PORTABLE ATOMIZER
AEROSOL GENERATOR
MODEL 3079A
OPERATION AND SERVICE MANUAL
P/N 6007492, REVISION A
JANUARY 2014
PORTABLE ATOMIZER
AEROSOL GENERATOR
MODEL 3079A
OPERATION AND SERVICE MANUAL
Safety
Introduction
1
Product
Description
2
Operation and
Maintenance
3
Troubleshooting
4
Applications
5
Specifications
6
Appendix
7
Part Number
6007492 / Revision A / January 2014
Copyright
TSI Incorporated / 2014 TOPAS GmbH. All rights reserved. / 225 14 10 EHW
Reproduction, reprinting or translation of this manual in whole or in part, in any form or by
any means is prohibited without the written permission of TSI Incorporated and TOPAS
GmbH.
Address
TSI Incorporated / 500 Cardigan Road / Shoreview, MN 55126 / USA
Fax No.
651-490-3824
E-mail Address
particle@tsi.com
Limitation of Warranty
and Liability
(effective June 2011)
(For country-specific terms and conditions outside of the USA, please visit www.tsi.com.)
Seller warrants the goods sold hereunder, under normal use and service as described in the
operator's manual, shall be free from defects in workmanship and material for twelve (12)
months, or if less, the length of time specified in the operator's manual, from the date of
shipment to the customer. This warranty period is inclusive of any statutory warranty. This
limited warranty is subject to the following exclusions and exceptions:
a. Hot-wire or hot-film sensors used with research anemometers, and certain other
Service Policy
Knowing that inoperative or defective instruments are as detrimental to TSI as they are to
our customers, our service policy is designed to give prompt attention to any problems. If
any malfunction is discovered, please contact your nearest sales office or representative, or
call TSI at 1-800-874-2811 (USA) or 651-490-2811 or TSI Instruments Ltd. +44 1494 459
200.
Trademarks
TSI logo and TSI Incorporated are registered trademarks of TSI Incorporated. Scanning
Mobility Particle Sizer is a trademark of TSI Incorporated. TOPAS is a registered trademark
of TOPAS Advanced Polymers.
components when indicated in specifications, are warranted for 90 days from the date of
shipment;
b. Pumps are warranted for hours of operation as set forth in product or operator’s manuals;
c. Parts repaired or replaced as a result of repair services are warranted to be free from
defects in workmanship and material, under normal use, for 90 days from the date of
shipment;
d. Seller does not provide any warranty on finished goods manufactured by others or on any
fuses, batteries or other consumable materials. Only the original manufacturer's warranty
applies;
e. Unless specifically authorized in a separate writing by Seller, Seller makes no warranty with
respect to, and shall have no liability in connection with, goods which are incorporated into
other products or equipment, or which are modified by any person other than Seller.
The foregoing is IN LIEU OF all other warranties and is subject to the LIMITATIONS stated
herein. NO OTHER EXPRESS OR IMPLIED WARRANTY OF FITNESS FOR PARTICULAR
PURPOSE OR MERCHANTABILITY IS MADE. WITH RESPECT TO SELLER’S BREACH
OF THE IMPLIED WARRANTY AGAINST INFRINGEMENT, SAID WARRANTY IS LIMITED
TO CLAIMS OF DIRECT INFRINGEMENT AND EXCLUDES CLAIMS OF CONTRIBUTORY
OR INDUCED INFRINGEMENTS. BUYER’S EXCLUSIVE REMEDY SHALL BE THE
RETURN OF THE PURCHASE PRICE DISCOUNTED FOR REASONABLE WEAR AND
TEAR OR AT SELLER’S OPTION REPLACEMENT OF THE GOODS WITH NONINFRINGING GOODS.
TO THE EXTENT PERMITTED BY LAW, THE EXCLUSIVE REMEDY OF THE USER OR
BUYER, AND THE LIMIT OF SELLER'S LIABILITY FOR ANY AND ALL LOSSES, INJURIES,
OR DAMAGES CONCERNING THE GOODS (INCLUDING CLAIMS BASED ON
CONTRACT, NEGLIGENCE, TORT, STRICT LIABILITY OR OTHERWISE) SHALL BE THE
RETURN OF GOODS TO SELLER AND THE REFUND OF THE PURCHASE PRICE, OR,
AT THE OPTION OF SELLER, THE REPAIR OR REPLACEMENT OF THE GOODS. IN THE
CASE OF SOFTWARE, SELLER WILL REPAIR OR REPLACE DEFECTIVE SOFTWARE
OR IF UNABLE TO DO SO, WILL REFUND THE PURCHASE PRICE OF THE SOFTWARE.
IN NO EVENT SHALL SELLER BE LIABLE FOR LOST PROFITS OR ANY SPECIAL,
CONSEQUENTIAL OR INCIDENTAL DAMAGES. SELLER SHALL NOT BE RESPONSIBLE
FOR INSTALLATION, DISMANTLING OR REINSTALLATION COSTS OR CHARGES. No
Action, regardless of form, may be brought against Seller more than 12 months after a cause
of action has accrued. The goods returned under warranty to Seller's factory shall be at
Buyer's risk of loss, and will be returned, if at all, at Seller's risk of loss.
Buyer and all users are deemed to have accepted this LIMITATION OF WARRANTY AND
LIABILITY, which contains the complete and exclusive limited warranty of Seller. This
LIMITATION OF WARRANTY AND LIABILITY may not be amended, modified or its terms
waived, except by writing signed by an Officer of Seller.
ii
Contents
Safety ...................................................................................................................................................... v
1 Introduction ...................................................................................................................................... 1-1
2 Product Description ........................................................................................................................ 2-1
Adjusting the Particle Production Rate by Regulation of the Volumetric Flow Rate ...................... 2-4
3 Operation and Maintenance ........................................................................................................... 3-1
Packing/Unpacking ........................................................................................................................ 3-1
Operation........................................................................................................................................ 3-1
Transport ........................................................................................................................................ 3-2
Maintenance ................................................................................................................................... 3-2
Changing the Internal HEPA Filter .......................................................................................... 3-2
4 Troubleshooting .............................................................................................................................. 4-1
5 Applications ..................................................................................................................................... 5-1
Testing HEPA/ULPA Filters ........................................................................................................... 5-1
Calculation of the Particle Concentration in the Produced Test Aerosol ....................................... 5-2
Calculation for the Adjustment of Model 3079A Aerosol Volume Flow Rate ................................. 5-3
PSL Aerosols ................................................................................................................................. 5-3
Generation of Tracer Particles ....................................................................................................... 5-4
Generation of Salt Aerosols ........................................................................................................... 5-4
Applications ............................................................................................................................. 5-5
6 Specifications .................................................................................................................................. 6-1
Instrument Specifications ............................................................................................................... 6-1
Specification of Generated DEHS Aerosol at Flow Rate of 250 L/h .............................................. 6-1
Accessories .................................................................................................................................... 6-2
7 Appendix .......................................................................................................................................... 7-1
Periodic Testing of Particulate Matter Air Filters in Cleanroom Equipment ................................... 7-1
Recommendations for Carrying out the Leak Test with only one Particle Counter (Figure 8) ...... 7-2
Estimating the Particle Concentration of the Test Aerosol ............................................................ 7-3
Calculation Formula for Two Types of Laminar Flow Boxes ................................................... 7-3
Aerosols Produced by the Aerosol Generator (no dilution) ..................................................... 7-4
Example ................................................................................................................................... 7-4
Used Symbols and Indices ............................................................................................................. 7-5
Physical Data of DEHS .................................................................................................................. 7-7
Physical Data of Emery 3004 ......................................................................................................... 7-8
Life Time of Aerosol ....................................................................................................................... 7-8
Characteristics of the Model 3079A ............................................................................................... 7-9
Flowmeter Calibration .................................................................................................................. 7-10
Disposal of End-of-Life Equipment .............................................................................................. 7-11
EC Declaration of Conformity ....................................................................................................... 7-12
iii
Contents
(This page intentionally left blank)
iv Model 3079A
Safety
C a u t i o n
Fire and explosion hazard!
The apparatus must NOT be used in explosive environments and NOT with highly
inflammable aerosol substances (pay attention to the data in the corresponding
safety data sheet).
C a u t i o n
Please read this instruction manual carefully before using the device. TSI Inc.
does not assume any liability for damages caused by improper operation,
application, cleaning or use of unsuitable materials.
The atomizer aerosol generator Model 3079A is an instrument for producing test aerosols with known
properties (according to guideline VDI 3491) e. g., for filter testing and for validation of cleanrooms.
Appropriate aerosol substances are fluids, preferably DEHS and Emery 3004 (PAO) (size of the
generated particles mainly in the range of 0.1 to 0.3 µm). Furthermore the device is applicable for
generating latex or salt aerosols.
The Model 3079A is only applicable for generating droplet aerosols, not for dusts.
All responsibility regarding the handling of the aerosol substance and the application of the generated
aerosols must be assumed by the user.
The implementation of appropriate safety precautions as well as the assessment of risk of biological
substances is in the accountability of the user.
The user assumes full responsibility in case of the use of radioactive substances. (Applicable
regulations for workplace risks according to Radiation Protection Ordinance and other appropriate
regulations have to be followed.) The implementation of appropriate safety precautions as well as the
assessment of risk of radioactive substances is in the accountability of the user.
v
Safety
(This page intentionally left blank)
vi Model 3079A
1 Introduction
The Model 3079A Atomizer Aerosol Generator is an instrument for producing test aerosols with known
properties according to German guideline VDI 3491. When DEHS is used as aerosol substance the
instrument is suitable for use as verifying instrument in cleanrooms according to standards VDI 2083
and EN 14644. The generated particles are in the range of the Most Penetrating Particle Size (MPPS)
between 0.1 and 0.3 µm and thereby guarantee a safe evaluation of high performance filters.
The design and implemented technological features guarantee the production of aerosols with
constant particle size distribution and concentration with a high reproducibility.
The Model 3079A can also produce Latex or salt aerosols. In this case, a diffusion dryer Model 3062 is
recommended to be used downstream of the aerosol generator in order to remove remaining water
droplets or prevent their formation.
1-1
Chapter 1
(This page intentionally left blank)
1-2 Model 3079A
2 Product Description
The Model 3079A Portable Atomizer Aerosol Generator is built for mobile use and has a very compact
and rugged design. It can be operated with a minimum of other utilities, i.e., no compressed air supply
is required.
Its design is focused on long life, high availability and robustness of the device.
The device is very suitable for cleanroom applications because it can easily be cleaned and
disinfected.
All pressure tubes of the atomizer are protected by the sheet steel casing against any exposure from
the outside. A pressure relieve valve protects the glass vessel.
Figure 1: Portable Atomizer Aerosol Generator Model 3079A with Adjustable Aerosol Flow Rate
2-1
Chapter 2
M
Silencer
Valve
Compressor
HEPA Filter
Atomizer
Atomizer vessel
with suspension
Flowmeter
with adjustable
needle valve
The socket for the power supply, the On / Off Switch, and the flowmeter with needle valve for adjusting
the aerosol flow rate are located at the front-side of the aerosol generator. To fill up the aerosol glass
vessel, unscrew the lid and remove the vessel. The instrument will be ready for operation within a very
short period of time.
A low-noise compressor produces the compressed air required for generating the aerosol. The air is
cleaned by a HEPA-filter before it is introduced to the atomizer.
The aerosol flow rate can be adjusted in the range of 60…300 L/h. This way the particle production
can be adapted to the corresponding application.
To adjust the aerosol flow rate of this model, use the needle valve on top of the flowmeter.
A pressure relief valve is integrated in the head of the atomizer to protect the glass vessel against
excess pressure if the outlet is blocked.
Figure 2: Schematic of the Model 3079A, Aerosol Flow Rate Adjustable
2-2 Model 3079A
Product Description
The newly developed atomizer is the key part of the Model 3079A (registered design GS 9408604.4).
It is made of high-quality stainless steel and works as a two-stream nozzle, based on the injection
principle. The unique feature is that the outlet points towards the wall of the glass vessel which works
as the baffle plate. This particle impaction section removes coarse spray droplets and results in a
particle size distribution mainly below 1 µm.
Figure 3: Components of the Atomizer
Model 3079A 2-3
Chapter 2
1,0E+08
1,0E+09
1,0E+10
1,0E+11
0 10 20 30 40
Scale
Particle/min (>0,3µm)
Adjusting the Particle Production Rate by Regulation of the Volumetric Flow Rate
The particle production rate of the Model 3079A is adjustable. This adjustment can be done with the
integrated needle valve and will be shown on the flow meter.
Closing the needle valve will throttle the volumetric flow rate and the operating point of the
Model 3079A will be altered. Lower volumetric flow rates will lead to a reduced particle production rate.
The following figure shows the correlation between the volumetric flow rate and the particle
production rate.
The particle production rate can be adjusted over a wide range of up to 300 times the minimum
concentration. Over the whole concentration range a high accuracy and reproducibility is given.
Figure 4: Correlation between Volumetric Flow Rate and Particle Production Rate
2-4 Model 3079A
3 Operation and Maintenance
Qty
Description
Model/Part Number
1
Atomizer Aerosol Generator
3079A
1
Power cord
1 Operation and Service Manual
6007492
C a u t i o n
Before using the instrument, remove the yellow protection cap from the aerosol
outlet.
C a u t i o n
Before start-up make sure the aerosol outlet is open. During operation ensure that
the produced aerosol can freely escape through tubes connected to the atomizer
outlet and that there are no bends in the outlet tubes.
The needle valve at the flowmeter must not be closed completely.
Packing/Unpacking
Use the information in this chapter to unpack and set up the Model 3079A Portable Atomizer Aerosol
Generator.
The packing list below shows the components shipped with the Model 3079A.
If anything is missing or appears to be damaged, please contact TSI immediately.
Operation
The aerosol generator should be placed on a rigid and even surface.
The atomizer glass vessel can be unscrewed and removed in order to be filled with aerosol substance.
For normal operation the volume of aerosol substance should be between 10 ml and 80 ml. A constant
aerosol production is ensured up to a minimum filling level of 10 ml.
For power supply, connect the power cord to the standard socket. The generator has a standardized
low-temperature device socket (IEC/EN 60320-1) as well as an integrated large range power supply
unit.
To stop and start operation, press the power switch.
3-1
Chapter 3
C a u t i o n
Be careful when transporting the Model 3079A with filled liquid vessel. Liquid may
run out via the aerosol outlet if the instrument is tilted too much.
W A R N I N G
Risk of electric shock. Disconnect power cord before opening.
Transport
The Model 3079A can be transported using the attached handle. The design of the casing ensures
safe carrying of the device.
Maintenance
The operation of the Model 3079A is maintenance free. Regular cleaning of the atomizer nozzle is
recommended. To clean the atomizer nozzle, unscrew the atomizer nozzle and clean it in an ultrasonic
bath or with compressed air. Avoid using sharp tools.
Note: After reassembling the nozzle, check the proper position of the O-rings.
Changing the internal HEPA filter can be done by the user (see “Changing the Internal HEPA Filter”
below).
Please contact TSI for all other service and maintenance.
Changing the Internal HEPA Filter
To change the internal filter cartridge, first open the Model 3079A. Follow these steps:
1. Unscrew the eight (8) screws at the sides of the casing with a Phillips screwdriver
2. Pull the aerosol generator casing from the chassis.
3. Remove the filter cartridge from the tubes and replace with a new one.
Note: Contact TSI to get new filter cartridge. Do NOT use any other filter product.
Reassembly of the casing is done in reverse order.
3-2 Model 3079A
4 Troubleshooting
Error Message/Symptom
Problem
Recommendation
No aerosol
No aerosol substance
Check level of aerosol
substance in atomizer vessel
Pump does not work
No power supply
Defect in the pump or power
supply unit
Exchange of fine fuses
Service
Flow rate by far lower than
300 L/h
Incorrect position of the
atomizer glass vessel
Flat gasket missing
Atomizer nozzle is blocked
Pressure drop of the HEPA
filter is too high
Check correct position of
glass vessel
Replace flat gasket
Clean atomizer nozzle
Change HEPA filter cartridge
Flow rate much higher than
300 L/h
Nozzle assembly may be
leaking
Test for leaks
4-1
Chapter 4
(This page intentionally left blank)
4-2 Model 3079A
5 Applications
0
1E+6
2E+6
3E+6
4E+6
5E+6
6E+6
7E+6
0 0,2 0,4 0,6 0,8
Particle size, µm
Concentration, Particle/cm³
Testing HEPA/ULPA Filters
A very important application for the Model 3079A is the testing of high efficiency filters, and the
verification of cleanrooms and laminar flow boxes.
The produced aerosol was analyzed by extensive measurements by means of a Scanning Mobility
Particle Sizer™ System; TSI Inc.). The resulting particle size distribution is shown in the following
diagram.
Figure 5: Particle Size Distribution of a DEHS Aerosol Measured by the Scanning Mobility Particle Sizer
The produced DEHS aerosols features very high particle concentration (>107 particles/cm3) for particle
sizes close to the so-called most penetrating particle size MPPS (0.1...0.3µm). The particle
concentration is also sufficiently high (1.5 107particles/cm3) in the measuring range of most optical
particle counters (0.3...0.5µm).
The following table shows the Model 3079A flow rates to adjust for various volumetric flow rates
through systems at three different particle concentrations. The particle concentrations assumed here
are well above the required concentrations as specified in the VDI 2083-3 and EN 14644-3 standards
and thereby enable the determination of the optimum scanning velocity with a sampling probe from
appropriate diagrams.
5-1
Chapter 5
Requested Particle Concentration in Test Aerosol, Particles/m³
Particle Concentration
in Total Flow
300 x 106 Particles/m
3
400 x 106 Particles/m
3
1000 x 106 Particles/m
3
Flow Rate Flow Rate Generator Flow Rate Generator Flow Rate Generator
Equipment, m3/h
L/h L/h L/h
50 91 92 98
100 94 96 107
200 100 104 128
300 105 111 150
600 123 136 226
700 130 145 259
800 136 154 296
900 143 164
1000 150 173
1200 164 193
1500 186 226
1600 193 237
1800 209 267
1900 217 281
2000 226 296
2200 243
2500 278
2800 311
C
total
=
AG
V
x
CAG
/
Unit
V
Particles/m3
L/h Particles/m3
m3/h
C
total
= x
2.7 x 109
/
C
total
=
Particles/m3
Calculation of the Particle Concentration in the Produced Test Aerosol
If other settings are requested, the formula shown below can be used to calculate the total
concentration in the test aerosol.
By entering the flow rate of the Model 3079A Aerosol Generator and the total flow rate, the generated
concentration in the test aerosol can be easily calculated as follows:
The conversion of the units has been considered in the formula.
5-2 Model 3079A
Applications
AG
V
=
Unit
V
x
C
ges
/
CAG
L/h m3/h
Particles/m3
Particles/m3
AG
V
= x /
2.7 x 109
AG
V
=
L/h
Calculation for the Adjustment of Model 3079A Aerosol Volume Flow Rate
The following formula allows the calculation of the Model 3079A flow rate that needs to be adjusted in
order to achieve a certain particle concentration in the test aerosol.
Entering the requested particle concentration and flow rate through the system will yield the flow rate
that needs to be adjusted on the needle valve.
The conversion of the units has been considered in the formula.
PSL Aerosols
The Model 3079A Aerosol Generator makes it possible to produce PSL aerosols according to certain
particle size standards.
For this purpose put a suitable latex suspension in the cleaned atomizer bottle. The concentration of
the PSL suspension is determining the number concentration of the produced aerosol.
Figure 6: Measurement Results of a 2,02 µm PSL Aerosol
Production of PSL aerosols with the Model 3079A is possible up to particle sizes of 3 µm. Due to the
excellent separation characteristics of the integrated baffle it is possible to prevent the formation of
agglomerates.
Model 3079A 5-3
Chapter 5
0%
20%
40%
60%
80%
100%
0,01 0,1 1 10 100
Particle diameter, µm
Cumulative mass
distribution
Calculated distribution of
a 200ppm NaCl-solution
measured
primary droplet size
distribution for H2O
Generation of Tracer Particles
The continuous and stable generation of particles is important when using optical methods for
measuring flow velocities and distributions. The Model 3079A meets these requirements and makes it
also suitable for tracer particle generation.
Generation of Salt Aerosols
The Model 3079A Atomizer Aerosol Generator is also suitable for salt aerosol production. The
resulting particle size dp depends on the droplet size generated by the atomizer dd and can be varied
by altering the salt solution concentration c according to the following equation:
In the diagram below, a calculated particle size distribution for a salt solution with a concentration of
200 ppm (e.g. 200 mg NaCl/1l H2O) is shown and compared with the droplet particle size distribution
of water which has been characterized by means of the “residual technique.”
The residual technique is very useful for characterizing droplet distributions of water, for instance,
which evaporates very quickly under normal conditions. In this method the produced droplet aerosol is
completely dried and the residual distribution is measured afterwards. From this residual distribution
the droplet distribution can be recalculated using the given equation.
Note: If liquids like water are atomized over longer periods (>1hour), the equipment connected to the
5-4 Model 3079A
Figure 7: Recalculated Size Distribution
Model 3079A cools down below the saturation temperature. In this case, droplets will
inevitably condense again. It is recommended to use a diffusion dryer and heat the connected
aerosol tubes for such applications.
Applications
Concentration of Salt Solution
Residual Size for
1 µm Droplet
Residual Size for
5 µm Droplet
5.000%
50000 ppm
0.368 µm
1.842 µm
1.000%
10000 ppm
0.215 µm
1.077 µm
0.500%
5000 ppm
0.171 µm
0.855 µm
0.100%
1000 ppm
0.100 µm
0.500 µm
0.020%
200 ppm
0.058 µm
0.292 µm
0.010%
100 ppm
0.046 µm
0.232 µm
0.005%
50 ppm
0.037 µm
0.184 µm
0.001%
10 ppm
0.022 µm
0.108 µm
The following table gives an overview of the expected particle size depending on salt solution
concentration and primary droplet size.
Applications
Generation of very fine aerosols with particle diameters <100 nm
Filter testing
Model 3079A 5-5
Chapter 5
(This page intentionally left blank)
5-6 Model 3079A
6 Specifications
Flow rate
max. 300 L/h
Temperature range
10°C ... 30°C
Max. counter pressure
20kPa (0.2bar)
Opening pressure of the relief valve
max. 90 kPa (0.9 bar)
(see certificate of instrument testing)
Aerosol substances
DEHS, Emery 3004 (PAO), Paraffin, PSL, Salt
solutions
Filling amount
min. 10 ml, max. 80 ml
Aerosol outlet
Quick connector, 8 mm
Device fuse
fuse 5x20 - 2A fast-acting
Power supply
100 ... 240 V AC
Dimensions
300 x 120 x 195 mm
Weight
4.8 kg
Number concentration
>108 particles/cm3
Number concentration (0.2 µm)
2 107 particles/cm3
Number concentration (0.5 µm)
5 105 particles/cm3
Number concentration (1 µm)
1 105 particles/cm3
Number concentration (class 0.3 … 0.5 µm)
1.5 10
7
particles/cm3
Number concentration (class 0.5 … 1.0 µm)
8 10
6
particles/cm3
Peak diameter (mode)
0.1 ... 0.5 µm
Mass flow rate
2.5 g/h
Max. continuous operation time
25 h (with 80 ml aerosol substance in vessel)
Instrument Specifications
Specification of Generated DEHS Aerosol at Flow Rate of 250 L/h
6-1
Chapter 6
Atomizer glass vessel
Model 3062 Diffusion Dryer, direct connection to Model 3079A Aerosol
Generator possible for generation of salt or PSL-aerosols
Quick-release tube connectors, straight or 90° (with mounting tool)
Model 3332 Dilution System for a defined aerosol dilution, suitable to verify
test aerosols using particle counters (test of cleanrooms, laminar flow
boxes, safety benches according to EN 14644 and VDI 2083-3)
Accessories
6-2 Model 3079A
Appendix
Particle counter for measuring
the clean air
Aerosol Generator
Particle counter and dilution
system for measuring the test
aerosol
Steps 1-4
Steps 7-8
MODEL 3332
MODEL 3079A
7 Appendix
Periodic Testing of Particulate Matter Air Filters in Cleanroom Equipment
In this chapter recommendations are given on how to efficiently combine various TSI instruments to
one test unit. Especially the aerosol generators Model 3079 and Model 3079A, the Model 3332 dilution
system the isokinetic sampling probe SYS 529 and the particle counter have been successfully
combined in the past for testing laminar flow boxes, safety work benches, and smaller cleanrooms. All
recommendations are based on the Standards EN 14644-3 and VDI 2083, sheet 3 for testing
particulate matter air filters.
Figure 8: Applications for TSI Instruments
Using a test aerosol with a defined number of particles is the basis for checking the quality of the filter.
In Germany this test procedure defines a minimum particle concentration of 106#/cf according to VDI
standard 2083. This particle number concentration enables a leak detection on an acoustical basis
because commonly used cleanroom particle counters feature a beep tone when a particle is detected.
Particle concentrations exceeding a critical value will cause a continuous beep signal. This way filters
with separation efficiencies according H13 and H14 can be tested. Leaks can easily be located by
scanning the downstream filter.
Model 3079A 7-1
Chapter 7
In order to measure the particle concentration of the test aerosol commonly used, cleanroom particle
counters require a dilution with a defined factor. The Model 3332 dilution systems have been
developed especially for this application.
The possibility of aerosol flow rate and concentration adjustment with the Model 3079A in combination
with the Model 3332 dilution system enable measurements of the particle number concentration of the
test aerosol with a high degree of accuracy.
Figure 9: Range of Volume Flow of the Model 3079A Aerosol Generator
Assuming this raw air particle concentration C
with volumetric flow rates of safety work benches from 75 to 21,000m³/h
for a filter area from 0.05 to 14.5m² (based on an downstream aerosol velocity of 0.4m/s).
the Model 3079A can be used:
test
Recommendations for Carrying out the Leak Test with only one Particle Counter (Figure 8)
1. Connect the Model 3079A Atomizer Aerosol Generator to the test aerosol inlet or put the outlet of
the aerosol generator at the inlet of the to be tested unit, set up the particle counter to the dilution
system DIL, connect the point of aerosol sampling with the dilution system inlet, adjust the dilution
system while the particle counter is operating.
2. Start up the aerosol generator and set the requested aerosol flow rate by using the above diagram
(Figure 9).
3. Adjust the particle number concentration of the test aerosol to >106#/cf by setting the aerosol flow
rate of the aerosol generator (a 1cfm particle counter will count >10,000#/min).
4. Measure the particle number concentration of the test aerosol 3 times per minute (using a dilution
system Model 3332).
5. Switch off the particle counter, remove tube from the aerosol sampling point and blank off,
continue to operate the aerosol generator.
6. Connect isokinetic sampling probe SYS 529 with absolute filter to particle counter, switch on
particle counter and operate until no more particles are detected, switch off pump.
7-2 Model 3079A
Appendix
total
AG
AG
total
AG
test
V
VC
V
N
C
total
AGtotal
room
AG
AG
total
roomAG
test
V
)VV(CVC
V
NN
C
Filter
Typ I
Typ II
VAG
CAG
V
total
C
room
C
test
V
total
C
clean
VAG
V
LAF
C
test
V
LAF
C
clean
V
room
C
room
VAG
CAG
V
total
C
test
7. Remove absolute filter from isokinetic sampling probe SYS 529, put probe underneath the filter to
be tested, switch on the pump, carry out leak test and clean air measurement.
8. Switch off the aerosol generator; blank off aerosol inlet of the tested unit.
9. Summarize the results in a report.
The scanning velocity for the leak test depends on the filter outlet velocity, the cross-section
dimensions of the sampling probe, and the particle concentration of the test aerosol.
It is shown in the diagram in Figure 10 for one of the rectangular TSI sampling probes (according to
DIN EN ISO 14644).
Estimating the Particle Concentration of the Test Aerosol
Calculation Formula for Two Types of Laminar Flow Boxes
For both types of laminar flow boxes the particle number concentration in the air can be calculated
with formula (1). The particle number concentration of the surrounding air is neglected in this formula.
(1)
If the particle number concentration of the surrounding air is to be considered, other formulas for the
two types of laminar flow boxes must be used [formula (2) and (3)].
Model I:
(2)
Model 3079A 7-3
Chapter 7
LAF
AGroom
room
AG
ATM
LAF
roomAG
test
V
)VV(CVC
V
NN
C
Particle/cm3
Particle/cf
Number concentration (total)
>108
2.810
12
Number concentration
(fractions 0.3 … 0.5µm):
5105
1.410
10
Number concentration
(fractions 0.5 … 1.0µm):
3105
8.510
9
LAF
AGtotal
room
AG
AG
LAF
roomAG
test
V
)VV(0.3CVC
V
NN
c
h
cm
10600
h
cm
)1025010600(0.3
cm
Particle
3.5
h
cm
10250
cm
Particle
108
test
C
3
6
3
36
3
3
3
3
6
cf
Particle
109.4
cm
Particle
3334C
7
3
test
Model II:
(3)
Aerosols Produced by the Aerosol Generator (no dilution)
Example
Laminar flow box type II
V
= 600 m3/h
LAF
V
= 70% V
LAF
V
= 30% V
room
C
(0.5 µm)= 3.5 Particle/cm3 (cleanroom standard 100000
room
US-Fed.Std. 209D or in Germany: VDI2083)
CAG (0.5 … 1.0µm) = 310
V
= 250 L/h = 250103 cm3/h
AG
Considering the allowed particle number concentration in the surrounding air, the particle
concentration in the produced aerosol will be calculated as follows:
= 0.7 V
total
= 0.3 V
total
total
total
5
Particle/cm
3
If the surrounding air is considered, the produced test aerosol concentration is calculated as
126 Particles/cm3 (3.6106 Particles/cf); whereas, without it, the concentration is 125 Particles/cm3.
This example shows that it is acceptable to neglect the particle number concentration in the
surrounding air and apply formula (1).
7-4 Model 3079A
Used Symbols and Indices
Symbol
Description
C
Particle number concentration
V
Dilution factor
V
Volumetric flow rate
N
Aerosol flow rate (aerosol generator)
AG
Aerosol generator
LAF
Laminar flow box
room
Surrounding air
test
Test aerosol
total
Total volumetric flow rate
clean
Clean air
Appendix
Model 3079A 7-5
Chapter 7
0.001
0.01
0.1
10 100 1000
Scanning velocity, m/s
H 14
U 15
U 16
U 17
Diagram for Determining the Scanning Velocity when using a Rectangular Probe
(Dimensions WP/DP=max. 6:1 according to
EN ISO 14 644, Probe WP=80 mm; DP=15 mm; air velocity 0,45 m/s)
Particle Concentration in the Test Aerosol, 106 Particle/m3
Figure 10: Scanning Velocity for Rectangular Sampling Probe
7-6 Model 3079A
Physical Data of DEHS
Name
Di ethyl hexyl sebacate
CAS-No.
[122-62-3]
Formula
C26H50O4
Molar mass
426.69 g/mol
Dynamic viscosity
0.023 Pa s
Kinematic viscosity
25.16 mm2/s
Density
0.912 kg/cm
3
(DIN 51757)
Melting point
225 K (-48 °C) (ISO 3016)
Boiling point
525 K (252 °C) (DIN 51751)
Vapor pressure (293 K)
<1 Pa
Flash point
>473 K (>200 °C) (ISO 2592)
Refractive index
Wavelength, nm
1.450
650
1.452
600
1.4535
550
1.4545
500
1.4585
450
Appendix
Vapor Pressure of DEHS vs. Temperature
Model 3079A 7-7
Chapter 7
Name
Polyalphaolefin
(Poly(1-decene), hydrogenated)
CAS-No.
[68649-12-7]
Formula
[-CH2CH[(CH2)7CH3]-]n
Density
0.819 kg/cm3
Dynamic viscosity
0.014 Pa s
Boiling point
474 K (201°C)
Refractive index
1.455
Droplet diameter,
µm
Life Time of
Water
DEHS
0.1
2 µs
84 min
0.3
73 µs
4 h
1.0
1 ms
57 h
3.0
7 ms
16 d
10.0
80 ms
160 d
Physical Data of Emery 3004
Life Time of Aerosol
Values for 20°C.
7-8 Model 3079A
Appendix
Flow rate
Generation
of particles
> 0.3 µm
fractions
sufficient for
0.3 to
0.5 µm
0.5 to
0.7 µm
0.7 to
1.5 µm
>1.5
µm
Filter area
of
Volume
flow of
L/h
SKT
#/min
% % % % m²
m³/h
310
40
2.65•10
10
52.26
25.38
19.82
2.53
13.6
19600
295
30
2.58•10
10
52.48
25.23
19.74
2.55
13.3
19200
275
25
2.42•10
10
52.33
25.19
19.97
2.51
12.4
17900
235
20
2.04•10
10
51.49
25.27
20.60
2.65
10.3
14900
190
15
1.58•10
10
49.66
25.28
22.12
2.94
7.7
11100
142
10
9.27•10
9
46.74
24.98
24.33
3.94
4.2
6100
95
5
1.44•10
9
39.91
23.46
29.27
7.36
0.6
800
70
2
1.43•10
8
36.83
22.66
31.48
9.03
0.05
75
Characteristics of the Model 3079A
Depending on the volume flow of the Model 3079A specified by the selected valve position, the
following performance characteristics have been determined to be seen in the table. The values were
determined with the substance DEHS and a particle counter, measuring range 0.3 to 20 µm.
The Model 3079A can cover a wide particle production range. From the above table it can be seen
that the maximum concentration is up to 300 times the minimum concentration.
For calculations regarding the verification of laminar flow boxes a filter outlet velocity of 0.4 m/s and a
particle concentration of 1.2106 #/cf was assumed. Only particles of the size 0.3 to 0.5 µm were taken
into consideration.
Model 3079A 7-9
Chapter 7
50
100
150
200
250
300
350
0 10 20 30 40 50
Scale
Flow rate, l/h
Flowmeter Calibration
7-10 Model 3079A
Appendix
Disposal of End-of-Life Equipment
End-of-life equipment has to be decontaminated in an appropriate professional manner.
Disposal must be handled according to legal provisions especially for electrical and electronic
equipment as well as according to special local regulations and recycling instructions.
Waste electrical and electronic equipment can be returned to the manufacturer only with an attached
completed declaration of decontamination. TSI does not cover shipping costs.
Model 3079A 7-11
Chapter 7
EC Declaration of Conformity
7-12 Model 3079A
USA Tel: +1 800 874 2811
UK Tel: +44 149 4 459200
France Tel: +33 4 91 11 87 64
Germany Tel: +49 241 523030
India Tel: +91 80 67877200
China Tel: +86 10 8219 7688
Singapore Tel: +65 6595 6388
TSI Incorporated – Visit our website www.tsi.com for more information.
P/N 6007492 Rev A ©2014 TSI Incorporated Printed in U.S.A.
Loading...