Rosemount Analytical designs, manufactures and tests its products to meet many national and
international standards. Because these instruments are sophisticated technical products, you
MUST properly install, use, and maintain them to ensure they continue to operate within their
normal specifications. The following instructions MUST be adhered to and integrated into your
safety program when installing, using, and maintaining Rosemount Analytical products. Failure to
follow the proper instructions may cause any one of the following situations to occur: Loss of life;
personal injury; property damage; damage to this instrument; and warranty invalidation.
•
Read all instructions prior to installing, operating, and servicing the product.
If you do not understand any of the instructions, contact your Rosemount Analytical repre-
•sentative for clarification.
Follow all warnings, cautions, and instructions marked on and supplied with the product.
•
Inform and educate your personnel in the proper installation, operation, and maintenance of the
•
product.
Install your equipment as specified in the Installation Instructions of the appropriate Instruction
•
Manual and per applicable local and national codes. Connect all products to the proper electrical and pressure sources.
To ensure proper performance, use qualified personnel to install, operate, update, program,
•
and maintain the product.
When replacement parts are required, ensure that qualified people use replacement parts speci-
•
fied by Rosemount. Unauthorized parts and procedures can affect the product’s performance,
place the safe operation of your process at risk, and VOID YOUR WARRANTY. Look-alike
substitutions may result in fire, electrical hazards, or improper operation.
•
Ensure that all equipment doors are closed and protective covers are in place, except
when maintenance is being performed by qualified persons, to prevent electrical shock
and personal injury.
The information contained in this document is subject to change without notice.
Logos, trademarks and copyrights are property of their respective owners.
Emerson Process Management
Rosemount Analytical Inc.
Process Analytic Division
1201 North Main Street
Orrville, Ohio 44667-09012
T (330) 682-9010
F (330) 684-4434
e-mail: gas.csc@EmersonProcess.com
Table 3-8.Calibration Log File Format ................................................................................. 3-19
Table 3-9.Alarm Log File Format ......................................................................................... 3-20
Table 3-10.Average Period Selection .................................................................................... 3-21
Instruction Manual
748467-A
January 2002
LIST OF TABLES
Rosemount Analytical Inc. A Division of Emerson Process ManagementContents v
Instruction Manual
748467-A
January 2002
Model MicroCEM
vi ContentsRosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
Model MicroCEM
PREFACE
The purpose of this manual is to provide information concerning the components, functions, installation and maintenance of the MicroCEM.
Some sections may describe equipment not used in your configuration. The user should become
thoroughly familiar with the operation of this module before operating it. Read this instruction
manual completely.
DEFINITIONS
The following definitions apply to DANGERS, WARNINGS, CAUTIONS and NOTES found throughout
this publication.
DANGER .
Highlights the presence of a hazard which will cause severe personal injury, death, or substantial
property damage if the warning is ignored.
748467-A
January 2002
WARNING .
Highlights an operation or maintenance procedure, practice, condition, statement, etc. If not
strictly observed, could result in injury, death, or long-term health hazards of personnel.
CAUTION.
Highlights an operation or maintenance procedure, practice, condition, statement, etc. If not
strictly observed, could result in damage to or destruction of equipment, or loss of effectiveness.
NOTE
Highlights an essential operating procedure,
condition or statement.
Rosemount Analytical Inc. A Division of Emerson Process ManagementPreface P-1
Instruction Manual
748467-A
January 2002
Model MicroCEM
INTENDED USE STATEMENT
The MicroCEM Continuous Emissions Monitor is intended for use as an industrial process measurement device only. It is not intended for use in medical, diagnostic, or life support applications,
and no independent agency certifications or approvals are to be implied as covering such applications.
SAFETY SUMMARY
If this equipment is used in a manner not specified in these instructions, protective systems may be
impaired.
AUTHORIZED PERSONNEL
To avoid explosion, loss of life, personal injury and damage to this equipment and on-site property,
do not operate or service this instrument before reading and understanding this instruction manual
and receiving appropriate training. Save these instructions.
DANGER.
ELECTRICAL SHOCK HAZARD
Do not open while energized. Installation requires access to live parts which can cause death or
serious injury.
For safety and proper performance this instrument must be connected to a properly grounded
three-wire source of power.
DANGER.
POSSIBLE EXPLOSION HAZARD
Do not operate without covers secure. Ensure that all gas connections are made as labeled and are
leak free. Improper gas connections could result in explosion and death.
P-2 PrefaceRosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
Model MicroCEM
DANGER.
TOXIC GAS
This device may contain explosive, toxic or unhealthy gas components. Before cleaning or changing parts in the gas paths, purge the gas lines with ambient air or nitrogen.
This unit’s exhaust may contain hydrocarbons and other toxic gases such as carbon monoxide.
Carbon monoxide is highly toxic and can cause headache, nausea, loss of consciousness, and
death.
WARNING: TOXIC GAS
Avoid inhalation of the exhaust gases at the exhaust fitting.
Connect exhaust outlet to a safe vent using stainless steel or Teflon line. Check vent line and connections for leakage.
Keep all tube fittings tight to avoid leaks. See Sections 2-5 for leak check information.
WARNING.
748467-A
January 2002
DEVICE HAZARDOUS AREA CERTIFICATION(S)
Any addition, substitution, or replacement of components installed on or in this device, must be
certified to meet the hazardous area classification that the device was certified to prior to any such
component addition, substitution, or replacement. In addition, the installation of such device or
devices must meet the requirements specified and defined by the hazardous area classification of
the unmodified device. Any modifications to the device not meeting these requirements, will void
the product certification(s).
WARNING.
PARTS INTEGRITY AND UPGRADES
Tampering with or unauthorized substitution of components may adversely affect the safety of this
instrument. Use only factory approved components for repair.
Because of the danger of introducing additional hazards, do not perform any unauthorized modification to this instrument.
Return the instrument to Rosemount Analytical Customer Service Center. See Section 8.
CAUTION.
PRESSURIZED GAS
This unit requires periodic calibration with a known standard gas. It also may utilizes a pressurized carrier gas, such as helium, hydrogen, or nitrogen. See General Precautions for Handling and
Storing High Pressure Gas Cylinders, page P-5.
Rosemount Analytical Inc. A Division of Emerson Process ManagementPreface P-3
Instruction Manual
748467-A
January 2002
CAUTION.
HEAVY WEIGHT
Use two persons or a suitable lifting device to move or carry the instrument.
Model MicroCEM
P-4 PrefaceRosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
748467-A
Model MicroCEM
January 2002
GENERAL PRECAUTIONS FOR HANDLING AND STORING HIGH
PRESSURE GAS CYLINDERS
Edited from selected paragraphs of the Compressed Gas Association's "Handbook of Compressed
Gases" published in 1981
Compressed Gas Association
1235 Jefferson Davis Highway
Arlington, Virginia 22202
Used by Permission
1. Never drop cylinders or permit them to strike each other violently.
2. Cylinders may be stored in the open, but in such cases, should be protected against extremes of
weather and, to prevent rusting, from the dampness of the ground. Cylinders should be stored in the
shade when located in areas where extreme temperatures are prevalent.
3. The valve protection cap should be left on each cylinder until it has been secured against a wall or
bench, or placed in a cylinder stand, and is ready to be used.
4. Avoid dragging, rolling, or sliding cylinders, even for a short distance; they should be moved by using a
suitable hand-truck.
5. Never tamper with safety devices in valves or cylinders.
6. Do not store full and empty cylinders together. Serious suckback can occur when an empty cylinder is
attached to a pressurized system.
7. No part of cylinder should be subjected to a temperature higher than 125°F (52°C). A flame should
never be permitted to come in contact with any part of a compressed gas cylinder.
8. Do not place cylinders where they may become part of an electric circuit. When electric arc welding,
precautions must be taken to prevent striking an arc against the cylinder.
Rosemount Analytical Inc. A Division of Emerson Process ManagementPreface P-5
Instruction Manual
748467-A
January 2002
Model MicroCEM
DOCUMENTATION
The following MicroCEM instruction materials are available. Contact Customer Service Center or the local representative to order (See Section 8).
This product may carry approvals from several certifying agencies. The certification marks appear on the
product name-rating plate.
CSA (Pending)
P-6 PrefaceRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
DESCRIPTION AND SPECIFICATIONS
1-1 OVERVIEW
The MicroCEM Analyzer Module is designed
to continuously determine the concentration of
, CO, and NOx in a flowing gaseous mix-
O
2
ture. The concentration is expressed in percent (%) or parts-per-million (PPM).
SECTION 1
Instruction Manual
748467-A
January 2002
and oxygen (O2). Some of the NO
NO
2
molecules produced are in an electronically excited state (NO
* where the * re-
2
fers to the excitation). These revert to the
ground state, with emission of photons
(essentially, red light). The reactions involved are:
2
The sampled gas is collected from the stack
and prepared by the Probe/Sample Handling
System for analysis and processing by the
Analysis Enclosure. The Analysis Enclosure
shall be a standalone, computer-controlled
unit, utilizing PC/104 as the system bus.
The MicroCEM is enclosed in a rugged NEMA
4X, IP65 type enclosure, for harsh environment. The analysis enclosure utilizes convection cooling with no air intake and air vents.
The analysis enclosure is modular, general
purpose and easily expandable. It utilizes industry standard components such as PC/104
boards, and modular signal conditioning modules.
1-2 TYPICAL APPLICATIONS
SCR
Emission Compliance per EPA 40 CFR Part
60
Gas Turbines
Natural Gas Fired Boilers
Process Heaters
NO2 + O3 → NO2* + O
2
NO2* → NO2 + red light
The sample is continuously passed
through a heated bed of vitreous carbon,
in which NO
is reduced to NO. Any NO
2
initially present in the sample passes
through the converter unchanged, and
any NO
is converted to an approximately
2
equivalent (95%) amount of NO.
The NO is quantitatively converted to NO
by gas-phase oxidation with molecular
ozone produced within the analyzer form
air supplied by an external source. During
the reaction, approximately 10% of the
NO
molecules are elevated to an elec-
2
tronically excited state, followed by immediate decay to the non-excited state,
accompanied by emission of photons.
These photons are detected by a photomultiplier tube which produces an output
proportional to the concentration of NOx
in the sample.
2
1-3 THEORY OF OPERATION
To minimize system response time, an
internal sample bypass feature provides
a. Chemiluminescense NO
X
high-velocity sample flow through the
analyzer.
The NOx analyzer continuously analyzes
a flowing gas sample for NOx [nitric oxide
(NO) plus nitrogen dioxide (NO
)]. The
2
sum of the concentrations is continuously
reported as NOx.
b. Non-Dispersive Infrared (NDIR) CO
The optical bench can selectively meas-
ure multiple components in a compact
design by using a unique dual optical
The MicroCEM NOx Analyzer Module
uses the chemiluminescense method of
detection. This technology is based on
NO’s reaction with ozone (O
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-1
) to produce
3
bench design. Depending on the applica-
tion, any two combinations of NDIR chan-
nels can be combined on a single
chopper motor/dual source assembly.
Instruction Manual
748467-A
January 2002
Model MicroCEM
Other application-dependent options include a wide range of sample cell materials, optical filters and solid state
detectors. The NDIR Microflow detector
consists of two chambers, measurement
and reference with an interconnected path
in which an ultra low flow filament sensor
is mounted. During operation, a pulsating
flow occurs between the two chambers
which is dependent upon: sample gas absorption, modulation by the chopper motor and the fill gas of the detector
chambers. The gas flow/sensor output is
proportional to the measured gas concentration. The optical bench is further
enhanced by a novel “Look-through” detector technique. This design allows two
detectors to be arranged in series --- enabling two different components to be
measured on a single optical bench. The
optical bench contains a unique eddy current drive chopper motor and source assembly. This design incorporates on
board “intelligence” to provide continuous
“self test” diagnostics.
c. Paramagnetic O2
measured. The gas-specific wavelengths
of the absorption bands characterize the
type of gas while the strength of the ab-
sorption gives a measure of the concen-
tration of the gas component being
measured.
An optical bench is employed comprising
an infrared light source, two analysis cells
(reference and measurement), a chopper
wheel to alternate the radiation intensity
between the reference and measurement
side, and a photometer detector. The de-
tector signal thus alternates between con-
centration dependent and concentration
independent values. The difference be-
tween the two is a reliable measure of the
concentration of the absorbing gas com-
ponent.
Depending on the gas being measured
and its concentration, one of two different
measuring methods may be used as fol-
lows:
Interference Filter Correlation (IFC)
Method
The determination of oxygen is based on
the measurement of the magnetic susceptibility of the sample gas. Oxygen is
strongly paramagnetic, while other common gases are not. The detector used is
compact, has fast response and a wide
dynamic range. The long life cell is corrosion resistant, heated and may be easily
cleaned. It has rugged self-tensioning
suspension and is of welded non-glued
construction.
1-4 DETECTOR METHODOLOGIES
The MicroCEM can employ up to three different measuring methods depending on the
configuration chosen. The methods are:
NDIR, Paramagnetic O
and Chemiluminescense.
a. Non-Dispersive Infrared (NDIR)
The non-dispersive infrared method is
based on the principle of absorption of infrared radiation by the sample gas being
, Electrochemical O2,
2
With the IFC method the analysis cell is
alternately illuminated with filtered infrared
concentrated in one of two spectrally
separated wavelength ranges. One of
these two wavelength bands is chosen to
coincide with an absorption band of the
sample gas and the other is chosen such
that none of the gas constituents ex-
pected to be encountered in practice ab-
sorbs anywhere within the band.
The spectral transmittance curves of the
interference filters used in the MicroCEM
analyzer and the spectral absorption of
the gases CO and CO
ure 1-1. It can be seen that the absorption
bands of these gases each coincide with
the passbands of one of the interference
filters. The forth interference filter, used
for generating a reference signal, has its
passband in a spectral region where none
of these gases absorb. Most of the other
gases of interest also do not absorb within
the passband of this reference filter.
are shown in Fig-
2
1-2 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
The signal generation is accomplished
with a pyroelectrical (solid-state) detector.
The detector records the incoming infrared radiation. This radiation is reduced by
the absorption of the gas at the corresponding wavelengths. By comparing the
measurement and reference wavelength,
an alternating voltage signal is produced.
This signal results from the cooling and
heating of the pyroelectric detector material.
Figure 1-1. Absorption Bands of Sample Gas and Transmittance of Interference Filters
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-3
Instruction Manual
748467-A
January 2002
Opto-Pneumatic Method
Model MicroCEM
In the opto-pneumatic method, a thermal
radiator generates the infrared radiation
which passes through the chopper wheel.
This radiation alternately passes through
the filter cell and reaches the measuring
and reference side of the analysis cell
with equal intensity. After passing another
filter cell, the radiation reaches the pneumatic detector.
The pneumatic detector compares and
evaluates the radiation from the measuring and reference sides of the analysis
cell and converts them into voltage signals proportional to their respective intensity.
The pneumatic detector consists of a gasfilled absorption chamber and a compensation chamber which are connected by a
flow channel in which a Microflow filament
sensor is mounted. This is shown in Figure 1-2.
In principle the detector is filled with the
infrared active gas to be measured and is
only sensitive to this distinct gas with its
characteristic absorption spectrum. The
absorption chamber is sealed with a window which is transparent for infrared radiation. The window is usually Calcium
Fluoride (CaF
).
2
When the infrared radiation passes
through the reference side of the analysis
cell into the detector, no pre-absorption
occurs. Thus, the gas inside the absorp-
tion chamber is heated, expands and
some of it passes through the flow chan-
nel into the compensation chamber.
When the infrared radiation passes
through the open measurement side of
the analysis cell into the detector, a part
of it is absorbed depending on the gas
concentration. The gas in the absorption
chamber is, therefore, heated less than in
the case of radiation coming from the ref-
erence side. Absorption chamber gas be-
comes cooler, gas pressure in the
absorption chamber is reduced and some
gas from the compensation chamber
passes through the flow channel into the
absorption chamber.
The flow channel geometry is designed in
such a way that it hardly impedes the gas
flow by restriction. Due to the radiation of
the chopper wheel, the different radiation
intensities lead to periodically repeated
flow pulses within the detector.
The Microflow sensor evaluates these
flow pulses and converts them into elec-
trical pulses which are processed into the
corresponding analyzer output.
Absorption chamber
Flow channel with
Microflow sensor
CaF2 Window
Compensation chamber
Figure 1-2. Opto-Pneumatic Gas Detector
1-4 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
Overall NDIR Method
In the case of dual-channel analyzers, the
broadband emission from two infrared
sources pass through the chopper wheel.
In the case of the Interference Filter Correlation (IFC) method, the infrared radiation then passes through combinations of
interference filters. In the case of the
opto-pneumatic method, the infrared radiation passes through an optical filter
Light Source
Chopper Blade
MOTOR
depending on the application and need for
reduction of influences. Then the infrared
radiation enters the analysis cells from
which it is focused by filter cells onto the
corresponding detector. The preamplifier
detector output signal is then converted
into the analytical results expressed di-
rectly in the appropriate physical concen-
tration units such as percent volume,
ppm, mg/Nm
3
, etc. This is shown in Fig-
ure 1-3.
Duplex Filter Disc
Adapter Cell
(high measuring range)
Analysis Cell
(measuring side)
Analysis Cell
(reference side)
Filter Cell
Gas Detector
Analysis Cell
(undivided)
Filter Cell
Preamplifier
Pyroelectric Detector
(solid-state detector)
Preamplifier
Chopper Blade
Figure 1-3. Overall NDIR Method
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-5
Instruction Manual
748467-A
January 2002
Model MicroCEM
b. Paramagnetic Oxygen Method
The paramagnetic principle refers to the
induction of a weak magnetic field, parallel and proportional to the intensity of a
stronger magnetizing field.
The paramagnetic method of determination of oxygen concentration utilizes nitrogen filled quartz spheres arranged at
opposite ends of a bar, the center of
which is suspended by and free to rotate
on a thin platinum wire ribbon in a cell.
Nitrogen (N
) is used because it is dia-
2
magnetic or repelled by a magnet.
A small mirror that reflects a light beam
coming from a light source to a photodetector, is mounted on the platinum ribbon.
A strong permanent magnet specifically
shaped to produce a strong, highly inhomogeneous magnetic field inside the
analysis cell, is mounted outside the wall
of the cell.
When oxygen molecules enter the cell,
their paramagnetism will cause them to
be drawn towards the region of greatest
magnetic field strength. The oxygen
molecules thus exert different forces on
the two suspended nitrogen filled quartz
spheres, producing a torque which
causes the mirror to rotate away from its
equilibrium position.
The rotated mirror deflects the incident
light onto the photodetector creating an
electrical signal which is amplified and fed
back to a coil attached to the bar holding
the quartz spheres, forcing the suspended
spheres back to the equilibrium position.
The current required to generate the re-
storing torque to return the quartz bar to
its equilibrium position is a direct measure
of the O
concentration in the sample gas.
2
The complete paramagnetic analysis cell
consists of an analysis chamber, perma-
nent magnet, processing electronics, and
a temperature sensor. The temperature
sensor is used to control a heat ex-
changer to warm the measuring gas to
about 55 °C. Refer to Figure 1-4.
Light
Source
Display
Permanent Magnet
Platinum Wire
Mirror
Quartz Sphere(s)
Wire Loop
Photodetector
Amplifier
Figure 1-4. Paramagnetic Oxygen Analysis
1-6 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
c. Electrochemical Oxygen Method
The electrochemical method of determining oxygen concentration is based on the
galvanic cell principle shown in Figure
1-5.
The electrochemical oxygen sensor (Figure 1-6) incorporates a lead and gold galvanic process with a lead anode and a
gold cathode, using an acid electrolyte.
Oxygen molecules diffuse through a nonporous Teflon membrane into the electrochemical cell and are reduced at the gold
cathode. Water is the byproduct of this
reaction.
On the anode, lead oxide is formed which
is transferred into the electrolyte. The lead
anode is continuously regenerated and,
therefore, the electrode potential remains
unchanged for a long time. The rate of
diffusion and corresponding response
time (t90) of the sensor is dependent on
the thickness of the Teflon membrane.
The electric current between the elec-
trodes is proportional to the O
concentra-
2
tion in the sample gas being measured.
The resultant signal is measured as a
voltage across the resistor and thermistor,
the latter of which is used for temperature
compensation. A change in the output
voltage (mV) represents oxygen concen-
tration.
NOTE
The electrochemical O2 cell requires a
minimum internal consumption of
oxygen. Sample gases with an oxygen
concentration of less than 2% could
result in a reversible detuning of sensi-
tivity and the output will become un-
stable. The recommended practice is
to purge the cell with conditioned am-
bient air between periods of measure-
ment. If the oxygen concentration is
below 2% for several hours or days,
the cell must be regenerated for about
one day with ambient air. Temporary
flushing with nitrogen (N
) for less than
2
one hour (analyzer zeroing) will have
no effect on the sensitivity or stability.
(Red)V out(Black)
Thermistor (5)Resistor (6)
(-)(+)
GoldLead
Cathode (2)Anode (1)
O2 + 4 H + 4 e → 2 H2O2 Pb + 2 H
Electrolyte (3)
(ph 6)
Summary reaction O
+ 2 Pb → 2 PbO
2
O → 2PbO + 4 H + 4 e
2
Figure 1-5. Reaction of Galvanic Cell
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-7
Instruction Manual
748467-A
January 2002
Lead Wire (Anode)
Lead Wire (Cathode)
Anode (Lead)
O-Ring
Plastic Disc
Model MicroCEM
Black
Red
Plastic Disk
Resistor
Thermistor
Acid Electrolyte
Sponge Disc
Cathode (Gold Film)
Teflon Membrane
Figure 1-6. Electrochemical Oxygen Sensor
1-8 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
1-5 CENTRAL PROCESSING UNIT
The CPU is an Embedded Pentium-like AT
Computer in 5.75” x 8” form factor. The peripherals integrated on board are: SVGA, 4
serial ports and one parallel port, Fast
Ethernet ctrl., IDE, Keyboard, Mouse, 2 USB.
The module is built around the Intel Tillamook
processor and is equipped with 64MB
SDRAM. The module also integrates one
socket for SSD that performs like an HDD unit
and can be used to store the operating system, the user’s programs and the data files.
Other peripherals available on board are the
Floppy disk controller, the parallel port. The
CPU is shown in Figure 1-7.
Ram/Rom disk: ............................. 1 x 32 pin socket (max. 288MB)
Operating System: ........................ WinNT
BIOS: ............................................ Standard with embedded extensions
Interfaces: ..................................... IDE ctrl
Floppy ctrl
SVGA-CRT
10/100 Mbps Fast Ethernet
2 USB ports
4 RS232 serial ports (one can be 485)
Parallel port (bi-directional EPP-ECP)
Keyboard PS/2
Mouse PS/2
Bus: .............................................. AT bus according to PC/104 spec.
Power Supply: .............................. AT/ATX
Connectors: .................................. COM1-4, SVGA, USB 1 and 2, PS/2 Mouse/Keyboard, ATX Power,
Parallel, IDE, Floppy, and Fast Ethernet
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-9
Instruction Manual
748467-A
January 2002
1-6 ANALOG/DIGITAL I/O BOARD
The Analog/Digital IO (ADIO) Board is an offthe-shelf, complete data acquisition system in
a compact PC/104 packaging. The analog
section contains 32 input channels, multiplexed A/D converter with 16 bit resolution
and 10uS conversion time. Input ranges are
+/-5v or +/- 10V. It also includes on-board
DMA support. The analog output section includes two 12 bit D/A converters. Both sections features simplified calibration using on
board programmable digital potentiometer.
The digital I/O section provides 24 digital I/O
lines, which feature high current TTL drivers.
The board requires only +5V from the system
power supply and generates its own +/-15V
analog supplies on board. The board operates
over the Extended Temperatures range of -25
to +85C. Figure 1-8 depicts the ADIO board
and Figure 1-9 depicts the ADIO block diagram.
1-10 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
c. Programmable Input Ranges
A programmable gain amplifier, programmable unipolar/bipolar range, and
programmable 5V/10V full-scale range
combine to give the ADIO board a total of
10 different possible analog input ranges.
All range settings are controlled in software for maximum flexibility.
The ADIO board has an extra A/D trigger
and sample control signals in the design.
Seven auxiliary digital I/O lines on the
analog I/O connector provide a sample/hold output signal, A/D trigger in and
out lines (to enable synchronization of
multiple boards) and external A/D clocking.
Gain
Input
Range
Resolution
e. Analog Outputs
The ADIO board contains 4 12-bit analog
outputs with autocalibration capability. Up
to 5mA of output current per channel can
be drawn from all channels simultane-
ously. Both unipolar and bipolar output
ranges are supported with jumper con-
figuration. And on power up, all outputs
are reset to 0V automatically.
Mode
Unipolar10V0-10V2.44mV
Unipolar5V0-5V1.22mV
Bipolar10V±10V4.88mV
Bipolar5V±5V2.44mV
f. FIFO and 16-Bit Bus Interface
An on-board 1024-byte FIFO enables the
ADIO board to work with Windows 95 and
NT by dramatically reducing the interrupt
overhead. Each interrupt transfers 256 2-
byte samples, or half the buffer, so the
interrupt rate is 1/256 the sample rate.
FIFO operation can be disabled at slow
sample rates, so there is no lag time be-
tween sampling and data availability. The
16-bit interface further reduces software
overhead by enabling all 16 A/D bits to be
read in a single instruction, instead of re-
quiring 2 8-bit read operations. The net
result of this streamlined design is that the
ADIO board supports gap-free A/D sam-
pling at rates up to 200,000 samples per
second, twice as fast as our previous
boards.
Full-
scale
Output
Range
Resolution
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-11
Instruction Manual
748467-A
January 2002
Model MicroCEM
+15V -15V
DC/DC
+15V
ADDR
CTRL
16-BIT DATA
AUTOCALIBRATION
CIRCUIT
1K X8
FIFO
MASTER
CONTROLLER
8255 CIRCUIT
16-BIT A/D
CONVERTER
X1,2,4,8
PROGRAMMABLE
GAIN AMP
12-BIT A/D
CONVERTERS
82C54
COUNTER/TIMER
10 MHZ
OSCILLATOR
INPUT MUX
HIGH CURRENT
DRIVE
ANALOG
INPUTS
0-31 SE
0-15 DI
ANALOG
OUTPUTS 0-3
TIMING AND
CONTROL SIGNALS
24 DIGITAL I/O
PC/104
BUS
Figure 1-9. ADIO Block Diagram
BUFFER
BUFFER
BUFFER
BUFFER
PORT A
PORT B
PORT CH
PORT CL
ACK/STROBE
1-12 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
g. Specifications
Analog Inputs
Number of inputs ................... 32 single-ended, 16 differential, or 16 SE + 8 DI; user selectable
A/D resolution ........................ 16 bits (1/65,536 of full scale)
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-13
Instruction Manual
748467-A
January 2002
Model MicroCEM
1-7 PCMCIA ADAPTER
The PCMCIA adapter board (Figure 1-10)
supports Type I, II and III PCMCIA cards. The
board is in full compliance with Microsoft FFSII, PCMCIA V.2 and JEIDA 4.1 specifications.
The PCMCIA socket accepts The following
PCMCIA cards:
Type IMemory, Flash/SRAM/ROM
Type IIFax, Modem, LAN, Wireless LAN,
and SCSI
Type III ATA mass storage
a. Features
Dimensions
Compliant with the PC/104 standard
Compatible with AT PC/104 CPU modules
Functions on board
2 PCMCIA slots
Optional remote socket
PCMCIA features
Supports PCMCIA V.1.0 and V.2.0
Supports PCMCIA types I, II and III
Supports both I/O and Memory Card
Supports Hot insertion
Operating Systems
DOS and Windows and any other RTOS
that supports PCMCIA
Software mappable memory windows and
one I/O window.
Jumperless interrupt steering from PC
Card to system.
Complete set of device drivers complying
with PCMCIA V2.1 /JEIDA V4.1, running
under MS-DOS or MS-WINDOWS:
• PCMCIA socket & card services drivers
• Flash File System
1-14 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
1-8 MODEM
Instruction Manual
748467-A
January 2002
The PC/104 Modular Modem is a selfcontained modem module that provides the
flexibility to include modem functionality into
embedded system, with minimal engineering
resources. The PC/104 Modular Modem is full
featured including high-speed data and fax
transmission. The PC/104 Modular Modems
support both dial-up and 2-wire leased-line.
Figure 1-11 depicts the Modem.
a. Features
V.90, 56 kbps data (560PC/104)
V.34, 33.6 kbps data (336PC/104)
14.4 kbps fax
Voice playback and record
DTMF decode
-40oC to 85oC operation
3.775" x 3.550" x 0.568" (with modular
phone jack)
3.775" x 3.550" x 0.435" (without modular
phone jack)
8 bit PC/104 bus type
V.42 and MNP 2-4 error correction
V.42bis, and MNP-5 data compression
FCC Part 68 registered
FCC Part 15 compliant
2 wire leased-line and dial up support
Industry Canada CS-03 certified
Figure 1-11. Modem
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-15
Instruction Manual
748467-A
January 2002
1-9 FLASH DRIVE
Model MicroCEM
Figure 1-12. 128MB Flash Drive
a. Specifications
System Performance
All values quoted are typical at ambient temperature and nominal supply voltage unless otherwise
stated.
All performance timing assumes the controller is in the default (i.e., fastest) mode.
Start-up Time
Sleep to Write................................ 2.5 msec max.
Sleep To Read .............................. 2.5 msec max.
Reset to Ready.............................. 50 msec typical, 400 msec max.
Weight .......................................... 9.1 oz (260 g) with battery
Operating Temperature ................. 32–104° F (0–40° C)
Storage Temperature ................... 32–140° F (0–60° C)
Humidity......................................... 90% relative humidity at 104° F (40° C)
Model MicroCEM
Figure 1-13. Pocket PC
1-18 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
Model MicroCEM
1-11 WIRELESS LAN ADAPTER
Wireless LAN adapter is an option to allow the user to remove the Pocket PC from the enclosure and to
operate the MicroCEM from a distance up to 1000 feet. Figure 1-14 depicts the wireless LAN adapter.
Figure 1-14. Wireless LAN Adapter
a. Specifications
Data Rate ...................................... 11 Mbps send/receive with automatic fallback for extended range
Useful Range................................. Up to 1000 feet (300 meters) open field; 300 feet (90 meters) typi-
cal indoor installations (intervening metal and thick concrete structures degrade performance and range)
Security.......................................... Supports Wired Equivalent Privacy (WEP) which provides 64-bit
and 128-bit data encryption; additional security through the use of a
32-character network system ID
Standard Support .......................... Interoperable with 2 Mbps IEEE 802.11 Direct Sequence Spread
Spectrum (DSSS) and 802.11b (11 and 5.5 Mbps) extension
OS Support.................................... NDIS drivers included for Windows 95, 98, ME and NT and 2000
Channels ....................................... Supports 11 US/Canada and 13 ETSI selectable, fully-independent
channels
Transmit Power ............................. 25mW typical
Radio Frequency ........................... 2.4 to 2.4835 GHz
748467-A
January 2002
Power Requirement....................... PC Card: 5 VDC @ 217 mA average with 338 mA maximum on
transmit; 215 mA continuous receive, 17 mA standby
PCI: 5VDC @ 247 mA average with 368 mA maximum on transmit;
245 mA continuous receive, 47 mA standby
Status lights ................................... 1 (Reports: Link, Power)
Regulatory Approval...................... US - FCC part 15B and 15C, IC RSS-210
ETSI - FCC part 15B, CE, ETS 300 328, ETS 300 826, C-Tick
(Australia)
Physical Specification.................... PC Card: PCMCIA Type II PC Card
External: 2.2dBi dipole; additional options for specific installation
needs
Rosemount Analytical Inc. A Division of Emerson Process ManagementDescription and Specifications 1-19
Instruction Manual
748467-A
January 2002
1-12 500 WATTS POWER SUPPLY
The 500 Watts power supply combine high performance midrange power with high power density (4.4
3
watts/in
cial and industrial systems. Providing tightly regulated DC power, the power supply delivers full output performance with only 300 Linear Feet per Minute (LFM) forced air-cooling by utilizing a factory installed fan.
Other features include remote sense, power fail, logic level inhibit, DC power good. Main channel current
sharing is provided for redundant applications. The power supply is approved to the latest international
regulatory standards, and displays the CE Mark.
),active Power Factor Correction (PFC) and high reliability to meet the requirements of commer-
Model MicroCEM
Figure 1-15. 500 Watts Power Supply
a. Features
• Power Factor Correction (PFC) Meets EN61000-3-2
• Fully Regulated Outputs
• Remote Sense
• Current Share, Power Fail, and Power Good Signals
• Overtemperature, Overvoltage, and Overcurrent Protected
• Available with Metric or SAE Mountings
• Input Transient & ESD Compliance to EN61000-4-2/-3/-4/-5
• Fan Output Voltage and Optional Fan
• Optional Isolation Diodes for Parallel or Redundant Operation
1-20 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
1-13 MicroCEM SPECIFICATIONS
a. Analyzer
Power ............................................ Universal Power Supply 85 – 264 VAC, 50 – 60 Hz, + 10%, 500
Sample Pump................................ 316 SS diaphragm type
Instrument Air Requirements......... Instrument grade air required. 15 SCFM @ 60 -100 PSIG (30 sec-
1
0-10ppm NOx range is <± 3%.
Permeation Tube (-30° C) dewpoint.
Customer instrument air required @ 5 L/M, -40° C dewpoint
spools)
Enclosure is 300'. (Response time is 20 seconds/100' w/1/4" tub-
ing).
to cut to length in field.)
onds 2 times per day). (Pressure Regulation by Customer.)
1-22 Description and SpecificationsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
SECTION 2
INSTALLATION
WARNING
ELECTRICAL SHOCK HAZARD
POSSIBLE EXPLOSION HAZARD
Do not open while energized. Do not operate without doors and covers secure.
Installation requires access to live parts
which can cause death or serious injury.
DANGER.
ELECTRICAL SHOCK HAZARD
Installation and servicing of this device requires access to components that may
present electrical shock and/or mechanical
hazards. Refer installation and servicing to
qualified service personnel.
CAUTION.
CODE COMPLIANCE
Installation of this device must be made in
accordance with all applicable national
and/or local codes. See specific references on the installation drawing located
in the rear of this manual.
CAUTION.
2-1 OVERVIEW
a. Limitations
Ambient Temperature:-30° to 50° Celsius
(-4° to 122° F)
Relative Humidity:5% to 99%
b. Mounting Options
Although the MicroCEM is enclosed in an
environmentally sealed enclosure, it
should be protected from direct sunlight.
In areas subjected to harsh winter climates, protection should be provided from
sun, rain and snow. A corrugated awning
or other suitable means can be provided
to meet these conditions.
2-2 LOCATION
The MicroCEM is designed to be installed in
an outdoor environmental location. It is recommended that the analyzer be located out of
direct sunlight and direct rain/snow to the extent possible.
The MicroCEM analysis enclosure should be
installed as near as possible to the
probe/sample handling enclosure, in order to
avoid low response time caused by long sample gas lines.
PRESSURIZED GAS
This unit requires periodic calibration with
a known standard gas. It also may utilizes
a pressurized carrier gas, such as helium,
hydrogen, or nitrogen. See General Precautions for Handling and Storing High
Pressure Gas Cylinders, page P-5.
Rosemount Analytical Inc. A Division of Emerson Process ManagementInstallation 2-1
Instruction Manual
748467-A
January 2002
Model MicroCEM
4.3
109.2
SAMPLE
CALIBRATION
GAS 3
GAS 2
GAS 1
OZONE / AIR
VENT
11.6
295.3
4.9
124.5
1.5
TYP
38.1
KEY LOCK
1.1
27.9
17.9
456.9
MOUNTING
DIMENSION
20.2
513.1
25.2
640.1
1.1
27.9
HINGE
TYP
24.6
624.8
25.5
647.7
MOUNTING
DIMENSION
CLEARANCE HOLE
FOR 3/8 BOLT
(4 PLACES)
7.1
180.3
4.9
124.5
AC POWER
INPUT
ANALOG
INTERFACE
1.5
38.1
DIGITAL
INTERFACE
TYP
RS232
INTERFACE
LAN
INTERFACE
RS485
INTERFACE
PHONE
ANTENNA
LINE
Figure 2-1. MicroCEM Outline and Mounting Dimensions
2-2 InstallationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
2-3 GASES
NOTE
For external gas lines, the use of new tubing throughout is strongly recommended.
The preferred type is teflon or stainless
steel, sealed at both ends.
a. Connection
Besides sample gas, the MicroCEM requires other gases for operation. In most
cases, one or more Calibration Standards
must be provided. These should be cylinders of gas which closely resemble the
expected sample, both in species and
concentrations. These calibration gases
are normally introduced into the system
as an input to the Sample Conditioning
Plate Option or sample conditioning may
be provided by others.
Each gas cylinder should be equipped
with a clean, hydrocarbon free two-stage
pressure regulator with indicating gauges
of approximately 0 to 3000 psig (0 to 20.7
bar) for cylinder pressure and 0 to 100
psig (0 to 6.7 bar) for delivery pressure.
Pressure regulators should have a metallic as opposed to elastomeric diaphragm,
and provide for ¼ inch compression fitting
outlet and should be LOX clean.
NOTE
All connections specified in the Installation Drawing, in conjunction with
the Application Data Sheet, should be
made.
b. Conditioning
system is used with corrosive gases, it
must be verified that there are no gas
components which may damage the gas
path components.
The gas conditioning must meet the following conditions:
Free of condensable constituents
•
Free of dust above 2 µm
•
Free of aggressive constituents which
•
may damage the gas paths
Temperature and pressure in accor-
•
dance with the specifications
When analyzing vapors, the dewpoint of
the sample gas must be at least 10 °C
below the ambient temperature in order to
avoid the precipitation of condensate in
the gas paths.
An optional barometric pressure compensation feature can be supplied. This requires a pressure sensor with a range of
800 – 1,100 hPa. The concentration values computer by the detectors will then
be corrected to eliminate erroneous
measurements due to changes in barometric pressure.
The gas flow rate must be in the range of
0.2 l/min to a maximum of 1.5 l/min. A
constant flow rate of 1 l/min is recommended.
NOTE
The maximum gas flow rate for paramagnetic oxygen detectors is 1.0
l/min!
All gases must be supplied to the analyzer as conditioned gases! When the
Rosemount Analytical Inc. A Division of Emerson Process ManagementInstallation 2-3
Instruction Manual
748467-A
January 2002
Model MicroCEM
SAMPLE
CAL
CAL GAS 3
CAL GAS 2
CAL GAS 1
OZONE AIR
EXHAUST
3-WAY
VALVE
2-WAY VALVE
MANIFOLD
ASSEMBLY
Figure 2-2. MicroCEM Gas Connections
IN
FLOWMETER
W/VALVE
GAUGE
638614
REGULATOR
904017
OZONE GENERATOR
659494
NDIR DETECTOR
90003225
PARAMAGNETIC
DETECTOR
90003311
CAPILLARY
VENT
634398
OUT
CONVERTER
656715
DETECTOR
659754
Figure 2-3. MicroCEM Flow Diagram
2-4 InstallationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Sample Inlet
½” FPT
Stack
Sample
Sample Handling System
Power In
115 VAC 60Hz 5A
Instruction Manual
748467-A
January 2002
MicroCEM Analyzer
Instrument
Air
¼” Teflon tubing. Customer supplied.
3
Drain to safe location.
2
Customer supplied.
1
3
2
Atmospheric
Pressure
Calibration Line
to Analyzer
3
Sample From
Analyzer
Dry Contact
Initiate Auto Calibration
O2 / NO
Mid Range
1
High Range
O2 / NO
1
Nitrogen
Electrical connections. See
Section 2-4 and Figure 2-5.
Figure 2-4. MicroCEM Installation and Test Setup Configuration
Rosemount Analytical Inc. A Division of Emerson Process ManagementInstallation 2-5
Instruction Manual
748467-A
January 2002
2-4 ELECTRICAL CONNECTIONS
NOTE
The enclosure is a NEMA 4. All entry locations must be sealed.
Connect all required signal cables to the connections at the bottom of the MicroCEM. The
cable locations are indicated on the inside
bottom cover of the MicroCEM box. The ac-
Model MicroCEM
tual electrical connections will be specified in
the Application Data package. All connections
are not necessary for every application.
Cable length for these signals should not exceed 3,000 feet (914 meters), to avoid excessive capacitance and corresponding signal
distortion.
All electrical connections are made through
the bottom of the MicroCEM enclosure using
circular connectors.
AC POWER
INPUT
ANALOG
INTERFACE
DIGITAL
INTERFACE
RS232
INTERFACE
LAN
INTERFACE
RS485
INTERFACE
PHONE
LINE
AC POWER INPUT – J1LAN INTERFACE – J5
ANALOG INTERFACE – J2RS485 INTERFACE – J6
DIGITAL INTERFACE – J3PHONE LINE – J7
RS232 INTERFACE - J4ANTENNA – J8
Figure 2-5. MicroCEM Electrical Connections
ANTENNA
2-6 InstallationRosemount Analytical Inc. A Division of Emerson Process Management
Connect AC power through a 10A circuit
breaker that is to be located close to the
MicroCEM. The circuit breaker will provide over current protection as well as a
means of disconnecting the power.
Maximum power requirements will be 380
watts, with most applications requiring
less than this amount.
b. Circular Connector Assembly Instruc-
tions
Wire Stripping
Strip insulation from end of wire to be
crimped. Do not cut or damage wire
strands. Refer to table for proper stripping dimensions.
A
2. Using correct crimp tool and locator,
cycle the tool once to be sure the indentors are open. Insert contact and
wire into locator. Squeeze tool handles firmly and completely to insure
a proper crimp. The tool will not release unless the crimp indentors in
the tool head have been fully actuated.
Wire SizeDim. A
22O or 22M*.125 (3.18)
20.188 (4.77)
16.188 (4.77)
12.188 (4.77)
*Inactive. Not recommended for new
design, replacement only.
Contact Crimping
1. Insert stripped wire into contact crimp
pot. Wire must be visible through inspection hole.
Visual Inspection Hole
3. Release crimped contact and wire
from tool. Be certain the wire is visible through inspection hole in contact.
2-8 InstallationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
Contact Insertion
1. Remove hardware from plug or receptacle and slip over wire bundle in
proper order for reassembly.
2. Using proper plastic or metal insertion
tool for corresponding contact, position wire in tip of the tool so that the
tool tip butts up against the contact
shoulder.
3. Press tool against contact shoulder
and, with firm and even pressure, insert wired contact and tool tip into
center contact cavity. A slight click
may be heard as metal retaining tines
snap into place behind contact shoulder.
4. Remove tool and pull back lightly on
wire to make sure contact is properly
seated. Repeat operation with remainder of contacts to be inserted,
beginning with the center cavity and
working outward in alternating rows.
5. After all contacts are inserted, fill any
empty cavities with wire sealing plugs.
Reassemble plug or receptacle hardware.
Rosemount Analytical Inc. A Division of Emerson Process ManagementInstallation 2-9
Instruction Manual
748467-A
January 2002
Contact Extraction
1. Remove hardware from plug or receptacle and slide hardware back
along wire bundle.
Model MicroCEM
4. Hold wire firmly in tool and extract
wired contact and tool. Repeat operation for all contacts to be extracted.
2. Using plastic or metal extraction tool
with proper color code corresponding
to contact size, place wire in tool.
3. Insert tool into contact cavity until tool
tip bottoms against the contact shoulder, expanding clip retaining tines.
5. Fill any empty wire cavities with wire
sealing plugs.
6. Reassembly plug or receptacle.
2-10 InstallationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
c. Interface Connections
Instruction Manual
748467-A
January 2002
ConnectionDesignator
AC PowerJ112316Table 2-2
Analog InterfaceJ2122226, 24, 22Table 2-3
Digital InterfaceJ3143726, 24, 22Table 2-4
RS232J4101328, 26, 24Table 2-5
LAN InterfaceJ58628, 26, 24, 22Table 2-7
RS485J68324, 22, 20Table 2-6
Phone Line (Modem)J78324, 22, 20Table 2-8
Antenna (Peltier Power)J816314, 12Table 2-9
Table 2-1. Interface Connections
SIGNAL NAMEDEFINITIONPIN
L1A
L2
GNDAC GroundB
Table 2-2. AC Power Connection Terminal Assignments
85-264 VAC, 47-440 Hz
Shell
Size
No.
Contacts
AWGTable
C
SIGNAL NAMEDEFINITIONPIN
O2CL+1
O2CL-
COCL+3
COCL-
NOX+5
NOX-
EXP1CL+7
EXP1CL-
EXP2CL+9
EXP2CLBAROP+11
BAROP-
Table 2-3.Analog Output Terminal Assignments
O2 Reading, 4-20 mA Output
CO Reading, 4-20 mA Output
NOX Reading, 4-20 mA Output
External process No. 1, Current Loop input, 4-20 mA
External process No. 2, Current Loop input, 4-20 mA
Barometric pressure Compensator 0-10V input
2
4
6
8
10
12
Rosemount Analytical Inc. A Division of Emerson Process ManagementInstallation 2-11
Data Carrier Detect Input
Data Set Ready Input
Receive Data Input
Request to Send Output
Transmit Data Output
Clear To Send Input
Data Terminal Ready Output
Ring Indicator Input
Rosemount Analytical Inc. A Division of Emerson Process ManagementInstallation 2-13
Instruction Manual
748467-A
January 2002
Model MicroCEM
2-5 ANALYTICAL LEAK CHECK
If explosive or hazardous gas samples are
being measured with the MicroCEM, it is recommended that gas line fittings and components be thoroughly leak-checked prior to
initial application of electrical power, bimonthly
intervals thereafter, and after any maintenance which involves breaking the integrity of
the sample containment system.
a. Flow Indicator Method
Supply air or inert gas such as nitrogen,
at 10 psig (689 hPa), to the analyzer
through a flow indicator with a range of 0
to 250 cc/min. Install a shut-off valve at
the sample gas outlet. Set the flow rate to
125 cc/min.
Close the outlet shut-off valve and notice
that the flow reading drops to zero. If the
flow reading does not drop to zero, the
system is leaking and must be corrected
before the introduction of any flammable
sample gas or application of power.
MicroCEM Analyzer
N
2
10 psig
(69 kPa)
Inlet Outlet
Flow Meter
Gas Outlet
Figure 2-7. Leak Test Flow Method
2-14 InstallationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
b. Manometer Method
Install a water-filled U-tube manometer at
the sample gas outlet. Install a shut-off
valve at the sample gas inlet. Admit air or
inert gas to the inlet shut-off valve until
the analyzer is pressurized to approximately 50 hPa. The water column will be
about 500 mm.
MicroCEM Analyzer
Inlet Outlet
Close the inlet shut-off valve and, following a brief period for pressure equilibrium,
verify that the height of the water column
does not drop over a period of about 5
minutes. If the water column height drops,
the system is leaking and must be corrected before the introduction of any
flammable sample gas or application of
power.
N
2
Water
Figure 2-8. Leak Test Manometer Method
Overpressure
Approx. 50 hPa
Rosemount Analytical Inc. A Division of Emerson Process ManagementInstallation 2-15
Instruction Manual
748467-A
January 2002
Model MicroCEM
2-16 InstallationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
CAUTION.
Instruction Manual
748467-A
January 2002
SECTION 3
OPERATION
Do not operate or service this instrument before reading and understanding
this instruction manual and receiving
appropriate training.
Refer to installation drawing supplied
with the application data package.
3-1 STARTUP PROCEDURE
Once the MicroCEM has been correctly assembled and installed in accordance with
the instructions in Section 2, the analyzer is
ready for operation.
Before operating the system, verify that the
leak checks have been performed and that
the sample handling unit is performing correctly.
Apply power to the system and verify that
sample gas is flowing.
NOTE
A warm-up time of from 15 to 50 minutes
is required depending on the installed
detector(s).
a. Connecting Pocket PC to MicroCEM
1. Open MicroCEM door. Refer to
Figure 3-2.
2. Plug RS232 plug into adapter located on front panel.
3. Plug power supply cable into 5V
adapter
4. Turn Pocket PC on
5. In order to assure no other windows are open press the reset
button. Reset button is located on
the back of the pocket PC.
6. Using the MicroCEM menu click on
“programs”
7. Click on “Connection” icon
8. Click on “uCEM” icon.
9. Go to tools menu and click on MicroCEM .
10. Unit will display data in 3 to 5 seconds.
Analyzer operation can be confirmed on the
screen of the pocket PC through the glass
window on the door. Upon power up, the
analyzer will perform a self-test routine.
This test will last approximately 60 seconds.
3-2 POCKET PC USER INTERFACE
The MicroCEM User Interface runs on a
Pocket-PC with Windows CE operating
system. It communicates with the MicroCEM via serial communication port. All input to the Pocket-PC is done using a
pointing device that comes with the PocketPC.
Rosemount Analytical Inc. A Division of Emerson Process Management Operation 3-1
Figure 3-1. Pocket PC
Instruction Manual
748467-A
January 2002
Printer
Connector
5V
Connector
VGA
Connector
RS232
Connector
Model MicroCEM
Flowmeter
Heartbeat
LED
Keyboard
Connector
Mouse
Connector
USB
Connector
Reset
Button
Floppy
Connector
IDE
Connector
Figure 3-2. MicroCEM Front Panel
Trouble
LED
Power Switch
3-2 OperationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
b. Main Display
The MicroCEM Main Display (Figure
3-3) provides the status of the three
emissions channels. The status includes the current reading (updated
approximately every 2 seconds), the
Drag the edge of the
column to resize.
last 1-minute average, and the last 15minute average. The status column
(Sts) indicates the status of the measurement and can be any of the values
in listed in Table 3-1. (“Status” shown in
order of precedence. Maintenance
mode status takes highest precedence.)
S. = Status
See Table 3-1.
Use the scrollbar to
see full set of data.
Tools Menu
Provides access to all
functionality.
Note: Exit is only be available
when current user has
administrative access.
Toolbar Buttons
About
Data Logs
MicroCEM Admin
MicroCEM Settings
Alarms
Figure 3-3. MicroCEM Pocket PC Display (Main Display Shown)
STATUSDESCRIPTION
MIndicates that maintenance mode is active.
CCalibration in process
IInvalid Reading. Indicates that the reading is invalid due to calibration failure or sensor failure.
VValid Reading
PCustomer Process Off Line (Dry contact by customer)
OMicroCEM System Off
Table 3-1. Status Values
Rosemount Analytical Inc. A Division of Emerson Process Management Operation 3-3
Instruction Manual
748467-A
January 2002
Model MicroCEM
c. MicroCEM Menu
Clicking on the Tools text in the lower
left corner of the display activates the
MicroCEM menu. From this menu, all
of the MicroCEM user-interface functions can be accessed.
d. MicroCEM Alarms
The MicroCEM Alarms dialog shows all
the current alarms. A current alarm is
one with an Active status of 1 (active)
or an Acknowledged state of 0 (not acknowledged).. If the Show Historical
Alarms checkbox is checked, all noncurrent alarms are also shown (nonactive acknowledged alarms). Up to
100 alarms will be shown. To see more
than the last 100 alarms, the web
based MicroCEM interface must be
used. If one or more alarms are current, the most recent of them will be
displayed on the main display. If more
than one alarm is current “(more)” will
be displayed after the name of the most
recent alarm on the main window to indicate that more than one alarm is active. Horizontal scroll bar is be used to
see Date and Time of the Alarms.
On-screen keyboard is available
at any time by clicking on the
keyboard button.
Figure 3-4. MicroCEM Menu
Figure 3-5. Pocket PC Alarms Screen
Alarms with a critical level will cause
the System trouble output to become
active when the alarm is active. When
all active critical alarms are acknowledged, the System trouble output will
become inactive.
3-4 OperationRosemount Analytical Inc. A Division of Emerson Process Management
Instruction Manual
748467-A
Model MicroCEM
ALARM NAMELEVELDESCRIPTION
O2 Calibration FailedCriticalO2 Calibration Failed to meet the maximum Drift requirements
CO Calibration FailedCriticalCO Calibration Failed to meet the maximum Drift requirements
January 2002
NOx Calibration FailedCritical
O2 High LimitCriticalO2 Sensor reading is above the minimal acceptable limit
O2 Low LimitCriticalO2 Sensor reading is below the minimal acceptable limit
CO High LimitCriticalCO Sensor reading is above the minimal acceptable limit
CO Low LimitCriticalCO Sensor reading is below the minimal acceptable limit
NOx High LimitCriticalNOx Sensor reading is above the minimal acceptable limit
NOx Low LimitCriticalNOx Sensor reading is below the minimal acceptable limit
24V Over MaxCritical24V diagnostic input exceeds the specified maximum
24 Low MinCritical24V diagnostic input is below the specified minimum
O2 Emission LimitWarningO2 reading is over the specified Limit
CO Emission LimitWarningCO reading is over the specified Limit
NOx Emission LimitWarningNOx reading is over the specified Limit
Converter Over TempCritical
Converter Low TempCriticalConverter temperature reading is below the specified minimum
Zone Over TempCriticalZone temperature reading exceeds the specified maximum
NOx Calibration Failed to meet the maximum Drift requirements
Converter temperature reading exceeds the specified maximum
Zone Low TempCriticalZone temperature reading is below the specified minimum
PDT Over TempCritical
PDT Low TempCritical
PMT Over TempCritical
PMT Low TempCritical
Warm-up Time LimitCriticalSystem Warm-up process exceeded the specified time limit
Rosemount Analytical Inc. A Division of Emerson Process Management Operation 3-5
Peltier Cooler (PDT) temperature reading exceeds the specified maximum
Peltier Cooler (PDT) temperature reading is below the specified
minimum
PDD Chamber temperature reading exceeds the specified
maximum
PDD Chamber temperature reading is below the specified
minimum
Table 3-2.Alarm Summary
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January 2002
Model MicroCEM
e. MicroCEM Login
The login dialog appears (Figure 3-6)
when first requesting the MicroCEM
Settings or MicroCEM Admin. If a valid
user name and password are entered,
the user logging in will have permission
to use the MicroCEM Settings and/or
the MicroCEM Administration (Refer to
the User Settings page of the MicroCEM Settings dialog). After logging in
the first time, it is not required again
until the user logs out, or is logged out
automatically because of a period of inactivity (Refer to the Auto Logout page
of the MicroCEM Administration dialog).
f. MicroCEM Login-Current User Indi-
cation
When a user is logged in, the MicroCEM main display will indicate the user
name of the logged in user as shown in
Figure 3-7. When the user logs off, the
current user and the Logoff button will
not be shown.
Current User
Logoff Button
Figure 3-7. Current User Indication
Figure 3-6. MicroCEM Login
3-6 OperationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
3-3 MicroCEM SETTINGS
The MicroCEM Settings dialog is only
available to users with MicroCEM Settings
permission. If a user is not currently logged
in, the login dialog will be displayed. If the
current user doesn’t have MicroCEM Settings permission, a message will be displayed which reads “Permission denied”.
When the MicroCEM Settings are invoked
from the Tools menu or the MicroCEM Settings button, the MicroCEM Settings tabbed
dialog is displayed. The Range page (tab)
is displayed initially.
a. Range
The Range Settings page is used to set
the range of the Emissions analog outputs. The outputs support dual range
mode. When the emission is below the
Range 1 value, the output switches to
Range 1 mode and the Range 1 value
becomes the full-scale value of the output. The range indication digital output
will change to the Range 1 state.
When the emission is above the Range
1 value, the output switches to Range 2
mode and the Range 2 value becomes
the full-scale value of the output. The
range indication digital output will
change to the Range 2 state. The
Range 2 settings cannot be changed
and are factory-set.
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Tabs allow selection of the
MicroCEM Settings pages
Figure 3-8. Range Settings
NOTE
If only one range is needed, set the
Range 1 values to the range 2 value.
This will disable the dual range feature.
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b. Auto Calibration
The Auto-Calibration settings are set on
the Auto-Calibration page of the MicroCEM settings. If auto calibration is
turned to the on position, then the user
can select time and/or frequency of the
auto calibration in the Auto Calibration
Frequency tab (Section 3-3c).
c. Auto Calibration Time and Fre-
quency
The Auto-Calibration Time and Frequency tab allows specifying time and
frequency of the auto-calibration. Time
field requires military time format.
Figure 3-9. Auto Calibration Settings
Figure 3-10. Auto Calibration Time and
Frequency
3-8 OperationRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
d. Manual Calibration
A dry-run Calibration may be initiated
from the Manual Calibration page of the
MicroCEM Settings. The results of the
calibration will not be applied and only
provide a dry run of the calibration. If
desired a partial calibration may be invoked for one or more of the emission
types. While the manual calibration is
in process, a calibration progress dialog
will be displayed as shown inFigure
3-26. When the manual calibration is
completed, the results are displayed in
the Manual Calibration Results dialog
as shown in Figure 3-12. If the Local
Calibration checkbox is checked, the
Local Calibration valve will be used
during the calibration rather than the
probe Calibration valve.
Instruction Manual
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January 2002
NOTE
“Start Autocalibration now” will invoke a real calibration and will apply
new correction factor results when
done.
Figure 3-12. Manual Calibration Results
Figure 3-11. Manual Calibration
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e. Limits
The emission limits alarms can be set
on the Limits page of the MicroCEM
Settings. When a measured emission
exceeds its limit, the emission will have
a limit-exceeded status. This is indicated on the main display and on the
Data-Logs display. It is also indicated
in the limit exceeded digital output.
f. Calibration Gas
The Calibration Gas emissions quantities and Gas Bottle allocation may be
set on the Calibration Gas page of the
MicroCEM Settings. This should be set
whenever a Calibration Gas container
is replaced.
Place the span gas value of the particular gas cylinder in the span column.
I mid calibration gas can also be
hooked up the MicroCEM. Insert its
span gas value in the mid span boxes.
If a dual range is used use the Mid
Span column.
Figure 3-13. Limit Settings
Figure 3-14. Calibration Gas Settings
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g. Maintenance Mode
Maintenance mode may be selected for
any of the emission types on the Maintenance Mode page of the MicroCEM
Settings.
Choosing maintenance mode will invoke an “M” flag” onto the data. Customer can perform routine maintenance
while in this setting
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Figure 3-15. Maintenance Mode Settings
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3-4 MicroCEM FACTORY SETTINGS
A MicroCEM Factory Settings program is
available for use by MicroCEM technicians
to set parameters in the MicroCEM or a
qualified customer technician. Enter the
Factory Settings password at the login dialog to enter the Factory Settings. This
password will not be provided to the customer. The list of settings is shown in Table 3-3 and Table 3-4.
The user must purchase a PC/104 to
mouse and PC/104 to monitor in order to
access the factory settings. Consult
Rosemount for details.
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Model MicroCEM
Calibration SettingDescription
O2ZeroDriftLimitO2 Allowed Zero Drift Limit.
COZeroDriftLimitCO Allowed Zero Drift Limit.
NOXZeroDriftLimitNOx Allowed Zero Drift Limit.
OSMidDriftLimitO2 Allowed Mid Drift Limit.
COMidDriftLimitCO Allowed Mid Drift Limit.
NOXMidDriftLimitNOx Allowed Mid Drift Limit.
O2SpanDriftLimitO2 Allowed Span Drift Limit.
COSpanDriftLimitCO Allowed Span Drift Limit.
NOXSpanDriftLimitNOx Allowed Span Drift Limit.
O2SlopeDefault value for the O2 slope
O2OffsetDefault value for the O2 offset
COSlopeDefault value for the CO slope
COOffsetDefault value for the CO offset
NOXSlopeDefault value for the NOx slope
NOXOffsetDefault value for the NOx offset
O2SpanDefDefault O2 Span Calibration Gas value
O2MidSpanDefDefault O2 Mid Span Calibration Gas value
COSpanDefDefault CO Span Calibration Gas value
COMidSpanDefDefault CO Mid Span Calibration Gas value
NOXSpanDefDefault NOx Span Calibration Gas value
NOXMidSpanDefDefault NOx Mid Span Calibration Gas value
Gas1AllocationDefault Gas 1 allocation
Gas2AllocationDefault Gas 2 allocation
Gas3AllocationDefault Gas 3 allocation
AutoCalFrequencyDefault Auto-Calibration frequency in hours and minutes (example: 24:00).
AutoCalTimeDefault Auto-Calibration time in hours and minutes (military time).
Purge1Default auto-calibration Purge 1 value in seconds.
Gas1Default auto-calibration gas 1 time in seconds.
Gas2Default auto-calibration gas 2 time in seconds.
Gas3Default auto-calibration gas 3 time in seconds.
Purge2Default auto-calibration Purge 2 value in seconds.
If the drift exceeds the allowed amount a drift alarm
will occur, and the readings on the channel will no
longer be valid until a successful calibration is completed.
Initial values for the emissions conversion slope and
offset used on a new system before the first Calibration is performed. These values should be set
manually before the first auto-calibration is performed.
This sets the O2 % low limit, below which a limit alarm will occur.
This sets the O2 % high limit, above which a limit alarm will occur.
This sets the CO low limit, below which a limit alarm will occur.
This sets the CO ppm high limit, above which a limit alarm will occur.
This sets the NOx low limit, below which a limit alarm will occur.
This sets the NOx ppm high limit, above which a limit alarm will occur.
This setting is used to record the MicroCEM Serial Number.
Percent O2 used in Diluent correction.
This is the minimum current that must be measured by a current analog input for a
heater/cooler/fan to be considered on. This is used for heater/cooler/fan failure detection.
This is the maximum current that must be measured by a current analog input for a
heater/cooler/fan to be considered off. This is used for heater/cooler/fan failure detection.
This indicates which NDIR reading is made when the sync goes from high to low:
Reference (R) or Sample Gas (S).
If the +24V measurement is below this level it will cause an alarm.
If the +24V measurement is above this level it will cause an alarm.
For calibration – The amount of time to wait after turning on a valve.
These limits are the default values. On the Pocket PC these values will be used
when one of the “Defaults” buttons are pressed.
1 = Sample pump is used. 0 = Sample pump not used.
Directory where log files are saved (C:\uCEM\Logs).
Maximum time allowed for the uCEM to warm-up when it is started up. If all temperature zones are not within allowed range within this period of time, the uCEM will
shutdown all heaters, coolers and processes.
The full path to the file which maintains the state of the uCEM.
(C:\uCEM\mcem.state)
The IP address to use when listening for incoming connections.
The IP Port to use when listening for incoming connections.
100
The full path to the file which maintains the current state of the alarms.
(C:\uCEM\alarms.state)
Auto Log-off time in minutes
The full path to the file that maintains the user list (C:\uCEM\mcem.userlist)
Table 3-4. Factory Settings - General
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Instruction Manual
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a. PID Control Loop Factory Settings
These settings can be set for each of
the temperature control loops. The
temperature control loops include the
Control LoopSection Name
Zone Heater/Cooler[PIDSettings ZoneLoop]
Converter Heater[PIDSettings ConverterLoop]
PMT Heater[PIDSettings PMTLoop]
PMT Photo Diode Cooler[PIDSettings PDTLoop]
Table 3-5. PID Settings – Section Names
Zone heater/cooler, Converter Heater,
PMT Heater, and PMT Photo Diode
Cooler. Table 3-5 shows the section
names in the INI file used for each
temperature control loop.
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PID SettingDescription
PSetting
ISetting
DSetting
MaxSpeedSetting
ResetIntegralError
IntegralMaxPercent
IntegralMinPercent
MaxPercentMaximum zone output power in percent (0-100).
MinPercentMinimum zone output power in percent (0-100).
MinAlternationPercentMinimum
SetPoint
LowTempLimit
HighTempLimit
MaxOffCurrent
MinOnCurrent
Model MicroCEM
Proportional Gain. This parameter is set by using typical PID
tuning methods. The P setting is mandatory and is the first parameter to adjust. It provides a command directly proportional to
the error.
Integral Gain. This parameter is set by using typical PID tuning
methods. The I setting is optional and is used to make small adjustments to correct a small error which persists for a period of
time.
Derivative Gain. This parameter is set by using typical PID tuning
methods. The D setting is optional. It is used to adjust the command based on change in error. It can be used to reduce overshoot, which typically occurs when the P settings is used by itself.
This parameter tends to amplify any noise present in the input.
Should be set to the typical warm-up/cool-down speed in
°C/second when the heater/cooler is operated at 100% power.
Increasing this value effectively decreases the Proportional, Integral and Derivative gain. Decreasing this value effectively increases the Proportional, Integral and Derivative gain.
Integral Reset Error. Setting used to reset Integral value when
error is larger than this value. This parameter is used to prevent
the integral value from building up while the error is large and
then causing overshoot when the setpoint is reached.
Maximum percent output power that can be accumulated by the
Integral component. (0-100) The default is 10 percent.
Minimum percent output power that can be accumulated by the
Integral component. (0-100) The default is 10 percent.
This is the temperature setpoint, in degrees Celsius, for this temperature control loop.
If the temperature (°C) is below this value during the MicroCEM
process (not including the warm-up phase) an alarm will occur.
If the temperature (°C) is above this value during the MicroCEM
process (not including the warm-up phase) an alarm will occur.
If the current reading is below the maximum-off current while the
heater is turned off, the heater has failed with a Heater Control
failure.
If the current reading is below the minimum-on current while the
heater is turned on, the heater has failed with a Heater Burnout
status.
Table 3-6. PID Settings – Sections Descriptions
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3-5 MicroCEM ADMINISTRATION
The MicroCEM Administration dialog is only
available to users with MicroCEM Administration permission. If a user is not currently logged in, the login dialog will be
displayed. If the current user doesn’t have
MicroCEM Administration permission, a
message will be displayed which reads
“Permission denied”. When the MicroCEM
Administration is invoked from the Tools
menu or the MicroCEM Administration
button, the MicroCEM Administration
tabbed dialog is displayed. The User Settings page (tab) is displayed initially.
a. User Settings
The user settings page of the MicroCEM Administration dialog allows users
to be added, deleted or modified. Each
user has a name, password, and permission settings. The permission settings include Settings permission that
allows access to the MicroCEM Settings dialog, and Administrative permission that allows access to the
MicroCEM Administration dialog. The
Settings permission also allows a user
to access the MicroCEM remotely using the web-based interface.
b. Auto Logoff
The number of minutes of inactivity after which a user is automatically logged
off is set on the Auto Logoff page of the
MicroCEM Administration.
Figure 3-17. Auto Logoff
Figure 3-16. User Settings
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3-6 MicroCEM DATA LOGS
The MicroCEM maintains a minimum of 3
months of history in three types of data log
files. The first type of log file is the measurement log, which contains emission
measurements (at 1 minute intervals),
alarm indications and maintenance mode
indications. The second type of log file is
the calibration log file, which contains information on each auto calibration done.
The third is the alarm log file, which records
any improperly functioning hardware. The
data will be stored in flat, ASCII, CSV
(comma-delineated) file. This file format
can be read directly by MS Excel and imported into many types of software applications. The following parameters is factory
set for each of the log file types.
a. Maximum Log File Size
This is how large a log file can get (in
bytes) before it is closed and a new log
file is opened.
b. Maximum Number of Log Files
This is how many log files can be created. When the maximum number of
log files is reached, the oldest file is
overwritten when new ones are created.
Emissions Log:6
Calib Log:6
Alarm Log:6
c. Log File Name Format
The log file name uses the date that the
file was created. It is of the format
TYYYYMMDD.CSV where T is the log
file type (E=Emissions, C=Calibration
and A=Alarm), YYYY is the Year, MM
is the month, and DD is the day of the
month. For example, the file name
E20010329.csv contains emissions
data and was created on March 29,
CO StatusV=Valid, M=Maintenance Mode, C=Calibration in process,
NOx StatusV=Valid, M=Maintenance Mode, C=Calibration in process,
V=Valid, M=Maintenance Mode, C=Calibration in process,
I=Invalid (calibration failed or sensor in failed state)
I=Invalid (calibration failed or sensor in failed state)
I=Invalid (calibration failed or sensor in failed state)
Table 3-7. Measurement Log File Format
The log file contains data in a flat, ASCII, CSV file. The following are the
fields of the file, in order of occurrence.
The log file size will be about 42 bytes
per entry. 3 months of data logs will
require about 5,443,200 bytes
V
V
V
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e. Calibration Log File Format
The log file contains data in a flat, ASCII, CSV file. The following are the
NameDescriptionExample
Date/TimeMonth-day-year Hours:Minutes:Seconds3-7-2001 10:24:57
Zero TimeTime that Zero span started, Hours:Minutes:Seconds10:25:30
Mid TimeTime That Mid span started, Hours:Minutes:Seconds10:27:30
Span TimeTime that span started, Hours:Minutes:Seconds10:28:30
Purge TimeTime that the final purge started,
Hours:Minutes:Seconds
Finish TimeTime that the final purge finishes10:31:00
O2 Measured ZeroMeasured percent O2 for Zero phase of calibration0.0
O2 Expected ZeroExpected percent O2 for Zero phase of calibration0.0
O2 Zero DriftPercent drift of O2 zero calibration0.0
O2 Measured Mid SpanMeasured percent O2 for Mid span phase of calibration10.1
O2 Expected Mid SpanExpected percent O2 for Mid span phase of calibration10.0
O2 Mid DriftPercent drift of O2 mid calibration.-0.4
O2 Measured SpanMeasured percent O2 for Span phase of calibration20.2
O2 Expected SpanExpected percent O2 for Span phase of calibration20.3
O2 Span DriftPercent drift of O2 span calibration0.4
CO Measured Zero 1
CO Expected Zero0
CO Zero Drift0.3
CO Measured Mid Span23
CO Expected Mid Span24
CO Mid Span Drift-0.3
CO Measured Span45
CO Expected Span45
CO Span Drift0
NOx Measured ZeroMeasured ppm NOx for zero phase of calibration15
NOx Expected ZeroExpected ppm NOx for zero phase of calibration15
NOx Zero Drift0
NOx Measured Mid SpanMeasured ppm NOx for mid span phase of calibration30
NOx Expected Mid SpanMeasured ppm NOx for mid span phase of calibration30
NOx Mid Span Drift0
NOx Measured spanMeasured ppm NOx for span phase of calibration59
NOx Expected spanMeasured ppm NOx for span phase of calibration59
NOx Span Drift0
fields of the file, in order of occurrence.
The log file size will be about 178 bytes
per entry. 3 months of data logs will
require about 16000 bytes (based on
Calibration performed every 24 hours).
10:30:30
Table 3-8. Calibration Log File Format
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f. Alarm Log File Format
The log file contains data in a flat, ASCII, CSV file. The following are the
fields of the file, in order of occurrence.
1 = CO Calibration Failed **
2 = NOx Calibration Failed
3 = O2 High Limit
4 = O2 Low Limit
5 = CO High Limit **
6 = CO Low Limit **
7 = NOx High Limit
8 = NOx Low Limit
9 = O2 Emission Limit
10 = CO Emission Limit **
11 = NOx Emission Limit
12 = 5 Volt Fault **
13 = 6 Volt Fault **
14 = 24V Over Max
15 = 24 Low Min
16 = Converter Over Temp
17 = Converter Low Temp
18 = Converter On Failed **
19 = Converter Off Failed **
20 = Zone Over Temp
21 = Zone Low Temp
22 = Zone Heater On Failed **
23 = Zone Heater Off Failed **
24 = Zone Cooler On Failed **
25 = Zone Cooler Off Failed **
26 = Heater Fan On Failed **
27 = Heater Fan Off Failed **
28 = Cooler Fan On Failed **
29 = Cooler Fan Off Failed **
30 = PDT Over Temp
31 = PDT Low Temp
32 = PDT On Failed **
33 = PDT Off Failed **
34 = PMT Over Temp
35 = PMT Low Temp
36 = PMT On Failed **
37 = PMT Off Failed **
38 = O2 Over Temp **
39 = O2 Low Temp **
40 = O2 On Failed **
41 = O2 Off Failed **
42 = Warmup Time Limit
70 = IO Board Failed
Fault DescriptionASCII string describing fault. Up to 200 characters.CO Calibration Failed
The days or months maintained in the
Alarm Log depends on how often trouble conditions are recorded. If there
are rarely alarm conditions recorded,
there is enough space for many years
of alarm logs to be recorded.
2
** - Alarm is not implemented in this version of software or reserved for future use.
Table 3-9. Alarm Log File Format
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3-7 VIEW DATA LOGS
View Data Logs will start Internet Explorer
and display the Emissions page of the Mi-
croCEM web pages (see Figure 3-18 and
Figure 3-19). This page can be used to
view the Emissions log. Other pages may
be selected to view the calibration log and
the alarm log.
If Most Recent is selected, the
month day and hour do not
need to be selected.
Select the ending hour to view
(applicable only to 1- minute
averages)
Note the page header was scrolled out of view to show all the selection
options, but it can be seen in
Figure 3-19.
Figure 3-18. View Data Logs
Average PeriodTime Range Displayed
1 Minute1 Hour
15 Minutes1 Day
1 Hour3 Days
12 Hours1 Month
24 Hours3 Months
Table 3-10. Average Period Selection
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NOTE
The Real-time, Config and Download are included in the navigation menu but these pages are
intended for remote desktop use. As an enhancement these items could be hidden if the pages
are browsed from a Windows CE version of Internet Explorer.
Model MicroCEM
The Emission Data-Logs
data is shown here.
Alarms and Calibration data
may also be viewed.
A Date is shown for 1 min or 15
minute averages. A date range
is shown for 1 hour or greater
averages.
Figure 3-19. View Data Logs Table
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3-8 VIEWING MicroCEM DATA WITH A WEB
BROWSER
The log files may be accessed using a web
browser that has access to the MicroCEM
over a Wireless LAN, serial port connection
(PPP) or Dialup Connection (RAS). The
MicroCEM has Window CE Web Server installed and provides a Web-based interface
to select and download the Data-Log files.
The downloaded Data-Log files will be in a
CSV (comma delineated ASCII) format.
The log files may also be viewed as a web
page in a tabular format.
a. Real-Time Page
The Real-Time page provides a realtime display of the emission values and
emission statuses. The display is refreshed every 10 seconds.
Figure 3-20. Real-Time Web Page
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b. Emissions Page
The Emissions Page can be used to
view emission history in a tabular webpage format. This page is used as part
of the MicroCEM User interface as well
as by a remote user (probably from a
desktop computer).
The Emission Data-Logs table is displayed (as shown in Figure 3-19) after
selecting the Date and Average Period
If Most Recent is selected, the
month day and hour do not
need to be selected.
and pressing the Display button. If desired a bookmark or shortcut may be
made to the page displaying the table.
In the future, the same table can be
displayed by selecting this bookmark.
If Most Recent Data was selected, the
book-marked page will always display
Most Recent Data. If a specific date
was specified, the book-marked page
will always display the same date.
Select the ending hour to
view (applicable only to 1
minute averages)
Figure 3-21. Emissions Selection
Figure 3-22. Emissions Table
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Figure 3-23. Calibration Table
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c. Download Page
The download page of the MicroCEM
allows the selection and download of
the three types of Data-Logs. To
quickly download recent data, a
“Download Most Recent Emissions
Data” selection is provided. For more
control over the date range, a “Download Emissions by Date Range” selection is available. Once the selection is
made, press the Download button to
start the HTTP download. The MicroCEM will create a temporary file that
contains the selected data. Due to
memory limitations there is a limit to the
number of files that can be downloaded
simultaneously. If this limit is exceeded, a message will be displayed
that reads “The simultaneous download
limit has been reached, please try
again later”.
Download Emissions
Log, Calibration Log or
Alarm Log
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3-9 VIEWING MicroCEM DATA WITH MS EX-
CEL
The MicroCEM Data may be view with MS Excel
using two different methods. The first method is
to open the data log files that have been downloaded onto a workstation. The files may then be
opened directly with Excel. The second method is
to create an Excel workbook, which links to the
MicroCEM web page. This is described in the
following paragraph.
An Excel spreadsheet may be linked to a MicroCEM web site, which periodically refreshes the
spreadsheet with data from the web site. To do
this, first make sure the MicroCEM web site is
available. The workstation needs access to the
MicroCEM web site via RAS (Dialup), LAN or the
Internet. Then in Excel, select Data menu, Get
External Data, New Web Query. The dialog
shown in Figure 3-25 will appear. Type in the address for a MicroCEM web page that contains a
table with the desired data. Then press OK and
click on the cell where the data should appear.
The data will then appear in the spreadsheet. To
have the data updated periodically, right-click on
one of the cells that contains the linked data and
select Data Range Properties. Check the box the
reads “Refresh Every” and set the refresh period.
For additional information refer to MS Excel
documentation.
Figure 3-25. New Web Query
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3-10 AUTO CALIBRATION
The Auto Calibration dialog is displayed
whenever calibration is in process. It dis-
plays the current emission values and the
status of the calibration. The calibration
may be canceled before it completes by
pressing the Cancel button.
Note: The title of this dialog will read either “Auto Calibration” or “Manual Calibration” to indicate how the calibration process was initiated.
Figure 3-26. Auto Calibration
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SECTION 4
SOFTWARE
4-1 OVERVIEW
The MicroCEM Software includes 3 main
components. One component is the MicroCEM control software that interfaces with the
instrumentation and records the emissions
measurements. A second component is the
User Interface Software that provides realtime status and configuration dialogs. A third
component is the web server software that
uses VB Script or Java Script to provide a
web-based interface to the MicroCEM.
4-2 MicroCEM USER INTERFACE SOFTWARE
Hardware Platform: Pocket PC
The MicroCEM User Interface Software communicates with the MicroCEM Control Software using TCP/IP. It may run locally on the
MicroCEM computer or remotely on a Pocket
PC with a RS232 connection to the MicroCEM
computer. It will not normally run locally since
there is no input device or display connected
to the MicroCEM processor.
4-3 MicroCEM WEB SERVER SOFTWARE
Web Browser: Internet Explorer 4.0 or Net-
scape 4.0
The Web Server Software provides the web
based interface described in this document. It
is implemented as a VB Script or Java Script.
The script will obtain much of the needed information directly from the Data-Log files or
configuration file. The real-time information
will be obtained from a memory segment
shared with the MicroCEM control software.
The web server support multiple simultaneous
clients. The maximum number of allowed
connections could be limited to a reasonable
number through the Windows CE Web Server
configuration dialogs.
uCEM User
Interface
Pocket PC
As an option a
Wireless Network
may be used.
Serial
Cable
uCEM Computer
HTML (TCP/
IP)
Shared
Memory
Segment
Data-Log
& Config
Files
Web
Server
Script
TCP/IP
Control Circuitry
uCEM
Control
Software
Device Drivers
Digital and
Analog IO
Sensors and
Figure 4-1. MicroCEM Software Block Diagram
HTML
Ethernet,
Modem or serial
Workstation
Rosemount Analytical Inc. A Division of Emerson Process ManagementSoftware 4-1
Instruction Manual
748467-A
January 2002
4-4 SOFTWARE DEVELOPMENT MANAGEMENT
Microsoft Visual SourceSafe is used for version control of all of the MicroCEM software.
Compuware’s Track Record is used for
change request management and defect
tracking.
Model MicroCEM
4-2 SoftwareRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
SECTION 5
MAINTENANCE AND SERVICE
DANGER.
ELECTRICAL SHOCK HAZARD
Disconnect power to the module(s) prior to
replacing components.
WARNING
QUALIFIED PERSONNEL
This equipment should not be adjusted or
repaired by anyone except properly qualified service personnel.
WARNING
PARTS INTEGRITY
Tampering with or unauthorized substitution of components may adversely affect
safety of this product. Use only factoryapproved components for repair.
5-1 OVERVIEW
The MicroCEM Analyzer Module requires very
little maintenance during normal operation.
Occasionally, the detector's reaction chamber
and sapphire window may require cleaning,
refer to Section 5-5.
White crystal deposits on the windows of the
reaction chamber and plugging of capillaries
and vent are usually due to sample contaminates such as ammonia reacting with the high
ozone levels and NO components. To eliminate the contaminates, the sampling system
should be reworked or a preventive maintenance program developed (if dropout is not
excessive). Another source of crystalline formation is contaminated air.
Several components may require replacement. These are discussed in the following
sections.
Rosemount Analytical Inc. A Division of Emerson Process ManagementMaintenance and Service 5-1
Instruction Manual
748467-A
January 2002
Valve Manifold
Assembly
Paramagnetic
Detector
Model MicroCEM
Converter
(Figure 5-2)
NDIR Detector
Ozone Generator
Thermoelectric Cooler
Power Relay
3-Way Valve
Transistor
Regulator
Chemiluminescense
Detector (Figure 5-4)
Power Supply Assembly
Fan
Personality Modules
(Figure 5-3)
Figure 5-1. MicroCEM Component Location
5-2 Maintenance and ServiceRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
5-2 CONVERTER
To replace the converter or sensor, disconnect the two pneumatic tubes and two electrical connections. Unlace the heater blanket,
ASSEMBLED SIDE VIEW
Sensor
Glass
Cloth
Heater
Jacket
655228
Converter
Tube 655227
Wrap with
aluminum foil
and remove the converter. Reassemble in reverse order, ensuring that the converter is oriented with the glass cloth at the bottom and
the sensor is oriented correctly inside the
heater jacket.
Sensor
655282
Figure 5-2. Converter Assembly
Rosemount Analytical Inc. A Division of Emerson Process ManagementMaintenance and Service 5-3
Instruction Manual
748467-A
January 2002
Model MicroCEM
5-3 OZONE GENERATOR
To replace the ozonator, remove the two large
straps and all tie-wraps, and disconnect the
one electrical connection. Reassemble in reverse order.
5-4 PERSONALITY MODULES
There are five different personality modules.
Depending on your unit, you may have three,
four or five modules installed. These person-
ality modules are installed on a custom backplane. See Figure 5-3.
To remove any on the personality modules.
Remove cables form module to be removed,
there are two screws at the bottom of each
module. You will have to loosen each screw
before you can remove the personality module.
Tag each cable and its location before disconnecting any wiring. This helps in reassembly.
EXIO
AUX
PDD
NDIR
PMD
Figure 5-3. Personality Modules and Backplane.
5-4 Maintenance and ServiceRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
5-5 CHEMILUMINESCENSE DETECTOR AS-
SEMBLY
Refer to Figure 5-4 and Figure 5-5.
a. Reaction Chamber
Removal
Disconnect the stainless steel tubing lines
at the Gyrolok fittings. Remove the (4)
nuts holding the Detector Assembly to
the chassis. Disconnect the plug from
connector J1 on the Signal Board and
remove the assembly from the chassis.
NOTE
Heatsink Compound. Care should be
taken to avoid getting heatsink compound on optical surfaces. If this substance is removed during the
disassembly process, a zinc oxide-filled, silicone grease (e.g., Dow
Corning 340 or EG&G Wakefield Engineering's Series 120 Thermal Joint
Compound) be reapplied in the reassembly of this component.
Although the heater and thermostat can
be removed to facilitate handling, contact
with the white heatsink compound can be
minimized by leaving these items in place.
Remove the (2) screws holding the top
plate of the Detector , and move the plate
along the wires and away from the Detector .
Remove the (2) screws holding the tube
assembly in place. Hold the tubing with
one hand while inverting the Detector
Housing with the other, allowing the Reaction Chamber O-ring and window to be
removed from below.
Installation
To reinstall, hold the housing in the inverted position while sliding the Reaction
Chamber O-ring and window into position
and the tubing into the slot in the housing.
Hold the Reaction Chamber in place while
rotating the housing upright. Replace the
hold-down screws.
NOTE
Component Positioning. The procedure described above is for the purpose of maintaining the relative
positions of windows and O-ring to the
Reaction Chamber during installation.
Replace the top cap and screws. Reverse
the removal procedure to reinstall the
Detector Assembly into the Analyzer
Module.
b. Photodiode
Removal
Remove the Detector Assembly as described above. Invert the housing to access the mounting bracket. Remove the
(3) screws and shoulder washers from the
bracket. Remove the bracket, insulating
disk and bottom plate as a unit to minimize the spread of the heatsink compound.
Remove the (2) screws holding the lower
section of the Detector Housing, then
slide the section along the cable and remove.
Remove the (2) screws holding the
socket, thermistor and photodiode in
place, being careful not to lose the washers that are used as shims.
Grasp the socket and photodiode base
while slowly rotating to separate the photodiode from the housing. Some friction
will be felt as an O-ring is used around the
photodiode as a seal.
Installation
To replace the photodiode, carefully remove the diode from the green socket,
and replace with a new one. Before
mounting the new diode, the top cap of
the enclosure should be temporarily removed and the (2) screws holding the
Reaction Chamber loosened about two
turns. This allows air which is trapped
between the O-ring seals to escape when
the diode is inserted. It also maintains the
Rosemount Analytical Inc. A Division of Emerson Process ManagementMaintenance and Service 5-5
Instruction Manual
748467-A
January 2002
Model MicroCEM
position of the O-ring and window in the
upper compartment.
The new photodiode should be slowly inserted into the housing while gradually
rotating the body. This allows the O-ring
to properly seat. Continue replacing
screws, washers, thermistors, etc., with
the thicker shim (washer) on the opposite
side of the socket from the thermistor.
Photodiode
Replace the lower section of the housing,
then the bottom cover, insulator and
bracket with the shoulder washers and
screws.
Re-tighten the screws in the Reaction
Chamber (upper section). Replace the top
cap and its screws.
To reinstall in the Analyzer Module, reverse the procedure for removal as indicated above.
Sapphire
Window
Reaction
Chamber
Thermistor
Assembly
Sample
Ozone
Exhaust
Figure 5-4. Chemiluminescense Detector Assembly
Photodiode Socket
Assembly
Detector Mounting
Bracket
5-6 Maintenance and ServiceRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
*
Heater
M3X0.5 x 16mm Screw (2)
3mm Spring Washer (2)
*
Heater
Thermostat
Instruction Manual
748467-A
January 2002
M3X0.5 x 25mm Screw (2)
3mm Spring Washer (2)
Detector Header
Retainer Gasket
*
Reaction Chamber
Photodiode
Cable
Insulator
(between Lower Cover
and Mounting Bracket)
Rosemount Analytical Inc. A Division of Emerson Process ManagementMaintenance and Service 5-7
Instruction Manual
748467-A
January 2002
Model MicroCEM
5-8 Maintenance and ServiceRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
SECTION 6
TROUBLESHOOTING
6-1 TROUBLESHOOTING LEAKS
Liberally cover all fittings, seals, and other possible sources of leakage with a suitable leak test
liquid such as SNOOP (part 837801). Bubbling
or foaming indicates leakage. Checking for bubbles will locate most leaks but could miss some,
as some areas are inaccessible to the application of SNOOP. For positive assurance that
system is leak free, perform one of the tests
above.
NOTE:
Refer to Specification in Preface for maximum pressure limitations.
For differential measurement, the leak check
must be performed for the measurement and
reference side separately.
For analyzers with parallel gas paths, the
leak check must be performed for each gas
path separately.
6-2 POCKET PC CONNECTION FAILURE
In the event the connection between the Pocket
PC and the MicroCEM fails, a connection failure
dialog will be displayed. It will display the following message:
Connection with uCEM lost, retrying…
A Cancel button will be displayed. The MicroCEM software will continue to attempt to reconnect with the MicroCEM indefinitely and will stop
when a connection is made or the cancel button
is pressed.
If the Cancel button is pressed, any setting
changes that were made without pressing OK to
accept will be lost. If Auto Calibration was in
process, it will be completed by the MicroCEM
even though the connection was lost.
6-3 TROUBLE LED
The Trouble LED output is activated whenever
there is a critical alarm that has not been acknowledged. This provides both an output from
the MicroCEM box and an LED indication.
Rosemount Analytical Inc. A Division of Emerson Process ManagementTroubleshooting 6-1
Instruction Manual
748467-A
January 2002
Model MicroCEM
6-2 TroubleshootingRosemount Analytical Inc. A Division of Emerson Process Management
Rosemount Analytical Inc. A Division of Emerson Process ManagementReplacement Parts 7-1
Instruction Manual
748467-A
January 2002
Model MicroCEM
7-2 Replacement PartsRosemount Analytical Inc. A Division of Emerson Process Management
Model MicroCEM
Instruction Manual
748467-A
January 2002
SECTION 8
RETURN OF MATERIAL
8-1 RETURN OF MATERIAL
If factory repair of defective equipment is required, proceed as follows:
1. Secure a return authorization from a
Rosemount Analytical Inc. Sales Office or
Representative before returning the
equipment. Equipment must be returned
with complete identification in accordance
with Rosemount instructions or it will not
be accepted.
2. In no event will Rosemount be responsible
for equipment returned without proper
authorization and identification.
3. Carefully pack the defective unit in a sturdy
box with sufficient shock absorbing material to ensure no additional damage occurs
during shipping.
4. In a cover letter, describe completely:
a. The symptoms that determined the
equipment is faulty.
b. The environment in which the equip-
ment was operating (housing, weather,
vibration, dust, etc.).
c. Site from where the equipment was
removed.
d. Whether warranty or non-warranty
service is expected.
e. Complete shipping instructions for the
return of the equipment.
5. Enclose a cover letter and purchase order
and ship the defective equipment according to instructions provided in the Rosemount Return Authorization, prepaid, to:
If warranty service is expected, the defective
unit will be carefully inspected and tested at
the factory. If the failure was due to the conditions listed in the standard Rosemount warranty, the defective unit will be repaired or
replaced at Rosemount’s option, and an operating unit will be returned to the customer in
accordance with the shipping instructions furnished in the cover letter.
For equipment no longer under warranty, the
equipment will be repaired at the factory and
returned as directed by the purchase order
and shipping instructions.
8-2 CUSTOMER SERVICE
For order administration, replacement parts,
application assistance, on-site or factory repair, service or maintenance contract information, contact:
Rosemount Analytical Inc.
Process Analytic Division
Customer Service Center
1-800-433-6076
8-3 TRAINING
A comprehensive Factory Training Program of
operator and service classes is available. For
a copy of the Current Operator and Service
Training Schedule, contact the Technical
Services Department at:
Rosemount Analytical Inc.
Phone 1-714-986-7600
FAX 1-714-577-8006
Rosemount Analytical Inc.
Process Analytic Division
Customer Service Center
1-800-433-6076
Rosemount Analytical Inc. A Division of Emerson Process ManagementReturn of Material 8-1
Instruction Manual
748467-A
January 2002
Model MicroCEM
8-2 Return of MaterialRosemount Analytical Inc. A Division of Emerson Process Management
WARRANTY
Goods and part(s) (excluding consumables) manufactured by Seller are warranted to be free from
defects in workmanship and material under normal use and service for a period of twelve (12)
months from the date of shipment by Seller. Consumables, glass electrodes, membranes, liquid
junctions, electrolyte, o-rings, etc., are warranted to be free from defects in workmanship and
material under normal use and service for a period of ninety (90) days from date of shipment by
Seller. Goods, part(s) and consumables proven by Seller to be defective in workmanship and/or
material shall be replaced or repaired, free of charge, F.O.B. Seller's factory provided that the
goods, part(s) or consumables are returned to Seller's designated factory, transportation charges
prepaid, within the twelve (12) month period of warranty in the case of goods and part(s), and in
the case of consumables, within the ninety (90) day period of warranty. This warranty shall be in
effect for replacement or repaired goods, part(s) and the remaining portion of the ninety (90) day
warranty in the case of consumables. A defect in goods, part(s) and consumables of the commercial unit shall not operate to condemn such commercial unit when such goods, part(s) and
consumables are capable of being renewed, repaired or replaced.
The Seller shall not be liable to the Buyer, or to any other person, for the loss or damage directly
or indirectly, arising from the use of the equipment or goods, from breach of any warranty, or from
any other cause. All other warranties, expressed or implied are hereby excluded.
IN CONSIDERATION OF THE HEREIN STATED PURCHASE PRICE OF THE GOODS,
SELLER GRANTS ONLY THE ABOVE STATED EXPRESS WARRANTY. NO OTHER WARRANTIES ARE GRANTED INCLUDING, BUT NOT LIMITED TO, EXPRESS AND IMPLIED
WARRANTIES OR MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE.
Limitations of Remedy. SELLER SHALL NOT BE LIABLE FOR DAMAGES CAUSED BY DELAY IN PERFORMANCE. THE SOLE AND EXCLUSIVE REMEDY FOR BREACH OF WARRANTY SHALL BE LIMITED TO REPAIR OR REPLACEMENT UNDER THE STANDARD
WARRANTY CLAUSE. IN NO CASE, REGARDLESS OF THE FORM OF THE CAUSE OF ACTION, SHALL SELLER'S LIABILITY EXCEED THE PRICE TO BUYER OF THE SPECIFIC
GOODS MANUFACTURED BY SELLER GIVING RISE TO THE CAUSE OF ACTION. BUYER
AGREES THAT IN NO EVENT SHALL SELLER'S LIABILITY EXTEND TO INCLUDE INCIDENTAL OR CONSEQUENTIAL DAMAGES. CONSEQUENTIAL DAMAGES SHALL INCLUDE, BUT
ARE NOT LIMITED TO, LOSS OF ANTICIPATED PROFITS, LOSS OF USE, LOSS OF REVENUE, COST OF CAPITAL AND DAMAGE OR LOSS OF OTHER PROPERTY OR EQUIPMENT.
IN NO EVENT SHALL SELLER BE OBLIGATED TO INDEMNIFY BUYER IN ANY MANNER
NOR SHALL SELLER BE LIABLE FOR PROPERTY DAMAGE AND/OR THIRD PARTY CLAIMS
COVERED BY UMBRELLA INSURANCE AND/OR INDEMNITY COVERAGE PROVIDED TO
BUYER, ITS ASSIGNS, AND EACH SUCCESSOR INTEREST TO THE GOODS PROVIDED
HEREUNDER.
Force Majeure. Seller shall not be liable for failure to perform due to labor strikes or acts beyond
Seller's direct control.
Instruction Manual
748467-A
January 2002
Model MicroCEM
Emerson Process Management
Rosemount Analytical Inc.
Process Analytic Division
1201 N. Main St.
Orrville, OH 44667-0901
T (330) 682-9010
F (330) 684-4434
E-mail: gas.csc@emersonprocess.com
ASIA - PACIFIC
Fisher-Rosemount
Singapore Private Ltd.