Advanced Instruments GPR-2500 A Manual (ATEX)

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Technical Specifications *
Accuracy: < 2% of FS range under constant conditions
Analysis:
Application:
Area Classification: General purpose Alarms:
Calibration:
Compensation: Barometric pressure and temperature Connections: 1/8" compression tube fittings Controls:
Display:
Enclosure: Fiberglass NEMA 4X, 4 x 9 x 3", 8 lbs. Flow Sensitivity: Not flow sensitive, 1-2 SCFH recommended Linearity: ±1% of full scale Pressure:
Power: 12-28 VDC non-loop or 110-220 VAC
0-1%, 0-5%, 0-10%, 0-25% FS ranges; auto-ranging or fixed single range
Oxygen analysis in inert, hydrocarbon, helium, hydrogen, mixed and acid (CO2) gas streams
Two user configurable alarms: magnetic coil relays rated 3A at 100 VAC, field programmable alarm time delays, alarm bypass for calibration and system fail alarm
Max interval—3 months. Air calibrate with clean source of certified span gas, compressed, or ambient (20.9% O2) air on 0-25% range.
Water resistant keypad; menu driven range selection, calibration and system functions
Graphical LCD 2.75” x 1.375”; resolution 0.001%; displays real time ambient temperature and pressure
Inlet - regulate to 5-30 psig to deliver 1-2 SCFH flow; vent - atmospheric
GPR-2500 A
Oxygen Analyzer
12-24 VDC Non-Loop or 110-220 VAC
Powered Oxygen Analyzer
Advanced Galvanic Sensor Technology with
Optional Sample Systems
Response Time: 90% of final reading in 13 seconds Sample System: None
Sensitivity: < 0.5% of FS range Sensor Model:
Sensor Life:
Signal Output: 4-20mA non-isolated or 1-5V; optional Modbus Operating Range: 5ºC to 45ºC (GPR sensor), -10º to 45ºC (XLT sensor)
Warranty: 12 months analyzer; 12 months sensor Wetted Parts: Stainless steel
Optional Equipment
Sample conditioning system - Contact factory.
* Subject to change without notice
2855 Metropolitan Place, Pomona, CA 91767 USA ♦ Tel: 909-392-6900, Fax: 909-392-3665, www.aii1.com, e-mail: [email protected] Rev 10/15
GPR-11-32-4 for non-acid (CO2) gas streams; XLT-11-24-4 for gases containing > 0.5% CO2
GPR-11-32-4 32 months in air at 25ºC and 1 atm XLT-11-24-4 32 months in air at 25ºC and 1 atm
2 Field Selectable Alarm Setpoints 12-24 VDC or 110-220 VAC Power 4-20 mA Signal Output Sensitivity 0.5% Full Scale 4 Ranges Standard Auto Ranging or Single Fixed Stainless Steel Wetted Parts
ISO 9001:2008 Certified
INTERTEK Certificate No. 485
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Advanced Instruments, Inc.
2855 Metropolitan Place, Pomona, CA 91767 USA ♦ Tel: 909-392-6900, Fax: 909-392-3665, e-mail: info@aii2 .com, www.aii2.com
GPR-2500A % Oxygen Transmitter
Owner’s Manual
Revised June 2014
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Table of Contents
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A/R
Introduction Quality Control Certification Safety Features & Specifications Operation Maintenance Spare Parts Troubleshooting Warranty Material Safety Data Sheets
Advanced Instruments, Inc.
Drawings
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1. Introduction
Your new oxygen transmitter incorporated an advanced electrochemical sensor specific to ox ygen along with state-of-the-art digital electronics designed to give you years of reliable precise oxygen measurements in a variety of industrial oxygen applications.
To obtain maximum performance from your new oxygen transmitter, please read and follow the guidelines provided in this Owner’s Manual.
Every effort has been made to select the most reliable state of the art materials and components, to design the transmitter for superior performance and minimal cost of ownership. This transmitter was tested thoroughly by the manufactur er prior to shipment for best performance.
However, all electronic devices do require service from time to time. The warranty included herein plus a staff of trained professional technicians to quickly service your transmitter is your assurance that we stand behind every transmitter sold.
The serial number of this transmitter may be found on the inside the transmitter. You should note the serial number in the space provided below and retain this Owner’s Manual as a permanent record of your purchase, for future reference and for warranty considerations.
Serial Number : _______________________
Advanced Instruments Inc. appreciates your business and pledges to make every effort to maintain the highest possible quality standards with respect to product design, manufacturing and service.
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2. Quality Control Certification

Date:

Customer: Order No.:

Pass

Model:

GPR-2500A Oxygen Transmitter
( ) XLT-11-24-4 oxygen Sensor
______________________

Accessories:

Owner’s Manual

Configuration:

A-1161-AIS-2 Rev C4 PCB Assembly Main Processing
A-1166-AIS-2 Rev H PCB Assembly Alarms/Power Connection
Software rev:
Ranges: 0-1%, 0-5%, 0-10%, 0-25%
Power: 12-24V DC
Barometric pressure and temperature compensation
NEMA 4X rated wall mount enclosure

Test:

Pass

Pass

Set default zero
Set default span @ 40uA
Alarm delay
Zero calibration
Alarm bypass
ALARM 2
Analog signal output 4-20mA full scale
Alarm function; ALARM 1, ALAR M 2
10-50% FS
period
defects

Options:

Notes:

Advanced Instruments, Inc.

Sensor: ( ) GPR-11-32-4 Oxygen Sensor

Serial Nos.: Transmitter ______________________ Sensor

Span Calibration Alarm configurations; ALARM 1,
Calibrates with adequate span adjustment within
Baseline drift on zero gas < ± 2% FS over 24 hour
Noise level < ± 1.0% FS
Alarm relays; ALARM 1, ALARM 2
Alarm system fail, dry contact
Overall inspection for physical
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3. Safety
General
This section summarizes the essential pre cautions applicable to the GPR-2500A Oxygen Transmitter. Additional precautions specific to individual transmitter are contained in the following sections of this manual. To operate the transmitter safely and obtain maximum performance follow the basic guidelines outlined in this Owner’s Manual.
Caution: This symbol is used throughout the Owner’s Manual to Caution and alert the user to recommended safety and/or operating guidelines.
Danger: This symbo l is used througho ut the Owner’s Manual to identify sources of immediate danger such as the presence of hazardous voltages.
Read Instructions: Before operating the transmitter read the instructions.
Retain Instructions: The safety precautions and operating instructions found in the Owner’s Manual
should be retained for future reference.
Heed Warnings: Follow all warnings on the transmitter, accessories (if any) and in this Owner’s Manual. Follow Instructions: Observe all precautions and operating instructions. Failure to do so may result in
personal injury or damage to the transmitter.
Pressure and Flow
Inlet Pressure: GPR-2500A Oxygen Transmitters are designed for flowing samples, equipped with 1/8”
bulkhead tube fitting connections on the side of the unit (unless otherwise indicated, either fitting can serve as inlet or vent) and are intended to operate at positive sample pressure regulated between 5-30 psig.
Caution: If equipped w ith a H2S scrubber as part of an optional sample conditioning system, inlet pressure must not exceed 30 psig.
Outlet Pressure: The sample gas must be vented to atmosphere or vent pipe with atmospheric pressure.
Installation
Oxygen Sensor: DO NOT open the sensor. The sensor contains a corrosive liquid electrolyte that could
be harmful if touched or ingested, refer to the Material Safety Data Sheet contained in the Owner’s Manual appendix. A vo id contact with any liquid or crystal type powder in or around the sensor or sensor housing, as either could be a form of electrolyte. Leaking sensors should be disposed of in accordance with local regulations.
Mounting of the Transmitter: The transmitter is approved for indoor or outdoor use. Mount the transmitter on a flat surface.
Power Requirement: Supply power to the transmitter only as rated by the specification or markings on the transmitter enclosure. The wiring that connects the transmitter to the power so urce should be installed in accordance with recognized electrical standards and so they are not pinched particularly near the power source and the point where they attach to the transmitter. Never yank wiring to remove it from an outlet or from the transmitter.
0
Operating Temperature: The maximum operating temperature is between 0
C to 45º C.
Heat: Situate and store the transmitter away from sources of heat. 5
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Liquid and Object Entry: The transmitter should not be immersed in any liquid. Care should be taken so that liquids are not spilled into and objects do not fall into the inside of the transmitter.
Handling: Do not use force when using the switches or terminal blocks. Before moving your transmitter, be sure to disconnect the wiring/power cord and any cables connected to the output terminals located on the transmitter.
Maintenance
Serviceability: Except for replacing the oxygen sensor, there are no parts inside the transmitter for the
operator to service. Only trained personnel with the authorization of their supervisor should conduct maintenance. Oxygen Sensor: DO NOT open the sensor. The sensor contains a corrosive liquid electrolyte that could
be harmful if touched or ingested, refer to the Material Safety Data Sheet contained in the Owner’s Manual appendix. A vo id contact with any liquid or crystal type powder in or around the sensor or sensor housing, as either could be a form of electrolyte. Leaking sensors should be disposed of in accordance with local regulations.
Troubleshooting: Consult the gui delines in Section 8 for advice on the common operating errors before concluding that yo ur transmitter is faulty.
Do not attempt to service the transmitter beyond those means described in this Owner’s Manual. Do not attempt to make repairs by yourself as this will void the warranty as per Section 1 0 and may result in electrical shock, injury or damage. All other servicing should be referred to qualified service personnel.
Cleaning: The transmitter should be cleaned only as recommended by the manufacturer. Wipe off dust and dirt from the out sid e of the unit with a soft damp cloth then dr y imm ediately. Do not use solvents or chemicals.
Nonuse Periods: If the transmitter is equipped with a range switch advance the switch to the OFF position and disco nnect the power when the transmitter is left unused for a long period of time.
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4. Features and Specification
Advanced Instruments, Inc.
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5. Operation
Principle of Operation
The GPR-2500A oxygen transmitter incorporates a variety of advanced galvanic fuel cell type sensors. The transmitter is a compact efficient package configured with the oxygen sensor and separate circuit boards for signal processing and terminals for incoming power, power supply, signal output and alarm relay contacts housed in a general purpose NEMA 4X rated enclosure.

Advanced Galvanic Sensor Technology

The sensors function on the same principle and are specific for oxygen. They measure the partial pressure of oxygen from low ppm to 100% levels in inert gases, gaseous hydrocarbons, helium, hydrogen, mixed gases, acid gas streams and ambient air. Oxygen, the fuel for this electrochemical transducer, diffusing into the sensor reacts chemically at the sensing electrode to produce an electrical current output pro portional to the oxygen concentrat ion in the gas phase. The sensor’s signal output is linear over all ranges and remains virtually consta nt over its useful life. The sensor requires no maintenance and is easily and safely replaced at the end of its useful life.

Electronics

The signal generated by the sensor is processed by state of the art low power micro-processor based digital circuitry. The first stage amplifies the signal. The second stage eliminates the low frequency noise. The third stage employs a high frequency filter and compensates for signal output variations caused by ambient temperature changes. The result is a very stable signal. Sample oxygen is analyzed very accurately. Response time of 90% of full scale is less than 10 seconds (actual experience may vary due to the integrity of sample line connections, dead volume and flow rate selected) on all ranges under ambient monitoring conditions. Sensitivity is typically 0.5% of full scale low range. Oxygen readings may be recorded by an external device via the 0-1V signal output jack.
The circuit for the 4-20mA signal output and two adjustable alarms is powered by a DC/DC transformer that requires a 12-24VDC power source a nd separate wiring for the signal outputs.
Caution: A loop power source is not sufficient to power this transmitter. Further, the 4-20mA signal output does not require any external power (applying power to 4-20 mA terminal will permanently
damage the transmitter and void transmitter warranty).

Sample System

The GPR-2500A is supplied without a sample conditioning system thereby giving users the opt ion of adding their own or purchasing a factory designed sample conditioning system. Whatever the choice, the sample must be properly presented to the sensor to ensure an accurate measurement. Users interested in adding their own sample conditioning system sho uld consult the factory. Advanced Instruments Inc. offers a full line of sample handling, conditioning and expertise to meet your application requirements. Contact us at 909-392-6900 or e-mail us at
Pressure and Flow Consideration All electrochemical oxygen sensors respond to partial pressure changes in oxygen. The inlet pressure
must always be higher than the pressure at the outlet vent which is normally at atmospheric pressure.

Flow-Through Configuration

The sensor is exposed to sample gas that must flow or be drawn through the sensor housing inside the transmitter. The GPR-2500A internal sample system in cludes 1/8” compression tube sample inlet and vent fittings, a Delrin or optio nal stainless steel sensor housing.
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Delrin Senor Housing with sensor installed.
Flow rates of 1-5 SCFH cause no appreciable change in the oxygen reading. However, flow rates above 5 SCFH generate backpressure and erroneous oxygen readings because the diameter of the integral tubing cannot evacuate the sample gas at the higher flow rate. The direction the sample gas flows is not important, thus either of the two tube fitting connectors can serve as the inlet or vent.
A flow indicator with an integral metering valve upstream of the sensor is recommended as a means of controlling the flow rate of the sample gas. A flow rate of 1-2 SCFH or 0.4-1 liter per minute is recommended for optimum performance.
Caution: Do not place your finger over the vent (it pressurizes the sensor) to test the flow indicator when gas is flowing to the sensor. Removing your finger (the restriction) genera tes a vacuum on the sensor and may damage
the sensor (voiding the sensor warranty).

Application Pressure - Positive:

A flow indicator with integral metering valve positioned upstream of the sensor is recommended for controlling the sample flow rate between 1-5 SCFH. If necessary, a pressure regula tor (pressure regulator with a metallic diaphragm is recommended for optimum accuracy, the use of more permeable materials may result in erroneous readings) upstream of the flow control valve should be used to regulate the inlet pressure between 5-30 psig.
Caution: If equipped with a H2S scrubber as part of an optional sample conditioning system, inlet pressure must not exceed 30 psig.

Application Pressure - Atmospheric or Slightly Nega t iv e :

For accurate oxygen measurements, an optional external sampling pump should be positioned upstream of the sensor to draw the sample from the process and push it through the sensor housing and out to atmosphere. A flow meter is not necessary if the discharge of the sampling pump approximates the recommended 1-2 SCFH flow rate.
If pump loading is a consideration, a second throttle valve on the pump’s inlet side may be necessary to provide a bypass path so the sample flow rate is within the above parameters.
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To avoid erroneous oxygen readings and damage to the sensor:

• Do not place your finger over the vent (it press urizes the sensor) to test the flow indicator whe n gas is flowing to the sensor. Removing your finger (the restriction) generates a vacuum on the sensor and may damage the sensor (voiding the sensor warranty).
• Assure there are no restrictions in the sample or vent lines
• Avoid drawing a vacuum that exceeds 14” of water column pressure – unless done gradually
• Avoid excessive flow rates above 5 SCFH which generate backpressure on the sensor.
• Avoid sudden releases of backpressure that can severely damage the sensor.
• Avoid the collection of particulates, liquids or condensation collect on the sensor that could block
the diffusion of oxygen into the sensor.
• If the transmitter is equipped with an optional integral sampling pump (positioned downstream of the sensor) and a flow control metering valve (positioned upstream of the sensor), completely open the flow control mete r ing valve to avoid drawing a vacuum on the sensor and placing an undue burden on the pump.
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Choices of Calibration & Accuracy
Single Point Calibration: As previously described the galvanic oxygen sensor genera tes an electrical
current sensor exhibiting an absolute zero, e.g. the sensor does not generate a current output in the absence of oxygen. Given these linearity and absolute zero properties, sing le point calibration is possible.
Pressure: Because sensors are sensitive to the partial pressure of oxygen in the sample gas their output is a function of the number of molecules of oxygen 'per unit volume'. Readouts in percent are permissible only when the total pressure o f the sa mple gas being analyzed remains constant. The pressure of the sample gas and that of the calibration gas(es) must be the same (reality < 1-2 psi).
Temperature: The rate oxygen molecules diffuse into the sensor is controlled by a Teflon membrane otherwise known as an 'oxygen diffusion limiting barrier' and all diffusion processes ar e temperature sensitive, the fact the sensor's electrical output will vary with temperature is normal. This variation is relatively constant 2.5% per ºC. A temperature compensation circuit employing a thermistor offsets this effect with an accuracy of +5% (over the recommended operating temperature range) or better and generates an output signal that is relatively independent of temperature. Note: There is no error if the calibration and sampling are performed at the same temperature or if the measurement is made immediately after calibration. Lastly, small temper ature variations of 10-15º produce < +1% error .
Accuracy: In light of the above parameters, the overall accuracy of an transmitter is affected by two types of errors: 1) those produci ng 'percent of reading errors', illustrated by Graph A below, such as + temperature compensation to make span adjustments and 2) thos e producing 'percent of full scale errors', illustrated by Graph B, such as +1-2% linearity errors in readout devices, which are really minimal due to today's technology and the fact that other errors are 'spanned out' during calibration.
Graph C illustrates these 'worse case' specifications that are typically used to develop an transmitter's overall accuracy statement of +2% of full scale at constant temperature or +5% over the operating temperature range. QC testing is typically <+0.5% prior to shipment.
circuit, tolerances of range resistors and the 'play' in the potentiometer used
5%
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Example: As illustrated by Graph A any error, play in the multi-turn span pot or the temperature compensation circuit, during a span adjustment at 20. 9% (air) of full scale range would be multiplied by a factor of 4.78 (100/20.9) if used for measurements of 95-100% oxygen concentrations. Conversely, an error during a span adjustment at 100% of full scale range is reduced proportionately for measurements of lower oxygen concentrations.
Recommendation: Calibrating with a span gas approximating 80% of the full scale range one or two ranges higher than the full scale range of interest is recommended for 'optimum c alibration accuracy'. Always calibrate at the same temperature and pressure of the sample gas stream.
Starting-up the Analyzer
The GPR-2500A Oxygen Transmitter has been tested, calibrated at the factory prior to shipment with the sensor installed and is fully operational from the shipping container. Allow the transmitters to stabilize for 30 minutes and then recalibrate the device as instructed below.
Installation Considerations
The GPR-2500A consists of two circuit boards, sensor housing and sample 1/8” sample inlet and vent connections housed in a NEMA 4X rated enclosure and is suitable for mounting on any vertical flat surface.
For optimum accuracy zero and calibrate a transmitter after it has been allowed to stabilize, typically 24­36 hours after installation. Assuming the initial zero is performed according to the procedure described herein, the analyzer should not require zeroing again until the either the sensor is replaced or a change is made to the sample system or gas lines. Following the initial zero and calibration, the analyzer should not require span calibration again for up to 3 months under “normal” application conditions as described in the published specifications.
Note: As described below, zeroing the transmitter is recommended only for measurements below 1% and not practical for measurement ranges above 1%. The low end sensitivity (zero capability) has been verified at the factory; however, no ZERO OFFSET adjustment has been made. A factory adjustment would be meaningless because of the difference in sample systems and leakage factors between the factory set-up and the actual application conditions.
Assemble the necessary hardware for mounting the transmitter and optional components - such as coalescing or particulate filters and pumps, 1/8” metal or plastic tubing for interconnecting the transmitter and optional components.
Temperature: The sample must be sufficiently cooled before it enters the transmitter and any optional components. A coiled 10 foot length of ¼” stainless steel tubing is sufficient for cooling sample gases as high as 1,800ºF to ambient.
Pressure & Flow as described above
Moisture & Particulates: Prevent water and/or particulates from entering the sample system. They can clog the tubing and damage the optional components such as pumps, scrubbers or sensors. Insta llation of a suitable coalescing or particulate filter is required to remove condensation, moisture and/or particulates from the sample gas to prevent erroneous analysis readings and damage to the sensor or optional components. Consult the factory for recommendations concerning the proper selection and installation of components.
Contaminant Gases: A gas scrubber and flow indicator with integral metering valve are required upstream of the transmitter to remove interfering gases such as oxides of sulfur and nitrogen or hydrogen sulfide that can produce false readings and reduce the expected life of the sensor. Installation of a suitable scrubber is required to remove the contaminant from the sample gas to prevent erroneous analysis readings and damage to the sensor or optiona l components. Cons ult the factory for recommendations concerning the proper selection and installatio n of components.
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Mounting Pads
Gas Connections: Inlet and outlet vent gas lines require 1/8” diameter tubing preferably metal. Power Connection: Locate a source of AC power to meet area classification and to plug in the charging
adapter. Zero Calibration: Required only for very low percentage range measurements, less than 5% of full
scale at the most sensitive range of the analyzer. Span Calibra ti o n: Users are responsible for certified spa n ga s cylinder, regulator and flow control valve.
The analyzer must be calibrated with a certified span gas and regular intervals, typically every 30 days of operation.
Mounting the Analyzer
The GPR-2500A is housed in a Fiber Glass NEMA4X rated enclosure. This configuration is designed to be mounted directly to any flat vertical surface, wall or bulkhead plate with four (4 ) of the appropriate size screws. To facilitate servicing the interior of the transmitters, position it approximately 5 feet off ground level.
• Loosen the four mounting pads at the rear of the enclosure.
• Select four appropriate mounting screws (customer supplied).
• Secure the enclosure to a vertical surface approximately 5 feet from the floor or a level accessible
to service personnel. This requires the user to supply four (4) additional proper size screws and anchors.
Caution: Do not remove or discard the gaskets from either the enclosure or junction box. The transmitters design provides protection from RFI that is maintained by leaving specific
mating areas of the enclosure unpai nted to maintain conductivity of the gasket, top and bottom sections of the smaller enclosure housing the electronics. These unpainted areas are protected by gaskets and contribute to maintaining the NEMA 4 rating as well as protection from RFI/EMI. Do no t paint these areas.
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Sample Vent
Sample In
Gas Connections
The GPR-2500A with its standard flow through configuration is designed for positive pressure samples and requires connections for incoming sample a nd outgoing vent lines. T he user is responsible for calibration gases and other required components, see below.
Flow rates of 1-5 SCFH cause no appreciable change in the oxygen reading. However, flow rates above 5 SCFH generate backpressure and erroneous oxygen readings because the diameter of the integral tubing cannot evacuate the sample gas at the higher flow rate. A flow indicator with an integral metering valve upstream of the sensor is recommended as a means of controlling the flow rate of the sample gas. A flow rate of 1-2 SCFH or 0.4-1 liter per minute is recommended for optimum performance.
Caution: Do not place your finger over the vent (it pressurizes the sensor) to test the flow indicator when gas is flowing to the sensor. Removing your finger (the restriction) generates a vacuum on the sensor and may damage the sensor (voiding the sensor warranty).

Procedure of Connecting Sample Gas:

• Designate one of the bulkhead tube fittings as the VENT and the other as SAMPLE.
• Regulate the sample/span gas pressure to 5-30 PSIG.
• Connect a 1/8” vent line to the compression fitting to be used for venting the sample.
• Connect a 1/8” ZERO, SPAN or SAMPLE line to the fitting designated SAMPLE.
• If equipped with optional fittings and/or sample system, connect the ZERO and or SPAN gas
lines.
• Allow gas to flow through the transmitters and set the flow rate to 1-2 SCFH.
Installing the Oxygen Sensor
• Loosen the two (2) anchors securing the top lid of the enclosure.
• Remove the oxygen sensor from the bag.
• Screw the oxygen sensor into the sensor flow-through housing, finger tighten plus one half (1/4)
turn to ensure a good seal from the o-ring affixed to the sensor.
• Remove the shorting device (looped wire) from the receptacle located at the rear of the sensor.
• Assure the keyway registration of the female plug on the cable and male receptacle on the
sensor match up.
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• Push the female plug on to the sensor mating connector
• Screw the knurled lock nut (attached to the cable) onto to the male connector (attached to the
sensor), tighten finger tight.
• Close the front cover of the transmitter and ensure that the gasket remains in place to maintain CE approval and NEMA 4 rating.
• Secure the lid by the two (2) anchors
Proceed to calibration (see below for details).

Remote Oxygen Sensor:

Applications requiring the sensor to be located remotely from the electronics dictate the separate packaging and shipment of the electronics enclosure, oxygen sensor and sensor flow-trough housing. The appropriate length of cable to connect the sensor to the electronics is supplied and connected to the electronics. To install the remote sensor:
• Locate the sensor flow housing and note the thro ugh holes in the flanged sections.
• Identify the spot for installation.
• Using two (2) 6/32 screws of the appropriate type and length secure the
sensor flow-through housing to a flat surface.
• Remove the oxygen sensor from the bag.
• Screw the oxygen sensor into the sensor flow housing (finger tighten plus
one quarter 1/4 turn to ensure a good seal between the o-ring af fi xed to the sensor and the sensor housing.
• Remove the shorting device (looped wire) from the receptacle located at the rear of the sensor.
• Assure the keyway registration of the female plug on the cable and male receptacle on the sensor match up.
• Push the female plug (including the knurled lock nut) molded to t he cable into the male receptacle of the sensor.
• Screw the knurled lock nut (attached the cable) onto to the male connector (attached to the sensor), tighten finger tight.
Proceed to calibration (see below for details).
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Two user selectable Alarms
12-24 VDC Power In
Power Fuse
4-20 mA Signal
Power Fail Alarm
Electrical Connections
All electrical connections are located in a small jun ction box located on the side of the larger enclosure. Power at the specified rating must be supplied via a two wire shielded cable. A safety fuse is also mounted in the junction box.
Do not supply power beyond the rating. Failure to do so may permanently damage the analyzer.
The integral 4-20mA converter is internally powered and does not require external power. DO NOT supply any voltage to either of the two terminals of the 4-20mA output connector. Failure to do so will permanently damage the 4-20mA converter .
Procedure
• Remove the front cover of the junction box located on left side of the transmitters by removing the four (4) screws securing the cover and set them aside for reinstallation.
• Loosen the nut of the cable gland (customer provide and mounted at the bottom of the smaller enclosure).
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Sensor installed
• Insert power and alarm and signal output wires through the cable gland. Strip ~ ¼ inch of the wires. Insert the stripped end of wires to the appropriate terminals and secure them by tightening the screws of the terminal block. Note: Use wires that comply with local regulatory requirements.
• Thread the wires through the cable gland into the i nside of the junction box.
• Ensure the positive and negative terminals of the power supply are connected to the appropriate
terminals.
• If using shielded cables, connect the shielding of the cable to the copper ground screw inside the junction box.
• Replace the junction box cover ensuring the gaskets are in place and tighten the four ( 4) screws.
• Tighten the cable gland to maintain NEMA 4 rating .

Installation of Oxygen Sensor

The GPR-2500A Oxygen Transmitter is normally equipped with an integra l oxygen sensor. It has been tested and calibrated by the manufacturer prior to shipment and are fully operational from the shipping container. However, when the application requires a remote sensor (external to the electronics enclosure) or other special circumstances, the oxygen sensor will be packaged separately and must be installed prior to operating the transmitter. If the sensor has not been installed at the factory, it will be necessary to install the sensor in the field.
Delrin Housing with Oxygen
Note: All transmitters must be calibra ted once the installation has been completed and periodically thereafter as described below. Following the i nitial installation and calibration, allow the transmitters to stabilize for 24 hours and perform a calibration again with a certified span gas.
Caution: DO NOT open the oxygen sensor. The se nsor contains a corrosive liquid electrolyte that could be harmful if touched or ingested, refer to the Material Safety Data Sheet contained
in the Owner’s Manual appendix. Avoid contact with any liquid or crystal type powder in or around the sensor or sensor housing, as either could be a form of electrolyte. Leaking sensors should be disposed of in manner similar to that of a common battery in accordance with local regulations.
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Span Calibration

Span Gas Preparation

One of the most accurate, reliable and inexpensive means of calibrating the GPR-2500A is to expose the sensor to the 20.9% oxyg en content fou nd in ambient air. However, exposing the sensor to ambient air with the GPR-2500A flow th rough configuration requires opening the enclosure and unscrewing the sensor from its flow housing. However, many users opt to calibrate with a certified span gas which requires additional components and time.
Caution: When using a certified span gas from a span gas cylinder, do not contaminate the span gas cylinder when connecting the pressure regulator. When installing the pressure regulator, bleed the air filled regulator to flush air from the regulator before securing it on the cylinder. When using a span gas, always bleed the pressure regulator before opening the span gas to the analyzer (this requires a bypass valve at the exit of the pressure regulator valve).
Note: Always use a certified span gas with an oxygen concentration, balance nitrogen, ap proximating 50-80% of the full scale range of interest or one range above the intended measuring range. You will require the following components to deliver a span gas to the analyzer/transmitter.
Set the span gas pressure as close as possible t o t he sample gas pressure. This will assure a smooth shift from sample to span or vise versa without the need to readjust the gas flow rate.
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12-24 VDC Power In
REV 2.15
Establishing Power to Electronics
Once the two wires bringing power to the transmitter are properly connected to the terminals inside the junction box, the digital display responds instantaneously. At power-up, the transmitter performs several diagnostic system status checks termed “START-UP TEST” as illustrated below:
START-UP TES T ELECTRONICS PASS TEMP SENSOR PASS BAROMETRIC SENSOR PASS
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77 F 100 KPa
77 F 100 KPa
After initial self diagnostics, the display shows the actual oxygen concentration and analysis range a long with ambient temperature and pressure
3.30 %
Auto Range 0-10%
Menu Navigation
The four (4) pushbuttons located on the front of the transmitter operate the micro-processor: Green ENTER (select) Yellow UP ARROW Yellow DOWN ARROW Blue MENU (escape)
Main Menu Access the MAIN MENU by pressing the MENU key:
MAIN MENU
AUTO SAMPLE MANUAL SAMPLE CALIBRATE
Range Selection
The GPR-2500A transmitter is equipped with four (4) standard measuring ranges (see specification) and provides users with a choice of sampling modes. By accessing the MAIN MENU, users may select either the AUTO SAMPLING (ranging) or MANUAL SAMPLING (to lock on a single range) mo de.
Procedure – Auto Sampling
• Access the MAIN MENU by pressing the MENU key.
• Advance the reverse shade cursor using the ARROW keys to highlight AUTO SAMPLE.
• Press the ENTER key to select the highlighted menu option.
• The display returns to the sampling mode:
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Advanced Instruments, Inc.
77 F 100 KPa
77 F 100 KPa
77 F 100 KPa
77 F 100 KPa
3.30 %
Auto Range 0-10%
The display will shift to the next higher range when the oxygen reading (actually the sensor’s signal output) exceeds 99.9% of the upper limit of the current range. The display will shift to the next lower range when the oxygen reading drops to 85% of the upper limit of the next lower range.
For example, if the transmitter is reading 1% on the 0-10% range and an upset occurs, the display will shift to the 0-25% range when the oxygen reading exceeds 9.9%. Conversely, once the upset condition is corrected, the display will shift back to the 0-10% range when the oxygen reading drops to 8.5%.
Procedure – Manual Sampling
Access the MAIN MENU by pressing the MENU key. Advance the reverse shade cursor using the ARROW keys to highlight MANUAL SAMPLE. Press the ENTER key to select the highlighted menu option. The following displays appears:
MAIN MENU
AUTO SAMPLE MANUAL SAMPLE CALIBRATION CONFIG ALARMS BYPASS ALARMS
MANUAL RANGE 25% 10% 5% 1%
Advance the reverse shade cursor using the ARROW keys to highlight the desired RANGE. Press the ENTER key to select the highlighted menu option. The following display appears with the range selected and oxygen concentration of the sample gas:
3.30%
Manual Range 0-10%
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Advanced Instruments, Inc.
77 F 100 KPa
The display will not shift automatically. Instead , when the oxygen reading (actually the sensor’s signal output) exceeds 110% of the upper limit of the current range an OVER RANGE warning will be displayed.
Once the OVER RANGE warning appears the user must advance the transmitter to the next higher range via the menu and keypad Press MENU, select MANUAL SAMPLING, press ENTER, select the appropriate MANUAL RANGE and press ENTER again.
12.5% OVER RANGE
Manual Range 0-10%
Start-Up is Complete…Proceed to Calibration Zero Calibration
In theory, the oxygen sensor produces no signal output when exposed to an oxygen free sample gas. However, the transmitter will generate an oxygen reading when sampling oxygen free sample gas due to:
Contamination or quality of the zero gas Minor leakage in the sample line connections Residual oxygen dissolved in the sensor’s electrolyte Tolerances of the electronic components
Recommendation
Zero calibration is recommended for measurements below 0.1% on the 0-1% range only. At ranges above 0-1%, the overall zero offset is negligible and does not contribute any erro r in me asurements.
Procedure
• Zero calibration should precede the span calibration and once performed should not have to be repeated with sub sequent span calibrations. Normally, zero calibrations are performed when a new sensor is installed or changes are made in the sample system connections.
• The overall zero offset from oxygen dissolved in the sensor electrolyte and or from the electronics is typically less than 0.05% (on 0-1% range). This offset can be nulled by using the zero calibration. Since the magnitude of zero of fset is low, it is not necessary to perform zero i f the measurements are to be made on ranges above 0-1% range.
Caution: Prematurely zeroing the transmitter can cause a negative reading in both the ZERO
• Access the MAIN MENU by pressing the MENU key.
• Advance the reverse shade cursor using the ARROW keys to highlight CALIBRATE.
• Press the ENTER key to select the highl ighted menu option.
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Advanced Instruments, Inc.
77 F 100 KPa
77 F 100 KPa
0.005%
77 F 100 KPa
• Select ZERO CALIBRATE. The following display appears
MAIN MENU
AUTO SAMPLE MANUAL SAMPLE CALIBRATE
CALIBRATION
SPAN CALIBRATE ZERO CALIBRATE DEFAULT SPAN DEFAULT ZERO
Allow the zero gas to flow through the transmitter until a stable oxygen reading is obtained. This may take from several minutes to a few hours. It is highly recommended to monitor oxygen trend on a chart recorder to ensure that the oxygen reading has stabilized; evidenced by a horizontal trend.
Press the ENTER key to ZERO calibrate or MENU key to abort and return to SAMPLING mode.
CALIBRTION IN PROCESS
ENTER TO CALIBRATE MENUE T O ABORT
ZERO
Pressing ENTER, the analyzer will complete ZERO calibration and return to Sample mode. If you press ENTER when the oxygen reading is outside of the acceptable zero offset limit, the analyze r will fail ZERO calibration and return to the Sample mode.
PASSED
CALIBRATION
FAILED
CALIBRATION
Note: The maximum zero calibration adjustment permitted is approximately 60% of the lowest full scale
range available. Thus the maximum zero calibration adjustment or zero offset for this analyzer is 0.6% oxygen.
Factory Default Zero
The software will eliminate any previous zero calibra tion adjustment and display the actual signal output of the sensor at a specified oxygen concentration. For example, assuming a zero gas is introduced, the display will reflect an oxygen reading representing basically zero oxygen contents. However, a small oxygen reading contributed by the sensor and electronics may be seen (typically less than 2% of the full scale of the most sensitive range of the transmitter. This feature allows the user to test the integrity of the sample system, sensor and electronics without removing the sensor from the sensor housing.
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Advanced Instruments, Inc.
77 F 100 KPa
77 F 100 KPa
77 F 100 KPa
77 F 100 KPa
MAIN MENU
AUTO SAMPLE MANUAL SAMPLE CALIBRATE
CALIBRATION
SPAN CALIBRATE ZERO CALIBRATE DEFAULT SPAN DEFAULT ZERO
Span Calibration
The transmitter is generally delivered calibrated and ready to use. However, in order to obtain reliabl e data, the transmitter must be calibrated at the initial start-up and periodically thereafter. The maximum calibration interval recommended is approximately 1-3 months, or as determined by the user’s application.
Calibration involves adjusting t he transmitter electronics gain (sensitivity) to t he sensor’s signal output at a given oxygen standard, e.g. a certified span gas with an oxygen content (balance nitrogen) approximating 80% of the range of analysis or one range above the intended measuring range is recommended for optimum accuracy, see Calibration and Accuracy. Calibrat ion with ambient or instrument air (20.9%) is recommended when installing a new sensor or when a certified gas is not available.
Factory Default Span
The embedded software will remove previous span calibration data and reset the SPAN adjustment to the factory default val ue based on the average oxygen sensor’s signal output. For example, after facto ry default span, when a span gas is introduced, the micro-processor will display oxygen reading within
50% of the span gas value when the sensor signal output is within its specification. If the sensor’s
+ signal output is outside of its specification, the oxygen reading will be beyond +/-50% of the span gas value. This feature allows t he user to test the sensor’s signal output without removing it from the sensor housing.
Access the MAIN MENU by pressing the MENU key. Advance the reverse shade cursor using the ARROW keys to highlight MANUAL SAMPLE. Press the ENTER key to select the highlighted menu option. The following display appears:
MAIN MENU
AUTO SAMPLE MANUAL SAMPLE CALIBRATE
CALIBRATION
SPAN CALIBRATE ZERO CALIBRATE DEFAULT SPAN DEFAULT ZERO
Manual Span
The user must ascertain that the oxyg en reading (actually the sensor’ s signal output) has reached a stable value within the acceptable limits before completing the span adjustment. Fa ilure to do so will result in an error.
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Advanced Instruments, Inc.
77 F 100 KPa
77 F 100 KPa
77 F 100 KPa
Procedure
For calibration purposes, use of the AUTO SAMPLE mode is recommended. However, the user can select the full scale MANUAL SAMPLE RANGE – for example, a span gas with an 8% oxygen concentration with the balance nitrogen would dictate the use of the 0-10% full scale range for calibration.
Regulate the span gas pressure between 5-30 psig and set flow rate between 1-2 SCFH. Allow the span gas to flow for 1-2 minutes to purge the air trapped in the span gas line. Disconnect the sample gas line and connect the span gas line to the sample IN. The transmitter will immediately respond to the spa n gas. Typically, within 5-10 minutes, oxygen reading
will stabilize. To perform span calibration Access the MAIN MENU by pressing the MENU key. Advance the reverse shade cursor using the ARROW keys to highlight AUTO SAMPLE. Press the ENTER key to select the highlighted menu option. Advance the reverse shade cursor using the ARROW keys to highlight CALIBRATE and press ENTER. The following displays appear:
MAIN MENU
AUTO SAMPLE MANUAL SAMPLE CALIBRATE
CALIBRATION SPAN CALIBRATE
ZERO CALIBRATE DEFAULT S PAN DEFAULT ZERO
Press the ENTER key to select the SPAN CALIBRATE option. The following display will appear.
20.09%
GAS CONCENTRATION
Use the ARROW keys to enter the first digit of the span value.

Press the ENTER key to advance the underline cursor right or press the MENU key to adva nce the underline cursor left.

Repeat steps until the complete span value has been entered. After entering the span value, the following display appears

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Advanced Instruments, Inc.
20.01% SPAN
CALIBRATION IN PROGRESS
ENTER TO CALIBRATE
MENU TO ABORT
Allow approximately 5-1 0 min for oxygen to stabilize and the press ENTER to complete span gas calibration
Both the Zero Calibrate and Span Cal ibrate functions result in the following displays sho wing either 'PASSED CALIBRATION" OR "FAILED CALIBRATION"
PASSED
CALIBRATION
FAILED
CALIBRATION
In either case, the transmitter returns to the SAMPLING mode and resume sampling. Disconnect the span gas line and replace it with sample gas line. Wait 10-15 minutes to ensure the reading is stable and then proceed to sampling.
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Advanced Instruments, Inc.
100.0
4-20 mA Signal Output Adjustment
In rare instances the 4-20mA signal output ma y not agree to the reading displayed on the LCD. This feature enables the user to adjust the 4mA signal output when the LCD displa ys 0 0.0 0. Note: Adjust the 20mA signal output with the OUTPUT SPAN option described below.
Access the MAIN MENU by pressing the MENU key. Advance the reverse shade cursor using the ARROW keys to highlight CALIBRATION. Press the ENTER key to select the highlighted menu option and the following displays appear:
GAS MAIN MENU
AUTO SAMPLE MANUAL SAMPLE CALIBRATE CONFIG ALARMS BYPASS ALARMS
CALIBRATION
SPAN CALIBRATE ZERO CALIBRATE DEFAULT SPAN DEFAULT ZERO OUTPUT SPAN OUTPUT ZERO
Advance the reverse shade cursor using the ARROW keys to highlight DEFAULT ZERO. Press the ENTER key to select the highlighted menu option and the following display appears:
OUTPUT ZERO OFFSET
PRESS UP OR DOWN TO CHANGE VALUE ENTER TO SAVE MENU TO RETURN
The default setting of 100 illustrates no adjustment t o the analog output signal. Compute the adjustment value as described in Appendix B or consult the factory. The true adjustment value must be determined empirically by trial and error. Adjust the initial value to above 100 to increase the analog signal value or decrease it below 100 to decrease the analog signal.
Press the ENTER key to advance the underline cursor right or press the MENU key to advance the underline cursor left to reach to the desired digit of the OUTPUT ZERO OFFSET value.
Press the ARROW keys to enter the OUTPUT ZERO OFFSET value. Repeat the OUTPUT ZERO OFFSET routine until the output is 4 mA . Save the adjustment value by pressing the ENTER key or abort by pressing the MENU key. After
adjustment, the system returns to the SAMPLING mode. Repeat the above procedure for 20 mA signal adjustment by selecting OUTPUT SPAN adjustment instead
of OUTPUT ZERO adjustment.
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Advanced Instruments, Inc.
Sampling
GPR-2500A Oxygen Transmitter requires positive pressure to flow the samp le through the sensor housing to measure the oxygen concentration in a sample gas.
Procedure
Following calibration, the transmitter returns automatically to the SAMPLE mode. Select the desired sampling mode - Auto or if Manual, the range that provides maximum resolution – as
described above. Use metal tubing to transport the sample gas to the transmitter. The main consideration is to eliminate air leaks which can affect oxygen measurements above or below
the 20.9% oxygen concentration in ambient air - ensure the sample gas tubing connections securely connected
For sample gases under positive pressure the user must provide a means of controlling the inlet pressure between 5-30 psig and the flow of the sample gas betw een 1-5 SCFH, a flow rate of 1-2 SCHF is recommended.
For sample gases under atmospheric or slightly negative pressure an optional sampling pump is recommended to push the sample through the transmitter. Ensure that sample flow is within the recommended range; if necessary, use a flow control valve to set the sample flow.
Assure the sample is adequately vented for optimum response and re c overy – and safety. Allow the oxygen reading to stabilize for approximately 10 minutes at each sample point. Avoid drawing a vacuum on the sensor that exceeds 14” of water column pressure. Avoid excessive flow rates above 5 SCFH which generate backpressure on the sensor. Avoid the collection of particulates, liquids or condensation collect on the sensor that could block the
diffusion of oxygen into the sensor.
Standby
The transmitter has no special storage requirements. The sensor should remain connected during storage periods. Store the transmitter with the power OFF. If storing for an extended period of time, store at temperature below 45 degree C and away from direct
heat.
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Advanced Instruments, Inc.
6. Maintenance
Generally, cleaning the electrical contacts or replacing filter elements is the extent of the maintenance requirements of this transmitter.
Sensor Replacement
Periodically, the oxygen sensor will require replacement. The operating life is determined by a number of factors that are influenced by the user and therefore difficult to predict. The Features & Specifications define the normal operating conditions and expected life of the standard sen sor utilized by the GPR­2500A transmitter. Expected sensor life is inversely proportional to changes in oxygen concentration, pressure and temperature. To replace sensor, follow the procedure outlined in the section “Operation”
Serviceability: Except for replacing the oxygen sensor, there are no parts inside the transmitter for the operator to service. Only trained personnel wi th the authorizati on of their supervisor should conduct maintenance.
Caution: DO NOT open the oxygen sensor. The sensor contains a corrosive liquid electrolyte that could be harmful if touched or ingested, refer to the Material Safety Data Sheet contained in the Owner’s Manual. Avoid contact with any liquid o r crystal type po wder in or around the s ensor or sensor housing, as either could be a form of electrolyte. Leaking sensors should be disposed of in accordance with local regulations.
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7. Spare Parts
Item No.
Description
GPR-11-32-4
Oxygen Sensor (GPR-2500A)
XLT-11-24-4
Oxygen Sensor (GPR-2500A)
Item No.
Description
A-2079
Bracket Sensor Mounting
CONN-1014
Cable Sensor with Female Socket
FITN-1018
Connector SS 1/8” MNPT to 1/ 8” Tube
FITN-1039
Elbow SS 1/8”
A-3051
Housing Flow Adaptor
MTR-1010
Meter Digital Panel LCD Backlight
A-2781
Nut Sensor Retaining
Rev C4
Recommended spare parts for the GPR-2500A Oxygen Transmitter:
Other spare parts:
Advanced Instruments, Inc.
A-1161-AIS-2-
A-1166-AIS-2 Rev H PCB Assembly Power Supply / Interconnections
PCB Assembly Main / Display
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8. Trouble Shooting

Symptom

Possible Cause

Recommended Action

Advanced Instruments, Inc.
No Display
Reading does not reflect expected values
Unable to span calibrate the sensor with ambient air or with a certified span gas
Slow response time
Inadequate power supply Incorrect polarity of power input
Sensor was not calibrated at similar vent pressure, flow rate and temperature anticipated in the sample gas stream
Indication sensor signal output is outside the acceptable limit
Longer sample line Low sample flow Liquid covering sensing membrane
Ensure that power to the transmitter is within the recommended range
Ensure that the polarity of the input power matches with the designation on the power input terminal
Recalibrate the analyzer at ambient conditions that resemble with sampling conditions.
Replace sensor, see Section 6 ­Maintenance.
Reduce the sample tubing to a minimum, set sample flow between 1-2 SCFH, gently remove any liquid that might have accumulated on the sensor’s sensing side. If condensable components are present, use a coalescing filter upstream of sensor
Erratic oxygen reading
No oxygen reading
High oxygen reading
Presence of interference gases. Damaged sensor cable and or sensor
housing bring sig nal to the PCB
No signal from sensor possibly due to defective/used up sensor or broken wire connections from sensor cable or sensor housing to PCB
Inadequate contr ol of pressure and sample flow rate
Consult factory, interfering gas such as H2S might need to removed from the sample gas, replace sensor.
Replace sensor cable Replace upper section of sensor
housing
Check for any physical damag e to sensor cable and or sensor housing. Use a voltmeter and check continuity from sensor housing to the Molex connector (the connector from sensor housing to the PCB)
Check sensor signal output in air (by using a voltmeter (set to measure micro-amp current). Sensor signal in air must be within 40-60 uA (% sensor) or 450-900 uA (PPM sensor).
Set sample gas pressure within recommended range of 5-30 PSIG
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Advanced Instruments, Inc.
Zero calibration.
Cannot perform Zero calibration
Excessive back pressure on sensor caused by high sample flow
Obstruction on sample vent line
Abnormality in span gas
Leak in sample/zero gas line Inadequate zero gas flow Contaminated zero gas Attempting to Zero calibrate
prematurely
Set sample flow between 1-2 SCFH Vent sample to atmosphere If venting sample to a vent pipe with
pressure above atmosphere, consult factory for rec ommendations.
Qualify span gas with a secondary analyzer
Check for any leakage in sample/zero gas line
Check the integrity of zero gas Set the gas flow rate between 1-2
SCFH Allow sufficient time for the oxygen
reading to stabilize before attempting
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Advanced Instruments, Inc.

What is covered:

transmitter.

For how long:

One year from shipment by manufacturer or purchase from a distributor with proof of purchase.

Who is warranted:

warranty extend to more than one customer.

What we will do:

reconditioned one of the same or upgraded design.

Limitations:

to province.

What is not covered:

transmitter; fire, flood, or acts of God; or other failure to follow the O wner’s Manual.
9. Warrant Policy
Any defect in mater ial and workmanship from normal use in accordance w ith the Owner’s Manual. This warranty applies to all transmitter purchased worldwide. Advanced Instruments Inc. reserves the
right in its sole discretion to invalidate this warranty if the serial number does not appear on the
This warranty is limited to the first customer who submits a claim. Under no circumstances will the
If your Advanced Instruments Inc. transmitter is defective with respect to material and workmanship, we will repair it or, at our option, replace it at no charge to you.
If we choose to replace your Advanced Instruments Inc. transmitter, we may use new or reconditioned replacement parts.
If we choose to replace your Advanced Instruments Inc. transmitter, we may replace it with a new or
Implied warranties, including those of fitness for a par ticular purpose and merchantability (an unwritten warranty that the product is fit for ordinary use), are limited to one year from the date of shipment by manufacturer or purchase from a di stributor with proof of purchase.
Advanced Instruments Inc. will not pay for: loss of time; inconvenience; loss of use of your Advanced Instruments Inc. transmitter or property damage caused by your Advanced Instru ments Inc. transmitter or its failure to work; any special, incidental or consequential damages; or any damage re sulting from alterations, misuse or abuse; lack of proper maintenance; unauthorized repair or modification of the transmitter; affixing of any attachment not provi ded with the transmitter or other failure to follow the Owner’s Manual.
Some states and provinces do not allow limitations on how an implied warranty lasts or the exclusion of incidental or consequential damages, so the above exclusions may not apply to you. This warranty gives you specific legal rights, and you may also have other rights which vary from state to state and province
This warranty does not cover installation; defects resulting from accidents; damage while in transit to our service location; damage resulting from alterations, misuse or abuse; lack of proper maintenance; unauthorized repair or modification of the transmitter; affixing of any attachment not provided with the
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Advanced Instruments, Inc.

Sole Warranty

There are no other express warranties.

How to obtain warranty service:

warranty.
This warranty is the only one we will give on your Advanced Instruments Inc. transmitter, and it sets forth all our responsibilities regarding your Advanced Instruments Inc. transmitter.
Do-It-Yourself-Service: Call Advanced Instruments Inc. at 909-392-6900 between 8:00am and 5:00pm Pacific Time weekdays.
Trained technicians will assist you in diagnosing the problem and arrang e to supply you with the required parts.
Service from Distributors: If warranty service is provided by a distributor, Advanced Instruments Inc. will provide all required parts
under warranty at no charge to you, but the distributor is an independent business and may render a service charge for their services. Advanced Instruments Inc. will not reimburse you or otherwise be responsible for those charges.
Return to Advanced Instruments Inc.: You may obtain warranty service by returning you transmitter, postage prepaid to:
Advanced Instruments Inc. 2855 Metropolitan Place Pomona, Ca 91767 USA
Be sure to pack the transmitter securely. Include your name, address, telephone number, proof of date of purchase and a description of the operating problem. After repairing or, at our option, replacing your Advanced Instruments Inc. transmitter, we will ship it to you at no cost for parts and labor.
Your choice of any one of the service options described above is your exclusive remedy under this
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Advanced Instruments, Inc.
Product Name
Oxygen Sensor Models CAD, GPR, PSR, SAF, 67013
Synonyms
Galvanic Fuel Cell, Electrochemical Transdu ce r
Manufacturer
Analytical Industries Inc.
2855 Metropolitan Place, Pomona, CA 91767 USA
Emergency Phone Number
909-392-6900
Preparation / Revision Date
January 1, 1995
electrolyte unless otherwise noted.
Carcinogens at levels > 0.1%
None
Others at levels > 1.0%
Potassium Hydroxide, Lead
CAS Number
Potassium Hydroxide = KOH 1310-58-3, Lead = Pb 7439-92-1
Family
Boiling Point Range
100 to 115° C
Melting Point Range
KOH -10 to 0° C, Lead 327° C
Freezing Point
-40 to 0° C
Molecular Weight
KOH = 56, Lead = 207
Specific Gravity
1.09 @ 20° C
Vapor Pressure
Not applicable
Vapor Density
Not applicable
pH
> 14
Solubility in H2O
Complete
% Volatiles by Volume
None
Evaporation Rate
Similar to water
Appearance and Odor
Colorless, odorless aqueous solution
Use
Potassium Hydroxide - electrolyte, Lead - anode
Handling
Rubber or latex gloves and safety glasses
Storage
Indefinitely

10. Material Safety Data Sheet [MSDS]

Product Identification

Notes Oxygen sensors are sealed, contain protective coverings and in normal
conditions do not present a health haz ard. Information applies to

Specific Generic Ingredients

Chemical (Synonym) and

Physical Properties

Potassium Hydroxide (KOH) - Base, Lead (Pb) - Metal

General Requirem en ts

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Fire and Explosion Data

Flash and Fire Points
Not applicable
Flammable Limits
Not flammable
Extinguishing Method
Not applicable
Special Fire Fighting Procedures
Not applicable
Hazards
Stability
Stable
Instability
Incompatibility
Avoid contact with strong acids
Products
Conditions to Avoid
None
Use a fresh towel each time.
disposal
Primary Route(s) of Entry
Ingestion, eye and skin contact
.05 mg/cubic meter
Effects of Exposure -
2433 mg/kg
of vision.
burn.
Inhalation
Liquid inhalation is unlikely.
Symptoms
Eye contact - bur ning sens a ti on; Skin co nt act - soapy slick feeling.
Medical Conditions Aggravated
None
not listed; OSHA - not listed
Other
Lead is listed as a chemical known to the State of Calif ornia to cause
Advanced Instruments, Inc.
Unusual Fire and Explosion

Reactivity Data

Conditions Contributing to
Hazardous Decomposition

Spill or Leak

Steps if material is released Sensor is packaged in a sealed protective plastic bag, check the se nsor
Waste Disposal Method In accordance with federal, state and local regulations for battery
Not applicable
None
None
inside for electrolyte leakage. If the sensor leaks inside the protective plastic bag or inside a
transmitter sensor housing do not remove it without rubber or latex gloves and safety glasses and a source of water.
Flush or wipe all surfaces repeatedly with water or wet paper towel.

Health Hazard Information

Exposure Limits Potassium Hydroxide - ACGIH TLV 2 mg/cubic meter; Lead - OSHA PEL
Ingestion Electrolyte could be harmful or fatal if swallowed. Oral LD50 (RAT) =
Eye Electrolyte is corrosive and eye contact could result in permanent loss
Skin Electrolyte is corrosive and skin contact could result in a chemica l
Carcinogenic Reference Data NTP Annual Report on Carcinogens - not listed; LARC Monogra p hs -
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birth defects or other reproductive harm.

Emergency First Aid

attention immediately.
contaminated clothing; If burning persists, seek me d ical attention.
medical attention immediately.
Inhalation
Liquid inhalation is unlikely.
Ventilation Requirements
None
Eye
Safety glasses
Hand
Rubber or latex gloves
Respirator Type
Not applicable
Other Protective Equipment
None
body may contain hazardous residue.
Transportation
Not applicable
Product Name
Oxygen Sensor Models XLT
Synonyms
Galvanic Fuel Cell, Electrochemical Transdu ce r
Manufacturer
Analytical Industries Inc.
2855 Metropolitan Place, Pomona, CA 91767 USA
Emergency Phone Number
909-392-6900
Preparation / Revision Date
January 1, 1995
Information applies to electrolyte unless otherwise noted.
Carcinogens at levels > 0.1%
None
Others at levels > 1.0%
Acetic Acid, Lead
CAS Number
Acetic Acid = 64-19-7, Lead = Pb 7439-92-1
Family
Boiling Point Range
100 to 117° C
Advanced Instruments, Inc.
Ingestion
Skin Contact Wash affected area repeatedly with plenty of water; Remove
Eye Contact Flush repeatedly with plenty of water for at least 15 minutes; Seek

Special Protection Information

Special Precautions

Precautions
Do not induce vomiting; Give plenty of cold water; Seek medical
Do not remove the sensor’s pr otective Teflon and PCB coverings; Do not probe the sensor with sharp objects; Wash hands thoroughly after handling; Avoid contact with eyes, skin and clothing; Empty sensor

Product Identification

Notes Oxygen sensors are sealed, contain protective coverings and in normal
conditions do not present a health haz ard.

Specific Generic Ingredients

Chemical (Synonym) and
Acetic Acid (CH3CO2H) - Acid, Lead (Pb) - Metal

Physical Properties

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Melting Point Range
Acetic Acid = not applicable, Lead 327° C
Freezing Point
-40 to -10° C
Molecular Weight
Acetic Acid = not applicable, Lead = 207
Specific Gravity
1.05 @ 20° C
Vapor Pressure
11.4 @ 20° C
Vapor Density (air = 1)
2.07
pH
2-3
Solubility in H2O
Complete
% Volatiles by Volume
None
Evaporation Rate
Similar to water
Appearance and Odor
Colorless, vinegar-like odor aqueous solution

General Requirem en ts

Use
Acetic Acid - electrolyte, Lead - anode
Handling
Rubber or latex gloves; Safety glasses
Storage
Indefinitely
Flash and Fire Points
Not applicable
Flammable Limits
Not flammable
Extinguishing Method
Not applicable
Special Fire Fighting Procedures
Not applicable
Hazards
Stability
Stable
Instability
Incompatibility
Avoid contact with strong bases
Products
Conditions to Avoid
Heat
Use a fresh towel each time.
disposal.
Advanced Instruments, Inc.

Fire and Explosion Data

Unusual Fire and Explosion

Reactivity Data

Conditions Contributing to
Hazardous Decomposition

Spill or Leak

Steps if material is released
Not applicable
None
Emits toxic fumes when heated
Sensor is packaged in a sealed protective plastic bag, check the sensor inside for electrolyte leakage. If the sensor leaks inside the protective plastic bag or inside an transmitter sensor housing do not remove it without rubber or latex gloves, safety glasses and a source of water. Flush or wipe all surfaces repeatedly with water or wet paper towel.
Waste Disposal Method In accordance with federal, state and local regulations for battery
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Advanced Instruments, Inc.
Primary Route(s) of Entry
Ingestion, eye and skin contact
mg/cubic meter
Effects of Exposure -
6620 mg/kg
of vision.
burn.
Inhalation
Liquid inhalation is unlikely.
Symptoms
Eye contact - bur ning sens a ti on; Skin co nt act - burning sensation.
Medical Conditions Aggravated
None
not listed; OSHA - not listed
to cause cancer.
Seek medical attention immediately.
contaminated clothing; If burning persists, seek m edical attention.
medical attention immediately.
Inhalation
Liquid inhalation is unlikely.
Ventilation Requirements
None
Eye
Safety glasses
Hand
Rubber or latex gloves
Respirator Type
Not applicable
Other Protective Equipment
None
body may contain ha zardous residue.
Transportation
Not applicable

Health Hazard Information

Exposure Limits Acetic Acid - ACGIH TLV / OSHA PEL 10 (TWA); Lead - OSHA PEL .05
Ingestion Electrolyte could be harmful or fatal if swallowed; Oral LD50 (RAT) =
Eye Electrolyte is corrosive and eye contact could result in permanent loss
Skin Electrolyte is corrosive and skin contact could result in a chemical
Carcinogenic Reference Data NTP Annual Report on Carcinogens - not listed; LARC Monogr ap hs -
Other Lead is listed as a chemical known to the State of California to cause
birth defects or other reproductive harm. Lead acetate formed as the sensor is used is listed as a chemical known to the State of California

Emergency First Aid

Ingestion
Skin Contact Wash affected area repeatedly with plenty of water; Remove
Eye Contact Flush repeatedly with plenty of water for at least 15 minutes; Seek

Special Protection Information

Special Precautions

Precautions
Do not induce vomiting; Give ple n ty of cold water or if available milk;
Do not remove the sensor’s pr otective Teflon and PCB coverings; Do not probe the sensor with sharp objects; Wash hands thoroughly after handling; Avoid contact with eyes, skin and clothing; Empty sensor
39
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