YSI 1320P User Manual

OPERATIONS MANUAL
pH/ISE 1320P
pH/ISE 1320
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TruLab pH/ISE 1320(P)
PH/ISE METER
TruLab pH/ISE 1320
For the most recent version of the manual, please visit www.ysi.com.
Contact YSI
1725 Brannum Lane Yellow Springs, OH 45387 USA Tel: +1 937-767-7241
800-765-4974 Email: environmental@ysi.com Internet: www.ysi.com
Copyright © 2014 Xylem Inc.
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TruLab pH/ISE 1320 Contents
TruLab pH/ISE 1320 - Contents
1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.1 TruLab pH/ISE 1320 meter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.2 TruLab pH/ISE 1320P meter. . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
1.3 Sensors. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1 Safety information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1.1 Safety information in the operating manual . . . . . . . . . . . . 9
2.1.2 Safety signs on the meter . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1.3 Further documents providing safety information . . . . . . . . 9
2.2 Safe operation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.2.1 Authorized use. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.2.2 Requirements for safe operation . . . . . . . . . . . . . . . . . . . 10
2.2.3 Unauthorized use. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
3 Commissioning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.1 Scope of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.2 Power supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.3 Initial commissioning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.3.1 Inserting the batteries . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
3.3.2 Connecting the power pack . . . . . . . . . . . . . . . . . . . . . . . 13
3.3.3 Mounting the stand . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
4 Printer (only TruLab pH/ISE 1320 P) . . . . . . . . . . . . . . . . . . 14
4.1 Commissioning / switching the printer on or off . . . . . . . . . . . . 14
4.2 Operation / printing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.3 Printer settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.4 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.4.1 Changing the roll of paper (thermal paper) . . . . . . . . . . . 15
4.5 What to do if... / printer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
5 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
5.1 General operating principles . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
5.1.1 Keypad. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
5.1.2 Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
5.1.3 Status information (meter) . . . . . . . . . . . . . . . . . . . . . . . . 18
5.1.4 Socket field . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
5.2 Switching on the meter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
5.3 Switching off . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
5.4 Navigation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
5.4.1 Operating modes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
5.4.2 Measured value display. . . . . . . . . . . . . . . . . . . . . . . . . . 21
5.4.3 Menus and dialogs. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
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Contents TruLab pH/ISE 1320
5.4.4 Elements in menus and dialogs . . . . . . . . . . . . . . . . . . . 21
5.4.5 Example 1 on navigation: Setting the language . . . . . . . 23
5.4.6 Example 2 on navigation: Setting the date and time . . . 25
5.5 Channel display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
5.5.1 Display of several sensors in the measuring mode 27
6 pH value. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
6.1 Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
6.1.1 Measuring the pH value . . . . . . . . . . . . . . . . . . . . . . . . . 28
6.1.2 Measuring the temperature . . . . . . . . . . . . . . . . . . . . . . 30
6.2 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
6.2.1 Why calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
6.2.2 When do you have to calibrate?. . . . . . . . . . . . . . . . . . . 31
6.2.3 Automatic calibration (AutoCal) . . . . . . . . . . . . . . . . . . . 31
6.2.4 Manual calibration (ConCal) . . . . . . . . . . . . . . . . . . . . . . 34
6.2.5 Calibration points . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
6.2.6 Calibration data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
6.2.7 Continuous measurement control (CMC function) . . 40
7 ORP voltage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
7.1 Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
7.1.1 Measuring the ORP . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
7.1.2 Measuring the relative ORP . . . . . . . . . . . . . . . . . . . . . . 43
7.1.3 Measuring the temperature . . . . . . . . . . . . . . . . . . . . . . 44
7.2 ORP calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
8 Ion concentration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
8.1 Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
8.1.1 Measuring the ion concentration . . . . . . . . . . . . . . . . . . 45
8.1.2 Measuring the temperature . . . . . . . . . . . . . . . . . . . . . . 47
8.2 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
8.2.1 Why calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
8.2.2 When to calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
8.2.3 Calibration (ISE Cal). . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
8.2.4 Calibration standards . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
8.2.5 Calibration data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
8.3 Selecting the measuring method . . . . . . . . . . . . . . . . . . . . . . . 53
8.3.1 Standard addition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
8.3.2 Standard subtraction . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
8.3.3 Sample addition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
8.3.4 Sample subtraction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
8.3.5 Standard addition with blank value correction (Blank value
addition) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
9 Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
9.1 Measurement settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
9.1.1 Settings for pH measurements . . . . . . . . . . . . . . . . . . . . 66
9.1.2 Buffer sets for calibration . . . . . . . . . . . . . . . . . . . . . . . . 68
9.1.3 Calibration interval . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
9.1.4 Settings for ORP measurements . . . . . . . . . . . . . . . . . . 72
9.2 Settings for ISE measurements . . . . . . . . . . . . . . . . . . . . . . . . 73
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TruLab pH/ISE 1320 Contents
9.3 Sensor-independent settings . . . . . . . . . . . . . . . . . . . . . . . . . . 75
9.3.1 System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
9.3.2 Data storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
9.4 Reset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
9.4.1 Resetting the measurement settings . . . . . . . . . . . . . . . 76
9.4.2 Resetting the system settings. . . . . . . . . . . . . . . . . . . . . 77
10 Data storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78
10.1 Manual data storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78
10.2 Automatic data storage at intervals . . . . . . . . . . . . . . . . . . 79
10.3 Measurement data storage . . . . . . . . . . . . . . . . . . . . . . . . . . . 81
10.3.1 Editing the measurement data storage. . . . . . . . . . . . . . 81
10.3.2 Erasing the measurement data storage . . . . . . . . . . . . . 83
10.3.3 Measurement dataset. . . . . . . . . . . . . . . . . . . . . . . . . . . 83
10.3.4 Storage locations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83
11 Transmitting data (USB interface). . . . . . . . . . . . . . . . . . . . . 84
11.1 Options for data transmission . . . . . . . . . . . . . . . . . . . . . . . . . 84
11.2 Connecting a PC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
11.3 MultiLab Importer. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
12 Maintenance, cleaning, disposal. . . . . . . . . . . . . . . . . . . . . . 87
12.1 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
12.1.1 General maintenance activities . . . . . . . . . . . . . . . . . . . 87
12.1.2 Replacing the batteries. . . . . . . . . . . . . . . . . . . . . . . . . . 87
12.2 Cleaning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88
12.3 Packing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88
12.4 Disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88
13 What to do if.... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89
13.1 pH/ORP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89
13.2 ISE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91
13.3 General information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93
14 Technical data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94
14.1 Measuring ranges, resolution, accuracy . . . . . . . . . . . . . . . . . 94
14.1.1 pH/ORP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94
14.1.2 ISE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
14.2 General data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96
15 Firmware update . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98
16 Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 99
17 Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101
18 Contact Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103
18.1 Ordering & Technical Support . . . . . . . . . . . . . . . . . . . . . . . . 103
18.2 Service Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103
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Contents TruLab pH/ISE 1320
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TruLab pH/ISE 1320 Overview
3
1
2
pH 1310

1 Overview

1.1 TruLab pH/ISE 1320 meter

The compact precision pH meter TruLab pH/ISE 1320 enables you to carry out pH measurements, ORP measurements and ion selective measurements quickly and reliably.
The TruLab pH/ISE 1320 provides the maximum degree of operating comfort, reliability and measuring certainty for all applications.
The USB interface can be used for data transmission to a PC and for software updates of the meter.
1 Keypad
2 Display
3 Socket field
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Overview TruLab pH/ISE 1320
Print
er
modul
1
2
3
4
5
pH 1310P

1.2 TruLab pH/ISE 1320P meter

The integrated printer of the TruLab pH/ISE 1320 P enables to document mea­surements according to GLP requirements.
The information concerning the printer of the TruLab pH/ISE 1320 P is given in a separate chapter (see TRULAB PH/ISE 1320 P), page 14).
section 4 PRINTER (ONLY
1 Keypad
2 Display
3 Socket field
4Printer
5 Control panel of the printer

1.3 Sensors

A measuring system ready to measure consists of the TruLab pH/ISE 1320 meter and a suitable sensor.
Suitable sensors are pH electrodes, ORP electrodes and ion selective elec­trodes (ISE).
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TruLab pH/ISE 1320 Safety

2 Safety

2.1 Safety information

2.1.1 Safety information in the operating manual

This operating manual provides important information on the safe operation of the meter. Read this operating manual thoroughly and make yourself familiar with the meter before putting it into operation or working with it. The operating manual must be kept in the vicinity of the meter so you can always find the infor mation you need.
Important safety instructions are highlighted in this operating manual. They are indicated by the warning symbol (triangle) in the left column. The signal word (e.g. "Caution") indicates the level of danger:
WARNING
indicates a possibly dangerous situation that can lead to seri­ous (irreversible) injury or death if the safety instruction is not followed.
-
CAUTION
indicates a possibly dangerous situation that can lead to slight (reversible) injury if the safety instruction is not fol lowed.
NOTE
indicates a possibly dangerous situation where goods might be damaged if the actions mentioned are not taken.

2.1.2 Safety signs on the meter

Note all labels, information signs and safety symbols on the meter and in the battery compartment. A warning symbol (triangle) without text refers to safety information in this operating manual.

2.1.3 Further documents providing safety information

The following documents provide additional information, which you should observe for your safety when working with the measuring system:
Operating manuals of sensors and other accessories
Safety datasheets of calibration or maintenance accessories (such as buffer solutions, electrolyte solutions, etc.)
-
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Safety TruLab pH/ISE 1320

2.2 Safe operation

2.2.1 Authorized use

This meter is authorized exclusively for pH, ORP and ISE concentrations measurements in the laboratory.
Only the operation and running of the meter according to the instructions and technical specifications given in this operating manual is authorized (see section 14 TECHNICAL DATA, page 94).
Any other use is considered unauthorized.

2.2.2 Requirements for safe operation

Note the following points for safe operation:
The meter may only be operated according to the authorized use specified above.
The meter may only be supplied with power by the energy sources mentioned in this operating manual.
The meter may only be operated under the environmental conditions mentioned in this operating manual.
The meter may only be opened if this is explicitly described in this operating manual (example: Inserting the batteries).

2.2.3 Unauthorized use

The meter must not be put into operation if:
it is visibly damaged (e.g. after being transported)
it was stored under adverse conditions for a lengthy period of time (storing conditions, see
section 14 TECHNICAL DATA, page 94).
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TruLab pH/ISE 1320 Commissioning

3 Commissioning

3.1 Scope of delivery

pH meter TruLab pH/ISE 1320
4 batteries 1.5 V Mignon type AA
Power pack
USB cable (A plug on mini B plug)
Stand
Stand holder
Comprehensive operating manual
Short instructions
CD-ROM with
– USB drivers
– detailed operating manual
– Software MultiLab Importer

3.2 Power supply

The TruLab pH/ISE 1320 is supplied with power in the following ways:
Mains operation with the supplied power pack
Battery operation (4 x alkaline manganese batteries, type AA)
USB operation via a connected USB-B cable

3.3 Initial commissioning

Perform the following activities:
Insert the supplied batteries
For mains operation: Connect the power pack
If necessary, mount a stand
Switch on the meter
(see section 5.2 SWITCHING ON THE METER, page 19)
Set the date and time
(see section 5.4.6 EXAMPLE 2 ON NAVIGATION: SETTING THE DATE AND TIME, page 25)
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Commissioning TruLab pH/ISE 1320
1

3.3.1 Inserting the batteries

You can operate the meter either with normal batteries or with rechargeable batteries (Ni-MH). In order to charge the batteries, an external charging device is required.
1 Battery compartment
1. Open the battery compartment (1) on the underside of the meter.
CAUTION
Make sure that the poles of the batteries are positioned cor­rectly. The ± signs on the batteries must correspond to the ± signs in the battery compartment.
2. Place four batteries (type Mignon AA) in the battery compartment.
3. Close the battery compartment (1).
4. Set the date and time
(see section 5.4.6 EXAMPLE 2 ON NAVIGATION: SETTING THE DATE AND
TIME, page 25).
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TruLab pH/ISE 1320 Commissioning
1
2

3.3.2 Connecting the power pack

CAUTION
The line voltage at the operating site must lie within the input voltage range of the original power pack (see
NICAL DATA, page 94).
section 14 TECH-
CAUTION
Use original power packs only (see section 14 TECHNICAL DATA, page 94).
1. Connect the plug of the power pack to the socket for the power pack on
the TruLab
2. Connect the original power pack to an easily accessible power outlet.
pH/ISE 1320.

3.3.3 Mounting the stand

The stand base can be mounted at the right side of the meter.
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Printer (only TruLab pH/ISE 1320 P) TruLab pH/ISE 1320
2
1
3
4

4 Printer (only TruLab pH/ISE 1320 P)

1 Operating LED
– Is illuminated: Printer is switched on
Switching on the
printer
– Flashes: Printer is switched off
2 Control panel with the keys <FEED> and <ON/OFF>
3 Lever to open the paper compartment
4 Lid of the paper compartment

4.1 Commissioning / switching the printer on or off

1. Connect the power pack to the TruLab pH/ISE 1320 P.
The LED lights up green. The printer is ready for operation. or When the printer had been switched off (LED flashing): Switch on the printer with <ON/OFF>. The LED lights up green. The printer is ready for operation.
If there is a USB-B connection at the same time (e.g. to a PC), the data are output to the PC only.
Switching off the
printer
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1. Switch off the printer with <ON/OFF>.
The LED flashes. The printer is switched off.
TruLab pH/ISE 1320 Printer (only TruLab pH/ISE 1320 P)

4.2 Operation / printing

Data are only output to the printer if the following requirements are met
Data are transmitted manually or automatically (see section 11.1 OPTIONS
FOR DATA TRANSMISSION, page 84)
The printer is switched on (LED illuminated)
There is no USB connection.

4.3 Printer settings

To open the Storage & config menu, press the <ENTER_> key in the measured value display. After completing the settings, switch to the measured value dis play with <M>.
Default settings are printed in bold.
-
Menu item Possible set-
Description
ting
System / Printer / Font size
12x20
8x16 7x16
Select the font size for the printer
A print sample (font of the printer) to view the available font sizes can be output with <ON/OFF_>.
System / Printer / Print test page
- The printer prints the meter informa-
tion from the menu, System / Ser- vice information. The current printer settings are used for the printout.

4.4 Maintenance

4.4.1 Changing the roll of paper (thermal paper)

1. Pull the lever (3) until the lid (4) of the paper compartment opens.
2. If necessary, remove any remains of the old roll of paper.
3. Insert the new roll of paper. The start of the paper should poke out of the
paper compartment.
4. Close the lid (4) of the paper compartment so that it clicks into place.
5. If necessary, move the printer paper forward with <FEED>.
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Printer (only TruLab pH/ISE 1320 P) TruLab pH/ISE 1320

4.5 What to do if... / printer

Integrated printer
does not print
Cause Remedy
– Printer switched off
(LED flashing)
– Switch on the printer
(LED illuminated)
– No power pack connected – Connect the power pack
– USB cable connected – Disconnect the USB cable from the
meter
Printer operating -
paper not being
printed
Integrated printer
prints automatically
– Function "store automatically at
intervals" with long intervals is switched on
– Switch off the function (see section
10.2 AUTOMATIC DATA STORAGE AT
INTERVALS, page 79)
– No paper available – Insert a roll of paper
Cause Remedy
– Paper inserted the wrong way up – Turn the roll of paper around and
insert it with the other side upwards
Cause Remedy
– The function "store automatically
at intervals" or "transmit data automatically at intervals" is switched on
– Switch off the functions (see sec-
tion 10.2 AUTOMATIC DATA STORAGE
AT INTERVALS, page 79 or
section 11.1 OPTIONS FOR DATA
TRANSMISSION, page 84)
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TruLab pH/ISE 1320 Operation
F1
F2
STOSTO
RCL
ARAR

5Operation

5.1 General operating principles

5.1.1 Keypad

In this operating manual, keys are indicated by brackets <..> . The key symbol (e.g. <ENTER>) generally indicates a short keystroke (under
sec) in this operating manual. A long keystroke (approx. 2 sec) is indicated
2 by the underscore behind the key symbol (e.g. <ENTER__>).
<F1>: <F1__>: <F2>: <F2__>:
Softkeys providing situation dependent functions, e.g.: <F2>/[USB output]:
Outputs data to the USB interface
<F2__>/[USB output]:
Configures the automatic data output to the USB inter-
face
<On/Off>: Switches the meter on or off
<M>: Selects the measured parameter / Quits the settings
<CAL>: <CAL__>:
<STO>: <STO__>:
<RCL>: <RCL__>:
Calls up the calibration procedure Displays the calibration data
Saves a measured value manually Opens the menu for the automatic save function
Displays the manually stored measured values Displays the automatically stored measured values
Menu control, navigation
<><>: <__><__>:
Increments, decrements values Increments, decrements values continuously
<ENTER>: <ENTER__>:
Opens the menu for measurement settings / confirms entries Opens the menu for system settings
<AR> Freezes the measured value (HOLD function)
Switches the AutoRead measurement on or off
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Operation TruLab pH/ISE 1320
HOLD AR
25.0
6.093
pH
°C
4
3
2
6 7 8 9
1
AutoCal
5
12.12.2012 12:12
USB output
YSI

5.1.2 Display

1 Status information (sensor)
2 Measured value (with unit)
3 Measured parameter
4 Continuous measurement control (CMC function)
5 Channel display: Plug position of the sensor
6 Sensor symbol (calibration evaluation, calibration interval)
7 Measured temperature (with unit)
8 Status information (meter)
9 Softkeys and date + time

5.1.3 Status information (meter)

AR Stability control (AutoRead) is active
HOLD Measured value is frozen (<AR> key)
Batteries are almost empty
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TruLab pH/ISE 1320 Operation
1
2
3
7
8
9
4
5
6

5.1.4 Socket field

1 pH electrode or ion selective electrode 1
2 Reference electrode 1
3 Temperature sensor 1
4 pH electrode or ion selective electrode 2
5 Reference electrode 2
6 Temperature sensor 2
7 Mini USB-B interface
8 Power pack
9 Service interface
CAUTION
Only connect sensors to the meter that cannot return any volt­ages or currents that are not allowed (> SELV and > current circuit with current limiting). Almost all customary sensors fulfill these conditions.

5.2 Switching on the meter

1. Switch the meter on with <On/Off>. The meter performs a self-test. The display shows the manufacturer's logo while the self-test is being performed. The measured value display appears.
ba76157e01 03/2014 19
Operation TruLab pH/ISE 1320
pH
6.949
25.0
°C
12.12.2012 12:12
USB output

5.3 Switching off

1. Switch the meter off with <On/Off>.
Automatic switch-off The instrument has an automatic switch-off function in order to save the
batteries (see switches off the measuring instrument if no key is pressed for an adjustable period.
The automatic switchoff is not active
if the communication cable is connected
if the Automatic data storage function is active, or with automatic data trans-
mission
if the power pack is connected
Display illumination The meter automatically switches off the display illumination if no key is
pressed for 30 again.
You can also generally switch the display illumination on or off (see section
9.3.1 SYSTEM, page 75).
section 9.3.1 SYSTEM, page 75). The automatic switchoff
seconds. The illumination is switched on with the next keystroke

5.4 Navigation

The principles of navigation in menus and dialogs are explained in the following sections.

5.4.1 Operating modes

The meter has the following operating modes:
20 ba76157e01 03/2014
TruLab pH/ISE 1320 Operation
Operating
Description
mode
Measuring The measurement data of the connected sensor are shown
in the measured value display
Calibration The course of a calibration with calibration information, func-
tions and settings is displayed
Storage in
The meter stores measuring data automatically or manually
memory
Transmit­ting data
The meter transmits measuring data and calibration records to a USB-B interface automatically or manually
Setting The system menu or a sensor menu with submenus, set-
tings and functions is displayed
Only those displays and functions are available in the active operating mode that are currently being required.

5.4.2 Measured value display

In the measured value display, open the setting menus with <MENU/ENTER>. The current functions of the softkeys are shown on the display.
Use <MENU/ENTER> (short pressure) to open the menu for calibration and
measurement settings for the displayed measured parameter.
Use <MENU/ENTER__> (long keystroke (approx. 2 s) to open the Storage
& config menu with the sensor-independent settings.
Use the keys of the keypad to carry out further functions such as storage or cali­bration (see section 5.1.1 KEYPAD, page 17). These functions are not available in other operating situations.

5.4.3 Menus and dialogs

The menus for settings and dialogs in procedures contain further submenus.
To select a subelement, use the <><> keys. The current selection is dis-
played with a frame.
To make further settings, switch to the next higher menu level with
<F1>[Back].
Use <M> to return to the measured value display.

5.4.4 Elements in menus and dialogs

Submenus
The name of the submenu is displayed at the upper edge of the frame. Sub­menus are opened by confirming with <MENU/ENTER>. Example:
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Operation TruLab pH/ISE 1320
General Interface Clock Service information Reset
System
12.12.2012 12:12
Back
Language: Deutsch Beep: Off Illumination: On Contrast
: 50 %
Switchoff time: 1 h Temperature unit
: °C
Stability control
: On
General
12.12.2012 12:12
Back
Calibration record Calibration data storage Serial number (sensor) Buffer
: TEC
One point calibration: Yes Calibration interval
: 7 d
Unit for slope
: mV/pH
i
2.00 4.01 7.00 10.01
pH
12.12.2012 12:12
Back
Settings
Settings are indicated by a colon. The current setting is displayed on the right-hand side. The setting mode is opened with <MENU/ENTER>. Subse quently, the setting can be changed with <><> and <MENU/ENTER>. Example:
-
Functions
Messages
22 ba76157e01 03/2014
Functions are designated by the name of the function. They are immediately carried out by confirming with <MENU/ENTER>. Example: Display the Calibration record function.
Information is marked by the i symbol. They cannot be selected. Example:
TruLab pH/ISE 1320 Operation
Calibration record Calibration data storage Serial number (sensor) Buffer
: TEC
One point calibration
: Yes
Calibration interval: 7 d Unit for slope
: mV/pH
i
2.00 4.01 7.00 10.01
pH
12.12.2012 12:12
Back
pH
6.949
25.0
°C
12.12.2012 12:12
USB output
System Data storage
Storage & config
12.12.2012 12:12
Back

5.4.5 Example 1 on navigation: Setting the language

1. Press the <On/Off> key. The measured value display appears. The instrument is in the measuring mode.
ba76157e01 03/2014 23
2. Using <MENU/ENTER__>, open the Storage & config menu. The instrument is in the setting mode.
3. Select the System submenu with <><>. The current selection is displayed with a frame.
4. Open the System submenu with <MENU/ENTER>.
Operation TruLab pH/ISE 1320
General Interface Clock Service information Reset
System
12.12.2012 12:12
Back
Language: Deutsch Beep: Off Illumination
: On
Contrast
: 50 %
Switchoff time: 1 h Temperature unit
: °C
Stability control
: On
General
12.12.2012 12:12
Back
Language: Deutsch Beep
: Off
Illumination
: On
Contrast
: 50 %
Switchoff time
: 1 h
Temperature unit
: °C
Stability control: On
General
12.12.2012 12:12
Back
5. Select the General submenu with <><>.
The current selection is displayed with a frame.
6. Open the General submenu with <MENU/ENTER>.
24 ba76157e01 03/2014
7. Open the setting mode for the Language with <MENU/ ENTER>.
8. Select the required language with <><>.
9. Confirm the setting with <MENU/ENTER>. The meter switches to the measuring mode. The selected language is active.
TruLab pH/ISE 1320 Operation
Date format: dd.mm.yyyy Date
: 12.12.2012
Time
: 12:12:25
Clock
12.12.2012 12:12
Back

5.4.6 Example 2 on navigation: Setting the date and time

The measuring instrument has a clock with a date function. The date and time are shown in the measured value display. When storing measured values and calibrating, the current date and time are automatically stored as well.
The correct setting of the date and time and date format is important for the fol­lowing functions and displays:
Current date and time
Calibration date
Identification of stored measured values.
Therefore, check the time at regular intervals.
After a fall of the supply voltage (empty batteries), the date and time are reset.
The date format can be switched from the display of day, month, year (dd.mm.yyyy) to the display of month, day, year (mm/dd/yyyy or mm.dd.yyyy).
1. In the measured value display: Using <MENU/ENTER__>, open the Storage & config menu. The instrument is in the setting mode.
2. Select and confirm the System / Clock menu with <><> and <MENU/ENTER>. The setting menu for the date and time opens up.
3. Select and confirm the Time menu with <><> and <MENU/ ENTER>. The hours are highlighted.
ba76157e01 03/2014 25
4. Change and confirm the setting with <><> and <MENU/ENTER>. The minutes are highlighted.
5. Change and confirm the setting with <><> and <MENU/ENTER>. The seconds are highlighted.
6. Change and confirm the setting with <><> and <MENU/ENTER>. The time is set.
Operation TruLab pH/ISE 1320
7. If necessary, set the Date and Date format. The setting is made similarly to that of the time.
8. To make further settings, switch to the next higher menu level with [Back]<F1>. or Switch to the measured value display with <M>. The instrument is in the measuring mode.
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TruLab pH/ISE 1320 Operation
Channel display Display of the plug position for the respective parameter. The filled bar indicates for each connected sensor to which plug position of the meter it is connected.
pH
6.949
24.8 °C
12.12.2012 12:12
USB output
pH
6.966
25.0
°C
12.12.2012 12:12
USB output

5.5 Channel display

The TruLab pH/ISE 1320 manages the connected sensors and displays which sensor is plugged to which connection.

5.5.1 Display of several sensors in the measuring mode

The measured values of the connected sensors can be displayed in the follow­ing ways:
Clear display of all connected sensors
Detailed display of one sensor
(e.g. incl. CMC feature with pH sensors)
With the softkey you can very easily switch between the two display types. The suitable softkey is displayed depending on the operating situation.
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pH value TruLab pH/ISE 1320
pH
6.949
24.8 °C
12.12.2012 12:12
USB output

6 pH value

6.1 Measuring

6.1.1 Measuring the pH value

NOTE
When connecting an earthed PC/printer, measurements cannot be performed in earthed media as the values would be incorrect. The USB interface is not galvanically isolated.
To ensure the high measurement accuracy of the measuring sys­tem, always measure with a calibrated electrode (see section 6.2 CALIBRATION, page 31).
1. Connect the pH electrode to the meter.
2. If necessary, select the measured parameter with <M>.
3. When measuring without temperature sensor: Temper the test sample or measure the current temperature and enter it with <>
4. Immerse the pH electrode in the test sample. The measured value is checked for stability (automatic stability control). The display of the measured parameter flashes.
5. Wait for a stable measured value. The display of the measured parameter no longer flashes.
<>.
Stability control
(AutoRead)
& HOLD function
The stability control function (AutoRead) continually checks the stability of the measurement signal. The stability has a considerable impact on the reproduc ibility of measured values.
The measured parameter flashes on the display
as soon as the measured value is outside the stability range
when the automatic Stability control is switched off.
You can activate or switch off the automatic Stability control function (see section 9.3.1 SYSTEM, page 75).
28 ba76157e01 03/2014
-
TruLab pH/ISE 1320 pH value
1. Freeze the measured value with <AR>. The [HOLD] status indicator is displayed. The HOLD function is active.
You can terminate the Stability control function and the HOLD func- tion with <AR> or <M> at any time.
2. Using <ENTER>, activate the Stability control function manually. The [AR] status indicator appears while the measured value is assessed as not stable. A progress bar is displayed and the display of the measured parameter flashes. The [HOLD][AR] status indicator appears as soon as a stable mea­sured value is recognized. The progress bar disappears and the dis­play of the measured parameter stops flashing. The current measurement data is output to the interface. Measurement data meeting the stability control criterion is marked by AR.
Criteria for a stable
measured value
You can prematurely terminate the Stability control function manu­ally with <ENTER> at any time. If the Stability control function is prematurely terminated, the current measurement data are output to the interface without the AutoRead info.
3. Using <ENTER>, start a further measurement with stability control.
or Release the frozen measured value again with <AR> or <M>. The [AR] status display disappears. The display switches back to the previous indication.
The Stability control function checks whether the measured values are stable within the monitored time interval.
Measured
Time interval Stability in the time interval
parameter
pH value 15 seconds : better than 0.01 pH
Temperature 15 seconds : better than 0.5 °C
The minimum duration until a measured value is assessed as stable is the monitored time interval. The actual duration is mostly longer.
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pH value TruLab pH/ISE 1320

6.1.2 Measuring the temperature

For reproducible pH measurements, it is essential to measure the temperature of the test sample. You have the following options to measure the temperature:
Automatic measurement of the temperature with the temperature sensor
30 or Pt 1000) integrated in the sensor.
(NTC
Measurement by an external temperature sensor.
Manual determination and input of the temperature.
The measuring instrument recognizes whether a suitable sensor is connected and automatically switches on the temperature measurement.
The display of the temperature indicates the active temperature measuring mode:
Temperatur
e sensor
Resolution of the
temp. display
Temp. measurement
yes 0.1 °C Automatic with temperature sensor
- 1 °C Manual
If you wish to measure (or calibrate) without temperature sensor, proceed as follows:
1. Measure the current temperature of the test sample.
2. Set the temperature value with <><>. or In the <MENU/ENTER>/pH/Man. temperature menu, set the tempera- ture value with <><>.
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