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A CAUTION notice denotes a hazard. It
calls attention to an operating
procedure, practice, or the like that, if
not correctly performed or adhered to,
could result in damage to the product
or loss of important data. Do not
proceed beyond a CAUTION notice
until the indicated conditions are fully
understood and met.
A WARNING notice denotes a hazard.
It calls attention to an operating
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could result in personal injury or
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Request for Installation
All preparations have been completed. Please arrange for the installation to be
completed as soon as possible. I understand that if the installation site is not
prepared in accordance with the enclosed instructions, additional installation
charges may apply.
Company name:
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Signed:
Date:
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 3
Requirements
The work area is prepared and meets requirements (see Chapter 3).
The power supply meets requirements (see Chapter 4).
A nitrogen gas supply for optics path purging is ready (Cary 100/300 needs the Extended
Sample Compartment option) (see Chapter 5).
The Cary instrument and accessories are on site and packages have been inspected (see
Chapter 6).
The computer meets requirements (see Chapter 7).
Computer type: _________________________
The Microsoft Windows operating system is installed (see Chapter 7).
Operator training is required (see Chapter 8).
Site Preparation Checklist
Your site must meet all requirements before you request installation. Complete
each requirement listed in the table. After completing each requirement, place a
check in the appropriate checkbox. Ensure you compare each item inside the
boxes with the packing list supplied with the boxes.
NOTE
Do not unpack the instrument. If unpacked incorrectly, equipment may become
damaged. Your Agilent representative will do this for you.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 4
Contents
Contents
Request for Installation 3
Site Preparation Checklist 4
1 Introduction 7
2 Safety Practices and Hazards 9
Instrument ventilation 9
Electrical hazards 9
3 Work Area 11
Suitability 11
Environmental conditions 11
Workbench 12
4 Electrical Specifications 15
Mains supply 15
Fuses 16
External connections 16
Mains inlet coupler 16
Mains power cord 16
5 Optional Nitrogen Supply 17
6 Equipment On-Site 19
Insurance 19
In-house transit routes 19
Inspecting for transit damage 19
7 Computer System Requirements 21
Recommended configuration 21
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 5
Contents
Recommended printer 22
IEEE 488.2 interface 22
Interconnecting cables 22
Setting up your computer 23
8 Operator Training 25
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 6
Introduction
1 Introduction
The range of Agilent Cary spectrophotometers are complete analysis systems that
have been fully tested and proven to specification before dispatch from the
manufacturing plant.
This manual contains general information relevant to the preparation of an
installation site, and details the facilities that must be provided to ensure that the
system can be effective. Detailed operating procedures are provided in the
operation manual that is supplied with the spectrophotometer.
You should complete the site preparation checklist on Page 4 and then send a copy
of the checklist to the Agilent sales and service office or local Agilent agent dealing
with the supply of the equipment. On receipt of this document, the Agilent
representative will contact you and arrange a convenient time for installation.
As a guide to the time required for installation by an Agilent representative, a typical
Cary system will be completed and ready for use within four hours. This time may
be extended if the system includes accessories. The installation time can be kept to
a minimum by ensuring proper preparation of the site and arrangement of all units
to allow for easy access.
NOTE
The remainder of this manual contains information such as the environmental
requirements and technical specifications for the Cary spectrophotometer, and it
should not be discarded — keep this manual for future reference.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 7
Introduction
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Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 8
Safety Practices and Hazards
2 Safety Practices and Hazards
Your Agilent Cary instrument and accessories have been carefully designed so that
when used properly you have an accurate, fast, flexible and safe analytical system.
If the equipment is used in a manner not specified by the manufacturer, the
protection provided by the equipment may be impaired.
Information on safety practices appears throughout the documentation (both
printed and online) provided with your instrument and accessories. Before using the
instrument or accessories, you must thoroughly read these safety practices.
Observe all relevant safety practices at all times.
Instrument ventilation
Ozone can be generated by radiation from the source lamps. Exposure to ozone
can result in severe irritation to the skin, eyes, and upper respiratory system. The
maximum permissible exposure level is 0.1 parts per million (0.2 milligrams per
cubic meter).
ALWAYS ventilate the area surrounding the spectrophotometer such that the
concentration of ozone does not exceed the maximum permissible level. All venting
must be to outside air, never within the building.
Electrical hazards
Good grounding/earthing is essential to avoid a potentially serious electric shock
hazard. Ensure that there is an integral ground connection between the metal base
of the spectrophotometer and accessories and the 3-pin earth-grounded
receptacle. Consult the manuals or product labels supplied with your computer,
monitor and printer for the relevant grounding requirements.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 9
Safety Practices and Hazards
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Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 10
The instrument is suitable only for indoor use. It is suitable for these categories:
Installation category II (EN 61010-1)
Pollution degree 2
Equipment class I
Environmental conditions
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 11
Sample preparation areas and materials storage facilities should be located in a
separate room.
For optimum performance the area should have a dust-free, low humidity
atmosphere. Air conditioning is recommended. The room should be temperaturecontrolled if your analyses are particularly sensitive.
Work Area
c vapors, such as acetone, must be
Instrument
Condition
Altitude (m, ft)
Temperature
(°C, °F)
Relative humidity,
non-condensing (%)
Cary 100/300
Non-operating
0–2133, 0–7000
5–45, 41–113
20-80
Operating within
specifications
0–2133, 0–7000
10–35, 50–95
8-80
Cary 4000/5000/
Non-operating
0–2133, 0–7000
5–45, 41–113
<90
Operating within
specifications
0–853, 0–2800
10–35, 50–95
15–80
CAUTION
The Cary instrument is designed for operation in clean air conditions. The work
area must be free of all contaminants that could have a degrading effect on the
instrument components. Dust, acid and organi
expelled from the work area. The instrument warranty will be void if the
equipment is operated in substandard conditions.
For optimum analytical performance, it is recommended that the ambient
temperature of the laboratory be between 20 and 25 °C (68 and 77 °F) and be held
constant to within ±2 °C (±3.6 °F) throughout the entire working day. When
performing the limiting resolution test on the Cary 4000/5000/6000i/7000 systems
Table 1. Suitable conditions during instrument transportation, non-operation and operation
6000i/7000
CAUTION
it is a requirement that these environment conditions are met.
performance
performance
853–2133, 2800–7000
10–25, 50–77
Operating specifications for the computer, monitor and printer may differ from
those for the Cary spectrophotometer. You must check in the literature provided
with these units and arrange the operating environment to suit the complete
system.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 12
Workbench
The workbench must be stable and strong enough to support the total weight of
equipment to be used.
Work Area
Instrument
Weights
Dimensions (width x depth x height)
Cary 100/300
Packed: 75 kg (165 lb)
Packed: 860 x 770 x 655 mm (34 x 30 x 26 in)
Unpacked: 45 kg (99 lb)
Unpacked: 640 x 650 x 320 mm (25 x 26 x 13 in)
Cary 4000/5000/
Packed: 141 kg (310 lb)
Packed: 1425 x 800 x 670 mm (56 x 31 x 26 in)
Unpacked: 91 kg (200 lb)
Unpacked: 1000 x 650 x 340 mm (40 x 26 x 14 in)
Table 2. Equipment weights and dimensions
6000i/7000
The bench tops should be large enough to permit a free circulation of air around
each unit in the system. Remember to provide space for the computer, monitor and
printer.
The workbench should be about 90 cm (36 in.) high.
To avoid damage through spillage of the samples being analyzed, the worktops
should be covered with a material that is corrosion-resistant and impervious to
liquids.
After the work area requirements have been met, check the checklist box: The work area is
prepared and meets requirements.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 13
Work Area
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Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 14
Electrical Specifications
Power rating
(typical)
Maximum power
consumption
Cary 100/300
100, 120, 220, 240 VAC, 50–60 Hz
270 VA
173 W
Cary 4000/5000/6000i/7000
100–240 VAC, 50–60 Hz
300 VA
185 W
4 Electrical Specifications
Mains supply 15
Fuses 16
External connections 16
Mains supply
The installation of electrical power supplies must comply with the rules and/or
regulations imposed by local authorities responsible for the supply of electrical
energy to the workplace.
WARNING
Table 3. Mains voltage requirements
System unit Required supply voltage
NOTE
Electrical Shock Hazard
Good electrical grounding is essential to avoid potentially serious shock
hazards. A 3-wire outlet with ground connection must be provided for the
instrument. Ensure that power outlets are earth-grounded at the grounding pin.
All power supplies must be single phase AC (alternating current) voltage, three wire
system (active, neutral, earth) and should be terminated at an appropriate power
outlet receptacle that is within reach of the instrument power cord assembly. For
safety reasons, a separate power outlet receptacle should be provided for each unit
in the system. Do not plan to use extension cords or outlet adaptors.
All Cary 100/300/4000/5000/6000i/7000 instruments are supplied with a 2 meter
(6 ft. 6 in.) long power cord and three-pin plug assembly that is compatible with
common standards applicable in the local area.
Avoid using power supplies from a source that may be subject to electrical or RF
interference from other services; for example, large electric motors, elevators, and
welders.
For the computer, refer to the literature provided with the computer for details of
individual power requirements.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 15
Table 4. Fuses
220-240 VAC
100-120 VAC
Cary 100/300
T4 AH 250 V, IEC60127-2 Sheet 5, 5x20 mm,
Littelfuse 0215004 or equivalent
For safety reasons, any other internal fuse or circuit breaker is not operator
accessible, and should be replaced only by Agilent authorized personnel.
NOTE
Fuse information on the rear of the instrument is the most up-to-date.
External connections
Mains inlet coupler
3/2 A 120/250 VAC 50–60 Hz IEC type
Mains power cord
After the power requirements have been met, check the checklist box: The power supply meets
requirements.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 16
Optional Nitrogen Supply
5 Optional Nitrogen Supply
The Cary 4000/5000/6000i instruments are fitted with connection points for
purging the optical system with nitrogen to enhance the performance of each
instrument at extremes of its range. More details are provided in the Cary User’s
Guide supplied with the instrument.
Nitrogen supplies are not available from Agilent but may be obtained from
commercial suppliers. Liquid nitrogen (in conjunction with a heat exchanger) is
recommended because it is generally less costly than compressed nitrogen and is
of better quality. Where compressed nitrogen must be used, the gas must be dry,
oil-free and uncontaminated.
CAUTION
NOTE
Do not use compressed nitrogen from a supplier who uses oil or water in the
compression process. These methods leave fine particles of oil or water
suspended in the nitrogen that may be deposited on the instrument optics. Only
use nitrogen from a supplier who fills containers from immersion pumps that are
lubricated with liquid nitrogen.
The instrument warranty will be void if damage is caused by the use of
contaminated nitrogen.
All gas supply installations must comply with the rules and/or regulations that are
imposed by the local authorities responsible for the supply of compressed gas
energy to the workplace.
Cylinders containing gas under pressure should be firmly secured to a rigid
structure and the storage area must be well ventilated. Never locate gas cylinders
near a source of ignition or in a position that is subject to direct heat. Gas storage
cylinders often incorporate a pressure relief device, which will discharge the gas at
a pre-determined temperature, usually around 52 °C (125 °F).
If gases are to be plumbed from a remote storage area to the instrument site,
ensure that the local outlets are fitted with shut-off valves and suitable regulators
that are easily accessible to the instrument operator.
Nitrogen supply tubing should be clean, flexible plastic tubing of 6 millimeters
(1/4 inch) internal diameter (polyvinylchloride or equivalent).
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 17
Optional Nitrogen Supply
1 Instrument
2 Sample compartment
3 Tubing
4 Flow meters
5 Shut off valves
6 Manifold
7 Pressure regulator
8 Nitrogen control valve
CAUTION
Do not use rubber tubing, as this is usually treated internally with talc, which will
be carried into and contaminate the instrument optics.
Operating pressure for the nitrogen purging system is 83 to 172 kPa (12 to 25 psi).
Use a suitable regulator and gauge assembly to ensure that the nitrogen supply is
maintained at the correct pressure.
The nitrogen system should include a manifold assembly with inlet from the supply
and two outlets for connection to the instrument. Manifold outlets should each be
fitted with a stop valve and flow meter for control of gas flow to the instrument.
Flow meters should be adjustable for flow rates of 0 to 30 liters per minute (0 to 64
cubic feet per hour). Refer to Figure 1 for more details.
NOTE
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 18
Figure 1. The position of flow meters when purging with nitrogen where:
The sample compartment of the Cary 100/300 instruments can be purged if the
optional Extended Sample Compartment is fitted. Refer to the Extended Sample
Compartment section of the Cary WinUV Help for specifications and instructions
for use.
After the gas requirements have been met, check the checklist box: A nitrogen gas supply for optics path purging is ready (Cary 100/300 needs the Extended Sample Compartment option).
Equipment On-Site
6 Equipment On-Site
Insurance
As the carrier’s liability ceases when the equipment is delivered, Agilent
recommends that the instrument owner arranges separate insurance to cover
transportation from the delivery point to the installation site. The delivery point will
vary according to the carrier, the shipping method and in some cases the terms of
sale. Some carriers will deliver only to their own distribution centre, while others
may deliver to your off-loading bay. Very few carriers will deliver to the actual
installation site.
In-house transit routes
In-house transit routes must be carefully considered. Vertical, horizontal and
turning clearances should be calculated from the shipping carton dimensions of the
spectrophotometer, which is the largest unit in any system configuration. See Page
13 for shipping dimensions.
Inspecting for transit damage
Transit damage can be obvious or concealed and in either case will be admitted by
the carrier only if it is reported within the terms of the carrier’s agreement. For any
claims against damage in transit, the following general rules apply:
Before accepting delivery, you must inspect the packages for signs of obvious
damage. The nature of any obvious damage must be noted on the carrier’s
waybill, which then must be countersigned by a representative of the carrier.
Within the time limit stated in the terms and conditions of carriage, a further
inspection must be made for concealed damage. If any damage is found at this
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 19
Equipment On-Site
stage, the carrier must be notified in writing. You must retain all packaging
material for subsequent inspection by a representative of the carrier.
A copy of any damage report must be forwarded to the Agilent sales office
dealing with the supply of your equipment.
WARNING
NOTE
Heavy Weight Hazard
As many of the packages are heavy, use mechanical lifting devices when
possible to avoid the chance of injury to personnel or accidental damage to
the equipment. If manual lifting is unavoidable, always use two or more
people to handle packages and lift equipment into position. Never attempt to
lift the packages alone.
Do not unpack the instrument. Your Agilent representative will do this for you.
After accepting delivery, take the equipment to the installation site.
Agilent instruments are inherently robust, and the packaging is designed to prevent
internal damage. However, the contents form part of a precision measuring system
and all packages should be handled with care. In transit, sharp jolts must be
avoided and the packages should not be inverted or tilted unnecessarily. Markings
on the shipping cartons generally indicate which side of the package should be kept
on top.
All shipping packages should be together for the Agilent service personnel prior to
installation. Compare all packages to the shipping list. Do not discard any
packaging components or filler materials.
After the requirements have been met, check the checklist box: The Cary instrument and accessories
are on site and packages have been inspected.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 20
Computer System Requirements
Workstation
Laptop
CPU
3.3 GHz, 8MB cache
2.4 GHz, 3 MB cache, 2 cores
RAM
Windows 7: 4 GB, Windows 10: 8 GB
Windows 7: 4 GB, Windows 10: 8 GB
Hard drive
500 GB 7200 RPM SATA Hard Drive
500 GB Hard Drive
Graphics
Intel HD Graphics P530
14-inch LED HD SVA
DVD drive
16X DVD+-RW
DVD±RW
Communications
PCIe GbE Controller; 2nd Serial Port Adapter
802.11 a/b/g/n/ac (2x2) +Bluetooth 4.2
Operating system
Microsoft Windows 7 64-bit SP1 or Microsoft
Windows 10 64-bit
Microsoft Windows 7 64-bit SP1 or Microsoft
Windows 10 64-bit
Expansion
8 USB 3.0 (2 front, 6 rear), 2 USB 2.0 (1 front,
1 front battery charging port)
3 USB 3.0 ports: 1 standard, 1 charging, and one
USB-C
Peripherals
Compatible keyboard and USB Optical Scroll
mouse
7 Computer System Requirements
Recommended configuration 21
Recommended printer 22
IEEE 488.2 interface 22
Interconnecting cables 22
Setting up your computer 23
Recommended configuration
The Cary spectrophotometers were evaluated under Agilent’s ISO9001 procedures
using Cary WinUV software and a desktop computer. We strongly recommend a
computer configuration that matches the system that was used during evaluations:
Agilent can supply a computer for the Cary WinUV software in the recommended
configuration. The computer will be formatted, partitioned and loaded with its
operating system. Computers ordered from Agilent will come with the software
NOTE
installed. All software disks and manuals will be supplied.
Computers supplied with Letter of Credit orders will be an international brand and
will be the recommended configuration or better.
Better computer components, for example, processor type, amount of memory,
screen size and resolution, operating system version, and so on, can be substituted
for those listed above.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 21
Computer System Requirements
Recommended printer
You can use any printer supported by your Microsoft Windows operating system.
IEEE 488.2 interface
The Cary instruments require a GPIB-USB-HS converter to be attached to the
computer. One will usually be included in your instrument order as a separate line
item:
GPIB-USB-HS converter
NOTE
The NI (National Instruments) AT-GPIB card will not work with the Cary WinUV
software.
The NI PCI-IEEE card will not work when purchasing the HP Compaq 8000 Elite
Small Form Factor Desktop or the HP Z210 SFF workstation.
Interconnecting cables
The monitor, printer keyboard and spectrophotometer are connected to the
computer via cables that plug into the back of the computer. The
spectrophotometer is connected via a USB-GPIB-HS converter provided with the
instrument. Consult your monitor, printer and keyboard manuals for details of their
individual cabling requirements.
After the computer requirements have been met, enter the computer type and then check the checklist
box: The computer meets requirements.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 22
Computer System Requirements
Setting up your computer
When setting up your own computer for use with the Cary WinUV software, ensure
that your computer meets the specified requirements listed on Page 21 and that:
The operating system is installed and all devices such as the sound and DVD
drive are working.
Microsoft Internet Explorer version 9* or later has been installed.
You have set your computer screen desktop area resolution to at least 800 x
600 pixels and have set the color palette to at least High Color.
RS232 serial port
One COM port if using the Agilent SPS 3 Sample Preparation System in
conjunction with the Internal Routine Sampler
Two COM ports if using the Agilent SPS 3 Sample Preparation System in
conjunction with the External Sipper accessory
* The Cary WinUV software uses functionality provided by Microsoft Internet
Explorer version 9.0 or greater. You do not need to use this as your Web browser. If
your company rules prevent the installation of Internet Explorer, you can use
another browser, with some loss in functionality.
NOTE
The Agilent representative will install the Cary WinUV software if the computer was
not purchased from Agilent. However, installation of a Windows operating system
is not included as part of the standard instrument installation.
After the operating system installation requirements have been met, check the checklist box: The
Microsoft Windows operating system is installed.
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 23
Computer System Requirements
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Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 24
Operator Training
8 Operator Training
Use - _Toc506206031If the Cary instrument is installed by Agilent field service, the
Agilent representative will demonstrate the basic operating procedures while
conducting the installation performance tests during the installation procedure. The
representative however, is not necessarily experienced in complex analytical
routines and is not authorized to conduct extensive training.
To ensure that your operators benefit the most from witnessing the installation
performance tests, operator training should be completed before your equipment is
installed. It is strongly recommended that you take advantage of the special
training courses that are conducted at various locations by the Agilent customer
support and sales organization.
In some areas it may be possible to arrange for operator training to be carried out
after the installation, using your own instrument. To investigate this possibility,
contact your local Agilent sales and service office.
The initial software installation and elementary performance tests will take around
thirty minutes. There is then a period of two hours that must be allowed for warmup before the detailed instrument tests for conformance to specification can be
carried out, and during this time the representative will demonstrate some of the
basic system operating procedures.
Detailed tests verifying the instrument is performing to specification are automated
NOTE
Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 25
and take around one hour to complete.
You must have a working knowledge of the computer operating system, as this
type of instruction is not provided by Agilent. The literature supplied with the
spectrophotometer provides step-by-step instructions for setting up the system
and detailed operating instructions for the analysis procedures — it does not
include instructions for operation of the computer.
If operator training is required, check the checklist box: Operator training is required.
Operator Training
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Agilent Cary 100/300/4000/5000/6000i/7000 Spectrophotometer Site Preparation Guide 26
This information is subject to change without notice.