration valve.
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NOTE
“Start Autocalibration now” will in­voke a real calibration and will apply new correction factor results when done.
Figure 3-12. Manual Calibration Results
Figure 3-11. Manual Calibration
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e. Limits

The emission limits alarms can be set on the Limits page of the MicroCEM Settings. When a measured emission exceeds its limit, the emission will have a limit-exceeded status. This is indi­cated on the main display and on the Data-Logs display. It is also indicated in the limit exceeded digital output.

f. Calibration Gas

The Calibration Gas emissions quanti­ties and Gas Bottle allocation may be set on the Calibration Gas page of the MicroCEM Settings. This should be set whenever a Calibration Gas container is replaced.
Place the span gas value of the par­ticular gas cylinder in the span column. I mid calibration gas can also be hooked up the MicroCEM. Insert its span gas value in the mid span boxes. If a dual range is used use the Mid Span column.
Figure 3-13. Limit Settings
Figure 3-14. Calibration Gas Settings
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g. Maintenance Mode

Maintenance mode may be selected for any of the emission types on the Main­tenance Mode page of the MicroCEM Settings.
Choosing maintenance mode will in­voke an “M” flag” onto the data. Cus­tomer can perform routine maintenance while in this setting
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Figure 3-15. Maintenance Mode Settings
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3-4 MicroCEM FACTORY SETTINGS

A MicroCEM Factory Settings program is available for use by MicroCEM technicians to set parameters in the MicroCEM or a qualified customer technician. Enter the Factory Settings password at the login dia­log to enter the Factory Settings. This
password will not be provided to the cus­tomer. The list of settings is shown in Ta­ble 3-3 and Table 3-4.
The user must purchase a PC/104 to mouse and PC/104 to monitor in order to access the factory settings. Consult Rosemount for details.
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Calibration Setting Description
O2ZeroDriftLimit O2 Allowed Zero Drift Limit.
COZeroDriftLimit CO Allowed Zero Drift Limit.
NOXZeroDriftLimit NOx Allowed Zero Drift Limit.
OSMidDriftLimit O2 Allowed Mid Drift Limit.
COMidDriftLimit CO Allowed Mid Drift Limit.
NOXMidDriftLimit NOx Allowed Mid Drift Limit.
O2SpanDriftLimit O2 Allowed Span Drift Limit.
COSpanDriftLimit CO Allowed Span Drift Limit.
NOXSpanDriftLimit NOx Allowed Span Drift Limit.
O2Slope Default value for the O2 slope
O2Offset Default value for the O2 offset
COSlope Default value for the CO slope
COOffset Default value for the CO offset
NOXSlope Default value for the NOx slope
NOXOffset Default value for the NOx offset
O2SpanDef Default O2 Span Calibration Gas value
O2MidSpanDef Default O2 Mid Span Calibration Gas value
COSpanDef Default CO Span Calibration Gas value
COMidSpanDef Default CO Mid Span Calibration Gas value
NOXSpanDef Default NOx Span Calibration Gas value
NOXMidSpanDef Default NOx Mid Span Calibration Gas value
Gas1Allocation Default Gas 1 allocation
Gas2Allocation Default Gas 2 allocation
Gas3Allocation Default Gas 3 allocation
AutoCalFrequency Default Auto-Calibration frequency in hours and minutes (example: 24:00).
AutoCalTime Default Auto-Calibration time in hours and minutes (military time).
Purge1 Default auto-calibration Purge 1 value in seconds.
Gas1 Default auto-calibration gas 1 time in seconds.
Gas2 Default auto-calibration gas 2 time in seconds.
Gas3 Default auto-calibration gas 3 time in seconds.
Purge2 Default auto-calibration Purge 2 value in seconds.
If the drift exceeds the allowed amount a drift alarm will occur, and the readings on the channel will no longer be valid until a successful calibration is com­pleted.
Initial values for the emissions conversion slope and offset used on a new system before the first Cali­bration is performed. These values should be set manually before the first auto-calibration is per­formed.
Default allocation for O2/NOx/CO. 1 = Zero, 2 = Mid Span, 3 = Span. Example: 133 = O2=Zero,NOx=Span,CO=Span
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Table 3-3. Factory Settings – Calibration
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General Setting
O2SensorLowLimit
O2SensorHighLimit
COSensorLowLimit
COSensorHighLimit
NOXSensorLowLimit
NOXSensorHighLimit
CCEM Serial Number
Diluent Percent
MinimumOnCurrent
MaximumOffCurrent
NDIR Sync Low
+24V Low Limit
+24V High Limit
ValveOnTime
O2EmissionLimit NOXEmissionLimit COEmissionLimit O2LowRange COLowRange NOXLowRange O2HighRange COHighRange NOXHighRange SamplePumpOn
LogsDir
MaxWarmUpTime
StateFile
ServerIP
ServerPort
ServerTimeout
AlarmsPersistFile
LogoffTimeout
UserListPersistFile
Description
This sets the O2 % low limit, below which a limit alarm will occur.
This sets the O2 % high limit, above which a limit alarm will occur.
This sets the CO low limit, below which a limit alarm will occur.
This sets the CO ppm high limit, above which a limit alarm will occur.
This sets the NOx low limit, below which a limit alarm will occur.
This sets the NOx ppm high limit, above which a limit alarm will occur.
This setting is used to record the MicroCEM Serial Number.
Percent O2 used in Diluent correction.
This is the minimum current that must be measured by a current analog input for a heater/cooler/fan to be considered on. This is used for heater/cooler/fan failure de­tection.
This is the maximum current that must be measured by a current analog input for a heater/cooler/fan to be considered off. This is used for heater/cooler/fan failure de­tection.
This indicates which NDIR reading is made when the sync goes from high to low: Reference (R) or Sample Gas (S).
If the +24V measurement is below this level it will cause an alarm.
If the +24V measurement is above this level it will cause an alarm.
For calibration – The amount of time to wait after turning on a valve.
These limits are the default values. On the Pocket PC these values will be used when one of the “Defaults” buttons are pressed.
1 = Sample pump is used. 0 = Sample pump not used.
Directory where log files are saved (C:\uCEM\Logs).
Maximum time allowed for the uCEM to warm-up when it is started up. If all tem­perature zones are not within allowed range within this period of time, the uCEM will shutdown all heaters, coolers and processes.
The full path to the file which maintains the state of the uCEM. (C:\uCEM\mcem.state)
The IP address to use when listening for incoming connections.
The IP Port to use when listening for incoming connections.
100
The full path to the file which maintains the current state of the alarms. (C:\uCEM\alarms.state)
Auto Log-off time in minutes
The full path to the file that maintains the user list (C:\uCEM\mcem.userlist)
Table 3-4. Factory Settings - General
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a. PID Control Loop Factory Settings

These settings can be set for each of the temperature control loops. The temperature control loops include the
Control Loop Section Name
Zone Heater/Cooler [PIDSettings ZoneLoop]
Converter Heater [PIDSettings ConverterLoop]
PMT Heater [PIDSettings PMTLoop]
PMT Photo Diode Cooler [PIDSettings PDTLoop]
Table 3-5. PID Settings – Section Names
Zone heater/cooler, Converter Heater, PMT Heater, and PMT Photo Diode Cooler. Table 3-5 shows the section names in the INI file used for each temperature control loop.
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PID Setting Description
PSetting
ISetting
DSetting
MaxSpeedSetting
ResetIntegralError
IntegralMaxPercent
IntegralMinPercent
MaxPercent Maximum zone output power in percent (0-100).
MinPercent Minimum zone output power in percent (0-100).
MinAlternationPercent Minimum
SetPoint
LowTempLimit
HighTempLimit
MaxOffCurrent
MinOnCurrent
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Proportional Gain. This parameter is set by using typical PID tuning methods. The P setting is mandatory and is the first pa­rameter to adjust. It provides a command directly proportional to the error.
Integral Gain. This parameter is set by using typical PID tuning methods. The I setting is optional and is used to make small ad­justments to correct a small error which persists for a period of time.
Derivative Gain. This parameter is set by using typical PID tuning methods. The D setting is optional. It is used to adjust the com­mand based on change in error. It can be used to reduce over­shoot, which typically occurs when the P settings is used by itself. This parameter tends to amplify any noise present in the input.
Should be set to the typical warm-up/cool-down speed in °C/second when the heater/cooler is operated at 100% power. Increasing this value effectively decreases the Proportional, Inte­gral and Derivative gain. Decreasing this value effectively in­creases the Proportional, Integral and Derivative gain.
Integral Reset Error. Setting used to reset Integral value when error is larger than this value. This parameter is used to prevent the integral value from building up while the error is large and then causing overshoot when the setpoint is reached.
Maximum percent output power that can be accumulated by the Integral component. (0-100) The default is 10 percent.
Minimum percent output power that can be accumulated by the Integral component. (0-100) The default is 10 percent.
This is the temperature setpoint, in degrees Celsius, for this tem­perature control loop.
If the temperature (°C) is below this value during the MicroCEM process (not including the warm-up phase) an alarm will occur.
If the temperature (°C) is above this value during the MicroCEM process (not including the warm-up phase) an alarm will occur.
If the current reading is below the maximum-off current while the heater is turned off, the heater has failed with a Heater Control failure.
If the current reading is below the minimum-on current while the heater is turned on, the heater has failed with a Heater Burnout status.
Table 3-6. PID Settings – Sections Descriptions
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3-5 MicroCEM ADMINISTRATION

The MicroCEM Administration dialog is only available to users with MicroCEM Admini­stration permission. If a user is not cur­rently logged in, the login dialog will be displayed. If the current user doesn’t have MicroCEM Administration permission, a message will be displayed which reads “Permission denied”. When the MicroCEM Administration is invoked from the Tools menu or the MicroCEM Administration button, the MicroCEM Administration tabbed dialog is displayed. The User Set­tings page (tab) is displayed initially.

a. User Settings

The user settings page of the Micro­CEM Administration dialog allows users to be added, deleted or modified. Each user has a name, password, and per­mission settings. The permission set­tings include Settings permission that allows access to the MicroCEM Set­tings dialog, and Administrative permis­sion that allows access to the MicroCEM Administration dialog. The Settings permission also allows a user to access the MicroCEM remotely us­ing the web-based interface.

b. Auto Logoff

The number of minutes of inactivity af­ter which a user is automatically logged off is set on the Auto Logoff page of the MicroCEM Administration.
Figure 3-17. Auto Logoff
Figure 3-16. User Settings
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3-6 MicroCEM DATA LOGS

The MicroCEM maintains a minimum of 3 months of history in three types of data log files. The first type of log file is the meas­urement log, which contains emission measurements (at 1 minute intervals), alarm indications and maintenance mode indications. The second type of log file is the calibration log file, which contains in­formation on each auto calibration done. The third is the alarm log file, which records any improperly functioning hardware. The data will be stored in flat, ASCII, CSV (comma-delineated) file. This file format can be read directly by MS Excel and im­ported into many types of software applica­tions. The following parameters is factory set for each of the log file types.

a. Maximum Log File Size

This is how large a log file can get (in bytes) before it is closed and a new log file is opened.

b. Maximum Number of Log Files

This is how many log files can be cre­ated. When the maximum number of log files is reached, the oldest file is overwritten when new ones are cre­ated.
Emissions Log: 6 Calib Log: 6 Alarm Log: 6

c. Log File Name Format

The log file name uses the date that the file was created. It is of the format TYYYYMMDD.CSV where T is the log file type (E=Emissions, C=Calibration and A=Alarm), YYYY is the Year, MM is the month, and DD is the day of the month. For example, the file name E20010329.csv contains emissions data and was created on March 29,
2001.

d. Measurement Log File Format

Emissions Log: 1 MB Calib Log: 4000 bytes Alarm Log: 4000 bytes
Name Description Example
Date/Time Month-day-year Hours:Minutes:Seconds 3-7-2001 10:24:57
O2 Percent O2 (percent) 10.5
CO CO parts per million 12
NOx NOx parts per million 15
CO Limit CO Limit exceeded alarm, 0=inactive, 1=active 0
NOx Limit NOx Limit exceeded alarm, 0=inactive, 1=active 0
O2 Status
CO Status V=Valid, M=Maintenance Mode, C=Calibration in process,
NOx Status V=Valid, M=Maintenance Mode, C=Calibration in process,
V=Valid, M=Maintenance Mode, C=Calibration in process, I=Invalid (calibration failed or sensor in failed state)
I=Invalid (calibration failed or sensor in failed state)
I=Invalid (calibration failed or sensor in failed state)
Table 3-7. Measurement Log File Format
The log file contains data in a flat, AS­CII, CSV file. The following are the fields of the file, in order of occurrence. The log file size will be about 42 bytes per entry. 3 months of data logs will require about 5,443,200 bytes
V
V
V
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e. Calibration Log File Format

The log file contains data in a flat, AS­CII, CSV file. The following are the
Name Description Example
Date/Time Month-day-year Hours:Minutes:Seconds 3-7-2001 10:24:57 Zero Time Time that Zero span started, Hours:Minutes:Seconds 10:25:30 Mid Time Time That Mid span started, Hours:Minutes:Seconds 10:27:30 Span Time Time that span started, Hours:Minutes:Seconds 10:28:30 Purge Time Time that the final purge started,
Hours:Minutes:Seconds Finish Time Time that the final purge finishes 10:31:00 O2 Measured Zero Measured percent O2 for Zero phase of calibration 0.0 O2 Expected Zero Expected percent O2 for Zero phase of calibration 0.0 O2 Zero Drift Percent drift of O2 zero calibration 0.0 O2 Measured Mid Span Measured percent O2 for Mid span phase of calibration 10.1 O2 Expected Mid Span Expected percent O2 for Mid span phase of calibration 10.0 O2 Mid Drift Percent drift of O2 mid calibration. -0.4 O2 Measured Span Measured percent O2 for Span phase of calibration 20.2 O2 Expected Span Expected percent O2 for Span phase of calibration 20.3 O2 Span Drift Percent drift of O2 span calibration 0.4 CO Measured Zero 1 CO Expected Zero 0 CO Zero Drift 0.3 CO Measured Mid Span 23 CO Expected Mid Span 24 CO Mid Span Drift -0.3 CO Measured Span 45 CO Expected Span 45 CO Span Drift 0 NOx Measured Zero Measured ppm NOx for zero phase of calibration 15 NOx Expected Zero Expected ppm NOx for zero phase of calibration 15 NOx Zero Drift 0 NOx Measured Mid Span Measured ppm NOx for mid span phase of calibration 30 NOx Expected Mid Span Measured ppm NOx for mid span phase of calibration 30 NOx Mid Span Drift 0 NOx Measured span Measured ppm NOx for span phase of calibration 59 NOx Expected span Measured ppm NOx for span phase of calibration 59 NOx Span Drift 0
fields of the file, in order of occurrence. The log file size will be about 178 bytes per entry. 3 months of data logs will require about 16000 bytes (based on Calibration performed every 24 hours).
10:30:30
Table 3-8. Calibration Log File Format
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f. Alarm Log File Format

The log file contains data in a flat, AS­CII, CSV file. The following are the fields of the file, in order of occurrence.
Name Description Example
Date/Time Month-day-year Hours:Minutes:Seconds 3-7-2001 10:24:57 Fault Level 1=informational, 2=warning, 3=critical 3 Fault Type 0 = O2 Calibration Failed
1 = CO Calibration Failed ** 2 = NOx Calibration Failed 3 = O2 High Limit 4 = O2 Low Limit 5 = CO High Limit ** 6 = CO Low Limit ** 7 = NOx High Limit 8 = NOx Low Limit 9 = O2 Emission Limit 10 = CO Emission Limit ** 11 = NOx Emission Limit 12 = 5 Volt Fault ** 13 = 6 Volt Fault ** 14 = 24V Over Max 15 = 24 Low Min 16 = Converter Over Temp 17 = Converter Low Temp 18 = Converter On Failed ** 19 = Converter Off Failed ** 20 = Zone Over Temp 21 = Zone Low Temp 22 = Zone Heater On Failed ** 23 = Zone Heater Off Failed ** 24 = Zone Cooler On Failed ** 25 = Zone Cooler Off Failed ** 26 = Heater Fan On Failed ** 27 = Heater Fan Off Failed ** 28 = Cooler Fan On Failed ** 29 = Cooler Fan Off Failed ** 30 = PDT Over Temp 31 = PDT Low Temp 32 = PDT On Failed ** 33 = PDT Off Failed ** 34 = PMT Over Temp 35 = PMT Low Temp 36 = PMT On Failed ** 37 = PMT Off Failed ** 38 = O2 Over Temp ** 39 = O2 Low Temp ** 40 = O2 On Failed ** 41 = O2 Off Failed ** 42 = Warmup Time Limit 70 = IO Board Failed
Fault Description ASCII string describing fault. Up to 200 characters. CO Calibration Failed
The days or months maintained in the Alarm Log depends on how often trou­ble conditions are recorded. If there are rarely alarm conditions recorded, there is enough space for many years of alarm logs to be recorded.
2
** - Alarm is not implemented in this version of software or reserved for future use.
Table 3-9. Alarm Log File Format
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3-7 VIEW DATA LOGS

View Data Logs will start Internet Explorer and display the Emissions page of the Mi-
Select 1 min., 15 min., 1 hour or 24 hour averages.
croCEM web pages (see Figure 3-18 and Figure 3-19). This page can be used to view the Emissions log. Other pages may be selected to view the calibration log and the alarm log.
If Most Recent is selected, the month day and hour do not need to be selected.
Select the ending hour to view (applicable only to 1- minute averages)
Note the page header was scrolled out of view to show all the selection options, but it can be seen in
Figure 3-19.
Figure 3-18. View Data Logs
Average Period Time Range Displayed
1 Minute 1 Hour
15 Minutes 1 Day
1 Hour 3 Days
12 Hours 1 Month
24 Hours 3 Months
Table 3-10. Average Period Selection
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NOTE
The Real-time, Config and Download are included in the navigation menu but these pages are intended for remote desktop use. As an enhancement these items could be hidden if the pages are browsed from a Windows CE version of Internet Explorer.
Model MicroCEM
The Emission Data-Logs data is shown here.
Alarms and Calibration data may also be viewed.
A Date is shown for 1 min or 15 minute averages. A date range is shown for 1 hour or greater averages.
Figure 3-19. View Data Logs Table
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3-8 VIEWING MicroCEM DATA WITH A WEB
BROWSER
The log files may be accessed using a web browser that has access to the MicroCEM over a Wireless LAN, serial port connection (PPP) or Dialup Connection (RAS). The MicroCEM has Window CE Web Server in­stalled and provides a Web-based interface to select and download the Data-Log files. The downloaded Data-Log files will be in a
CSV (comma delineated ASCII) format. The log files may also be viewed as a web page in a tabular format.

a. Real-Time Page

The Real-Time page provides a real­time display of the emission values and emission statuses. The display is re­freshed every 10 seconds.
Figure 3-20. Real-Time Web Page
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b. Emissions Page

The Emissions Page can be used to view emission history in a tabular web­page format. This page is used as part of the MicroCEM User interface as well as by a remote user (probably from a desktop computer).
The Emission Data-Logs table is dis­played (as shown in Figure 3-19) after selecting the Date and Average Period
If Most Recent is selected, the month day and hour do not need to be selected.
and pressing the Display button. If de­sired a bookmark or shortcut may be made to the page displaying the table. In the future, the same table can be displayed by selecting this bookmark. If Most Recent Data was selected, the book-marked page will always display Most Recent Data. If a specific date was specified, the book-marked page will always display the same date.
Select 1 min., 15 min., 1 hour or 24 hour averages.
Select the ending hour to view (applicable only to 1 minute averages)
Figure 3-21. Emissions Selection
Figure 3-22. Emissions Table
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Figure 3-23. Calibration Table
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c. Download Page

The download page of the MicroCEM allows the selection and download of the three types of Data-Logs. To quickly download recent data, a “Download Most Recent Emissions Data” selection is provided. For more control over the date range, a “Down­load Emissions by Date Range” selec­tion is available. Once the selection is
made, press the Download button to start the HTTP download. The Micro­CEM will create a temporary file that contains the selected data. Due to memory limitations there is a limit to the number of files that can be downloaded simultaneously. If this limit is ex­ceeded, a message will be displayed that reads “The simultaneous download limit has been reached, please try again later”.
Download Emissions Log, Calibration Log or Alarm Log
Choose from:
1 Minute / 8 Hours 1 Minute / 1 Day 1 Minute / 1 Week 15 Minutes / 1 Day 15 Minutes / 1 Week 15 Minutes / 1 Month 15 Minutes / 3 Months 1 Hour / 1 Week 1 Hour / 1 Month 1 Hour / 3 Months
Figure 3-24. Download Web Page
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3-9 VIEWING MicroCEM DATA WITH MS EX-
CEL
The MicroCEM Data may be view with MS Excel using two different methods. The first method is to open the data log files that have been down­loaded onto a workstation. The files may then be opened directly with Excel. The second method is to create an Excel workbook, which links to the MicroCEM web page. This is described in the following paragraph.
An Excel spreadsheet may be linked to a Micro­CEM web site, which periodically refreshes the spreadsheet with data from the web site. To do this, first make sure the MicroCEM web site is
available. The workstation needs access to the MicroCEM web site via RAS (Dialup), LAN or the Internet. Then in Excel, select Data menu, Get External Data, New Web Query. The dialog shown in Figure 3-25 will appear. Type in the ad­dress for a MicroCEM web page that contains a table with the desired data. Then press OK and click on the cell where the data should appear. The data will then appear in the spreadsheet. To have the data updated periodically, right-click on one of the cells that contains the linked data and select Data Range Properties. Check the box the reads “Refresh Every” and set the refresh period. For additional information refer to MS Excel documentation.
Figure 3-25. New Web Query
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3-10 AUTO CALIBRATION

The Auto Calibration dialog is displayed whenever calibration is in process. It dis-
plays the current emission values and the status of the calibration. The calibration may be canceled before it completes by pressing the Cancel button.
Note: The title of this dialog will read either “Auto Calibration” or “Manual Calibration” to indicate how the cali­bration process was initiated.
Figure 3-26. Auto Calibration
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SECTION 4

SOFTWARE

4-1 OVERVIEW

The MicroCEM Software includes 3 main components. One component is the Micro­CEM control software that interfaces with the instrumentation and records the emissions measurements. A second component is the User Interface Software that provides real­time status and configuration dialogs. A third component is the web server software that uses VB Script or Java Script to provide a web-based interface to the MicroCEM.

4-2 MicroCEM USER INTERFACE SOFTWARE

Hardware Platform: Pocket PC
The MicroCEM User Interface Software com­municates with the MicroCEM Control Soft­ware using TCP/IP. It may run locally on the MicroCEM computer or remotely on a Pocket PC with a RS232 connection to the MicroCEM
computer. It will not normally run locally since there is no input device or display connected to the MicroCEM processor.

4-3 MicroCEM WEB SERVER SOFTWARE

Web Browser: Internet Explorer 4.0 or Net- scape 4.0
The Web Server Software provides the web based interface described in this document. It is implemented as a VB Script or Java Script. The script will obtain much of the needed in­formation directly from the Data-Log files or configuration file. The real-time information will be obtained from a memory segment shared with the MicroCEM control software. The web server support multiple simultaneous clients. The maximum number of allowed connections could be limited to a reasonable number through the Windows CE Web Server configuration dialogs.
uCEM User
Interface
Pocket PC
As an option a
Wireless Network
may be used.
Serial
Cable
uCEM Computer
HTML (TCP/
IP)
Shared
Memory
Segment
Data-Log & Config
Files
Web Server Script
TCP/IP
Control Circuitry
uCEM
Control
Software
Device Drivers
Digital and
Analog IO
Sensors and
Figure 4-1. MicroCEM Software Block Diagram
HTML
Ethernet,
Modem or serial
Workstation
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4-4 SOFTWARE DEVELOPMENT MANAGEMENT

Microsoft Visual SourceSafe is used for ver­sion control of all of the MicroCEM software. Compuware’s Track Record is used for change request management and defect tracking.
Model MicroCEM
4-2 Software Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
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SECTION 5

MAINTENANCE AND SERVICE

DANGER.
ELECTRICAL SHOCK HAZARD
Disconnect power to the module(s) prior to replacing components.
WARNING
QUALIFIED PERSONNEL
This equipment should not be adjusted or repaired by anyone except properly quali­fied service personnel.
WARNING
PARTS INTEGRITY
Tampering with or unauthorized substitu­tion of components may adversely affect safety of this product. Use only factory­approved components for repair.

5-1 OVERVIEW

The MicroCEM Analyzer Module requires very little maintenance during normal operation.
Occasionally, the detector's reaction chamber and sapphire window may require cleaning, refer to Section 5-5.
White crystal deposits on the windows of the reaction chamber and plugging of capillaries and vent are usually due to sample contami­nates such as ammonia reacting with the high ozone levels and NO components. To elimi­nate the contaminates, the sampling system should be reworked or a preventive mainte­nance program developed (if dropout is not excessive). Another source of crystalline for­mation is contaminated air.
Several components may require replace­ment. These are discussed in the following sections.
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Valve Manifold Assembly
Paramagnetic Detector
Model MicroCEM
Converter (Figure 5-2)
NDIR Detector
Ozone Generator
Thermoelectric Cooler
Power Relay
3-Way Valve
Transistor
Regulator
Chemiluminescense Detector (Figure 5-4)
Power Supply Assembly
Fan
Personality Modules (Figure 5-3)
Figure 5-1. MicroCEM Component Location
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Instruction Manual
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5-2 CONVERTER

To replace the converter or sensor, discon­nect the two pneumatic tubes and two electri­cal connections. Unlace the heater blanket,
ASSEMBLED SIDE VIEW
Sensor
Glass
Cloth
Heater
Jacket
655228
Converter
Tube 655227
Wrap with aluminum foil
and remove the converter. Reassemble in re­verse order, ensuring that the converter is ori­ented with the glass cloth at the bottom and the sensor is oriented correctly inside the heater jacket.
Sensor 655282
Figure 5-2. Converter Assembly
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5-3 OZONE GENERATOR

To replace the ozonator, remove the two large straps and all tie-wraps, and disconnect the one electrical connection. Reassemble in re­verse order.

5-4 PERSONALITY MODULES

There are five different personality modules. Depending on your unit, you may have three, four or five modules installed. These person-
ality modules are installed on a custom back­plane. See Figure 5-3.
To remove any on the personality modules. Remove cables form module to be removed, there are two screws at the bottom of each module. You will have to loosen each screw before you can remove the personality mod­ule.
Tag each cable and its location before dis­connecting any wiring. This helps in re­assembly.
EXIO
AUX
PDD
NDIR
PMD
Figure 5-3. Personality Modules and Backplane.
5-4 Maintenance and Service Rosemount Analytical Inc. A Division of Emerson Process Management
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5-5 CHEMILUMINESCENSE DETECTOR AS-
SEMBLY
Refer to Figure 5-4 and Figure 5-5.

a. Reaction Chamber

Removal
Disconnect the stainless steel tubing lines at the Gyrolok fittings. Remove the (4) nuts holding the Detector Assembly to the chassis. Disconnect the plug from connector J1 on the Signal Board and remove the assembly from the chassis.
NOTE
Heatsink Compound. Care should be taken to avoid getting heatsink com­pound on optical surfaces. If this sub­stance is removed during the disassembly process, a zinc ox­ide-filled, silicone grease (e.g., Dow Corning 340 or EG&G Wakefield Engi­neering's Series 120 Thermal Joint Compound) be reapplied in the re­assembly of this component.
Although the heater and thermostat can be removed to facilitate handling, contact with the white heatsink compound can be minimized by leaving these items in place. Remove the (2) screws holding the top plate of the Detector , and move the plate along the wires and away from the De­tector .
Remove the (2) screws holding the tube assembly in place. Hold the tubing with one hand while inverting the Detector Housing with the other, allowing the Re­action Chamber O-ring and window to be removed from below.
Installation
To reinstall, hold the housing in the in­verted position while sliding the Reaction Chamber O-ring and window into position and the tubing into the slot in the housing. Hold the Reaction Chamber in place while rotating the housing upright. Replace the hold-down screws.
NOTE
Component Positioning. The proce­dure described above is for the pur­pose of maintaining the relative positions of windows and O-ring to the Reaction Chamber during installation.
Replace the top cap and screws. Reverse the removal procedure to reinstall the Detector Assembly into the Analyzer Module.

b. Photodiode

Removal
Remove the Detector Assembly as de­scribed above. Invert the housing to ac­cess the mounting bracket. Remove the (3) screws and shoulder washers from the bracket. Remove the bracket, insulating disk and bottom plate as a unit to mini­mize the spread of the heatsink com­pound.
Remove the (2) screws holding the lower section of the Detector Housing, then slide the section along the cable and re­move.
Remove the (2) screws holding the socket, thermistor and photodiode in place, being careful not to lose the wash­ers that are used as shims.
Grasp the socket and photodiode base while slowly rotating to separate the pho­todiode from the housing. Some friction will be felt as an O-ring is used around the photodiode as a seal.
Installation
To replace the photodiode, carefully re­move the diode from the green socket, and replace with a new one. Before mounting the new diode, the top cap of the enclosure should be temporarily re­moved and the (2) screws holding the Reaction Chamber loosened about two turns. This allows air which is trapped between the O-ring seals to escape when the diode is inserted. It also maintains the
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position of the O-ring and window in the upper compartment.
The new photodiode should be slowly in­serted into the housing while gradually rotating the body. This allows the O-ring to properly seat. Continue replacing screws, washers, thermistors, etc., with the thicker shim (washer) on the opposite side of the socket from the thermistor.
Photodiode
Replace the lower section of the housing, then the bottom cover, insulator and bracket with the shoulder washers and screws.
Re-tighten the screws in the Reaction Chamber (upper section). Replace the top cap and its screws.
To reinstall in the Analyzer Module, re­verse the procedure for removal as indi­cated above.
Sapphire Window
Reaction Chamber
Thermistor
Assembly
Sample
Ozone
Exhaust
Figure 5-4. Chemiluminescense Detector Assembly
Photodiode Socket Assembly
Detector Mounting Bracket
5-6 Maintenance and Service Rosemount Analytical Inc. A Division of Emerson Process Management
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*
Heater
M3X0.5 x 16mm Screw (2) 3mm Spring Washer (2)
*
Heater
Thermostat
Instruction Manual
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M3X0.5 x 25mm Screw (2) 3mm Spring Washer (2)
Detector Header
Retainer Gasket
*
Reaction Chamber
Photodiode Cable
Insulator (between Lower Cover and Mounting Bracket)
Photodiode Case Ground
*
Heater/Thermostat Assembly 655235.
Tubing Cover
Lower Cover
Nylon Shoulder Washers (3)
M3X0.5 x 16mm Screw (3)
O-Ring 876478
Photodiode Assembly (see detail below)
M3X0.5 x 20mm Screw (2)
(see detail below)
3mm Spring Washer (2)
Detector Cover
M3X0.5 x 16mm Screw (2) 3mm Spring Washer (2)
Photodiode 655258
O-Ring 854540
Sapphire Window
Cushioning Gasket
Thermistor 655216
Thermistor Shim
Photodiode Socket Assembly
Thermistor Spacer
No. 6 Flat Washer (2)
Assembly of Photodiode
Figure 5-5. Chemiluminescense Detector Assembly – Exploded View
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Instruction Manual
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SECTION 6

TROUBLESHOOTING

6-1 TROUBLESHOOTING LEAKS

Liberally cover all fittings, seals, and other pos­sible sources of leakage with a suitable leak test liquid such as SNOOP (part 837801). Bubbling or foaming indicates leakage. Checking for bub­bles will locate most leaks but could miss some, as some areas are inaccessible to the applica­tion of SNOOP. For positive assurance that system is leak free, perform one of the tests above.
NOTE:
Refer to Specification in Preface for maxi­mum pressure limitations.
For differential measurement, the leak check must be performed for the measurement and reference side separately.
For analyzers with parallel gas paths, the leak check must be performed for each gas path separately.

6-2 POCKET PC CONNECTION FAILURE

In the event the connection between the Pocket PC and the MicroCEM fails, a connection failure dialog will be displayed. It will display the fol­lowing message:
Connection with uCEM lost, retrying…
A Cancel button will be displayed. The Micro­CEM software will continue to attempt to recon­nect with the MicroCEM indefinitely and will stop when a connection is made or the cancel button is pressed.
If the Cancel button is pressed, any setting changes that were made without pressing OK to accept will be lost. If Auto Calibration was in process, it will be completed by the MicroCEM even though the connection was lost.

6-3 TROUBLE LED

The Trouble LED output is activated whenever there is a critical alarm that has not been ac­knowledged. This provides both an output from the MicroCEM box and an LED indication.
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6-2 Troubleshooting Rosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
SECTION 7

REPLACEMENT PARTS

1020839-100 PMD Module Assembly 1020840-100 NDIR Module Assembly 1020841-101 PDD Module Assembly 1020842-100 AUX Module Assembly 1020843-100 EXIO Module Assembly 1020869-100 Thermoelectric Cooler Assembly 1020973-100 Thermistor 1020987-100 Heater Assembly 42706504 Desiccant Bulbs 42711801 Electrical Cable 634398 Capillary, Vent 638614 Pressure Gauge 655216 Thermistor Assembly 655250 Converter Assembly 655289 Restrictor, Bulkhead 657716 Power Supply, Ozonator 657719 Ozone Generator 658157 Restrictor, Brass 659754 Photodiode Detector 90003311 Paramagnetic Detector 902124 Flowmeter 905778 4-Port Manifold 905779 2-Way Valve 905780 3-Way Valve 905871 Relay, Power 15A
Instruction Manual
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January 2002
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Model MicroCEM
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Instruction Manual
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SECTION 8

RETURN OF MATERIAL

8-1 RETURN OF MATERIAL

If factory repair of defective equipment is re­quired, proceed as follows:
1. Secure a return authorization from a Rosemount Analytical Inc. Sales Office or Representative before returning the equipment. Equipment must be returned with complete identification in accordance with Rosemount instructions or it will not be accepted.
2. In no event will Rosemount be responsible for equipment returned without proper authorization and identification.
3. Carefully pack the defective unit in a sturdy box with sufficient shock absorbing mate­rial to ensure no additional damage occurs during shipping.
4. In a cover letter, describe completely:
a. The symptoms that determined the
equipment is faulty.
b. The environment in which the equip-
ment was operating (housing, weather, vibration, dust, etc.).
c. Site from where the equipment was
removed.
d. Whether warranty or non-warranty
service is expected.
e. Complete shipping instructions for the
return of the equipment.
5. Enclose a cover letter and purchase order and ship the defective equipment accord­ing to instructions provided in the Rose­mount Return Authorization, prepaid, to:
If warranty service is expected, the defective unit will be carefully inspected and tested at the factory. If the failure was due to the condi­tions listed in the standard Rosemount war­ranty, the defective unit will be repaired or replaced at Rosemount’s option, and an oper­ating unit will be returned to the customer in accordance with the shipping instructions fur­nished in the cover letter.
For equipment no longer under warranty, the equipment will be repaired at the factory and returned as directed by the purchase order and shipping instructions.

8-2 CUSTOMER SERVICE

For order administration, replacement parts, application assistance, on-site or factory re­pair, service or maintenance contract informa­tion, contact:
Rosemount Analytical Inc.
Process Analytic Division
Customer Service Center
1-800-433-6076

8-3 TRAINING

A comprehensive Factory Training Program of operator and service classes is available. For a copy of the Current Operator and Service Training Schedule, contact the Technical Services Department at:
Rosemount Analytical Inc.
Phone 1-714-986-7600
FAX 1-714-577-8006
Rosemount Analytical Inc.
Process Analytic Division
Customer Service Center
1-800-433-6076
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8-2 Return of Material Rosemount Analytical Inc. A Division of Emerson Process Management

WARRANTY

Goods and part(s) (excluding consumables) manufactured by Seller are warranted to be free from defects in workmanship and material under normal use and service for a period of twelve (12) months from the date of shipment by Seller. Consumables, glass electrodes, membranes, liquid junctions, electrolyte, o-rings, etc., are warranted to be free from defects in workmanship and material under normal use and service for a period of ninety (90) days from date of shipment by Seller. Goods, part(s) and consumables proven by Seller to be defective in workmanship and/or material shall be replaced or repaired, free of charge, F.O.B. Seller's factory provided that the goods, part(s) or consumables are returned to Seller's designated factory, transportation charges prepaid, within the twelve (12) month period of warranty in the case of goods and part(s), and in the case of consumables, within the ninety (90) day period of warranty. This warranty shall be in effect for replacement or repaired goods, part(s) and the remaining portion of the ninety (90) day warranty in the case of consumables. A defect in goods, part(s) and consumables of the com­mercial unit shall not operate to condemn such commercial unit when such goods, part(s) and consumables are capable of being renewed, repaired or replaced.
The Seller shall not be liable to the Buyer, or to any other person, for the loss or damage directly or indirectly, arising from the use of the equipment or goods, from breach of any warranty, or from any other cause. All other warranties, expressed or implied are hereby excluded.
IN CONSIDERATION OF THE HEREIN STATED PURCHASE PRICE OF THE GOODS, SELLER GRANTS ONLY THE ABOVE STATED EXPRESS WARRANTY. NO OTHER WAR­RANTIES ARE GRANTED INCLUDING, BUT NOT LIMITED TO, EXPRESS AND IMPLIED WARRANTIES OR MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE.
Limitations of Remedy. SELLER SHALL NOT BE LIABLE FOR DAMAGES CAUSED BY DE­LAY IN PERFORMANCE. THE SOLE AND EXCLUSIVE REMEDY FOR BREACH OF WAR­RANTY SHALL BE LIMITED TO REPAIR OR REPLACEMENT UNDER THE STANDARD WARRANTY CLAUSE. IN NO CASE, REGARDLESS OF THE FORM OF THE CAUSE OF AC­TION, SHALL SELLER'S LIABILITY EXCEED THE PRICE TO BUYER OF THE SPECIFIC GOODS MANUFACTURED BY SELLER GIVING RISE TO THE CAUSE OF ACTION. BUYER AGREES THAT IN NO EVENT SHALL SELLER'S LIABILITY EXTEND TO INCLUDE INCIDEN­TAL OR CONSEQUENTIAL DAMAGES. CONSEQUENTIAL DAMAGES SHALL INCLUDE, BUT ARE NOT LIMITED TO, LOSS OF ANTICIPATED PROFITS, LOSS OF USE, LOSS OF REVE­NUE, COST OF CAPITAL AND DAMAGE OR LOSS OF OTHER PROPERTY OR EQUIPMENT. IN NO EVENT SHALL SELLER BE OBLIGATED TO INDEMNIFY BUYER IN ANY MANNER NOR SHALL SELLER BE LIABLE FOR PROPERTY DAMAGE AND/OR THIRD PARTY CLAIMS COVERED BY UMBRELLA INSURANCE AND/OR INDEMNITY COVERAGE PROVIDED TO BUYER, ITS ASSIGNS, AND EACH SUCCESSOR INTEREST TO THE GOODS PROVIDED HEREUNDER.
Force Majeure. Seller shall not be liable for failure to perform due to labor strikes or acts beyond Seller's direct control.
Instruction Manual
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Model MicroCEM
Emerson Process Management
Rosemount Analytical Inc. Process Analytic Division
1201 N. Main St. Orrville, OH 44667-0901 T (330) 682-9010 F (330) 684-4434 E-mail: gas.csc@emersonprocess.com
ASIA - PACIFIC Fisher-Rosemount Singapore Private Ltd.
1 Pandan Crescent Singapore 128461 Republic of Singapore Phone: 65-777-8211 Fax: 65-777-0947
http://www.processanalytic.com
© Rosemount Analytical Inc. 2001
EUROPE, MIDDLE EAST, AND AFRICA Fisher-Rosemount Ltd.
Heath Place Bognor Regis West Sussex PO22 9SH England Phone: 44-1243-863121 Fax: 44-1243-845354
EUROPEAN TECHNOLOGY CENTER Fisher-Rosemount GmbH & Co.
Industriestrasse 1 63594 Hasselroth Germany Phone: 49-6055-884 0 Fax: 49-6055-884209
LATIN AMERICA Fisher - Rosemount
Av. das Americas 3333 sala 1004 Rio de Janeiro, RJ Brazil 22631-003 Phone: 55-21-431-1882
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