Vernier Go Direct, GDX-MLT User Manual

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6. Click or tap Done to enter data­collection mode.
Connecting the Sensor
See the following link for up-to-date connection information:
www.vernier.com/start/gdx-mlt
Using the Product
Connect the sensor following the steps in the Getting Started section of this user manual.
1. Load a small portion of a solid substance into a capillary tube.
2. Carefully place the capillary tube of solid into one of the three slots in the aluminum heating block of the Melt Station. You can tilt the Melt Station toward you slightly for a better look at the heating block.
3. Tilt the Melt Station up or down slightly to get the best view of the solid sample through the viewing lens.
4. Click Collect to begin data collection. On the Melt Station, turn the control knob to the Rapid Heat area. The red LED will come on, indicating the Melt Station is heating. Rapid Heat will warm your solid sample at a rate of >10°C/min.
5. Observe the temperature vs. time graph. When the temperature is within about 10°C of the expected melting temperature of your solid sample, turn the control knob to that temperature, slowing the heating rate to ~1.5°C/min.
6. Carefully observe your sample. At the first indication of the solid melting, note and record the temperature. When the entire solid has melted, note and record the temperature. The examine line can be used to help mark these spots while monitoring the substance melting. Text can be added using the Text Annotation feature in Graphical Analysis.
7. Stop data collection. The run is automatically stored. On the Melt Station, turn the control knob to the Fan/Cooling setting. The blue LED will come on, indicating that the Melt Station is cooling.
8. Prepare a second solid sample to test. Observe the temperature of the heating block in the meter. After the heating block cools to a suitably low temperature, you can begin heating the Melt Station again.
Care and Maintenance
Cleaning Outside Surfaces
Clean the outside metal surfaces of the Melt Station with a cloth dampened with a mild detergent solution. Do not use organic solvents to clean the Melt Station.
Removing Broken Capillary Tubes
Follow the steps below to remove a broken capillary tube from the Melt Station. Caution: Do not handle a broken capillary tube with your fingers. Wear safety glasses or safety goggles.
Go Direct®Melt Station
(Order Code GDX-MLT)
The Go Direct Melt Station is a sensor used to measure the melting temperature of solid substances.
Note: Vernier products are designed for educational use. Our products are not designed nor are they recommended for any industrial, medical, or commercial process such as life support, patient diagnosis, control of a manufacturing process, or industrial testing of any kind.
What's Included
l Go Direct Melt Station l Package of 100 capillary tubes, each with a closed end l ACpower supply l Micro USBCable
Compatible Software
See www.vernier.com/manuals/gd x-mlt for a list of software compatible with the Go Direct Melt Station.
Getting Started
Please see the following link for platform-specific connection information:
www.vernier.com/start/gdx-mlt
Bluetooth C onnection USB Connection
1. Install Graphical Analysis 4 on your computer, Chromebook™, or mobile device. See www.vernier.com/ga4 for software availability.
2. Turn on your sensor by plugging in the AC power and turn the temperature knob to the cooling fan. The Bluetooth®LED will blink red.
3. Launch Graphical Analysis 4.
4. Click or tap Sensor Data Collection.
5. Click or tap your Go Direct sensor from the list of Discovered Wireless Devices. Your sensor's ID is located near the barcode on the sensor. The Bluetooth LED will blink green when it is successfully connected.
1. Install Graphical Analysis 4 on your computer or Chromebook. If using LabQuest 2, make sure LabQuest App is up to date. See www.vernier.com/ga4 for software availability or www.vernier.com/downloads to update LabQuest App.
2. Plug the sensor into AC power and turn the temperature knob to the cooling fan.
3. Connect the sensor to the USB port.
4. Launch Graphical Analysis 4 or turn on LabQuest 2. You are now ready to collect data.
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l Check the temperature of the heating block before inserting a capillary tube
of solid sample.
l The heating block can remain hot for a short period of time after use, even
when off.
l Use the Melt Station in a well-ventilated room. l The Melt Station is not designed for liquids or wet environments. l The Melt Station is not designed or intended for use with samples that could
explode or ignite by heat, friction, or spark.
l While some routine maintenance can be performed on the Melt Station,
these tasks should be performed only by qualified personnel.
l Do not use the Melt Station if any malfunction is suspected. l Do not modify or install additional parts to the Melt Station. l Unplug the Melt Station before storing.
Safety Automatic Shut Off
An important safety feature of the Melt Station is the Automatic Shut Off. After you turn the control knob to heating, an internal timer starts a 60-minute countdown. After 60 minutes have elapsed, the Melt Station will automatically turn off the heating element and the yellow LED will come on. To reset the Melt Station, simply turn the control knob to the cooling position or the Off position.
Specifications
Dimensions Base–13 cm × 15 cm × 1.5 cm, Body–9 cm × 9 cm ×
24 cm
Melt Station weight 1.0 kg (2.2 lbs.)
Melt Station + AC adapter weight: 1.2 kg (2.6 lbs.)
Range Ambient to 260°C
Temperature sensor Class A, Platinum Resistance Temperature Detector
(RTD)
Resolution 0.10°C
Accuracy ±0.31 + 0.0006T, where T is the temperature in
Celsius
Typical ±0.4°C (<200°C); ± 0.5 deg C (>200°C)
Calibration Factory calibrated
Power 24VDC to unit,universal AC adapter 100–
240 VAC 50–60 Hz input
Power consumption 40W max., < 0.5A @ 110V
Safety shut down Heating block is automatically powered down after
approximately sixty minutes of heating
1. Turn off the Melt Station and allow it to cool to room temperature. Unplug the power cord from the device.
2. Place the Melt Station unit on its back side so the capillary tube slots are as close to horizontal as possible. This will make it easier to safely remove the glass shards.
3. Remove the two threaded screws holding the lens panel in place. Set the screws and the viewing lens aside.
4. Use a 3/32 inch hex key to remove the two screws holding the metal spring fingers in place. Set the screws and spring fingers aside. Use the same hex key to loosen the screw holding the glass window in place. Slide the glass window up to remove it, and set it aside. Caution: The edges of the glass may be sharp.
5. Use an appropriate tool to carefully remove the broken capillary tube from its slot and deposit it in a glass waste container. If the capillary tube is loose in the slot, you can very carefully tip the Melt Station over to slide the tube into a waste container.
6. Replace the glass window, metal fingers, and viewing lens. Carefully tighten the screws to be snug rather than extremely tight. Remember that you may want to remove these pieces again in the future.
Safety
The Melt Station is designed for use in an academic laboratory. Its intended purpose is to determine the melting temperature of a solid substance in the temperature range between ambient and 260°C. The safety guidelines listed below must be followed strictly during the operation of this device. Failure to comply with these guidelines violates the standards of safety set forth in this document and the standards expected as good laboratory practice.
l Always wear safety goggles or safety glasses when using the Melt Station. l Do not use the Melt Station for any purpose other than its intended use,
which is to measure the melting point of a solid substance.
l Use the Melt Station under the supervision of a qualified chemistry
instructor.
l Place the Melt Station on a clean, level surface. l Make sure the Melt Station is a safe distance from solvents, containers of
liquid or gaseous substances, and sources of water.
l Do not use the Melt Station with flammable liquids or gases. l Do not allow the device to become wet. If it does, disconnect power to the
device immediately and allow it to thoroughly dry.
l Do not leave the device unattended while heating; monitor temperature at
all times.
l Turn off the Melt Station immediately after all testing is completed. l Do not alter or remove the protective metal walls that surround the heating
block of the Melt Station.
l The Melt Station is designed to operate in an upright position. l Do not touch the heating block while it is hot.
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support@vernier.com or call 888-837-6437. Support specialists will work with you to determine if the unit needs to be sent in for repair. At that time, a Return Merchandise Authorization (RMA) number will be issued and instructions will be communicated on how to return the unit for repair.
Accessories/Replacements
Item Order Code
Micro USBCable
CB-USB-MICRO
Warranty
Vernier warrants this product to be free from defects in materials and workmanship for a period of five years from the date of shipment to the customer. This warranty does not cover damage to the product caused by abuse or improper use. This warranty covers educational institutions only.
Disposal
When disposing of this electronic product, do not treat it as household waste. Its disposal is subject to regulations that vary by country and region. This item should be given to an applicable collection point for the recycling of electrical and electronic equipment. By ensuring that this product is disposed of correctly, you help prevent potential negative consequences on human health or on the environment. The recycling of materials will help to conserve natural resources. For more detailed information about recycling this product, contact your local city office or your disposal service.
The symbol, shown here, indicates that this product must not be disposed of
in a standard waste container.
Federal Communication Commission Interference Statement
This equipment has been tested and found to compl y with the limi ts for a Clas s B digi tal device, pursuant to Part 15 of the FCC rules. These li mits are designed to provide reasonable protection against harmful i nterference i n a residential ins tallation. This equipment generates, uses and c an radiate radio frequency energy and, if not install ed and used i n ac cordance with the ins tructions, may c ause harmful interference to radio communicati ons. However, there i s no guarantee that i nterference will not oc cur in a particular ins tallation. If this equipment does cause harmful i nterference to radio or televis ion reception, which can be determined by turning the equipment off and on, the user is encouraged to try to correct the interference by one or more of the following measures:
Reorient or relocate the receivi ng antenna.
Increase the separation between the equipment and receiver.
Connect the equi pment into an outlet on a ci rcuit different from that to which the recei ver is c onnected.
Consult the dealer or an experienced radio/TV technici an for hel p.
FCC Caution
This devi ce complies with Part 15 of the FCC Rules. O peration is s ubject to the following two conditi ons:
(1)thi s device may not c ause harmful interference and
(2)thi s device must accept any interference received, includi ng interference that may c ause undes ired operation
RF Exposure Warning
The equipment compl ies with RF ex posure li mits set forth for an unc ontrolled envi ronment.The antenna(s)us ed for thi s transmitter must not be co-located or operating in conjuncti on with any other antenna or transmitter. You are cauti oned that changes or modificati ons not expressly approved by the party responsibl e for c ompliance could void your authority to operate the equipment.
IC Statement
This devi ce complies with Industry Canada lic ense-exempt RSS s tandard(s).Operation is subj ect to the fol lowing two conditi ons:
(1)thi s device may not c ause i nterference, and
Capillary tubes 1.4–1.8 mm outside diameter, 100 mm length
Capillary tube slots 3
Viewing lens 27 mm diameter (functional), 30 mm (actual)
Lighting of capillary slots
3 white LEDs
Lighting of control dial Red LED (indicates heating mode), blue LED
(indicates cooling mode with cooling fan running), yellow LED (safety shut off activated)
How the Sensor Works
The Melt Station contains an aluminum heating block. There are three slots for capillary tubes in the heating block. A capillary tube containing a solid substance is placed in the heating block and the block is heated by an embedded element. An RTD-based temperature sensor, also embedded in the heating block, measures the temperature of the heating block and therefore the capillary tube of substance. The temperature sensor connects to Vernier data­collection software. The substance to be melted is viewed through a 6X lens.
The temperature control on the Melt Station is divided into three regions.
l The first area, next to the Off position, is for cooling the heating block after
you have completed a melting temperature run. When you turn the control knob to the cooling position, the fan and the blue LED will come on.
l The second area is divided into specific temperature settings. These
temperatures correspond to the expected melting temperature of the substance. You will choose one of these settings when the Melt Station has warmed to within about 10°C of the expected melting temperature of your solid sample. The warming rate will slow to ~1.5°C/min at each of these settings.
l The third area is Rapid Heat. In Rapid H eat, the Melt Station will warm at a
rate of >10°C/min.
Calibration
The temperature sensor embedded in the aluminum heating block of the Melt Station will never need to be calibrated. The sensor is carefully calibrated before it ships, and this unique calibration is stored on a smart chip in the sensor. Note: There is no method to perform a calibration of this sensor in any of our software programs.
Troubleshooting
For troubleshooting and FAQs, see www.vernier.com/til/3852
Repair Information
If you have followed the troubleshooting steps and are still having trouble with your Go Direct Melt Station, contact Vernier Technical Support at
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(2)thi s device must accept any interference, includi ng interference that may cause undesired operation of the dev ice.
Industry Canada - ClassB This digital apparatus does not exceed the Class B l imits for radio noise emissi ons from digital apparatus
as s et out in the i nterference-causing equipment standard entitl ed “Digital Apparatus,” ICES-003 of Industry Canada. O peration is subj ect to the following two conditi ons: (1)thi s device may not c ause i nterference, and
(2)thi s device must accept any interference, includi ng interference that may cause undesired operation of the dev ice.
To reduce potential radio i nterferenceto other users, the antenna type and its gain should be so c hosen that the equiv alent isotropicall y radiated power (e.i.r.p.)i s not more than that permitted for s uccess ful communication.
RF exposure warning: The equi pment compli es with RF exposure limits s et forth for an uncontrolled environment. The antenna(s) used
for this transmitter must not be co-located or operating in conj unction with any other antenna or transmitter.
Le présent appareil est conforme aux CNR d’Industrie Canada applicabl es aux appareils radio exempts de li cence. L’exploi tation es t autorisée aux deux conditions sui vantes :
(1)l ’appareil ne doit pas produire de brouill age, et
(2)l ’appareil doit ac cepter tout i nterférence radioélectrique, même s i cela résulte à un brouillage suscepti ble d’ en compromettre le fonctionnement.
Cet appareil numérique respecte les l imites de bruits radioélec triques appli cables aux appareils numériques de Classe B prescrites dans la norme s ur le matériel i nterférant-brouilleur: “Appareils Numériques,”NMB-003 édic tée par i ndustrie Canada. L’ utilis ation es t s oumise aux deux condi tions suivantes:
(1)c et appareil ne peut causer d’interférences, et
(2)c et appareil doit accepter toutes interférences, y c omprises c elles sus ceptibles de provoquer un dis fonctionnement du disposi tif.
Afin de réduire les i nterférences radio potentiell es pour les autres util isateurs, le type d’ antenne et s on gain doiv ent être choi sie de tel le façon que l’équiv alent de puis sance isotrope émis (e.i.r.p) n’est pas plus grand que celui permis pour une c ommunication établie.
Avertissement d’exposition R F: L’équipement es t conforme aux l imites d’expos ition aux RF établies pour un env ironnement non
supervisé. L’antenne (s) uti lis ée pour ce transmetteur ne doit pas être jumel és ou fonctionner en conjonc tion av ec toute autre antenne ou transmetteur.
Note: This product is a sensiti ve measurement device. For best results, use the cables that were provided. Keep the devi ce away from
electromagnetic noi se s ources, s uch as mi crowaves, monitors, electric motors, and applianc es.
Vernier Software & Technology
13979 SW MillikanWay • Beaverton, OR 97005-2886
Toll Fr ee (888) 837- 6437 • (503) 277- 2299 • F ax ( 503) 277-2440
info@vernier.com • www.vernier.com
Rev. 04/ 02/ 18
Go Direct, Graph ical Analys is, LabQuest , and oth er marks shown are ou r t rademarks or regist ered t rademarks i n the United States . All ot her marks not own ed by us that appear herein are the p roperty of their respective owners, who may or may not be affiliated wit h, con nected to, o r sp onso red b y u s.
The Bl uetoo th®word mark and logo s are reg ist ered trademarks own ed by th e Bluet oot h SIG, Inc. and any u se o f such marks b y V ernier Soft ware & T echnol ogy is under license. Other trademarks and trade names are t hos e of their respectiv e ow ners.
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