Electrothermal Integrity 10 Instruction Manual [en, de, es, fr, it]

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Page 1

Integrity 10

Operation Manual

rev 6.0

Page 2

Page 3

Contents

1. Symbols and using this instruction book .................................................................................................. 5

2. Safety information .....................................................................................................................................6

2.1. Consignes de sécurité ..................................................................................................................... 8

2.2. Sicherheitsinformationen .............................................................................................................. 11

2.3. Información de seguridad ............................................................................................................. 14

2.4. Informazioni sulla sicurezza ..........................................................................................................16

3. Introduction...............................................................................................................................................20

3.1. Instrumentspecication ................................................................................................................ 21

4. Unpacking and contents ..........................................................................................................................22

5. Installation ................................................................................................................................................23

6. Environmental protection ........................................................................................................................26

6.1. Battery disposal ............................................................................................................................26

7. Product operation ................................................................................................................................... 27

7.1. Product overview .......................................................................................................................... 27

7.2. Reductionsleeves-ttingandremoval ......................................................................................... 28

7.3. Insert SD card ............................................................................................................................... 30

7.4. Turn unit ON ................................................................................................................................30

7.5. Turn unit OFF ................................................................................................................................30

7.6. Power up ......................................................................................................................................31

7.7. Time and date setting ...................................................................................................................32

7.8. Communication protocol selection (for use with external control) .................................................33

7.9. Viewrmwarereleaseset .............................................................................................................34

7.10. Manual control ............................................................................................................................. 35

7.10.1. Setting the temperature ..........................................................................................................36

7.10.2. Setting the stir speed: .............................................................................................................. 37

7.10.3. Setting the run time ................................................................................................................37

7.10.4. Setting the ramp rate ..............................................................................................................37

7.10.5. Setting the maximum upper limit ............................................................................................38

7.10.6. Copy function .........................................................................................................................38

7.10.7. Adjusting the settings of a running cell in manual control ........................................................ 39

7.10.8. Home screen when operational ...............................................................................................40

7.11. Prolecontrol ...............................................................................................................................41

7.11.1. Prolesetup ...........................................................................................................................41

7.11.2. Setting the initial temperature .................................................................................................42

7.11.3. Setting the initial hold time .....................................................................................................42

7.11.4. Setting the initial ramp ............................................................................................................ 43

7.11.5. Setting the target temperature ................................................................................................43

7.11.6. Setting the maximum upper limit ............................................................................................44

7.11.7. Setting the plateau time .......................................................................................................... 44

7.11.8. Final temperature ....................................................................................................................45

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7.11.9. Final ramp ............................................................................................................................... 46

7.11.10. Setting the hold time ............................................................................................................... 46

7.11.11. Stir speed ................................................................................................................................ 47

7.11.12. Profile loop .............................................................................................................................47

7.11.13. Copyandpasteaprole..........................................................................................................48

7.11.14. In the event of power loss .......................................................................................................49

7.12. Namingandsavingaprole .........................................................................................................49

7.13 Storedproleviewandcopy ........................................................................................................51

7.13.1. Storingaprole.......................................................................................................................51

7.13.2. Deleteastoredprole .............................................................................................................54

7.14. Saving an experiment ...................................................................................................................55

7.15. Reviewing stored experiment data ................................................................................................ 57

7.15.1. Accessing stored experiment data ............................................................................................57

7.15.2. Viewing data in graphical format ............................................................................................. 59

7.15.3. Deleting experimental data ...................................................................................................... 60

7.16. OutputtingstoreddataviaUSBashdrive .................................................................................... 60

7.17. Control by contents ...................................................................................................................... 61

7.17.1.

7.17.2.

7.18. External control – optional ............................................................................................................ 63

7.18.1. PC control: ..............................................................................................................................63

8. Chemical resistance...................................................................................................................................64

Installation of the Multi-Temp .................................................................................................61

Operating the Multi-Temp ....................................................................................................... 62

Reaction block dimensions ....................................................................................................................... 70

10.Powersupplyunit(PSU) specifications

11. Maintenance, service and repair..............................................................................................................72

11.1. Maintenance ................................................................................................................................72

11.2. Spillage procedure ........................................................................................................................73

11.3. Decontamination ..................................................................................................................... 73

11.4. Servicing .......................................................................................................................................73

11.5. Error and warning messages ......................................................................................................... 73

11.5.1. Heat exchanger over temperature error ...................................................................................74

11.5.2. Motor stall error ......................................................................................................................75

11.5.3. Cell failure error ......................................................................................................................75

11.5.4. Over voltage error ...................................................................................................................76

11.5.5. Under Voltage error ................................................................................................................. 76

11.5.6. Probe error ..............................................................................................................................77

12. Customer support ..................................................................................................................................... 78

13. Spares and accessories ............................................................................................................................79

14. Notes .......................................................................................................................................................... 80

15.

EU Declaration of conformity ..................................................................................................................8

................................................................................................... 71

Appendix 'A'...................................................................................................................................................82

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1. Symbols and using this instruction book

Throughoutthisinstructionbookthesymbolsdenedbelowareusedtoidentifyconditionsthatposeahazard

to the user or actions that should be observed. These symbols are also shown on the product or its packaging. When a symbol is shown next to a paragraph or statement it is recommended the user takes particular note of that instruction in order to prevent damage to the equipment or to prevent injury to one’s self or other people.

The Responsible Body and the Operator should read and be familiar with this Instruction book in order to preserve the protection offered by the equipment.

To prevent injury or equipment damage it is the manufacturer’s recommendation that all persons using this equipment are suitably trained before use.

Caution, risk of danger. See note or adjacent symbol.

Protective conductor terminal to be earthed.

Do not loosen or disconnect.

Caution / Risk of electric shock.

Recyclable Packaging Material.

Coin Battery

Do not dispose of product in normal domestic waste.

Caution. Hot surface.

Bio Chemical Hazard.

Caution required. Will require decontamination.

Contains CR2032 button coin battery.

To be disposed of according to regulations - not customer serviceable.

Refer to Instruction manual.

Port communication symbol.

Cooling ﬂuid. Connect inlet supply to Left hand side connector

Cooling ﬂuid. Connect inlet supply to Right hand side connector

Standby

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2. Safety information

DO NOT

Integrity PSU

Never

Do not

Integrity 10

Power Supply Unit

To prevent a risk of fire or electric shock,

DO NOT

open the

Integrity PSU

case without authorisation. Only qualified Service personnel should attempt to repair/service the PSU.

Ensure the Mains Power Supply conforms to ratings found on the

data plate

located on the underside of the PSU.

Never

Operate this equipment without connection to earth/ground. Ensure the mains supply voltage is correctly earthed/grounded in accordance with current area legislation.

Do not

position the

Integrity 10

on top of the

Power Supply Unit

In the event of a single fault condition causing a cell within the unit to go over- temperature, there is additional protection within the cell in the form of a Thermal Fuse.

The Thermal Fuse is designed to protect a faulty cell continually heating beyond a temperature of approx. 190°C.

The Thermal Fuse is not designed to protect individual samples being heated beyond a specified temperature; additional means should be employed if that level of protection is required.

Do not

Integrity 10 or Power Supply Unit

Do not

Integrity 10 or Po

wer Supply Unit

This product has been designed for safe operation when used as detailed in accordance with the Manufacturer’s instructions.

NOTE: Failure to use this equipment in accordance with the manufactures operating instructions may compromise your basic safety protection afforded by the equipment and may invalidate the warranty/guarantee. The warranty/guarantee does not cover damage caused by faulty installation or misuse of the equipment.

Prevention of Fire and Electric Shock

To prevent a risk of fire or electric shock, case without authorisation. Only qualified Service personnel should attempt to repair/service the PSU.

Ensure the Mains Power Supply conforms to ratings found on the data plate located on the underside of the PSU.

General Safe Operating Practice

Operate this equipment without connection to earth/ground. Ensure the mains supply voltage is correctly earthed/grounded in accordance with current area legislation.

position the

In the event of a single fault condition causing a cell within the unit to go overtemperature, there is additional protection within the cell in the form of a Thermal Fuse.

The Thermal Fuse is designed to protect a faulty cell continually heating beyond a temperature of approx. 190°C.

The Thermal Fuse is not designed to protect individual samples being heated beyond a specified temperature; additional means should be employed if that level of protection is required.

on top of the

open the

Alway

s follow good laboratory practice when using this equipment. Give due recognition to your company’s safety and legislative health & safety procedures and all associated legislation applicable to your areas of operation. Check laboratory procedures for substances being heated and ensure all hazards (e.g. risk of explosion, implosion or the release of toxic or flammable gases) that might arise have been suitably addressed before proceeding. When heating certain substances the liberation of hazardous gases may require the use of a fume cupboard or other means of extraction. (Consult your company practice).

Ensur

e equipment is used on a clean, dry, non-combustible, solid work surface with at least 300mm of suitable clearance all around from other equipment.

Ensur

e the PSU is positioned on a clean, dry, non-combustible surface with a sufficient space for the power cable to Integrity 10 and mains input lead and plug set to enter/exit without undue bend stresses. Ensure a suitable clearance for air flow and heat dissipation.

position the

connect/disconnect from the power cable assembly.

position the

connect/disconnect from the coolant fluid supply.

so that it is difficult to

Page 7

Do not

position the

Integrity 10 or Power Supply Unit

Do not

not

Do not

Touch Screen Warning.

Warning

Care must be taken

connect/disconnect data and communication cables.

position the PSU so that the on/off switch or IEC mains socket

located on the rear is inaccessible.

immerse any part of this equipment in water/fluid.

spill substances on the touch screen. Case materials are protected as defined in Table 8.1 Chemical resistance chart. If spillage does occur, disconnect unit from mains supply and follow instructions as detailed in Section ‘Maintenance, Service and Customer Repair’.

Do not cover the Integrity 10 or PSU (ESPECIALLY VENTILATION SLOTS) whilst in use.

It is operation.

Only use Original Equipment Manufacture’s Parts and Accessories. Ref Section 11.

The equipment is not spark, flame or explosion proof and has not been designed for use in hazardous areas in terms of BSEN 60079-14:1997. Keep flammable, low flash point substances away from the apparatus.

Take care when handling HOT & COLD glassware

recommended to leave any heating apparatus unattended during

operate or handle any part of this product with wet hands.

touch the inside of the cells when the product is in operation.

so that it is difficult to

Ensure the unit has reached ambient temperature before removing the top cover.

When the top cover has been removed and the inside of the unit is exposed do not put fingers into the front or rear of the unit as there is the risk that they can become trapped.

lean or stretch over the unit when in operation.

Keep the Mains Plug and Lead set cable away from the heating surface.

The screen is impervious to acetone. It is

recommended that any chemical spillage is wiped off the screen immediately.

: Standard glassware supplied for the Integrity product is not designed for high pressure applications. Maximum operating pressure of standard glassware with cap fitted is 0.5bar.

: Glass vessels can explode or implode violently, either spontaneously from stress failure caused by pressure or vacuum, or from accidental impact. Carefully check glass vessels for star cracks, scratches or etching marks before each use. Cracks can increase the likelihood of breakage or may allow chemicals to leak into the equipment. Conduct all pressure and vacuum operations in glass vessels behind adequate shielding and use Personnel Protective Equipment (Full face guard, gloves, protective clothing) during handling.

: Glass vessels which have been located in a block at a high temperature should not be placed into a cold block as this is likely to shatter the vessel.

when using flammable solvents. Approaches which could be adopted to reduce the risk of fire include introducing an inert atmosphere inside of the reaction tubes and/or using the equipment in a properly ventilated area, e.g. under a fume hood.

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Additional safety information

ATS20002 and ATS20003 PTFE caps

For individual components see below.

Viton (main seal) and O rings.

Viton is resistant to a wide range of chemicals including oils, aqueous media and most other fluids.

It is recommended that the user checks the chemical compatibility prior to use.

PFTE Cap PTFE is resistant to a wide range of chemicals including ozone, chlorine,

acetic acid, ammonia sulphuric acid and hydrochloric acid. The only chemicals known to affect these coatings are molten alkali metals and highly reactive fluorinating agents.

It is recommended that the user checks the chemical compatibility prior to use.

Silicone Cap Septum

Peroxide cross linked HTV silicone rubber, classified in accordance with ASTM D 1418 as VMQ. It is recommended that the user checks the chemical compatibility prior to use.

316 Stainless steel 2mm dia sampling hole bung

It is recommended that the user checks the chemical compatibility prior to use.

2.1. CONSIGNES DE SÉCURITÉ

ATS20002 For individual components see below. and ATS20003 PTFE caps

Viton (main Viton is resistant to a wide range of chemicals including oils, aqueous media and most other

seal)andO uids.

rings. It is recommended that the user checks the chemical compatibility prior to use.

PTFE Cap PTFE is resistant to a wide range of chemicals including ozone, chlorine, acetic acid,

SiliconeCap PeroxidecrosslinkedHTVsiliconerubber,classiedinaccordancewithASTMD1418as

Septum VMQ. It is recommended that the user checks the chemical compatibility prior to use.

ammonia sulphuric acid and hydrochloric acid. The only chemicals known to affect these

coatingsaremoltenalkalimetalsandhighlyreactiveuorinatingagents.

It is recommended that the user checks the chemical compatibility prior to use.

316 Stainless steel It is recommended that the user checks the chemical compatibility prior to use. 2mm dia sampling

hole bung

PTFE sampling hole bung

2.1. Consignes de sécurité

Ce produit a été conçu pour fonctionner en toute sécurité lorsqu’il est utilisé conformément aux instructions du fabricant.

REMARQUE : Ne pas utiliser ce matériel en conformité avec les instructions de fonctionnement du fabricant peut compromettre la protection de sécurité de base offerte par ce matériel et peut annuler la garantie. La garantie ne couvre pas les dommages causés par une mauvaise installation ou une mauvaise utilisation du matériel.

Prévention des incendies et des chocs électriques

PTFE is resistant to a wide range of chemicals including ozone, chlorine, acetic acid, ammonia sulphuric acid and hydrochloric acid. The only chemicals known to affect these

coatingsaremoltenalkalimetalsandhighlyreactiveuorinatingagents.

commended that the user chIt is re ecks the chemical compatibility prior to use.

Pour éviter tout risque d'incendie ou de choc électrique, N'OUVREZ PAS le bloc d'alimentation Integrity sans autorisation. Seul du personnel de

maintenance qualifié peut tenter de réparer ou d'entretenir le bloc d'alimentation. Veillez à ce que l'alimentation électrique du secteur soit conforme aux classes figurant sur la plaque signalétique située sur la partie inférieure du bloc d'alimentation. Ne jamais faire fonctionner le matériel sans mise à la terre/masse. Veillez à ce que la tension du secteur soit correctement mise à la terre/masse conformément à la législation en vigueur dans votre pays.

Ne placez pas l'Integrity 10 au dessus du bloc d'alimentation

En cas de défaillance causant la surchauffe d'une cellule de l'appareil, il existe une protection supplémentaire à l'intérieur de la cellule sous la forme d'un fusible thermique.

Le fusible thermique est conçu pour protéger une cellule défectueuse continuant à chauffer au delà de 190 °C environ.

Page 9

Le fusible thermique n'est pas conçu pour protéger des échantillons

Ne placez pas

l'Integrity 10

ou le bloc d'alimentation

Ne placez pas

l'Integrity 10 ou le bloc d'alimentation

Ne placez pas

l'Integrity 10 ou le bloc d'alimentation

Ne placez pas

n'e

st pas

individuels qui seraient chauffés au delà d'une température spécifique ; des moyens supplémentaires doivent être utilisés si ce niveau de protection est nécessaire.

Pratiques de base pour une utilisation sûre

Suivez toujours les bonnes pratiques de laboratoire lors de l'utilisation de cet appareil. Portez une attention particulière aux procédures de santé et de sécurité de votre entreprise et aux procédures réglementaires, ainsi qu'à toutes les lois applicables associées en vigueur dans votre pays. Vérifiez les procédures de laboratoire pour connaître les substances qui sont chauffées et veillez à ce que tous les dangers (par exemple le risque d'explosion, d'implosion et de dégagement de gaz toxiques ou inflammables) qui peuvent survenir ont été convenablement traités avant de poursuivre. Lorsque certaines substances sont chauffées, le dégagement de gaz dangereux peut nécessiter l'utilisation d'une hotte aspirante ou d'autres moyens d'extraction. (Consultez les pratiques de votre entreprise). Veillez à ce que le matériel soit utilisé sur une surface propre, sèche, incombustible et solide avec un espace suffisant d'au moins 300 mm tout autour du matériel.

Veillez à ce que le bloc d'alimentation soit placé sur une surface propre, sèche et incombustible avec suffisamment d'espace afin que le câble d'alimentation allant vers l'Integrity 10 et l'ensemble des câbles et fiches secteur puissent être insérés ou sortis sans être pliés de manière excessive. Veillez à maintenir un espace suffisant pour la circulation d'air et la dissipation de la chaleur.

difficile de raccorder ou de débrancher l'ensemble des câbles d'alimentation.

difficile de raccorder ou de débrancher l'alimentation en fluide de refroidissement.

difficile de raccorder ou de débrancher les câbles de transfert de données et de communication.

le bloc d'alimentation de sorte que le commutateur

marche/arrêt ou la prise secteur CEI situés à l'arrière soient inaccessibles.

plongez pas de pièces de cet appareil dans de l'eau ou dans un fluide.

de sorte qu'il soit

renversez pas de substances sur l'écran tactile. Les matériaux du boîtier sont protégés tel que défini dans le tableau 8.1 listant les résistances chimiques. Si une substance est renversée, débranchez l'appareil du secteur et suivez les instructions détaillées dans le paragraphe « Maintenance, entretien et réparation par le client ».

Ne couvrez pas l'Integrity 10 ou le bloc d'alimentation (EN PARTICULIER LES FENTES D'AÉRATION) lorsqu'ils fonctionnent.

Il surveillance pendant son fonctionnement.

N'utilisez que des pièces et des accessoires d'origine provenant du fabricant du matériel. Réf. paragraphe 11.

Le matériel n'est pas résistant aux étincelles, au feu ou aux explosions et n'a pas été conçu pour être utilisé dans des zones dangereuses au sens de la norme BSEN 60079-14:1997. Maintenez les substances inflammables à point éclair bas éloignées de l'appareil.

faites fonctionner ni ne manipulez aucune pièce de ce produit avec les

mains mouillées.

recommandé de laisser tout appareil de chauffage sans

Page 10

touchez pas l'intérieur des cellules lorsque l'appareil est en

Avertissement concernant l'écran tactile.

Attention

Atte

ntion

Des précautions doivent être prises

fonctionnement.

Faites attention lorsque vous manipulez de la verrerie CHAUDE ou FROIDE.

Veillez à ce que l'appareil ait atteint la température ambiante avant d'ôter le couvercle.

Lorsque mettez pas vos doigts à l'avant ou à l'arrière de l'appareil car ils risqueraient d'être piégés.

fonctionnement.

Éloignez les fiches secteurs et les câbles de toute surface chauffante.

Il est recommandé d'essuyer immédiatement tout produit chimique renversé sur l'écran.

conçue pour des utilisations à haute pression. La pression de fonctionnement maximale d'une verrerie standard équipée d'un bouchon est de 0,5 bar.

soit spontanément par rupture de contrainte causée par la pression ou le vide, ou à cause d'un impact accidentel. Avant chaque utilisation, vérifiez soigneusement les récipients en verre à la recherche de craquelures étoilées, de rayures ou de marques de gravure. Les craquelures peuvent augmenter la probabilité de casse ou permettre aux produits chimiques de s'infiltrer dans l'appareil. Réalisez toutes les opérations sous pression ou sous vide dans des récipients en verre derrière une protection adaptée et utilisez des équipements de protection individuels (protection faciale complète, gants, vêtements de protection) pendant la manipulation.

le couvercle a été ôté et que l'intérieur de l'appareil est exposé, ne

vous penchez pas ou ne vous allongez pas sur l'appareil lorsqu'il est en

L'écran est résistant à l'acétone.

: La verrerie standard fournie pour l'appareil Integrity n'est pas

: Les récipients en verre peuvent exploser ou imploser violemment,

: Les récipients en verre qui ont été placés dans un bloc à haute température ne doivent pas être placés dans un bloc froid car cela est susceptible de les briser.

lorsque des solvants inflammables sont utilisés. Les approches qui pourraient être adoptées pour réduire le risque d'incendie incluent l'introduction d'une atmosphère inerte à l'intérieur des tubes de réaction et/ou l'utilisation de l'appareil dans une zone correctement ventilée, comme par exemple sous une hotte aspirante.

Informations complémentaires concernant la sécurité

Bouchons en PTFE ATS20002 et ATS20003. Viton (joint principal) et joints toriques.

Bouchon en PTFE

Pour les composants individuels, voir ci-dessous.

Le Viton est résistant à un grand nombre de produits chimiques tels que l'huile, les milieux aqueux et la plupart des autres fluides.

Il est recommandé à l'utilisateur de vérifier la compatibilité chimique avant toute utilisation.

Le PTFE est résistant à un large éventail de produits chimiques y compris l'ozone, le chlore, l'acide acétique, le sulfate d'ammonium et l'acide chlorhydrique. Les seuls produits chimiques connus pouvant avoir un effet sur ces revêtements sont les métaux alcalins fondus et les agents de fluoration très réactifs.

Il est recommandé à l'utilisateur de vérifier la compatibilité chimique avant

Page 11

toute utilisation.

Bouchon et cloison en silicone

Caoutchouc de silicone HTV réticulé au peroxyde, classé de type VMQ selon la norme ASTM D 1418. Il est recommandé à l'utilisateur de vérifier la compatibilité chimique avant toute utilisation.

Bouchon du trou de l'échantillon de 2 mm de diamètre en acier inoxydable 316

Il est recommandé à l'utilisateur de vérifier la compatibilité chimique avant toute utilisation.

2.2. SICHERHEITSINFORMATIONEN

Dieses Produkt kann unter Einhaltung der Herstelleranweisungen sicher betrieben werden.

HINWEIS: Wird das Gerät nicht gemäß den Bedienungsanweisungen des Herstellers verwendet, kann dies dazu führen, dass Ihr grundlegender Sicherheitsschutz durch das Gerät beeinträchtigt und die Gewährleistung/Garantie ungültig wird. Die Gewährleistung/Garantie deckt keine Schäden durch fehlerhafte Installation oder falsche Verwendung des Geräts ab.

Vermeiden von Feuer und Stromschlägen

niemals

Integrity 10

nicht

Netzteil

Bouchon et cloison en silicone

Bouchon du trou de l'échantillon

2.2. Sicherheitsinformationen

Dieses Produkt kann unter Einhaltung der Herstelleranweisungen sicher betrieben werden.

de 2 mm de diamètre en acier inoxydable 316

Caoutchouc de silicone HTV réticulé au peroxyde, classé de type VMQ selon la norme ASTM D 1418. Il est recommandé à l'utilisateur de vérifier la compatibilité chimique avant toute utilisation.

Il est recommandé à l'utilisateur de vérifier la compatibilité chimique avant toute utilisation.

Verwendung des Geräts ab.

Vermeiden von Feuer und Stromschlägen

Um die Gefahr von Bränden oder Stromschlägen zu verhindern, öffnen Sie das Gehäuse des Integrity-Netzteils NICHT ohne Genehmigung. Nur qualifiziertes Wartungspersonal darf das Netzteil reparieren/warten.

Allgemeine sichere Betriebspraxis

Stellen Sie sicher, dass die Netzstromversorgung den auf dem Datenschild auf der Unterseite des Netzteils angegebenen Nennleistungen entspricht.

Betreiben Sie das Gerät sicher, dass die Netzspannung in Übereinstimmung mit der entsprechenden aktuellen Gesetzgebung korrekt geerdet ist.

Stellen Sie das

Bei Auftreten eines Einzelfehlers, der dazu führt, dass eine Zelle im Netzteil eine Übertemperatur aufweist, besteht ein zusätzlicher Schutz in der Zelle in Form einer thermischen Sicherung.

Die thermische Sicherung sorgt dafür, dass sich die fehlerhafte Zelle nicht über eine Temperatur von etwa 190 °C hinaus aufheizt.

Die thermische Sicherung ist nicht dafür ausgelegt, einzelne Proben vor der weiteren Aufheizung über eine bestimmte Temperatur hinaus zu schützen; falls dieser Schutz erforderlich ist, sind zusätzliche Mittel zu verwenden.

Befo Beachten Sie die Sicherheitsverfahren Ihres Unternehmens, die gesetzlichen Gesundheits- und Sicherheitsverfahren sowie sämtliche, damit verbundenen Rechtsvorschriften, die für Ihre Arbeitsgebiete gelten. Überprüfen Sie die Laborverfahren für die erhitzten Stoffe und stellen Sie sicher, dass alle potenziellen Gefahren (z.B. Explosionsgefahr, Implosionsgefahr bzw. Gefahr der Freisetzung von toxischen oder entzündlichen Gasen) auf angemessene Weise berücksichtigt wurden, bevor die Arbeit fortgesetzt wird. Beim Erhitzen von bestimmten Stoffen kann es durch die Freisetzung von gefährlichen Gasen eventuell notwendig sein, dass ein Laborabzug oder eine andere Art des Abzugs verwendet wird. (Orientieren Sie sich an den

ohne Erd-/Masseverbindung. Stellen Sie

auf das

lgen Sie bei der Verwendung des Geräts immer die gute Laborpraxis.

Page 12

Vorgehensweisen Ihres Unternehmen

s.)

Integrity 10

Gerät bzw. das Netzteil

nicht

Integrity 10

Gerät bzw. das Netzteil

nicht

Integrity 10

Gerät bzw. das Netzteil

nicht

kein

keine

nicht

keine

nicht,

Stellen Sie sicher, dass sich das Gerät auf einer sauberen, trockenen, nicht brennbaren und festen Arbeitsfläche mit einem geeigneten Abstand von mindestens 300 mm in jede Richtung von anderen Geräten befindet.

Überprüfen Sie, dass sich das Netzteil auf einer sauberen, trockenen, nicht brennbaren Fläche befindet und ausreichend Platz für das Stromkabel zum Integrity 10-Gerät und die Netzeingangsleitung bzw. den Steckersatz für den Eingang/Ausgang vorhanden ist und keine unzulässige Biegebeanspruchung herrscht. Achten Sie auf einen geeigneten Abstand für die Luftströmung und Wärmeabgabe.

Stellen Sie das Anschluss an bzw. die Trennung vom Stromkabel erschwert wird.

Stellen Sie das Anschluss an bzw. die Trennung von der Kühlflüssigkeitszuführung erschwert wird.

Stellen Sie das Anschluss bzw. die Trennung von Daten- und Kommunikationskabeln erschwert wird.

Stellen Sie das Netzteil Netzsteckdose auf der Rückseite unzugänglich sind.

Tauchen Sie

Verschütten Sie Gehäusematerialien verfügen über den in Tabelle 8.1 "Darstellung der chemischen Beständigkeit" angegebenen Schutz. Wurden Stoffe verschüttet, trennen Sie die Einheit von der Netzstromversorgung und befolgen die Anweisungen des Abschnitts "Wartung, Instandhaltung und Reparaturen". Verdecken Sie das Integrity 10-Gerät bzw. das Netzteil

(INSBESONDERE BELÜFTUNGSSCHLITZE) während der Nutzung nicht.

Es wird zu lassen.

Teil dieses Gerätes in Wasser/eine Flüssigkeit.

Stoffe auf dem Touch Screen. Die

empfohlen, ein Heizgerät während des Betriebs unbeaufsichtigt

so hin, dass der An-/Aus-Schalter oder die IEC-

so hin, dass der

Verwenden Sie nur Teile und Zubehör von Originalgeräteherstellern. Siehe Abschnitt 11.

Das Gerät ist nicht funkengeschützt, flammbeständig oder explosionsgeschützt und wurde nicht für die Nutzung in gefährlichen Bereichen gemäß BSEN 60079-14:1997 ausgelegt. Halten Sie entzündliche Stoffe mit niedrigem Flammpunkt vom Gerät fern. Bedienen bzw. fassen Sie

Berühren Sie das Innere der Zellen befindet.

Vorsicht bei der Handhabung von HEISSEN & KALTEN Glaswaren

Achten Sie darauf, dass die Einheit Raumtemperatur erreicht hat, bevor Sie die obere Abdeckung entfernen.

Teile des Produkts mit nassen Händen an.

wenn sich das Produkt in Betrieb

Page 13

nicht

Touch Screen

Warnung.

Warnung

Vorsicht

tecken Sie, nachdem die obere Abdeckung entfernt wurde und das Innere der Einheit offen ist, Ihre Finger nicht in den vorderen oder hinteren Teil der Einheit, da sie eingeklemmt werden könnten.

hnen bzw. beugen Sie sich während des Betriebs

Halten Sie den Netzstecker und das Leitungskabel von der Heizfläche fern.

Der Bildschirm ist unempfindlich gegen Aceton. Es wird empfohlen, eventuell verschüttete chemische Stoffe sofort vom Bildschirm abzuwischen.

: Standardglas, das für das Integrity-Produkt geliefert wird, ist nicht für Hochdruckanwendungen geeignet. Der maximale Betriebsdruck für Standardglas mit installierter Kappe beträgt 0,5 bar.

: Glasbehälter können entweder spontan aufgrund von zu starker Belastung durch den Druck oder das Vakuum oder durch unbeabsichtigte Einwirkung heftig explodieren oder implodieren. Prüfen Sie Glasbehälter vor jeder Nutzung sorgfältig auf Risse, Kratzer oder Ätzspuren. Risse können die Wahrscheinlichkeit eines Bruchs erhöhen bzw. dazu führen, dass Chemikalien in das Gerät gelangen. Führen Sie alle Druck- und Vakuumvorgänge in Glasbehältern nur hinter geeigneten Blenden durch und tragen Sie während der Handhabung eine Persönliche Schutzausrüstung (vollständige Gesichtsmaske, Handschuhe, Schutzkleidung).

: Glasbehälter, die in einen Block mit einer hohen Temperatur gestellt wurden, dürfen nicht in einen kalten Block gestellt werden, da der Behälter dadurch wahrscheinlich zerspringen wird.

über die Einheit.

bei der Verwendung von entzündlichen Lösungsmitteln. Maßnahmen zur Verringerung der Brandgefahr umfassen u.a. die Schaffung einer inerten Atmosphäre in den Reaktionsgefäßen und/oder Verwendung des Geräts in einem gut belüfteten Bereich, z. B. unter einer Abzugshaube.

Weitere sicherheitsinformationen

ATS20002

Was einzelne Komponenten betrit, siehe unten.

und

ATS20003 PTFEKappen

Viton (Hauptdichtu

Viton ist beständig gegen eine Vielzahl von Chemikalien, darunter Öle,

wässrige Medien und die meisten anderen Flüssigkeiten. ng) und ORinge.

Es wird empfohlen, dass der Nutzer die chemische Verträglichkeit vor der

Verwendung prüft.

PTFE-Kappe

PTFE ist beständig gegen eine Vielzahl von Chemikalien, darunter Ozon, Chlor, Ethansäure, Ammoniak, Schwefelsäure und Chlorwasserstosäure. Die einzigen Chemikalien, die diese Beschichtungen nachweislich angreifen, sind geschmolzene Alkalimetalle und hochreaktive Fluorierungsmittel.

Es wird empfohlen, dass der Nutzer die chemische Verträglichkeit vor der Verwendung prüft.

Silikonkappe nseptum

Peroxidisch vernetzter HTV-Silikonkautschuk, klassiziert gemäß ASTM D 1418 als VMQ. Es wird empfohlen, dass der Nutzer die chemische Verträglichkeit vor der Verwendung prüft.

Page 14

316 Edelstahl 2 mm Durchmesser Stöpsel Probenahme

-Loch

Es wird empfohlen, dass der Nutzer die chemische Verträglichkeit vor der Verwendung prüft.

2.3. INFORMACIÓN DE SEGURIDAD

Este producto ha sido diseñado para funcionar de forma segura si se emplea de acuerdo con las instrucciones del fabricante.

NOTA: de no utilizarse este equipo de acuerdo con las instrucciones de manejo del fabricante, la protección básica de seguridad del usuario que ofrece el equipo puede verse comprometida y podría invalidarse la garantía. La garantía no cubre los daños derivados de una instalación incorrecta o del uso indebido del equipo.

Nunca

Integrity

fuente de alimentación

316

Edelstahl

-Loch

Es wird empfohlen, dass der Nutzer die chemische Verträglichkeit vor der

2 mm Durchmesser Stöpsel Probenahme

Verwendung prüft.

2.3. Información de seguridad

Este producto ha sido diseñado para funcionar de forma segura si se emplea de acuerdo con las instrucciones del fabricante.

Prevención de incendios y descargas eléctricas

Para evitar riesgos de incendio o descarga eléctrica, NO abra la caja de la fuente de alimentación (PSU) de Integrity sin autorización. Solo el personal debidamente cualificado debe realizar las tareas de reparación o mantenimiento de la PSU.

Asegúrese de que la conexión a la red eléctrica cumple las especificaciones indicadas en la placa de identificación situada en la cara inferior de la PSU.

utilice este equipo sin conexión a tierra. Asegúrese de que la tensión de la red eléctrica tiene conexión a tierra de acuerdo con la legislación vigente local.

coloque la

sobre la

En caso de que se produjera un fallo que causara el sobrecalentamiento de una celda de la unidad, esta dispone de protección adicional en forma de termofusible.

termofusible está diseñado para proteger celdas defectuosas que se

sobrecalientan continuamente por encima de los 190 °C aproximadamente.

El termofusible no está diseñado para proteger muestras individuales que sobrepasan una determinada temperatura; deben emplearse otros medios en caso de que sea necesario ese nivel de protección.

Práctica operativa y de seguridad estándar

ga siempre las buenas prácticas de laboratorio cuando use este equipo. Tenga debidamente en cuenta los procedimientos legislativos de seguridad y de salud y seguridad de su compañía y toda la legislación asociada aplicable en las zonas de operación. Compruebe los procedimientos de laboratorio relacionados con las sustancias susceptibles de calentarse y asegúrese de controlar todos los riesgos (p. ej. riesgo de explosión, implosión o liberación de gases tóxicos o inflamables) que puedan surgir antes de continuar. Cuando caliente determinadas sustancias, la liberación de gases peligrosos puede exigir el uso de una campana de humos u otros medios de extracción. (Consulte las prácticas de su empresa.) As

egúrese de que el equipo se utiliza sobre una superficie de trabajo firme, limpia, seca y no combustible y que esté separado al menos 300 mm de otros equipos de su entorno.

Page 15

Asegúrese de que la PSU se encuentra en una superficie limpia, seca y no

Integrity

10 o la fuente de alimentación

Integrity

10 o la fuente de alimentación

Integrity

10 o la fuente de alimentación

Advert

encia sobre la pantalla táctil.

Advertencia

combustible con espacio suficiente para el cable de alimentación que se conecta a Integrity 10 y que el cable de alimentación y el enchufe de la red pueden conectarse y desconectarse sin que se doblen. Asegúrese que hay espacio suficiente para que fluya el aire y se disipe el calor.

coloque la

difícil conectarlas o desconectarlas del conector del cable de alimentación.

coloque la

difícil conectarlas o desconectarlas del suministro de líquido refrigerante.

coloque la

difícil conectar o desconectar los cables de datos y comunicación.

coloque la PSU de modo que el interruptor de encendido y apagado o la

toma de corriente IEC situada en la parte posterior queden inaccesibles.

sumerja ninguna pieza de este equipo en agua o líquidos.

derrame sustancias sobre la pantalla táctil. Los materiales de la carcasa

están protegidos tal y como se indica en la Tabla 8.1 Tabla de resistencia química. Si se produce algún derrame, desconecte el equipo de la red eléctrica y siga las indicaciones de la sección "Mantenimiento, servicio y reparación por parte del cliente".

No cubra la Integrity 10 ni la PSU (ESPECIALMENTE LAS RANURAS DE VENTILACIÓN) mientras están en funcionamiento.

es recomendable dejar desatendido ningún aparato calefactor mientras

está funcionando. Utilice únicamente piezas y accesorios del fabricante del equipo original.

Consúltese la sección 11.

de modo que resulte

Este equipo no ha sido diseñado a prueba de chispas, llamas o explosión y no ha sido concebido para su uso en zonas peligrosas previstas en la norma BSEN 60079-14:1997. Mantenga alejadas del aparato las sustancias que sean inflamables y tengan un punto de ignición bajo.

utilice ni manipule ninguna pieza de este producto con las manos

húmedas.

toque el interior de las celdas cuando el aparato esté funcionando.

Extreme la precaución cuando maneje vidrio CALIENTE y FRÍO

Asegúrese de que la unidad alcanza la temperatura ambiente antes de retirar la tapa superior.

Una vez que se retire la tapa superior y quede expuesto el interior de la unidad, no introduzca los dedos en la parte delantera o trasera de dicha unidad ya que podría pillárselos.

se apoye o estire sobre la unidad cuando esté funcionando.

Mantenga el enchufe de red y el cable separados de la superficie de calentamiento.

La pantalla es impermeable a la acetona. Se recomienda limpiar inmediatamente cualquier derrame de sustancias químicas sobre la pantalla.

: el vidrio estándar suministrado para el producto Integrity no está diseñado para aplicaciones a altas presiones. La presión máxima de funcionamiento del vidrio estándar con la tapa puesta es de 0,5 bares.

: los recipientes de vidrio pueden explotar o implosionar de forma violenta, ya sea de manera espontánea por un fallo de tensión debido a la presión o el vacío, ya sea por un golpe accidental. Compruebe bien que los recipientes de vidrio no presentan grietas, arañazos

Page 16

o marcas de grabado antes de usarlos. Las grietas pueden aumentar la

Advertencia

Deben extremarse las precauciones

probabilidad de rotura o de fugas de productos químicos en el equipo. Realice todas las operaciones de presión y vacío en los recipientes de vidrio tras una pantalla de protección adecuada y utilice equipos de protección personal (máscara completa, guantes y prendas de protección) durante su manipulación.

: los recipientes de vidrio que se hayan colocado en un bloque a altas temperaturas no deben introducirse en un bloque frío, ya que es probable que se hagan añicos.

inflamables. Algunos métodos que pueden emplearse para reducir el riesgo de incendio consistirían en introducir una atmósfera inerte en los tubos de reacción o emplear los equipos en zonas bien ventiladas, p. ej. bajo una campana de humos.

Información complementaria acerca de la seguridad

Tapones de politetrauoroetileno (PTFE) ATS20002 y ATS20003.

Juntas de Viton (junta principal) y tórica.

Para componentes individuales, véase más abajo.

El Viton es resistente a una gran variedad de agentes químicos como los aceites, los medios acuosos y la mayoría del resto de líquidos.

Se recomienda al usuario que compruebe la compatibilidad química antes de su utilización.

cuando se utilicen disolventes

Tapón de PTFE.

Diafragma del

tapón

de silicona.

Tapón para

agujeros de muestreo de acero inoxidable 316 de 2 mm de diámetro.

2.4. Informazioni sulla sicurezza

Il presente prodotto è stato progettato per un funzionamento sicuro quando utilizzato secondo le istruzioni del fabbricante.

El PTFE es resistente a una gran variedad de agentes químicos como el ozono, cloro, ácido acético, ácido sulfúrico de amoníaco y ácido hidroclórico. Los únicos productos químicos que se sabe que afectan a estos revestimientos son los metales alcalinos fundidos y los agentes uorantes altamente reactivos.

Se recomienda al usuario que compruebe la compatibilidad química antes de su utilización.

Caucho silicónico HTV reticulado por peróxido, clasicado de acuerdo con ASTM D 1418 como VMQ. Se recomienda al usuario que compruebe la compatibilidad química antes su utilización.

Se recomienda al usuario que compruebe la compatibilidad química antes su utilización.

NOTA: Il mancato rispetto delle istruzioni operative fornite dal fabbricante può compromettere la sicurezza di base offerta dall’apparecchiatura e rendere nulla la garanzia. La garanzia non copre i danni causati da un’installazione scorretta o da un uso improprio dell’apparecchiatura.

Page 17

NON

mai

Non

Integrity 10

unità di alimentazione (PSU)

Non

Integrity 10 o l'unità di alimentazione

Non

Integrity 10 o l'unità di alimentazione

Non

Integrity 10 o l'unità di alimentazione

Non

Prevenzione degli incendi e delle scosse elettriche

Per evitare il rischio di incendio o scossa elettrica, dell'unità di alimentazione (PSU) di Integrity senza autorizzazione. Solo il personale qualificato addetto alla manutenzione può tentare di riparare/manutenere l'unità di alimentazione (PSU). Assicurarsi che l'alimentazione della rete elettrica sia conforme ai dati nominali indicati nella targhetta identificativa posizionata sul lato inferiore dell'unità di alimentazione (PSU). Non utilizzare terra/massa. Assicurarsi che la tensione di alimentazione sia correttamente messa a terra/massa in conformità con la legislazione vigente nel proprio paese.

posizionare

Se si verifica una condizione di primo guasto che fa sì che una cella all'interno dell'unità sia in sovratemperatura, nella cella è presente un fusibile termico che funge da ulteriore protezione.

Il fusibile termico è progettato per proteggere una cella in guasto che riscalda continuativamente a una temperatura che supera approssimativamente i 190 °C .

Il fusibile termico non è progettato per proteggere i singoli campioni che vengono riscaldati oltre una determinata temperatura; se si necessita di un tale livello di protezione occorre adottare altre misure.

questa apparecchiatura senza il collegamento di

sopra l'

aprire l'alloggiamento

Pratica di utilizzo sicuro generale

Seguire sempre le buone pratiche di laboratorio quando si utilizza questa apparecchiatura. Prendere conoscenza e implementare le procedure per la salute e la sicurezza vigenti, quelle stabilite dalla propria azienda e da qualsiasi normativa applicabile alla propria area di lavoro. Controllare le procedure di laboratorio per le sostanze che vengono riscaldate e assicurarsi che tutti i rischi potenziali (ad es. rischio di esplosione, implosione o rilascio di gas tossici o infiammabili) siano stati adeguatamente presi in considerazione prima di procedere. Quando si riscaldano determinate sostanze, il rilascio di gas pericolosi può rendere necessario l'utilizzo di una cappa aspirante da laboratorio o di altri mezzi di estrazione. (Consultare le pratiche stabilite dalla propria azienda).

sicurarsi che l'apparecchiatura venga utilizzata su una superficie di lavoro

As pulita, asciutta, non combustibile e solida con una distanza idonea su ogni lato di almeno 300 mm da altre apparecchiature.

Assicurarsi che l'unità di alimentazione (PSU) sia posizionata su una superficie pulita, asciutta e non combustibile con uno spazio sufficiente per il cavo di alimentazione di Integrity 10 e che il cavo di alimentazione di rete e la spina possano essere collegati/scollegati senza flessioni ingiustificate. Assicurarsi che via sia uno spazio idoneo per il flusso dell'aria e la dissipazione del calore.

posizionare

rendere difficile il collegamento o lo scollegamento dei cavi di alimentazione.

posizionare rendere difficile il collegamento o lo scollegamento dell'alimentazione del fluido refrigerante.

posizionare rendere difficile il collegamento o lo scollegamento dei cavi di comunicazione/dati.

posizionare l'unità di alimentazione (PSU) in modo tale da rendere inaccessibili l'interruttore di on/off o la presa di alimentazione IEC collocata sul retro.

immergere alcuna parte di questa apparecchiatura in acqua/fluidi.

in modo tale da

Page 18

Non

lasciar cadere alcuna sostanza sul touchscreen. I materiali

sconsiglia

Non

Touchscreen, avvertenza.

Avvertenza

Prestare attenzione

dell'alloggiamento sono protetti come stabilito nella Tabella 8.1 Resistenza chimica. Se si verifica un versamento, scollegare l'unità dall'alimentazione di rete e seguire le istruzioni indicate nella sezione "Manutenzione, assistenza e riparazioni del cliente".

Non coprire Integrity 10 o l'unità di alimentazione (PSU) (IN PARTICOLARE I CONDOTTI DI AERAZIONE) durante l'uso.

Si durante il funzionamento.

Utilizzare esclusivamente accessori e parti OEM. Fare riferimento alla sezione 11.

L'apparecchiatura non è a prova di scintilla, fiamma o esplosione e non è stata progettata per l'uso in aree pericolose secondo la norma BSEN 6007914:1997. Tenere lontano dall'apparecchiatura le sostanze infiammabili e a basso punto di infiammabilità.

utilizzare o manipolare nessuna parte di questa apparecchiatura con le

mani bagnate.

toccare la parte interna delle celle mentre il prodotto è in funzione.

Prestare attenzione quando si manipolano oggetti di vetro FREDDI O CALDI

Assicurarsi che l'unità abbia raggiunto la temperatura ambiente prima di rimuovere la copertura superiore.

Quando la copertura superiore è stata rimossa e l'interno dell'unità è esposto, non inserire le dita nella parte anteriore o posteriore dell'unità per evitare che rimangano incastrate.

di lasciare incustodito qualsiasi apparecchio riscaldante

appoggiarsi o allungarsi sull'unità durante il funzionamento.

Tenere il cavo di alimentazione e la presa lontano dalla superficie riscaldante.

Lo schermo è resistente all'acetone. Si consiglia di rimuovere immediatamente dallo schermo qualsiasi versamento di sostanze chimiche.

: Gli strumenti standard in vetro forniti per il prodotto Integrity non sono progettati per applicazioni ad alta pressione. La pressione massima di esercizio degli strumenti standard in vetro con cappuccio inserito è di 0,5 bar.

: I recipienti in vetro possono esplodere o implodere violentemente, in modo spontaneo per le sollecitazioni dovute alla pressione o al vuoto, oppure a causa di un impatto accidentale. Verificare attentamente che i recipienti in vetro non presentino crepe a raggiera, graffi o segni di corrosione prima dell'uso. La presenza di crepe può aumentare la probabilità di rottura o consentire alle sostanze chimiche di penetrare nell'apparecchiatura. Eseguire tutte le operazioni in pressione o vuoto nei recipienti di vetro dietro adeguata protezione e utilizzare dispositivi per la protezione individuale (protezione completa del viso, guanti, abbigliamento protettivo) durante l'uso.

: I recipienti di vetro che sono stati posizionati in un blocco ad alta temperatura non devono essere collocati in uno a bassa temperatura in quanto potrebbero frantumarsi.

quando si utilizzano solventi infiammabili. Le misure che possono essere adottate per ridurre il rischio di incendio comprendono l'introduzione di un'atmosfera inerte all'interno delle provette di reazione e/o l'utilizzo dell'apparecchiatura in un'area adeguatamente ventilata, ad esempio sotto una cappa aspirante.

Page 19

Informazioni aggiuntive sulla sicurezza

Cappucci in PTFE ATS20002 e ATS20003 Anello di tenuta Viton (tenuta principale) e Oring.

Per i singoli componenti vedere qui di seguito.

L'anello di tenuta Viton è resistente a un'ampia gamma di sostanze chimiche tra cui oli, mezzi acquosi e numerosi altri fluidi.

Si consiglia all'utente di verificare la compatibilità chimica prima dell'uso.

Cappuccio in PFTE

Setto del cappuccio in silicone

Tappo per foro di campionamento, diametro 2 mm, in acciaio inossidabile 316

Il PTFE è resistente a un'ampia gamma di sostanze chimiche tra cui ozono, cloro, acido acetico, ammoniaca, acido solforico e acido cloridrico. Le uniche sostanze chimiche note per attaccare questi rivestimenti sono i metalli alcalini fusi e gli agenti di fluorurazione altamente reattivi.

Si consiglia all'utente di verificare la compatibilità chimica prima dell'uso.

Gomma siliconica HTV reticolata con perossido, classificata in conformità con ASTM D 1418 come VMQ. Si consiglia all'utente di verificare la compatibilità chimica prima dell'uso.

Si consiglia all'utente di verificare la compatibilità chimica prima dell'uso.

Page 20

3. Introduction

The Integrity 10 Reaction Station’s evolutionary design allows the user to perform multiple reactions independently and simultaneously. Each cell position can be heated/cooled and stirred independently of the cell, next to, or adjacent to it.

The product can be used inside a fume cupboard, mounted onto a robotic platform or simply operated free standing on a laboratory work surface. For user safety, the Integrity 10 is driven by a low voltage power supplied by the PSU (Power Supply Unit). An Ethernet socket provides a means for connecting and controlling the Integrity 10 as part of an integrated system. RS485 / 232 and a Gilson Serial Input/Output Channel (GSIOC) protocol add to the versatility of the product.

The ‘Integrity’ control software friendly, intuitive interface.

When used together with the ‘Integrity’ software, additional accessories can be added to customise the Integrity

10specicallyforgiventasks,these include infraredprobesformeasurementofparticlespresentin anygiven

solution. Solution sample temperatures in each cell position can be accurately measured using the Electrothermal

‘Multitemp’probeset.ThesystemcanalsobeusedwithaReuxunitdesignedtopreventuidsamplesolution

loss from open, exposed glass vessels / test tubes (See section 13 on accessories).

In standalone use the Integrity 10 is easy to set up using the touch screen. With an intuitive menu system,

operationisbothquickandsimpleallowingtheusertosetupandoperateasimpleproleoroperatewithfull manual control. Experimental data can be stored and extracted via a USB ash key. The operating system is

Microsoft© Windows CE. Firmware is stored on the SD card supplied which can be easily updated.

(ATS11005), is available as an accessory and provides the user with a user

Page 21

3.1. Instrumentspecification

Unit

Number of Positions 10 Cell Cavity diameter

Glassvessellllevel

Temperature range Max ~Temperature difference

between any two positions. Temperature Overshoot Maximum controlled heating rate Maximum controlled cooling rate

Note: - See Appendix 'A'. Integrity cooling guide for the cooling specification

Stir speed range 350 - 1200 RPM Viscosity capacity Glycerine at 25°C Recommended stir bar AZS4235 10 Pack 12 x 4.5mm (cylindrical)

Note - Stir performance only guaranteed when using recommended stir bar

ecommendedspecificationofcoolingsystem

25mm

10-50mm

-30°C to 150°C Nominal 180°C s

<2°C when measuring in contents. 5°C / min 5°C / min

AZS4206 10 Pack 10 x 6mm (Oval)

ee note below

Working temperature range

Cooling capacity

Flowrate Pressure Inlinefilter

Internal Unit Measurement

Measured temperature range Temperature resolution Temperature accuracy Measured stir speed range Stir Speed Resolution Stir Speed Accuracy

Control Ports

5 to -5ºC

1.1kW (1100W) between 5ºC to -5ºC

≥5Litresperminute ≥2Bar 50micron

-30°C to +160°C

0.01°C ±0.5°C 350 to 1200 RPM 10 RPM ±10 RPM

RS232/485 Via 10 Pin GSIOC Via 8 Pin USB Master. USB Slave. Aux 485 Bus extension

Page 22

4.0. UNPACKAGING AND CONTENTS

4.1. Please check the contents of your carton against the diagram.

For your future reference

Item

Description

Qty

1 Instruction book 1

2 Integrity 10 - PSU 1 3 Integrity 10 - UNIT 1 4 Mains cord and lead set

(illustration only)

A/R

5 Stir bars (x10) 1 6 Power cable assembly

(illustration only)

7 Coolant supply hoses 2 8 Programmed SD card –

Pre inserted in the unit.

Item

Description

Qty

4. Unpacking and contents

Please check the contents of your carton against the diagram.

For your future reference please record your product’s

please record your products Serial and Model numbers.

Serial and Model numbers

1 Instruction book 1

2 Integrity 10 - PSU 1 3 Integrity 10 - UNIT 1 4 Mains cord and lead set

(illustration only)

5 Stir bars (x10) 6 Power cable assembly

(illustration only)

7 Coolant supply hoses 2 8 Programmed SD card –

Pre inserted in the unit.

Unit Serial Number Unit Model/Cat Number

Unit Serial Number Unit Model/Cat Number.

A/R

2 1

Page 23

5. Installation

Electrical safety and installation This equipment is designed to be used safely under the following conditions:-

• Indoor u

se only

• Use in a well ventilated area

• Altitude up to 2000 meters

• Ambient temperature range +5°C to +35°C

• Altitude to 2000m

• Relative humidity not exceeding 80% for temperatures up to 25°C decreasing linearly to 50% relative humidity at 35°C

• Mains supply voltage fluctuations up to ± 10% of the nominal voltage

• Over-voltage category II IEC60364-4-443 applicable

• Pollution degree 2

• Use with a minimum distance all round of 200mm from walls or other items

The Power Supply Unit (PSU) for the Integrity 10 has been subjected to electrical safety testing as part of the manufacturing process. However, it is acknowledged that some end users may wish to undertake further electrical safety testing as part of the installation process.

AC dielectric withstand (Flash/Hi Pot) must not be undertaken on this equipment as damage may

Electrical safety and installation This equipment is designed to be used safely under the following conditions:-

• Indoor u

se only

• Use in a well ventilated area

• Altitude up to 2000 meters

• Ambient temperature range +5°C to +35°C

• Altitude to 2000m

• Relative humidity not exceeding 80% for temperatures up to 25°C decreasing linearly to 50% relative humidity at 35°C

• Mains supply voltage fluctuations up to ± 10% of the nominal voltage

• Over-voltage category II IEC60364-4-443 applicable

• Pollution degree 2

• Use with a minimum distance all round of 200mm from walls or other items

AC dielectric withstand (Flash/Hi Pot) must not be undertaken on this equipment as damage may

result. Such testing will invalidate warranty.

DC dielectric withstand (flash/Hi Pot) may be applied to the PSU only (i.e. The Integrity 10 unit must not be connected when the PSU is being tested. The Integrity 10 unit operates at low voltage (15V DC) and must not be subjected to dielectric withstand (Flash/Hi Pot) testing.

DC dielectric withstand (flash/Hi Pot) testing shall only be undertaken by competent trained personnel using suitable test equipment / environment. DC test voltage should be no more than 1.414 times normal AC test value for a class I (grounded) equipment.

The test equipment/process should incorporate a discharge procedure to remove any stored DC charge that may remain on the PSU.

This equipment must be earthed/grounded to a fixed earth/grounded mains socket outlet. The mains

Electrical safety and installation This equipment is designed to be used safely under the following conditions:-

• Indoor u

se only

• Use in a well ventilated area

• Altitude up to 2000 meters

• Ambient temperature range +5°C to +35°C

• Altitude to 2000m

• Relative humidity not exceeding 80% for temperatures up to 25°C decreasing linearly to 50% relative humidity at 35°C

• Mains supply voltage fluctuations up to ± 10% of the nominal voltage

• Over-voltage category II IEC60364-4-443 applicable

• Pollution degree 2

• Use with a minimum distance all round of 200mm from walls or other items

AC dielectric withstand (Flash/Hi Pot) must not be undertaken on this equipment as damage may

result. Such testing will invalidate warranty.

The test equipment/process should incorporate a discharge procedure to remove any stored DC charge that may remain on the PSU.

This equipment must be earthed/grounded to a fixed earth/grounded mains socket outlet. The mains supply is to be earthed/grounded in accordance with current international and local legislation as applicable in the country/state of operation.

Ensure only the correct rated mains input fuses are fitted. (Where applicable ensure the correct Mains cord and moulded IEC plug and lead set fuse if fitted). See Technical Specification, Section 8 of this Instruction book.

Check the voltage on the product data label on this product unit and those of any accompanying electrical accessory. Ensure the rating conforms to your local supply.

It is recommended this product should be connected to a mains supply source which incorporates an RCD or GFCI device that has a tripping current of 30mA or less. The RCD or GFCI residual Current Device cuts off power to the equipment immediately it detects a current leakage fault.

o not install this product or accessories on a surface which may become wet from use with

Electrical safety and installation

This equipment is designed to be used safely under the following conditions:-

• Indoor use only

• Use in a well ventilated area

• Altitude up to 2000 meters

• Ambient temperature range +5°C to +35°C

• Altitude to 2000m

• Relative humidity not exceeding 80% for temperatures up to 25°C decreasing linearly to 50% relative humidity at 35°C

• Mainssupplyvoltageuctuationsupto±10%ofthenominalvoltage

• Over-voltage category II IEC60364-4-443 applicable

• Pollution degree 2

• Use with a minimum distance all round of 300mm from walls or other items

AC dielectric withstand (Flash/Hi Pot) must not be undertaken on this equipment as damage may result. Such testing will invalidate warranty.

dielectricwithstand(ash/HiPot)maybeappliedtothePSU only (i.e. The Integrity 10 unit must not

be connected when the PSU is being tested. The Integrity 10 unit operates at low voltage (15V DC) and must not be subjected to dielectric withstand (Flash/Hi Pot) testing.

DCdielectricwithstand(ash/HiPot)testingshallonlybeundertakenbycompetenttrainedpersonnel

using suitable test equipment / environment. DC test voltage should be no more than 1.414 times normal AC test value for a class I (grounded) equipment.

The test equipment/process should incorporate a discharge procedure to remove any stored DC charge that may remain on the PSU.

Thisequipmentmustbeearthed/groundedtoaxedearth/groundedmainssocketoutlet.Themains

supply is to be earthed/grounded in accordance with current international and local legislation as applicable in the country/state of operation.

Ensureonlythecorrectratedmainsinputfusesaretted.(WhereapplicableensurethecorrectMains cordandmouldedIECplugandleadsetfuseiftted).SeeTechnicalSpecication,Section10ofthis

Instruction manual.

Check the voltage on the product data label on this product unit and those of any accompanying electrical accessory. Ensure the rating conforms to your local supply.

Do not install this product or accessories on a surface which may become wet from use with other equipment.

The unit is supplied with a Mains cord and moulded plug wired as follows.

Green/Yellow or Green = Earth/Ground

Blue or White = Neutral Brown or Black = Live/line hot.

Page 24

Connect the power cable between the Integrity 10 PSU and the Integrity 10 unit. Push the plug into the socket

White

Neutral

Black

Live/line hot.



. Repeat the process for

Green/Yellow

or Green = Earth/Ground

Blue

White

Neutral

Brown

Black

Live/line hot.

Connect the power cable bet

ween the Integrity 10 PSU and the Integrity 10 unit. Push the plug into the

socket ensuring the lugs engage



and twist the lock ring clockwise to secure



. Repeat the process for

attaching the other end of the power cable to the PSU.

Connect the coolant supply to the Integrity 10 unit ensuring the supply outlet feeds the indicated reaction block inlet and the return is connected to the indicated outlet. Turn on the coolant supply and check there are no signs of any water leaks around the connectors. (Turn off the chilled water supply after checking for leaks).

To ensure efficient heating and cooling, the Integrity cell design incorporates high quality copper heat sink components that ensure optimum heat transfer between the process and the cooling media. When good quality coolant water is used, no service problems will be experienced associated with internal corrosion or blockages. However, if coolant water is deficient (e.g. hard water, high oxygen content, turbid, contaminated, debris, etc. and this results in the internal corrosion, or blockage of the cooling system, then this is beyond the control of the equipment manufacturer. As such Bibby Scientific Limited cannot support warranty claims for blockages, corroded cells etc. that are attributable to poor quality coolant water.

To guard against poor water quality and its affects, the following recommendations are made.

1. At installation, the end user should ensure that the cooling water supply is of distilled water quality.

2. Additives are not recommended

3. A coolant inline filter is recommended to filter to 75 micron. This should be checked / cleaned at intervals to suit local operating conditions.

4. Minimal annual service check by Bibby Scientific Limited, or its designated service agent, is recommend which includes flushing/back flushing/removal and inspection of cell conditions for any early signs of coolant water problems.

Note: The chilled water flow rate through this equipment must be continuous at minimum rate of 2.5 litres/min at 5 The coolant system should be able to dissipate heat energy at 1100W with a coolant temperature of 5

°°°°

C. Running all 10

cell positions at -25

°°°°

without a chilled water set at 5

°°°°

C supply may cause stress on the electrical components and

result in a reduced performance which may result in shorter service intervals.

For temperatures below 5°C, or as

recommended in the chiller manual, a coolant must be used. A mix

of 1:1 laboratory grade ethylene glycol and water is recommended. DO NOT use deionised water.

WARNING:

ensuring the lugs engage 1 and twist the lock ring clockwise to secure 2. Repeat the process for attaching the other end of the power cable to the PSU.

To ensure efcient heating and cooling, the Integrity cell design incorporates high quality copper heat sink components that ensure optimum heat transfer between the process and the cooling media. When good quality coolant water is used, no service problems will be experienced associated with internal corrosion or blockages. However, if coolant water is decient (e.g. hard water, high oxygen content, turbid, contaminated, debris, etc. and this results in the internal corrosion, or blockage of the cooling system, then this is beyond the control of the equipment manufacturer. As such ColeParmer Limited cannot support warranty claims for blockages, corroded cells etc. that are attributable to poor quality coolant water.

To guard against poor water quality and its affects, the following recommendations are made.

1. At installation, the end user should ensure that the cooling water supply is of distilled water quality.

2. Additives are not recommended

3. A coolant inline lter is to suit local operating conditions.

Minimal annual service check by Cole-Parmer Limited, or its designated service agent, is recommended

which includes ushing/back ushing/removal and inspection of cell conditions for any early signs of

coolant water problems.

See Appendix 'A'. Integrity cooling guide for more information

For temperatures below 5°C, or as recommended in the chiller manual, a coolant must be used. A mix of 1:1 laboratory grade ethylene glycol and water is recommended. DO NOT use deionised water.

recommended to filter to 50 micron. This should be checked / cleaned at intervals

Operating pressure up to 2.0bar - Maximum safe pressure 4.5bar.

WARNING:

•Donotuseammablecoolants.

•Consultthechillermanualtoensureacompatibleuidisused.

•Theuidmustbecompatiblewiththeincubator’swettedpartswhicharecopper,stainless303,

aluminium and nitrile.

• Ensure all tubing is kept free of kinks and restrictions and is held tidily in place using tie wraps if

necessary.

Page 25

(For PC connection only) Connect a USB data cable between the host PC and the Integrity 10 unit as illustrated.

Connect the PSU to the mains supply using the plug and lead set supplied with the Integrity. Turn on the mains power supplying the PSU.

Page 26

6. Environmental protection

Electrothermal has given due consideration to environmental issues within the design and manufacturing process of this product without compromising product performance and value.

Packaging materials have been selected such that they may be sorted for recycling.

Electrothermal has given due consideration to environmental issues within the design and manufacturing process of this product without compromising product performance and value.

Packaging materials have been selected such that they may be sorted for recycling.

At the end of your product and accessories life, it must not be discarded as domestic waste. Ref: EU

Packaging materials have been selected such that they may be sorted for recycling.

This product and accessories must be accompanied by a completed Decontamination

Packaging materials have been selected such that they may be sorted for recycling.

This product and accessories must be accompanied by a completed Decontamination Certificate prior to any disposal. Copies of the Certificate are available from your distributor of Electrothermal products, alternatively you may copy and enlarge from ‘Appendix A’ of this instruction book.

This product contains a Lithium Cell button Battery (CR2032) on the control PCB

Electrothermal has given due consideration to environmental issues within the design and manufacturing process of this product without compromising product performance and value.

Packaging materials have been selected such that they may be sorted for recycling.

At the end of your product and accessories life, it must not be discarded as domestic waste. Ref: EU Directive 2002/96/EC on Waste Electrical and Electronic Equipment Directive (WEEE).

*Please contact your distributor / supplier for further information. For end users outside of the EU consult applicable regulations.

This product should only be dismantled for recycling by an authorised recycling company.

This product and accessories must be accompanied by a completed Decontamination Certificate prior to any disposal. Copiesofthecertificateareavailablefrom distributor/Manufacturer.

6.1. Battery disposal

This product contains a Lithium Cell button Battery (CR2032) on the control PCB located in the front Pod of the Integrity 10 Unit. All batteries must be disposed of in accordance with regulations. DO NOT dispose of product in a fire as batteries may explode.

Cole-Parmer’s Electrothermal branded product range is registered with the Environment Agency under the name of as Electrothermal Engineering Limited as being a producer of WEEE (Waste Electronic and Electrical Equipment) through b2b Compliance, an authorised waste collection compliance scheme.

Page 27

7. Product operation

7.0.

PRODUCT OPERATION

7.1. Product overview

The illustrations below show a detailed layout of the product.

7.1. Product overview

The illustrations below show a detailed layout of the product.

Integrity 10 Unit

1 Latch – drip tray release 2 Drip tray 3 Reaction well 4 Refer to Instruction book warning 5 Bus socket (for driving accessories) 6 In / out coolant water supply 7

Plug for power cable

8 Data plate label – found on underside of the reaction unit

9 Touch sensitive screen 10 USB ports (Master and Slave) 11 Ethernet RJ45 Socket 12 GSIOC protocol socket 13 RS232 / 485 protocol socket 14 SD card slot

Power supply overview

On / Off (standby) button

15 16 Front grill – cooling vents 17 Earth test point 18 IEC mains input socket 19

Socket for power cable

20 Data plate label – found on underside of the PSU unit

21 Cooling vents

Page 28

On / Off button switch

Front grill – cooling vents

Earth test point

IEC mains input socket

4 pin socket for power cable

Data plate label – found on underside of the PSU unit

Cooling vents

7.2. Reduction Sleeves - Fitting and Removal

Always ensure the cell temperatures are at a safe temperature to touch. (Between 40°C and -

On / Off button switch

Front grill – cooling vents

Earth test point

IEC mains input socket

4 pin socket for power cable

Data plate label – found on underside of the PSU unit

Cooling vents

7.2. Reduction Sleeves - Fitting and Removal

Always ensure the cell temperatures are at a safe temperature to touch. (Between 40°C and -

 Reductionsleev

.2.

es - fittingandremoval

Always ensure the cell temperatures are at a safe temperature to touch. (Between 40°C and -5°C)

Always turn off the coolant water supply before removing the drip tray.

Insert reduction sleeve

Insertreduction sleeves by pushing them straight intothe cells. Reduction sleeves may be tted into any cell

position.

Remove reduction sleeve

To remove the reduction sleeves, release the latch on the top of the Integrity unit and lift off the drip tray.

Push in the oil seal retention clip and lift out oil seal.

Page 29

Lift reduction sleeves out of cells.

Replace the oil seal and reposition the retention clip.

Replace the drip tray ensuring the latch is engaged properly.

Page 30

7.3. Insert SD card

Note: Your Integrity 10 unit will have been not function without it fitted.

Insert the SD card supplied into the SD card slot, with the card contacts facing the back. Leave the SD card in place during use. The SD card is acting as the system hard drive.

Note: Your SD card has been programmed for use specically with the Integrity system for which it was supplied. If the card is swapped with another SD card programmed for use with another integrity system the touch screen buttons may not align with the screen touch sensing points.

Observe the correct orientation of the SD card.

DO NOT r corruption may result.

emove the SD

card

when

despatched with the card already in position. Your Integrity unit will

the

unit

powered up or operating. Loss of data and program

7.4. Turn unit ON

Note: Ice will form round the Integrity 10 cell assemblies when the unit is run for extended periods at temperatures below 0°C .

Ensure coolant supply and mains power are connected and turned on. See Appendix 'A'. Integrity cooling guide for the cooling specification. Make sure to turn the water on before turning on the power. If

this is not done an error message may appear.

Press the button on top of the Power Supply Unit to commence operation. Observe the green luminance of the

power on switch.

The Integrity 10 can be used in conjunction with STEM Integrity control software (ATS11005), or it can be run in standalone mode. InstandalonemodetheIntegrity10canbesetupandrunviamanualcontrolorviaa

profileset-up.

7.5. Turn unit OFF

Depress the Power Supply button once again to turn off the unit.

Page 31

7.6. Power up

Typical splash screen for the Integrity 10 Unit.

WhentheIntegrity10isrstpoweredupitwillgothroughaselfcheckandwarmupcyclewhichwilltakeafew

minutes. During this time period a splash screen will be displayed.

After the Splash screen has been displayed the home screen will come into view.

Typical splash screen for the Integrity 10 Unit.

Home screen for the Integrity 10

Page 32

7.7. Time and date setting

7.7. Clock and Date Setting

The first time the Integrity 10 system is used the time clock and date must be set. The clock and date setting is performed using the following method.

Note: Accurate clock time is required when using data storage facility as the experiment data stored is time stamped.

Touch the settings Icon to enter settings mode.

Note: Settings mode cannot be accessed if any cell positions are in use.

Touch the clock Icon to enter the clock and date settings mode.

Clock Icon

7.7. Clock and Date Setting

The first time the Integrity 10 system is used the time clock and date must be set. The clock and date setting is performed using the following method.

Note: Accurate clock time is required when using data storage facility as the experiment data stored is time stamped.

Touch the settings Icon to enter settings mode.

Note: Settings mode cannot be accessed if any cell positions are in use.

Touch the clock Icon to enter the clock and date settings mode.

From the clock setting screen use the up/down arrowed buttons to set the correct time and date.

Clock Icon

ThersttimetheIntegrity10systemisusedthetimeclockanddatemustbeset.Thetimeanddatesettingis

performed using the following method.

Note: Accurate clock time is required when using data storage facility as the experiment data stored is time stamped.

Touch the settings Icon to enter settings mode.

Note: Settings mode cannot be accessed if any cell positions are in use.

Touch the clock Icon to enter the clock and date settings mode.

Clock icon

From the clock setting screen use the up/down arrowed buttons to set the correct time and date.

Once the correct date and time has been entered press the Green tick button to accept the setting entered. You are now taken back to the home screen from which you commence operation.

Page 33

ALTERNATIVE METHOD

Touchthedisplayeldyouwishtoset.

Display Field

Select the setting required from the touch pad screen. Touch the green tick to except the setting or touch the

redcrosstocleartheeldandre-entertheeldsetting.Thegreenbackarrowwilltakeyoubacktotheprevious

screen.

Note: Daylight saving time settings will need to be adjusted using the time setting process as described above. Note: The date will automatically adjust for leap years.

7.8. Communication protocol selection (for use with external control)

To change the protocol to accept GSIOC ensure your host systems communication platforms protocol is GSIOC driven.

Touch the settings Icon to enter settings mode.

Note: Settings mode can only be entered immediately after the Integrity has been switched on. Once run settings have been made the settings icon will disappear.

To enter ‘settings mode’ at any time ensure all cells are turned off.

Touch the communication Icon in the settings screen to enter communication selection.

Note:

GSIOC mode must be selected to control via ATS11005 Integrity software.

Page 34

Communication icon

From selection screen touch the GSIOC facility selection.

Once th

From se

e settings protocol has been changed the Integrity 10 must

lection screen touch the GSIOC facility selection.

be switched off and then turned back on

before the new settings will become active.

Unless using this equipment with GSIOC protocol enabled systems leave the communication protocol set for STEM.

From the home screen touch the settings Icon to access the settings screen. is

To check you have the latest software version, please contact [email protected].

.9.

iewfirmwarereleaseset

displayed across the bottom of the settings screen.

The software version set number

Page 35

Press the green back arrow to return to the home menu.

the green back arrow to return to the home menu.

7.10. Manual control

This view of the Home Screen is typical of the Integrity 10 without any cell position operational.

The graph area will represent real time data when the unit is running.

Version number

A highlighted cell button showing real time temperature and stir speed

Individual cell adjustment and settings: By touching any one of the cell position buttons the correlating cell

canbesettoruninmanualcontrolorprolemodeasdeterminedbytheuser.

TheuserisnowpromptedtoselectwhethertheywishtoruntheIntegrity10in‘ManualControl’or‘ProfileMode’.

Select ‘Manual Control’ by lightly touching the button position on the touch screen panel.

Page 36

button to accept the value

button will remove the setting entered in that field.

hetemperature field must be filled however all other fields are optional.

Greyedouteldsindicateanoptionalsetting.

7.10.1. Setting the temperature

Touchtheeldboxonthe display screen to enter asettingintothe appropriate eld. Toenter a temperature setting,touchthetemperatureeldbox.

Use the keypad to enter the required temperature setting. Press the button to accept the value entered.

Touchingthebuttonwillremovethesettingenteredinthateld.

Page 37

Note: When a temperature value has been entered both Ramp rate and Upper limit elds may be selected.

button to accept the value entered.

7.10.2. Setting the stir speed:

TouchtheStirspeedeld.

As with the process for entering a temperature you may enter the stir speed using the key pad.

Press the button to accept the value entered.

7.10.3. Setting the run time

Thelengthoftimetheuserwishestheunittorunthecellforissetviathiseld.Bytouchingthe‘Time’elda

run time period may be set. Enter the required run time in minutes. Example, 4 hours 25 minutes is 265 minutes.

Note: The maximum run time entry is 9999 minutes = 166 hours and 39 minutes.

Press the button to accept the value entered.

7.10.4. Setting the ramp rate

TheoptionaleldofRampratemaybechangedusingthesameprocedure.Touchtheeldboxtoselectthe

setting keypad.

Note: The default setting for ramp rate is 5.0°C per minute. Graduations can be set as low as 0.1°C per minute. When

0.0 is entered, maximum ramp rate is achieved as default, however, this is uncontrolled ramping.

Page 38

Enter the required ramp rate using the keypad. Press the button to accept the value entered.

button to accept the value entered.

. The cell will commence running as per the inputted settings.

and selecting the green tick all the

button to accept the value entered.

7.10.5. Setting the maximum upper limit

To help control an exothermic reaction a maximum upper temperature limit may be set. When the Integrity 10 senses an unexpected change in temperature state, action will be taken to prevent the change exceeding the set

maximumtemperaturelimit.Thesetdefaultofthiseldis165.0°C.

Enter the setting using the keypad. Press the button to accept the value entered.

7.10.6. Copy function

Oncetheuserhascompletedenteringalltherequiredeldentriestheenteredsettingsmaybecopiedoverinto

another cell. Touch the copy button to write the settings to the internal clipboard.

Pressingbackwillnowshowthehomescreen.Touchthecellyouwishtopastethevalueintoandtheeldswill havethecopiedvaluelledin.

You may now press The cell will commence running as per the inputted settings.

Copy all: By selecting the copy all check spot and selecting the green tick all the setting made are automatically copied into all the other vacant cell positions.

If ‘copy all cells’ is selected pressing ‘start’ will cause all cells to commence operation. The home screen is then displayed.

Note: The Paste button is only visible once the copy button has been selected.

Page 39

7.10.7. Adjusting the settings of a running cell in manual control

and selecting the green tick all the

button to accept the value entered.

Touch the active cell button for adjustment. The screen will ask you to ‘Turn cell off’ or ‘Adjust setting’.

Touch the adjust button and then select the ‘Manual control’ from the next screen.

Selecttheeldoreldstobeadjustedaspertheoriginalrunsetup.

Check the ‘All cells’ spot if you wish to apply the change to all cells, or touch the copy button for pasting the change into selected other cells.

Touch the button to accept and commence running the change.

Note: The ‘Start’ button isn’t visible when adjusting a running cell

Page 40

7.10.8. Home screen when operational

Cell temperature increase.

Cell tem

perature decrease.

Cell temperature increase.

Cell tem

perature decrease.

Control

by contents

Shown in this example is a typical home screen with all the cells operational. The graph on display is from cell 2. To change the graph view between cells, touch the cell number at the top of the graph.

Note: If a cell is not operational it will not be possible to select the tab.

By touching the graph screen area it is possible to toggle sequentially from one screen to the next operational screen in ascending order.

The graph is accumulative and will auto rescale as a cell is run.

When a green band is seen around the cell, this indicates the cell has a setting written to the field(s). The cell may not

be running but it has been set ready for operation.

Aredbandaroundthecellindicatesthecellhasnishedarunandassociatedactivitiesarecomplete.Seesection

7.14‘SavinganExperiment’.Oncethecellhasfinished,the

cell can be used again.

A grey band indicates that the cell is not in use and that no data is sitting behind awaiting a storage decision.

On screen symbols

experimentmustbeeithersavedordeletedbeforethe

The real time temperature and stir speed are shown within the cell box.

Cell temperature increase.

Cell temperature decrease.

Control by contents

Temperature °C Stir speed RPM

Page 41

7.11. Profile control

and if required repeat that same cycle as

Note: It is possible to have some cells running in prole mode while others are running via manual control.

Aprolewillallowtheusertosetupandrunastepcycleandifrequiredrepeatthatsamecycleasmanyas10

times (when using the optional Integrity PC software this is increased to 999 times).

7.11.1. Profile set up

Fromthehomescreen,touchtherequiredcelltheproleistobesetupin. Thistimeselectthe‘Prolesetup’button.

This next screen shows a prole step. To complete the prole all elds must be completed. Once a eld has

changed from a grey state it can have setting parameters added and amended. The screen layout is intended to

visiblyshowthestepsrequiredtocompleteaprolesetup.

Note: It is possible to set up a profile that is the inverse of the one displayed by selecting a target temperature below that of the initial temperature.

Page 42

7.11.2. Setting the initial temperature

ual control the will take you back to the previous screen. The button is

ill take you back to the previous screen. The button is

s used to remove an incorrect field entry. Use the keypad

Touchtheinitialtemperatureeldtoactivatetheeldinputscreen.Usethekeypadtoinputyourrequiredstart temperature.Theinitialstarttemperatureisthetemperatureyouwishtheproletocommencefrom.Itcanbe

different to the ambient temperature of the cell.

Note: To enter -25.6°C Press 2, then 5, then 6, followed by the minus sign.

Note: the - minus symbol will only appear when you start entering the temperature.

As with manual control the will take you back to the previous screen. The button is used to accept a

valueandthe is used to remove an incorrect field entry. Use the keypad to enter your initial start

temperature.

7.11.3. Setting the initial hold time

Thisissimilarinoperationtothepreviouseld.Touchtheeldtoentertherequiredsetting.Allwhiteeldboxes musthaveavalueentered.Greyeldboxesareoptionalsettingsanddonotneedtohaveasettingentered.

Use the keypad to enter the time value (minutes) for the length of time you wish the initial temperature to be held at.

Note: Enter the time in minutes. Example, 4 hours 25 minutes is 265 minutes.

Page 43

Touch

Touc

h to except the time entered in the Initial hold time field.

7.11.4. Setting the Initial Ramp: The initial ramp rate is the rate of temperature change required. The Initial ramp may be set to decrease in temperature as well as increase. Touch the field to enter the required setting.

Note: The default setting for ramp rate is 5.0°C per minute. Graduations can be set as low as 0.1°C per minute. When 0.0 is entered the ramp rate will climb as rapidly as

possible to the desired target temperature.

Use the keypad to make the field entry. Touch the button to accept the value set.

button to accept the value entered.

7.11.4. Setting the initial ramp

The initial ramp rate is the rate of temperature change required. The initial ramp may be set to decrease in tem-

peratureaswellasincrease.Touchtheeldtoentertherequiredsetting.

Note: The default setting for ramp rate is 5.0°C per minute. Graduations can be set as low as 0.1°C per minute.

When 0.0 is entered the ramp rate will climb as rapidly as possible to the desired target temperature.

Usethekeypadtomaketheeldentry.Touchthebuttontoacceptthevalueset.

toexceptthetimeenteredintheinitialholdtimefield.



7.11.5. Setting the target temperature

Thetargettemperatureisthetemperaturetheuserwishestheproletoattain.This can be a minus temperature as well as a positive one.Touchtheeldtoentertherequiredsetting.

Usethekeypadtomaketheeldentry.Touchthebuttontoacceptthesetvalue.

Note: To enter -25.6 Press 2, then 5, then 6, followed by the minus sign.

Page 44

7.11.6. Setting the maximum upper limit

button to accept the value entered.

maximumtemperaturelimit.Thesetdefaultofthiseldis165.0°C.

Enter the setting using the keypad. Press the button to accept the value entered.

Note: The maximum upper limit may be set to a minus Celsius value.

Toclearthedataeldtouchthe‘redcross’.Ifyounolongerwishtosetamaximumupperlimit,touchtheback

button to return to the previous screen and then touch the ‘red cross’.

Note: To enter -25.6°C Press 2, then 5, then 6, followed by the minus sign.

7.11.7. Setting the plateau time

Thisisthelengthoftimetheuserwishestohavetheunitrunatthetargettemperature.Thedataeldrequires

the user to enter a time in minutes.

Note: Enter the time in minutes. Example, 4 hours 25 minutes is 265 minutes.

Page 45

7.11.8. Final temperature

The final temperature is the temperature at which the user wishes the profile to conclude the final step at. Touch the field to bring up the keypad for entering the required settings.

Usethekeypadtoenterthenaltemperaturevalue.This can be either a positive or negative value.

Note: To enter -25.6 Press 2, then 5, then 6, followed by the minus sign.

Page 46

7.11.9. Final ramp

7.11.9. Final ramp: The final ramp is the rate of temperature change from the target temperature to

the final temperature. The final ramp rate can be set to either increase or decrease in temperature. Touch the field to enter the required setting.

Note: The default setting for ramp rate is 5.0°C per minute. Graduations can be set as low as 0.1°C per minute. When 0.0 is entered the ramp rate will climb as rapidly as

possible to the set target temperature.

7.11.9. Final ramp: The final ramp is the rate of temperature change from the target temperature to

the final temperature. The final ramp rate can be set to either increase or decrease in temperature. Touch the field to enter the required setting.

Note: The default setting for ramp rate is 5.0°C per minute. Graduations can be set as low as 0.1°C per minute. When 0.0 is entered the ramp rate will climb as rapidly as

possible to the set target temperature.

Use the keypad to make the field entry. Touch the green tick button to accept the set value.

Thenalrampistherateoftemperaturechangefromthetargettemperaturetothenaltemperature.Thenal rampratecanbesettoeitherincreaseordecreaseintemperature.Touchtheeldtoentertherequiredsetting.

Note: The default setting for ramp rate is 5.0°C per minute. Graduations can be set as low as 0.1°C per minute.

When 0.0 is entered the ramp rate will climb as rapidly as possible to the set target temperature.

Usethekeypadtomaketheeldentry.Touchthegreentickbuttontoacceptthesetvalue.

7.11.10. Setting the hold time

Thisisthetimeatwhichtheuserwishestoholdthenaltemperature,afterwhichtheusercanchoosetoeither stoptherunorrepeattheproleonaloopsetting.

Use the keypad to enter the hold time value in minutes.

Note: Enter the time in minutes. Example, 4 hours 25 minutes is 265 minutes.

Page 47

7.11.11. Stir speed

7.11.11

. Stir Speed: The stir speed is set to 0 RPM by default. At this setting the stir facility is

turned off. Turn the stir function on by entering a value. The lowest stir speed that may be selected is 350RPM. The maximum stir speed value that may be set is 1200RPM. Touch the field to enter a value.

Use the keypad to enter a stir speed value.

The stir speed is set to 0 RPM by default. At this setting the stir facility is turned off. Turn the stir function on by entering a value. The lowest stir speed that may be selected is 350RPM. The maximum stir speed value that may be set is 1200RPM.

Touchtheeldtoenteravalue.

Use the keypad to enter a stir speed value.

7.11.12. Profile loop

By selecting the profile loop the user is given the facility to enter the number of times they wish to loop the

prole.Thedefaultvaluefornumberofloopsissetto1.Tochangethenumberoftimestheproleisrepeated, touchtheeldboxandusethekeypadtoenterthedesiredvalue.

Note: A maximum of 10 loops may be set per profile (when using the optional integrity PC software this is increased to 999 times).

Note: The start temperature for all subsequent loops will be the same temperature as the nish temperature of the preceding loop.

Touch the back arrow to return to the ramp loop selection screen.

Page 48

Youarenowpresentedwiththenalsettingscreenfromwhichanychangesmaystillbemadebytouchingthe

You are now presented with the final setting screen from which any changes may still be made by touching the relevant settings field. The user has the facility to select ‘Save profile’. From here the user is taken through menu screens which enable to user to store the profile so that it may be used at a future date. (See ‘Save Profile’). The user may select to copy the profile to the clipboard so that it can be pasted into other cell profiles. Touch the green tick to return to register the entry and return to the profile screen.

7.11.13. Copy and Paste a Profile: Once the copy button has been pressed this profile is copied to the internal clip board and can be pasted into other cells as per 7.10.6.

Touch the Start button to commence running the profile or touch the green tick to accept the profile settings. Both functions will take the user to the main Home screen. From the home screen touch the cell you wish to paste the copied profile to.

relevantsettingseld.Theuserhasthefacilitytoselect‘Saveprole’.Fromheretheuseristakenthroughmenu screenswhichenabletousertostoretheprolesothatitmaybeusedatafuturedate.(See‘SaveProle’).The usermayselecttocopytheproletotheclipboardsothatitcanbepastedintoothercellproles.Touchthegreen ticktoreturntoregistertheentryandreturntotheprolescreen.

7.11.13. Copy and paste a profile

Oncethecopybuttonhasbeenpressedthisproleiscopiedtotheinternalclipboardandcanbepastedinto

other cells as per 7.10.6.

TouchtheStartbuttontocommencerunningtheproleortouchthegreenticktoaccepttheprolesettings.

Both functions will take the user to the main Home screen. From the home screen touch the cell you wish to

pastethecopiedproleto.

Touchthe‘Paste’buttontoloadthesavedprolesettingintothiscell.Oncethenewprolehasbeenpopulated youhavethesameeditingfacilitiesaspertheoriginalprole.Simplytouchtherequiredeldforeditinganduse

the keypad to re-enter data. Touch the green tick to commence cell operation and return to the home screen. If

youdecidetoremovethepastedprole,touchthe‘redcross’.

Note: The saved prole remains on the clipboard. You may select another cell and paste the prole into it.

Page 49

7.11.14. In the event of power loss

TheIntegrity10willturnoff.Alleldsettingswillbelost.Partwrittendatamaybeextractedmanuallyfromthe

SD card using an SD card reader. All previously stored data written to the SD card will be safe.

7.12.

Thepro composition of the experiment may be added. This profile setting information can be recalled at any time inthe futureandreloadedintoanygivencellpositioninordertore-runtheprole.Namingandstoringprolesmaybe

undertaken while other cells are in operation.

Note: This feature is only available as an option from the prole setting facility.

Tosavetheprolesettingstouchthe‘SaveProle’button

Youare now taken to the eld selection screen as illustrated below.

Naming and saving a profile

lethathasbeensetinsection7.11.maybenamed.Inaddition,extrainformationaboutthenaturean

d

Page 50

The fields can be completed in any order. All fields must be completed before the profile can be saved.

ill take you back to the previous screen.

button is used to accept the field entry. By touching this button the field entry is accepted.

ouchtherequir redfieldpositiontobetakentotherespectivedatainputscreen.



The back button will take you back to the previous screen.

Profile Name:

The back button will take you back to the previous screen. Use this button to remove an incorrect

eldentry.

n w

From the screen below use the keyboard to name the profile.

Thisbuttonisusedtoaccepttheeldentry.Bytouchingthisbuttontheeldentryisaccepted. YouaretakenbacktotheProleeldselectionscreen.

Usingthesamemethodllinthe‘Owner’,‘Recipe’,‘Composition’and‘Concentration’elds.

Uponcompletionwithinthesaveprolescreenagreentickisnowshown.Touchthetickbuttontoacceptthe eldentriesandsavetheprole.

Toeditanyoftheeldstouchtherespectiveeldandeditusingthekeyboard.

Page 51

7.13

button.

Stored profile view and copy

Theconceptofstoredproleretrievalistocallupanystoredproleandviewitseldentriesasenteredin section7.12.Furthermorealloftheprolesettingscanalsobeviewed.Itisalsopossibletoselectandcopy astoredprolewhichcanthenbepastedtoanyvacantcellposition.Allprolesettingsmaybeeditedandif requiredtheprolecanberenamedandeditedandstoredasanewprole.

StoredprolescanbeviewedatanytimeregardlessofwhatotherfunctionstheIntegrity10isperforming.Theonly

exception to this is when the screen is locked because of an external control source. See section 7.18.

Note: A prole can’t be stored once the associated experiment run has been completed. It can only be stored before and during the run of an experiment.

All of this may be undertaken while other cells are in use.

7.13.1. Storing a profile

From the home screen, with or without any cells in use touch the ‘View results /

Proles’ button.

Thenextscreenaskstheuseriftheywishtoviewstoredprolesorviewstoredexperimentdata.Toviewastored proletouchthetickbuttonassociatedwiththestoredprolestatement.

Page 52

Note: The back button will take you back to the home screen.

Note: T

he back button will take you back to the home screen.

All stored profiles will appear in a list box as shown below. They appear alphabetically and are listed by profile name.

Note: T

he back button will take you back to the home screen.

All stored profiles will appear in a list box as shown below. They appear alphabetically and are listed by profile name.

(Example of named profiles)

Touch the profile title to be viewed. It will then become highlighted.

(Example of named profiles)

to accept and view selected profile.

will take you back to the home screen.

Allstoredproleswillappearina listboxasshownbelow.Theyappearalphabeticallyand arelistedbyprole

name.

(Example of named proles)

Touchtheproletitletobeviewed.Itwillthenbecomehighlighted.

Touchthegreentickbutton toacceptandviewselectedprole.

Youarenowabletoviewtheselectedprole.Scrolldownusingthescrollbarstoviewtheprolesettingsaswell asnamedeldentries.

Page 53

will take you back to the home screen.

. The profile is now copied to

button to return to the profile selection screen.

button to return to the home screen in order to select a different

Touchthegreentick buttontoreturntotheproleselectionscreen.

Touch the green back arrow button to return to the home screen.

Tocopytheproleintoothercellstouchthe‘copy’button .Theproleisnowcopiedtoaninternal

clipboard.

Touchthecellbuttonthatistohavetheprolecopiedto.

Note: Ensure the cell selected is one that is not in operation.

TouchtheProleSetupbuttontobringuptheproleentryeldscreen.

Touchthepastebuttontopopulatealltheeldswiththecopiedprolesettings.

Touch the green back arrow button to return to the home screen in order to select a different cell.

Page 54

7.13.2. Delete a stored profile

Fromtheproleinformationdisplayscreentouchthe‘DeleteProle’button.

Touchthegreenticktodeletetheprole.Touchthe‘redcross’tocanceltheproledeletion.

Page 55

7.14. Saving an experiment

will take you back to the home screen.

Stored experiments are time and date stamped. You should ensure the clock settings are correct (See section 7.7.).

Theprincipledifferencebetweensavingaproleandsavinganexperimentisthataproleissavedwhenithas beencreated.Aprolecannotbesavedoncetheassociatedexperimentrunhasbeencompleted.

An experiment can

set up or manual control modes.

When an experiment run is complete or the experiment has been stopped a red ring is displayed around to the cell button. To clear the ring and use the cell again the user must either save the experiment data or decline the

saveexperimentoption.Thisisdonefirstlybytouchingthecell button highlighted with a red ring.

You will now see the screen as illustrated below.

only be saved once it has completed its run. An experiment can be saved from both the profile

Touchtherequiredeldpositiontoinputtherespectiveentry.

The back button will take you back to the home screen.

Note: The elds can be completed in any order.

Experiment name: Use the keyboard to input the experiment name.

Page 56

Thebackbuttonwilltakeyoubacktothehomescreen.Usethe button to remove an incorrecteld

button is used to accept the field entry, by touching this button the field entry is accepted

entry.

Thebuttonisusedtoaccepttheeldentry,bytouchingthisbuttontheeldentryisacceptedandtheuser istakenbacktotheexperimenteldselectionscreen.

CompletetheExperimentOwner,Recipe,CompositionandConcentrationeldsusingthesamemethodasabove.

CLEARING A CELL WITHOUT SAVING DATA: Touch the highlighted cell button.

Now press the Red cross button.

Note: If the elds are lled touching this button will clear out all eld entries.

Ifalltheeldsareblankthenyouaretakentothefollowingcanceloperationscreenasillustrated.

Touchthegreenticktoacceptdatacancellationorthe‘redcross’toreturntotheeldentryscreen.

The red cell ring will change back to grey. The cell is now ready for further use.

Page 57

7.15. Reviewing stored experiment data

tton.

Stored experiment data can be viewed at anytime regardless of what other functions the Integrity 10 is performing. The only exception to this is when the screen is locked because of an external control source. See section 7.18.

7.15.1. Accessing stored experiment data

From the home screen, with or without any cells in use, touch the

‘Viewresults/Proles’

button.

Thenextscreenaskstheuseriftheywishtoviewstoredprolesorviewstoredexperimentdata.ToviewStored ExperimentDatatouchthetickbuttonassociatedwiththestoredprolestatement.

Note: The back button will take you back to the home screen.

Page 58

You are now taken to the screen as illustrated below.

ch date in the cascade tree can be expanded by touching on the expansion button. From here you can view all the stored experiments for that date. Touch the expansion again to close the cascade.

Select the experiment to be viewed by touching on it to highlight it. Confirm the selection by touching the green tick.

Use the scroll bars to view all settings and title information associated with the experiment.

Each date in the cascade tree can be expanded by touching on the expansion button.

From here you can view all the stored experiments for that date. Touch the expansion again to close the cascade.

Selecttheexperimenttobeviewedbytouchingonittohighlightit.Conrmtheselectionbytouchingthegreen

tick.

Use the scroll bars to view all settings and title information associated with the experiment.

Touch the green tick button to view the raw recorded data.

Page 59

The screen will look like the illustration below.

to view the data

button is used to accept the field entry, by touching this button the field entry is accepted

7.15.2. Viewing data in graphical format

Touch the Graph button to view the data presented in a graphical format.

To return to raw data format, touch the green tick button.

Page 60

7.15.3. Deleting experimental data

data in graphical format: Touch the Graph button to view the data

presented in a graphical format.

. You are now asked to confirm experiment deletion. Touch the green tick to

From the raw data screen touch the Delete Experiment button . Youarenowaskedtoconrm

experiment deletion. Touch the green tick to accept or the red cross and return to the raw data screen.

7.16. Outputting stored data via USB flash drive

Select the view experiment set-up or the Raw Data Screen (see section 7.15). Insert a USB Flash Drive into the

master USB socket found on the front of the Integrity unit (see 7.1). After 10 seconds or less the USB download

button will appear on the screen.

Touch the button and the raw data and a ‘read me’ le containing the experiment parameter settings will

automatically download.

Once the download is complete a download statement will appear conrming its completion. Touch the OK button.ItisnowsafetoremovetheUSBashdrive.

erawdatam

Th aybeviewedbyopeninginMicrosoftExcel.ThereadmefileisaMicrosoftnotepadfile.

Page 61

7.17. Control by contents

module – ATS10001 Optional)

Ensure the Integrity 10 is turned off before commencing the installation of Multitemp

module – ATS10001 Optional)

Ensure the Integrity 10 is turned off before commencing the installation of Multitemp

module – ATS10001 Optional)

Ensure the Integrity 10 is turned off before commencing the installation of Multitemp

Use the Multitemp in conjunction with the Electrothermal operating instruction book supplied

with thi uct.

ATTENTION.

Do not install the Multitemp on a surface which may become wet as the

s temperature. Thermocouples placed in the chemical solutions are

ATS10001 Option accessory) and

Do not install the Multitemp on a surface which may become wet as the

s temperature. Thermocouples placed in the chemical solutions are

ATS10001 Option accessory) and

Do not install the Multitemp on a surface which may become wet as the

ATS10001 Option accessory) and

(Using the optional Electrothermal ATS10001 Multi-Temp module)

Ensure the Integrity 10 is turned off before commencing the installation of Multi-Temp

Use the Multi-Temp in conjunction with the Electrothermal operating instruction book (M7559) supplied

with this product.

ATTENTION Do not install the Multi-Temp on a surface which may become wet as the result of

using chilled water.

The Multi-Temp is used when accurate control of the sample temperature is imperative. The Multi-Temp is used to control the contents temperature. Thermocouples placed in the chemical solutions are connected to the

Multi-Temp which feeds back constant information on the exact sample temperature. The Integrity 10 measures the temperature from the thermocouples via the Multi-Temp then adjusts and monitors the sample temperature according to the temperature settings under both manual and profile control.

7.17.1. Installation of the Multi-Temp

Take the Multi-Temp unit (ATS10001 optional accessory) and connect it to the Integrity 10 unit. Plug the 'D' type connector into the RS232 socket found on the back of the Multi-Temp case.

Connect the other end of the lead to the RS232, 10 pin output of the Integrity 10 unit.

RS232

Using the power supply supplied with the Multi-Temp, plug in the jack plug to the 12 Volts DC in socket on the rear panel of the Multi-Temp. Connect the other end to a suitably rated A.C. mains power source.

Fill the required glassware with solution and place it in the required cells. (If required use in conjunction with other

Electrothermalaccessories,e.g.thereuxunit,ATS20100).

12VDC

Page 62

button to select the cell for operation.

Plug the thermocouples into the respective Multi-Temp front panel position that corresponds to the Integrity 10 cells to be used. Example use thermocouple plug position 1 for Integrity 10 cell position 1, thermocouple position 2 for Integrity 10 cell position 2 and so on.

Place the probe tip ends of the thermocouples into the appropriate cell glassware ensuring the end of the thermocouple is placed well inside the solution.

7.17.2. Operating the Multi-Temp

Turn on the Integrity 10 unit and operate as previously described. Again the home screen will be seen after the warm up.

Note: the thermometer symbol indicating connection.

Press the cell button to select the cell for operation.

IntheManualorProlecontrolselectionscreen,touchthecheckboxtoconrmtheuseof‘controlbycontent’

using

the Multi-Temp.

the check box only appears when a Multi-Temp is connected.

Note:

Select‘ManualControl’or‘ProleSetup’andinputthesettingasdescribedpreviously.

Check Control by Contents

Page 63

Observe: The cell button of a ‘Control by Contents’ cell will also display the ‘Multi-Temp present’

suited for the controlling application.

Thermometer Icon.

NOTE: The temperature value displayed in the cell button and shown on the graph is the measured temperature of the contents, NOT the block temperature.

7.18. External control – optional

7.18.1. PC control:

Connect the host PC to the Integrity 10 unit using the appropriate input socket as suited for the controlling application.

Open the Integrity software application (ATS11005 on the host PC (see M8162 instruction manual for Integrity software).

With all the services connected to the Integrity, turn on and wait for the home screen to appear.

A lock icon will appea able to control the Integrity 10 unit through the host PC and Integrity 10 software.

RS232/485

Ethernet

GSIOC

Protocol

USB

Master

USB

Slave

r on all the cell positions and you will not be able to use the touchscreen. You will only be

Note: You can’t operate cells under external control using the Integrity 10 touch screen.

Upon completion of a run, turn off the Integrity 10 using the Power Supply I/O button as detailed in section 7.5.

Page 64

8. Chemical resistance

Resistance Resistance

It is recommended that any chemical spillages are cleaned up immediately.

Side Panels / Front pod Drip plate FRPS/ABS Polypropylene

Chemical 20°C 60°C 20°C 60°C

Acetaldehyde Major Effect Major Effect No data No data Acetic acid (10%) Excellent

Resistance Acetic acid (glac./anh) Acetic anhydride Major Effect Major Effect No data No data Aceto-acetic ester Major Effect Major Effect No data No data Acetone Major Effect Major Effect Major Effect Major Effect Other Ketones Major Effect Major Effect No data No data Acetonitrile No data No data No data No data Acetylene No data No data No data No data Acetyl salicylic Acid Major Effect Major Effect No data No data Acid fumes Major Effect Major Effect No data No data Acid salt No data No data Excellent

Alchols Major Effect Major Effect No data No data Aliphatic esters Major Effect Major Effect No data No data Alkyl chlorides Major Effect Major Effect No data No data Alum Excellent

Aluminium chloride

Aluminium sulphate

Ammonia anhydrous

Ammonia, aqueous

Ammonium chloride Amyl acetate Major Effect Major Effect No data No data

Aniline Major Effect Major Effect

Antimony tricloride

Aqua ammonia No data No data Aqua regia Major Effect Major Effect No data No data Aromatic solvents Major Effect Major Effect No data No data Ascorbic acid Major Effect Major Effect No data No data

Basic salt

Beer

Benzaldehyde Benzene Major Effect Major Effect No data No data

Benzoic acid

Benzoyl peroxide

Boric acid Brines, saturated Excellent Excellent No data No data

Major Effect Major Effect Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance Major Effect No data No data

Excellent

Resistance Major Effect No data No data

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance No data No data No data

Excellent

Resistance

Excellent

Resistance No data No data No data

Excellent

Resistance

Major Effect Excellent

Resistance

Excellent Resistance Excellent Resistance No data No data Excellent Resistance No data No data

Excellent Resistance No data No data

Excellent Resistance Excellent Resistance No data No data

Excellent Resistance

No data No data

Excellent Resistance Excellent Resistance

Excellent Resistance

Page 65

Resistance Resistance Excellent

Excellent

Side Panels / Front pod Drip plate

FRPS/ABS Polypropylene

Chemical 20°C 60°C 20°C 60°C

Bromine (K) solution Bromine Major Effect Major Effect No data No data Bromine liquid, tech Major Effect Major Effect No data No data Bromine water, saturated aqueous Major Effect Major Effect No data No data

Butyl acetate No data No data

Calcium chloride calcium hydroxide No data No data No data No data

Carbon dioxide

Carbon monoxide Carbon disulphide Major Effect Major Effect Major Effect Major Effect

Carbonic acid carbonic tetrachloride Major Effect Major Effect Major Effect Major Effect Caustic soda & potash Cellulose paint No data No data No data No data Chlorhydric acid (10%) No data No data Chlorhydric acid (37%) No data No data Chlorates of Na, K, Ba

Chlorine, dry

Chlorine, wet Chloroacetic acid Major Effect Major Effect No data No data Chlorobenzene Major Effect Major Effect Major Effect Major Effect Chloroform Major Effect Major Effect No data No data Chlorosulphic acid Major Effect Major Effect No data No data

Chromic acid (80%)

Citric acid

Copper salts (most) Cresylic acids (50%) Major Effect Major Effect No data No data Cyclohexane Major Effect Major Effect No data No data

Detergents, synthetic Esters Major Effect Major Effect No data No data Ether Major Effect Major Effect No data No data

Fatty acids (>C6)

Ferric chloride

Ferrous sulphate Fluorinated refrigerants Major Effect Major Effect No data No data Fluorine, dry Major Effect Major Effect No data No data Fluorine, wet Major Effect Major Effect No data No data Fluorosilicate acid Major Effect Major Effect No data No data

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance Major Effect

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance Major Effect No data No data

Excellent

Resistance

Excellent

Resistance

Excellent

Resistance

Resistance No data No data

Excellent

Resistance Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance

Excellent Resistance No data No data

Excellent Resistance

Excellent Resistance No data No data Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance No data No data

Excellent Resistance No data No data Excellent Resistance No data No data Excellent Resistance No data No data

Excellent

Resistance Excellent Resistance

Excellent

Resistance Excellent Resistance

Excellent

Resistance Excellent Resistance

Excellent

Resistance Excellent Resistance

Excellent

Resistance Excellent Resistance

Excellent

Resistance Major Effect

Excellent

Resistance Major Effect

Excellent

Resistance Major Effect

Excellent

Resistance Excellent Resistance

Excellent

Resistance Excellent Resistance

Page 66

Resistance Resistance

Bromine (K) solution

Excellent Resistance

Excellent

Resistance No data No data Bromine Major Effect Major Effect No data No data Bromine liquid, tech Major Effect Major Effect No data No data Bromine water, saturated aqueous Major Effect Major Effect No data No data

Butyl acetate No data No data

Excellent Resistance Excellent Resistance

Calcium chloride

Excellent Resistance

Excellent

Resistance

Excellent Resistance Excellent Resistance

calcium hydroxide No data No data No data No data

Carbon dioxide

Excellent Resistance

Excellent

Resistance

Excellent Resistance Excellent Resistance

Carbon monoxide

Excellent Resistance

Excellent

Resistance

Excellent Resistance Excellent Resistance

Carbon disulphide Major Effect Major Effect Major Effect Major Effect

Carbonic acid

Excellent Resistance

Excellent

Resistance No data No data carbonic tetrachloride Major Effect Major Effect Major Effect Major Effect Caustic soda & potash

Excellent Resistance

Excellent

Resistance

Excellent

Resistance Excellent Resistance Cellulose paint No data No data No data No data Chlorhydric acid (10%) No data No data

Excellent

Resistance Excellent Resistance Chlorhydric acid (37%) No data No data

Excellent

Resistance Major Effect Chlorates of Na, K, BaExcellent

Resistance

Excellent Resistance No data No data

Chlorine, dry

Excellent Resistance

Excellent

Resistance Major Effect

Chlorine, wet

Excellent Resistance

Excellent

Resistance Major Effect Chloroacetic acid Major Effect Major Effect No data No data Chlorobenzene Major Effect Major Effect Major Effect Major Effect Chloroform Major Effect Major Effect No data No data Chlorosulphic acid Major Effect Major Effect No data No data

Chromic acid (80%)

Excellent Resistance Major Effect

Excellent

Resistance Excellent Resistance

Citric acid

Excellent Resistance

Excellent

Resistance Excellent Resistance

Copper salts (most)

Excellent Resistance

Excellent

Resistance No data No data Cresylic acids (50%) Major Effect Major Effect No data No data Cyclohexane Major Effect Major Effect No data No data

Detergents, synthetic

Excellent

Resistance Major Effect No data No data Esters Major Effect Major Effect No data No data Ether Major Effect Major Effect No data No data

Fatty acids (>C6)

Excellent

Resistance

Excellent Resistance No data No data

Ferric chloride

Excellent

Resistance

Excellent Resistance No data No data

Ferrous sulphate

Excellent

Resistance

Excellent

Resistance No data No data Fluorinated refrigerants Major Effect Major Effect No data No data Fluorine, dry Major Effect Major Effect No data No data Fluorine, wet Major Effect Major Effect No data No data Fluorosilicate acid Major Effect Major Effect No data No data Formaldehyde (40%) Excellent Excellent No data No data

Side Panels / Front pod Drip plate

Resistance Resistance

FRPS/ABS Polypropylene

Chemical 20°C 60°C 20°C 60°C

Excellent

Formic acid

Fruit juice

Gelatin

Glycerin

Glycol, ethylene Glycols Major Effect Major Effect No data No data Glycolic acid Major Effect Major Effect No data No data Hexamethylene diamine No data No data No data No data Hexamine Major Effect Major Effect No data No data Hydrazine No data No data No data No data Hydrobromic acid (50%) Hydrochloric acid (10%) Hydrochloric acid (conc)

Hydrocyanic acid Hydrofluoric acid (40%) Hydrofluoric acid (75%) Major Effect Major Effect No data No data Hydrogen peroxide (30-90%)

Hydrogen sulphide No data No data Hypochlorite’s (Ma 12-14%) Iso-butyl-acetate No data No data No data No data

Lactic acid (90%)

Lead acetate Lead perchlorate No data No data No data No data

Lime (CaO)

Maleic acid Manganate, potassium (K)

Meat Juice

Mercuric chloride

Mercury Methanol Major Effect Major Effect No data No data Methylene chloride Major Effect Major Effect Major Effect Major Effect

Milk products

Moist air

Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance

Excellent Resistance Major Effect Excellent Resistance Excellent Resistance Major Effect No data No data Excellent Resistance Excellent Resistance Major Effect No data No data

Excellent Resistance Major Effect No data No data

Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Major Effect No data No data Excellent Resistance

Excellent Resistance Major Effect No data No data Excellent Resistance

Excellent Resistance No data No data Excellent Resistance No data No data Excellent Resistance No data No data Excellent Resistance No data No data Excellent Resistance No data No data

Excellent Resistance No data No data

Excellent Resistance

Excellent Resistance No data No data Excellent Resistance No data No data

Excellent Resistance No data No data Excellent Resistance Excellent Resistance No data No data Excellent Resistance No data No data

Excellent Resistance No data No data

Excellent Resistance Major Effect

Excellent Resistance Excellent Resistance

Page 67

Picric acid No data No data No data No data

Side Panels / Front pod Drip plate

Resistance Resistance

Formic acid

Excellent Resistance

Excellent

Resistance No data No data

Fruit juice

Excellent Resistance

Excellent

Resistance No data No data

Gelatin

Excellent Resistance

Excellent

Resistance No data No data

Glycerin

Excellent Resistance

Excellent

Resistance No data No data

Glycol, ethylene

Excellent Resistance

Excellent

Resistance No data No data Glycols Major Effect Major Effect No data No data Glycolic acid Major Effect Major Effect No data No data Hexamethylene diamine No data No data No data No data Hexamine Major Effect Major Effect No data No data Hydrazine No data No data No data No data Hydrobromic acid (50%)

Excellent Resistance Major Effect

Excellent

Resistance Major Effect Hydrochloric acid (10%)

Excellent Resistance

Excellent

Resistance No data No data Hydrochloric acid (conc)

Excellent Resistance Major Effect No data No data

Hydrocyanic acid

Excellent Resistance

Excellent

Resistance

Excellent

Resistance Excellent Resistance Hydrofluoric acid (40%)

Excellent

Resistance Major Effect No data No data Hydrofluoric acid (75%) Major Effect Major Effect No data No data Hydrogen peroxide (30-90%)

Excellent

Resistance Major Effect No data No data

Hydrogen sulphide No data No data

Excellent

Resistance Excellent Resistance Hypochlorite’s (Ma 12-14%)

Excellent Resistance Major Effect No data No data

Iso-butyl-acetate No data No data No data No data

Lactic acid (90%)

Excellent Resistance

Excellent Resistance No data No data

Lead acetate

Excellent Resistance

Excellent Resistance No data No data

Lead perchlorate No data No data No data No data

Lime (CaO)

Excellent Resistance

Excellent Resistance No data No data

Maleic acid

Excellent Resistance

Excellent

Resistance Excellent Resistance Manganate, potassium (K)

Excellent Resistance

Excellent Resistance No data No data

Meat Juice

Excellent Resistance

Excellent Resistance No data No data

Mercuric chloride

Excellent Resistance Major Effect No data No data

Mercury

Excellent Resistance

Excellent

Resistance No data No data Methanol Major Effect Major Effect No data No data Methylene chloride Major Effect Major Effect Major Effect Major Effect

Milk products

Excellent Resistance Major Effect No data No data

Moist air

Excellent Resistance

Excellent

Resistance No data No data

FRPS/ABS Polypropylene

Chemical 20°C 60°C 20°C 60°C

Excellent

Molasses

Monoethanolamine Major Effect Major Effect No data No data

Naphtha Naphthalene Major Effect Major Effect No data No data

Neutral salt

Nickel salts Nitrates of Na, K and NH3

Nitric acid (<25%) Major Effect Major Effect Nitric acid (<50%) Major Effect Major Effect Major Effect Major Effect Nitric acid (<90%) Major Effect Major Effect Major Effect Major Effect Nitric acid (fuming) Major Effect Major Effect Major Effect Major Effect

Nitrite (Na) Nitrobenzene Major Effect Major Effect Major Effect Major Effect Oils, diesel No data No data No data No data

Oils, essential Oils, lubricating + aromatic additives Major Effect Major Effect No data No data

Oils, mineral Oils, vegetable and animal

Oleic acid No data No data

Oxalic acid Ozone Major Effect Major Effect No data No data

Paraffin wax

Perchloric acid No data No data Petroleum sprit Major Effect Major Effect Major Effect Major Effect

Phenol Major Effect Major Effect Phosphoric acid (20%) Phosphoric acid (50%) Phosphoric acid (95%) Phosphorous chloride No data No data No data No data Phosphorous pentoxide No data No data No data No data

Phthalic acid No data No data Potassium bicarbonate No data No data Potassium permanganate No data No data

Potassium hydroxide No data No data

Resistance Major Effect No data No data

Excellent Resistance Major Effect No data No data

Excellent Resistance Excellent Resistance Excellent Resistance

Excellent Resistance Major Effect No data No data

Excellent Resistance

Excellent Resistance Excellent Resistance

Excellent Resistance Major Effect

Excellent Resistance

Excellent Resistance Major Effect Excellent Resistance Major Effect Excellent Resistance Major Effect

Excellent Resistance Excellent Resistance No data No data Excellent Resistance No data No data

Excellent Resistance No data No data

Excellent Resistance No data No data Excellent Resistance No data No data

Excellent Resistance No data No data

Excellent Resistance Excellent Resistance

Excellent Resistance Major Effect

Excellent Resistance Major Effect Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance

Page 68

Side Panels / Front pod Drip plate

Monoethanolamine Major Effect Major Effect No data No data

Naphtha

Excellent Resistance Major Effect No data No data

Naphthalene Major Effect Major Effect No data No data

Neutral salt

Excellent Resistance

Excellent

Resistance

Excellent Resistance Excellent Resistance

Nickel salts

Excellent Resistance

Excellent

Resistance No data No data Nitrates of Na, K and NH3

Excellent Resistance

Excellent

Resistance No data No data

Nitric acid (<25%) Major Effect Major Effect

Excellent

Resistance Major Effect Nitric acid (<50%) Major Effect Major Effect Major Effect Major Effect Nitric acid (<90%) Major Effect Major Effect Major Effect Major Effect Nitric acid (fuming) Major Effect Major Effect Major Effect Major Effect

Nitrite (Na)

Excellent

Resistance Major Effect No data No data Nitrobenzene Major Effect Major Effect Major Effect Major Effect Oils, diesel No data No data No data No data

Oils, essential

Excellent

Resistance

Excellent

Resistance No data No data Oils, lubricating + aromatic additives Major Effect Major Effect No data No data

Oils, mineral

Excellent Resistance

Excellent

Resistance No data No data Oils, vegetable and animal

Excellent Resistance

Excellent

Resistance No data No data

Oleic acid No data No data

Excellent Resistance Major Effect

Oxalic acid

Excellent Resistance Major Effect

Excellent Resistance Excellent Resistance

Ozone Major Effect Major Effect No data No data

Paraffin wax

Excellent Resistance

Excellent

Resistance No data No data

Perchloric acid No data No data

Excellent Resistance Excellent Resistance

Petroleum sprit Major Effect Major Effect Major Effect Major Effect

Phenol Major Effect Major Effect

Excellent

Resistance Excellent Resistance Phosphoric acid (20%)

Excellent Resistance Major Effect

Excellent

Resistance Excellent Resistance Phosphoric acid (50%)

Excellent Resistance Major Effect

Excellent

Resistance Excellent Resistance Phosphoric acid (95%)

Excellent Resistance Major Effect

Excellent

Resistance Excellent Resistance Phosphorous chloride No data No data No data No data Phosphorous pentoxide No data No data No data No data

Phthalic acid No data No data

Excellent

Resistance Excellent Resistance Potassium bicarbonate No data No data

Excellent

Resistance Excellent Resistance Potassium permanganate No data No data

Excellent

Resistance Excellent Resistance

Potassium hydroxide No data No data

Excellent

Resistance Excellent Resistance Picric acid No data No data No data No data Pyridine Major Effect Major Effect No data No data

FRPS/ABS Polypropylene

Chemical 20°C 60°C 20°C 60°C

Excellent

salicylic aldehyder

Sea water

Silica acid Silicon fluids No data No data No data No data

Silver nitrate

Sodium carbonate

Sodium cyanide

Sodium peroxide

Sodium silicate

Sodium sulphide Stannic chloride Major Effect Major Effect No data No data

Starch

Sugar, syrups & jams Sulphamic acid No data No data No data No data Sulphates (Na, K, Mg, Ca)

Sulphites Sulphonic acids No data No data No data No data

Sulphur

Sulphur dioxide, dry

Sulphur dioxide, wet Sulphur dioxide, (96%) Major Effect Major Effect No data No data

Sulpher trioxide Sulphuric acid (<50%) Major Effect Major Effect

Sulphuric acid (70%) Major Effect Major Effect Sulphuric acid (95%) Major Effect Major Effect Major Effect Major Effect Sulphuric acid, fuming Major Effect Major Effect No data No data Sulphur chlorides No data No data No data No data

Tallow

Tannic acid (10%) No data No data

Tartaric acid Trichloroethylene Major Effect Major Effect Major Effect Major Effect

Urea (30%)

Vinegar

Resistance No data No data No data

Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance No data No data No data Excellent Resistance Major Effect No data No data Excellent Resistance Major Effect No data No data

Excellent Resistance Major Effect No data No data Excellent Resistance

Excellent Resistance Excellent Resistance Major Effect No data No data

Excellent Resistance No data No data No data Excellent Resistance Major Effect Excellent Resistance Major Effect

Excellent Resistance

Excellent Resistance Excellent Resistance

Excellent Resistance No data No data Excellent Resistance No data No data

Excellent Resistance No data No data Excellent Resistance No data No data Excellent Resistance

Excellent Resistance No data No data

Excellent Resistance

Excellent Resistance Excellent Resistance

Excellent Resistance Major Effect Excellent Resistance Major Effect

Excellent Resistance Excellent Resistance Excellent Resistance Major Effect

Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance

Page 69

Sea water

Excellent Resistance

Excellent Resistance No data No data

Silica acid

Excellent Resistance

Excellent Resistance No data No data

Silicon fluids No data No data No data No data

Silver nitrate

Excellent Resistance

Excellent Resistance No data No data

Sodium carbonate

Excellent Resistance

Excellent Resistance No data No data

Sodium cyanide

Excellent Resistance

Excellent

Resistance Excellent Resistance

Sodium peroxide

Excellent Resistance No data No data No data

Sodium silicate

Excellent Resistance Major Effect No data No data

Sodium sulphide

Excellent Resistance Major Effect No data No data

Stannic chloride Major Effect Major Effect No data No data

Starch

Excellent Resistance Major Effect No data No data

Sugar, syrups & jams

Excellent Resistance

Excellent

Resistance No data No data Sulphamic acid No data No data No data No data Sulphates (Na, K, Mg, Ca)

Excellent Resistance

Excellent

Resistance No data No data

Sulphites

Excellent Resistance Major Effect No data No data

Sulphonic acids No data No data No data No data

Sulphur

Excellent Resistance No data No data No data

Sulphur dioxide, dry

Excellent Resistance Major Effect

Sulphur dioxide, wet

Excellent Resistance Major Effect

Excellent

Resistance Major Effect Sulphur dioxide, (96%) Major Effect Major Effect No data No data

Sulpher trioxide

Excellent Resistance

Excellent

Resistance No data No data Sulphuric acid (<50%) Major Effect Major Effect

Excellent Resistance Excellent Resistance

Sulphuric acid (70%) Major Effect Major Effect

Excellent

Resistance Major Effect Sulphuric acid (95%) Major Effect Major Effect Major Effect Major Effect Sulphuric acid, fuming Major Effect Major Effect No data No data Sulphur chlorides No data No data No data No data

Tallow

Excellent Resistance

Excellent Resistance No data No data

Tannic acid (10%) No data No data

Excellent

Resistance Excellent Resistance

Tartaric acid

Excellent Resistance

Excellent

Resistance Excellent Resistance Trichloroethylene Major Effect Major Effect Major Effect Major Effect

Urea (30%)

Excellent Resistance

Excellent

Resistance Excellent Resistance

Excellent

Side Panels / Front pod Drip plate

FRPS/ABS Polypropylene

Chemical 20°C 60°C 20°C 60°C

Vinegar

Water, distilled

Water, soft

Water, Hard Wetting agents (<5%)

Yeast Zinc chloride Major Effect Major Effect No data No data

Resistance Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance Excellent Resistance Major Effect No data No data

Resistance Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance

Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance

Excellent Resistance Excellent Resistance Excellent Resistance Excellent Resistance

Page 70

9. Reaction block dimensions

9. DIMENSIONS (UNIT)

Weight 9.5kg

Not to Scale

Location dimensions (For use in robotic stations)

Not to Scale

Page 71

10. P

Mains in

put supply voltage

230/115/100V ~ AC ± 10% at 50/60Hz

Power Consumption 1500 max

Watts (2x750W)

Mains cord and moulded IEC plug and lead s

et cable (UK) 16A BS1362

3 core earthed / ground. 2 meters long. Moulded IEC plug and Lead set – supply cord H05 V V- F – Replace only with equivalent cable.

Mains cord and moulded IEC plug and lead s

et cable Schuko (Europe)

3 core earthed / ground. 2 meters long. Moulded IEC plug and Lead set – supply cord H05 V V- F – Replace only with equivalent cable.

Mains cord and moulded IEC plug and lead s

et cable (USA)

3 core earthed / ground. 2 meters long. Moulded IEC plug and Lead set – supply cord SJT V W 1

- 105° – Replace only with equivalent cable.

Lead set plug and fuse (UK – Only) 13A BS1362

Dimensions (PSU

)

owersupplyunit(PSU) specifications

Mains input supply voltage

Power Consumption

Mains cord and moulded IEC plug 3 core earthed / ground. 2 meters long. Moulded IEC

andleadsetcable(UK)16ABS1363 plugandLeadset–supplycordH05VV-F

Mains cord and moulded IEC plug 3 core earthed / ground. 2 meters long. Moulded IEC and lead set cable Schuko (Europe) plug and Lead set – supply cord H05 V V- F

Mains cord and moulded IEC plug 3 core earthed / ground. 2 meters long. Moulded IEC and lead set cable (USA) plug and Lead set – supply cord SJT V W 1 - 105°

Leadsetplugandfuse(UK–Only) 13ABS1363

Dimensions (PSU)

230/115/100V ~ AC ± 10% at 50/60Hz Max 1500 watts

– Replace only with equivalent cable.

Weight 10.5kg

The Ingress Protection rating for the Integrity 10 Unit and power supply is IPX0.

Not to Scale

Page 72

11. Maintenance, service and repair

module – ATS10001 Optional)

Ensure the Integrity 10 is turned off before commencing the installation of Multitemp

module – ATS10001 Optional)

Ensure the Integrity 10 is turned off before commencing the installation of Multitemp

Use the Multitemp in conjunction with the Electrothermal operating instruction book supplied

with thi

s product.

ATTENTION.

Do not install the Multitemp on a surface which may become wet as the

Ensure the Integrity 10 is turned off before commencing the installation of Multitemp

Use the Multitemp in conjunction with the Electrothermal operating instruction book supplied

s product.

ATTENTION.

Do not install the Multitemp on a surface which may become wet as the

module – ATS10001 Optional)

Ensure the Integrity 10 is turned off before commencing the installation of Multitemp

Use the Multitemp in conjunction with the Electrothermal operating instruction book supplied

with thi

s product.

ATTENTION.

Do not install the Multitemp on a surface which may become wet as the

11.1. Maintenance

Unplug the unit from the mains voltage supply and allow it to cool before undertaking any maintenance tasks.

Maintenance should only be carried out by an approved Cole-Parmer representative. Failure to do so

may result in

With proper care in operation this equipment has been designed to give many years of reliable service. Contamination or general misuse will reduce the effective life of this product and may cause a hazard.

Maintenance for the Integrity Unit and Power Supply should include:

• Periodic electrical safety testing (an annual test is recommended as the minimum for the PSU).

AC dielectric withstand (Flash / Hi Pot) must not be undertaken on this equipment as damage may result. Such

testing will invalidate warranty.

DCdielectricwithstand(ash/HiPot)maybeappliedtothePSU only (i.e. The Integrity 10 unit must not be

connected when the PSU is being tested. The Integrity 10 unit operates at low voltage (15V DC) and must not be subjected to dielectric withstand (Flash / Hi Pot) testing.

damage to the product and in extreme cases be a danger to the end user

DCdielectricwithstand(ash/HiPot)testingshallonlybeundertakenbycompetenttrainedpersonnelusing

suitable test equipment / environment. DC test voltage should be no more than 1.414 times normal AC test value for a class I (grounded) equipment.

The test equipment / process should incorporate a discharge procedure to remove any stored DC charge that may remain on the PSU.

• The Integrity PSU: Routine cleaning of the equipment should be undertaken using a water moistened, clean cloth.

• The Integrity Unit: Side panels and drip tray may be cleaned using mild warm soapy water and must be wiped dry before use. Do not use anything abrasive on the Touch LCD screen. Before cleaning the touch LCD screen, ensure the unit is turned off and SD card removed. Clean the screen using PC screen wipes or a water dampened, clean non-abrasive cloth.

DO NOT USE SOLVENTS OR ABRASIVE CHEMICALS FOR CLEANING ANY PART OF THIS EQUIPMENT.

ATTENTION. THERE ARE NO SERVICEABLE PARTS WITHIN THE INTEGRITY 10 POWER SUPPLY – IF IN DOUBT CONSULT MANUFACTURE OR SUPPLIER.

Page 73

11.2. Spillage procedure

In case of solution spillage, turn off the Integrity 10 unit via the Power Supply On / Off switch. For light spillage wipe off the solution using a water dampened cloth and dry thoroughly before further use.

For spillage involving liquid solution spilt into a reaction well, turn off the Integrity 10 unit via the Power Su

pply On / Off switch. Turn off the chilled water supply and disconnect the supply hoses. Uncouple and remove any peripheral cables linked to a PC or accessories. Remove mains power input and mains connection cable.

Take the unit and tip any spillage out of the reaction cells

. (**) Clean the unit using a water dampened

cloth and dry thoroughly. Ensure the unit is dry before further use. The Responsible Body shall

check the electrical safety of the unit. Only if all safety requirements are met can the unit be used again. The above procedure is intended as a guide. Should spillage occur with a toxic or hazardous fluid then special precautions may be necessary.

(**) Observe special precautions for handling contaminated substances see Section 11.3

If the equipment has been exposed to toxic, radiological or biological contamination,

. (**) Clean the unit using a water dampened

For spillage involving liquid solution spilt into a reaction well, turn off the Integrity 10 unit via the Power Supply On / Off switch. Turn off the chilled water supply and disconnect the supply hoses. Uncouple and remove any peripheral cables linked to a ble. PC or accessories. Remove mains power input and mains connection ca

Take the unit and tip any spillage

(**) out of the reaction cells taking care to support the unit on the block.

Do not place undue pressure on the front pod as this may damage the unit and invalidate any warranty.

Clean the unit using a water dampened cloth and dry thoroughly. Ensure the unit is dry before further use. The Responsible Body shall check the electrical safety of the unit. If all safety requirements are met the unit can be used again. The above procedure is intended as a guide. Should spillage occur

with a toxic or hazardous fluid then special precautions may be necessary.

(**) Observe special precautions for handling contaminated substances see Section 11.3 .

11.3. Decontamination

If the equipment has been exposed to toxic, radiological or biological contamination, the Responsible Body is responsible for carrying out appropriate decontamination. If hazardous material has been spilt on or inside the equipment, decontamination should only be undertaken under the control of the Responsible

Body with due recognitio

n of possible hazards. Before using any cleaning or decontamination method, the

Responsible Body should check with the manufacturer that the proposed method will not damage the equipment.

DECONTAMINATION CERTIFICATE

NOTE:

In the event of any part of this unit becoming damaged, the damaged item(s) should be returned to

the manufacturer for repair accompanied by a decontamination certificate. Copies of the Certificate are

availablefromDistributor/Manufacturer.Atthe endoflifethisproductmustbe accompaniedwitha

ontaminationCertificate.

Dec

11.4. Servicing

Please contact your local Cole-Parmer Technical Sales Specialist or contact:

E-mail:

[email protected]

Phone: +44 (0)1785 810475

11.5. Error and warning messages

Error and warning messages will be displ

ayed if the equipment status moves outside of the normal operating

limits. The message will indicate recovery instructions or service support actions as appropriate.

Error and warning messages have been included to help the user determine the state of malfunction. In some

instancesthemessagewilldisplayamethodforfaultconditionrectication.

When the warning symbol appears in a single cell button and the cell button turns red, touch the cell button to display the fault condition.

Page 74

11.5.1. Heat exchanger over temperature error

This warning shows a fault condition with the cell number 2. Please contact the manufacturer or your distributor for service support.

Ifallthecellsareaffectedanotherwarningmessagewillbedisplayed.Apossiblecauseforthisisablockedow

chamber in the cell heat exchanger. Check water coolant supply for debris contamination.

To return to the home screen and view the performance of other operational cells touch the back button.

Fromthisscreenitcanbeseenthatallcellsheatexchangersareaffected.Thisiscausedbythecoolantwaterow

rate being too low for the cells to operate or the coolant water temperature being too high (above 35°C).

IftheproblemiscausedbylackofwaterowratetheIntegrity10willshutdowntoprotectinternalpartsfrom

damage. Once chilled water has been restored the unit will automatically recommence operation and the warning message screen will disappear.

If the problem is caused by the water temperature being too high the Integrity 10 will shut itself down as previously mentioned in order to protect internal parts from damage. Again when the correct temperature chilled water is restored the unit will recommence operation and the message screen disappears.

Possible reasons for chilled water becoming too hot include but are not exclusive to:

• Failed chiller unit.

• More than one appliance connected to the chiller system returning water at temperature greater than the chiller can cope with.

•

Integrity 10 connected in series with another piece of equipment returning chilled water at a temperature above 35°C

•

Low coolant flow rate which is insufficient to remove the heat from the heat exchangers (less than 5/L per minute).

See Appendix 'A'. Integrity cooling guide for more information

Page 75

11.5.2. Motor stall error

°°°°

without a chilled water set at 5

°°°°

without a chilled water set at 5

°°°°

without a chilled water set at 5

°°°°

without a chilled water set at 5

°°°°

This illustration screen shot shows a stir motor fault with cell position number 2. The cell position may still be used in heating / cooling mode but the cell will not stir. The cell will have to be replaced.

Contact the manufacturer as detailed in section 12 customer support.

To return to the home screen and view the performance of other operational cells, touch the back button.

11.5.3. Cell failure error

This illustration screenshot shows a cell failure with cell position number 2. The cell will have to be replaced. Contact the manufacturer as d

To return to the home screen and view the performance of other operational cells touch the back button.

etailed in section 12 customer support.

Page 76

11.5.4. Over voltage error

This indicates a fault with the Power Supply Unit. Contact the manufacturer as detailed in section 12 customer support. Turn off the Integrity 10 and disconnect from the mains electricity supply.

11.5.5. Under Voltage error

As above this indicates a fault with the Power Supply Unit. Contact the manufacturer as detailed in section 12 customer support. Turn off the Integrity 10 and disconnect from the mains electricity supply.

Page 77

11.5.6. Probe error

If an external probe is being used and it is either left out of the sample solution or drops out of the sample solution during a run, the following screen will appear if the probe is faulty.

When the Integrity unit senses a block temperature that is 20°C above the solution temperature this error condition is created.

Oncethefaulthasbeenrectiedtouchthecellbuttonandselectmethodofoperation. e.g.,manualorprolecontrolandrestartthecell.

To return to the home screen and view the performance of other operational cells touch the back button.

Page 78

12. Customer support

If you require further technical or application assistance please contact:

E-mail: [email protected] Phone: +44 (0)1785 810433

For servicing information please contact:

Service Department Cole-Parmer Ltd Beacon Road Stone Staffordshire ST15 0SA

E-mail: [email protected] Phone: +44 (0)1785 810475

We are continually striving to improve our products and software. If you have any comments or suggestions on how we can do things better please send them to us at:

E-mail: [email protected]

Page 79

13. Spares and accessories

ACCESSORIES

Order Number Quantity

ATS20100 1

ATS20002

ATS10075

ATS20003

ATS20004

ATS10001 1

ATS10027

ATS10027/10 1

ATS10232E

ATS10360/1 1

ATS10230 1

ATS10394/1 1

ATS11005 1

AZS4206

Description

Reflux

/ inertingblockforintegrity10

Inerting caps, SVL 22 thread for use with ATS20100, pack of 10

Glass tubes 24/150mm, SVL22 thread, pack of 10

Inertingcaps,KimblethreadforusewithATS20100, pack of 10

Glasstubes24/150mm,Kimblethread, pack of 10

Multi-Temp 12 plug in box

Temperature probes, pack of 6

Temperature probes, pack of 10

Multi-IR 10 plug in unit

Non-intrusive IR sensor

Small intrusive IR probe in stainless steel PID-NIR5-BNSD

Hellma intrusive IR probe with high chemical resistance

Integrity PC software

Stirrer bars 10/6mm oval shaped for round bottomed tubes, pack of 10

1

AZS4235

ATS10055

ATS10056 1

ATS10101

ATS10209

M7438

Stirrerbars12/4.5mmforflatbottomedtubes, pack of 10

Small volume test tubes 24-16mm taper (3ml), pack of 10

Reducing sleeves for ATS10055, pack of 10

Reducing sleeves 24 – 11mm, pack of 10

Micro-volume test tubes 24-11mm taper (1ml), pack of 10

Spare coolant supply hoses

1

Please contact your local sales specialist or email [email protected] to enquire about available spares.

Please visit www.electrothermal.com for a full list of available accessories.

Page 80

14. Notes

Page 81

15. EU Declaration of conformity

This product meets the applicable harmonized standards for radio frequency interference and may be expected not to

interfere with, or be affected by, other equipment with

similar qualiﬁcations. We cannot be sure that other

equipment used in its vicinity will meet these standards

and so we cannot guarantee that interference will not

occur in practice. Where there is a possibility that injury,

damage or loss might occur if equipment malfunctions due to radio frequency interference, or for general

advice before use, contact the manufacturer.

EU Declaration of Conformity

Product

Manufacturer

This declaration of conformity is issued under the sole responsibility of the manufacturer

Object of Declaration

Laboratory Equipment

Cole-Parmer Ltd Beacon Road Stone, Staffordshire ST15 0SA United Kingdom

Integrity 10 Reaction Station

(reference the attached list of catalogue numbers)

File Number

Authorised Representative

P225

Cole-Parmer Beacon Road Stone, Staffordshire ST15 0SA United Kingdom

The object of the declaration described above is in conformity with the relevant Union Harmonisation Legislation:

Low Voltage Directive 2006/95/EC

2014/35/EU

EMC Directive

RoHS Directive

References to the relevant harmonised standards used or references to the other technical specications in relation

to which conformity is declared:

Safety requirements for electrical equipment for

IEC/EN 61010-1:2010

IEC/EN 61010-2-010:2014

IEC/EN 61010-2-051:2003

IEC/EN 61326-1:2006

Signed for and on behalf of the above manufacturer

Additional Information

Place of Issue

Date of Issue

Authorised Representative

Title

Signature

measurement, control and laboratory use. Part 1: General requirements.

Particular requirements for laboratory equipment for the heating of materials.

Particular requirements for laboratory equipment for mixing and stirring.

Electrical equipment for measurement, control and laboratory use. EMC requirements. Part 1: General requirements (Class A).

Year of CE Marking: 2010

Stone, Staffordshire, UK

18 May 2011. Revised 29 September 2017

P Day

General Manager

2004/108/EC

2011/65/EC

(until 19 April 2016) (from 20 April 2016)

Declaration of Conformity is also available to view online at www.electrothermal.com

Page 82

Cooling Guide

THE INTEGRITY 10 COMPANION GUIDE

The Integrity 10 reacon staon must be used with an appropriately rated cooling system at all mes, even when the equipment is only used for heang applicaons.

Failure to use an appropriately rated cooling system will negavely impact the performance of the Integrity 10. In some circumstances this could reduce the life of the product, increase service frequency or cause permanent damage.

Damage caused to the Integrity 10 through the use of inappropriately rated cooling systems is

ot covered under warranty.

Damage caused to the Integrity 10 through the use of unﬁltered or contaminated coolant is not covered under warranty.

Integrity 10 Cooling Requirements

The Integrity 10 is capable of independently cooling each of its 10 cells down to a minimum temperature of -30°C, but this is only achievable when the product is coupled to a cooling system that can remove heat at a rate g

It is important to understand the importance of this relaonship and to select an appropriate cooling system so that you can achieve the performance needed for your applicaon and get the results you expect.

reater or equal to that collected by the Integrity.

Understanding the systems relaonship

Each of the Integrity’s cells contain a cooling device (the TEC). While operang in cooling mode, these devices remove heat from the reacon vessel and pass it onto the cooling system via a heat exchanger. The temp by the chiller and rejected into the air.

erature of the coolant increases which is the

It is important to note that even when a cell is heang and not using the cooling feature, a cooling system is sll required to ensure damage is not sustained to the sensive cells during operaon.

n pumped out of the Integrity, where it’s cooled

 When appropriately matched, the cooling system and Integrity work in harmony and are able

to achieve the performance expected.

 If inappropriately matched, the cooli

upon it. In this situaon, the cooling performance of the Integrity is negavely impacted reducing the rate of cooling and/or liming the minimum temperature the cell is able to achieve.

ng system is unable to kee

p up with the demands placed

Page 83

THE INTEGRITY 10 COMPANION GUIDE

In extreme circumstances i.e. when a cooling system is severely under-rated, the chillers reservoir of coolant will progressively increase in temperature unl the cooling system displays an error message and potenally stops operaon.

Managing the load on the cooling system

Knowing how to manage the load placed upon your cooling system will help you achieve the performance you require and will also help you save energy.

There are three main factors which contribut

o The number of cells being cooled at any me. o The cooling rate selected. o The minimum temperature required.

Example 1 Cooling 10 cells in parallel places a higher load on the cooling system than only cooling 2 cells in parallel.

Example 2 Cooling at a rate of 5°C/minute places a higher load on the cooling system than cooling at 1°C/minute.

Example 3 Cooling down to a temperature of -30°C places a higher load on the cooling system than cooling down to a temperature of -10°C.

In a worst case scenario, an expe uncontrolled ramping proﬁle. Uncontrolled ramping is when a user hasn’t speciﬁed a ramp-rate in the Integrity sengs. In this situaon, both the Integrity and cooler will need to work their hardest to reach the desired temperature.

The Integrity is easily capable of cooling all 10 cells down to a temperature of -30°C, provided it is coupled to an appropriately rated cooling system. The me taken to reach a temperature of -30°C using uncontro

mping is subjecve and dependant on:

lled ra

rimen

e to the load on the cooling system:

t would demand all 10 cells to cool to -30°C in parallel, using an

 The performance capabilies of the cooler.  The ambient temperature in the laboratory.  The contents of the vessel and its heat capacity (i.e. the amount of energy which must be

removed from the contents in order to yield a measurable temperature change).

 The nature of the experiment being performed (e.g. exothermic reacons).

Page 84

THE INTEGRITY 10 COMPANION GUIDE

Reducing the load on the cooling system

If you believe your system is struggling to meet the performance demands placed upon it, consider the following list of suggesons to help reduce the load on the system:

 Increase the temperature of the experiment.  Reduce the number of cells which are cooling in parallel.  Ensure your cooling system is regularly serviced and is maintained in line with the

manufacturer’s recommendaons.

 Ensure the coolers condenser is clean and has unrestric  Ensure coolant is clean with no contaminates which can block the Integrity heat exchangers.  Reduce the cooling ramp-rate of the experiment.  Reduce the ambient temperature of the laboratory using air condioning.

A good indicaon that your cooling system is under-rated for your experiment is when you observe a temperature plateau when working below ambient temperatures.

For example: You set up the Integrity to cool all 10 cells down to a temperature of -20°C however

you noced that the cells have demands placed upon it because the rate at which heat is gathered by the Integrity now matches the capability of the cooler. (You may also observe an undulaon in the minimum temperature as the coolers compressor cycles on and oﬀ in an aempt to maintain the coolants temperature.)

only reached -15°C. The cooler is struggling to meet the

ted air-ﬂow.

Selecng a cooling system

Now that we’ve explained the relaonship between the Integrity 10 and the cooling system, we shall discuss the important speciﬁcaons of

There are four primary consideraons when selecng a cooling system:

1 Working temperature range

The ﬁrst parameter to consider when selecng your recirculang cooler is the working temperature range. In order for the Integrity to reach a minimum temperature of -30°C, the cooler will need to be capable of working between 5°C and -5°C.

The working temperature you use will be subjecve to your experiment and is typically determined empirically. We recommend you start at you achieve the performance required.

Tip: Don’t set your chiller cooler than needed - it is always best pracce to use the warmest working temperature possible which achieves your performance requirements to avoid unnecessary condensaon and to avoid wasng energy.

2 Cooling Capacity

The cooling capacity is a characterisc which determines how quickly the cooler can remove the heat collected by the Integrity. As menoned previously, th that of the Integrity, so that the performance of the whole system can be comfortably maintained.

the cooling system.

5°C and progressively reduce the coolers temperature unl

e cooler needs a capacity greater or equal than

It is recommended that you select a product with a cooling capacity of at least 1.1KW (1100W) between the working temperature of range of 5 to -5°C. With this cooling capacity, you will be able to use the Integrity 10 to its maximum potenal.

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THE INTEGRITY 10 COMPANION GUIDE

Most manufacturers of recirculang coolers typically specify the cooling capacity of their equipment using a table, because there is a relaonship between working temperature and cooling capacity of such systems.

For example, see the ﬁcous table below:

Working temperature (°C) 20 10 0 -10

Cooling Capacity (kW) 2.5 1.8 1 0.4

As you can see from this table, the cooling capacity decreases signiﬁcantly as the working temperature is reduced.

It should be noted that manufacturers of recirculang coolers would adverse this system as a

nominal 2.5kW system. This is in fact the cooling capacity at 20°C only. You should always determine

the cooling capacity over the recommended working temperature range of the Integrity.

It’s possible to run the Integrity using a lower rated cooling capacity, although this isn’t recommended. Please see the next sec

on on ‘lower rated systems’ for more informaon about this.

3 Flow Rate

The cooler should be capable of providing coolant at a rate of at least 5 Litres per minute, directly into the Integrity.

If you are sharing your cooling system with other equipment or accessories, you must ensure that the

supply of 5 Litres per minute is maintained for the duraon of your work.

Do not compromise the ﬂow rate of the coolant into the Integrity by using incorrectly speciﬁed

ancillary items such as couplers, reducers or te

eces, for example.

e-pi

4 Pressure

In order to obtain the ﬂow rate discussed above, the coolers pump must be capable of providing a pressure of at least 2 bar.

If you are sharing your cooling system with other equipment or accessories, you must ensure that the

pressure of at least 2 bar is maintained for the duraon of your work.

Lower rated systems

It is not recommended that you use the Integrity with a lower rated system than explained above. If you do, you will not necessarily be ab nor will you be able to exploit the full potenal of the Integrity 10 and cool all cells down to a minimum temperature of -30°C

le to reach the performance characteriscs required by your work

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THE INTEGRITY 10 COMPANION GUIDE

Filtering requirements

When coupling your Integrity 10 to a cooling system it is required that you also ﬁt a 50 micron inline ﬁlter (if one is not present in the cooler) to prevent the ingress of contaminates into the cell heat exchangers. The ﬁlter should be installed on the outlet of the chiller.

Paral restricon or blockage of heat exchangers caused by contaminates will impact the system

performance and potenally void your warranty.

Summary of cooling system speciﬁcaon

Working temperature range 5 to -5°C Cooling Capacity 1.1kW (1100W) between 5°C to -5°C Flow Rate ≥ 5 Litres per minutes Pressure ≥ 2 bar Inline Filter 50 micron

Table 1 - Recommended speciﬁcaon of Integrity 10 cooling system

Circulang Fluids

Once you have selected your cooling system, you will need to follow the manufacturer’s recommendaon and use a ﬂuid suitable for your applicaon. Manufacturers will recommend avoiding an-freeze intended for cars, instead prompng use of ﬂuids designed speciﬁcally for lab equipment.

When working with refrigerated and other cooling equipment, it is important to use a ﬂuid that will not freeze because the temperatu temperature.

Circulang Fluids – Cooling

Water-based synthec ﬂuids are popular choices for cooling. They can be used across a broad temperature range, especially when used in sealed or vacuum systems. Glycols, when mixed with water, become anfreeze. This does not mean that you can buy and use automove anfreeze. What’s good for your car is not necessarily good for your lab equipment. There are tw used: Ethylene glycol (EG) and propylene glycol (PG). Of the two, EG has slightly beer thermal properes and can cool in a broader temperature range. However, it is highly toxic and not usable in all applicaons. In those cases, PG is a good alternave. We recommend mixing with dislled water; the best mix rate is 50/50.

Circulang Fluids – Mixes

Mixes are oﬀered as a convenience and are made up of one or more of the ﬂuids, described above, like a mix of ethy ﬁlling common-sized equipment like chillers.

lycol, water and algaecide. They are usually sold in volumes that make sense for

lene g

re inside the cooling equipment may be signiﬁcantly colder than the set

o g

lycols which are commonly

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Cole-Parmer Ltd.

Beacon Road, Stone, Staffordshire, ST15 0SA, United Kingdom Tel: +44 (0)1785 812121 Email: [email protected] Web: www.electrothermal.com