Trans instruments WalkLAB HP 9010 Operation Manual

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WalkLAB

Professional pH Meter

HP 9010

Operations Manual

Page 2

INTRODUCTION

Your purchase of this professional pH meter marks a step forward for you into the field of precision measurement. Although this meter is a complex and delicate instrument, its usability will allow many years of use if proper operating techniques are observe and practice.

1. FEATURES:

• Multiple display of pH, mV and temperature

• Automatic buffer recognition with built in ISO and NIST standard

• Manual setting of customize pH buffer standard

• Up to 5 points calibration

• Auto-lock / automatic-endpoint detection function

• 99 memory with real time clock recording

• RS232 online data logging to PC (sold separately)

2. CONTENT:

Carefully unpack the box. It should contain the following items: a. Main unit b. Combination pH electrode c. Temperature probe d. Calibration buffer solution pH7.00 & pH4.01 of 90ml each. e. Operations manual

3. SPECIFICATION:

pH mV Temperature

Range

-2 to 16 pH ±700.0mV ±2,000mV

0 to 120ºC

Resolution

0.01pH 0.1mV 1mV 0.1ºC

Accuracy

±0.02pH ±0.5mV ±2mV

±0.1 ºC

±0.5ºC (Probe)

Calibration

Min. 2 point, Max. 5 point

Buffer Recognition

up to 60ºC or 95ºC depending on buffer type

Automatic Temperature Compensation

pH electrode temperature error compensation

0 to 120ºC

Memory

99 data with real time clock

Power source

4 x 1.5Volt AAA size battery

Operating temperature

5 to 40ºC

Storage temperature

-20 to 60ºC

Operating humidity

Up to 95% RH

Page 3

TO CLOSE BATTERY COVER

1 Align arrow to top of casing 2 Press

here

to snap down cover

4. PRODUCT LAYOUT:

pH Electrode

Socket

Temperature

Probe Socket

Battery Cover

Lift up

latch

here to

open

Battery

Cover

On/Off Button

Press once to switch ON. To switch OFF, press and hold-down.

Liquid

Crystal Display

Buttons

correlate

to display

Legend

Page 4

5. DISPLAY PANEL:

Display put on hold or freezed

8888

-188.8

D A

Y M O N T H

Y E A R

88 18 : 88

RECALL

EXIT

M+

CAL

ENTER

SETUP

MODE

READ

ºC

ºF

SELECT

Memory

Thousand Feet

Thousand Meter

ppt

ppm

kPa

ION

Cond

Salinity

TDS

µS

....

. .

....

ATC

Button keys legend

(correlate to button key)

Indicator will blink while the

function mode is active.

Date or Time display

Low

battery

indicator

Memory

counter

Automatic

Temperature

Compensation

indicator

Auto-

lock

indicator

Measuring

mode

indicator

Temperature reading or

SETUP Sub-

display

indicator

Page 5

6 SETTING UP THE UNIT:

6.1 Before you begin using the unit, it is important to define your measuring requirements. This will allow the unit to display accurately on the condition of sample that is measured.

6.2 While the unit is switched ON, press the SELECT button once and the Button Keys Legend will show SETUP appear.

6.3 Press the SETUP key to enter setup mode.

6.4 Display will show SETUP blinking, indicating you are in setup mode.

6.5 Press the SELECT button up to move to next setting or down to the previous setting parameter displayed on screen.

6.6 After setting, meter will retain the info until you reset them.

6.7 Below are the description for each setting parameter:

* Anytime during setup, press EXIT to cancel the setting.

Alc

- AUTO LOCK SETTING

Auto-lock feature allows the meter to automatically sense a stabilized reading and locks the endpoint reading. Factory preset is Yes

YesYes

Yes.

1. Press the ENTER key to set; display will show

Yes

Yes Yes

Yes

blinking.

2. Press the SELECT key up or down to choose

between

yes

yesyes

yes

and

nono

3. Press the ENTER key to confirm.

4. Press the SELECT key up for next setting.

- DATA TRANSMISSION TO PC

(Note: will not appear if no data saved)

This setting allows you to download saved memory data to PC via the RS232 connector & CD software kit (connector & software kit sold separately).

1. Download the software and run on PC.

2. Follow the CD instructions to setup software and

PC connection with RS232 connector.

3. Press the ENTER key and display will alternate

between

trtr

and

out

outout

out

, indicate transfer in progress.

4. When display return to

trtr

, transfer completed.

Check the PC for the transferred file.

5. Press the SELECT key up for next setting.

SETUP ENTER

SELECT

EXIT

Yes

ALc

SETUP ENTER

SELECT

EXIT

Auto Lock

Page 6

Bvf

- CALIBATION BUFFER STANDARDS

This setting allows you to select ISO, NIST or customized buffer standard. Factory preset is ISO standard.

ISO (IIIISO

SOSO

SO)buffer standards are pH1.68, 7.00, 4.01, 10.01,

12.45 and NIST (I7

I7I7

I7 I

I I

ISt

StSt

St) buffer standards are pH1.68,

4.01, 6.86, 9.18 and 12.45, which are preset in this

meter, and will be automatically recognized during calibration. Select customize (CvSt

CvStCvSt

CvSt) if you have other standards

other than standard buffer solutions.

1. Press the ENTER key to set; display will show IIIISO

SOSO

blinking.

2. Press the SELECT key up or down to select from IIIISO

SOSO

SO,

I7I7

I7 I

I I

Ist

stst

st or CvSt

CvStCvSt

CvSt and press the ENTER key to confirm.

Press the SELECT key up for next setting.

stAt

PrB

PrBPrB

PrB

- PROBE ELECTRODE STATUS

This setting allows you to review the last calibration information about the electrode conditions.

A good pH electrode should have an Offset value no greater than ±60mV and a Slope value of above 75% and below 115%. Otherwise, the electrode should be replaced.

There are 5 calibration points for review as follow:

Displayed Value Calibration Point within range

OFF

OFFOFF

OFF

Offset in mV pH7.00

SL1

SL1SL1

SL1

% of slope pH 7.00 to 4.01

SL2

SL2SL2

SL2

% of slope pH 7.00 to 10.01

SL3

SL3SL3

SL3

% of slope pH 4.01 to -2.00

SL4

SL4SL4

SL4

% of slope pH 10.01 to 16.00

1. Press the ENTER key to set; display will show the mV

value with Off

OffOff

Off blinking.

2. Press the SELECT key up to review Slope point 1,

display will show the % of slope with sl1

sl1sl1

sl1 below.

3. Press the SELECT key up sequentially to review all

the rest of slope value 2, 3, 4 and then back to Offset in a cyclical mode.

When finish, press the EXIT key once followed by the SELECT key up for next setting.

IsO

bvf

SETUP ENTER

SELECT

EXIT

98.5

sl2

stAt

Prb

SETUP ENTER

SELECT

EXIT

0.5

Off

SETUP ENTER

SELECT

EXIT

SETUP ENTER

SELECT

EXIT

Page 7

Clr

- CLEAR SAVED MEMORY

This setting will clear all saved memory in the unit.

1 Press the ENTER key to set; display will show No

No No

blinking.

2. Press the SELECT key up or down to choose

between yes

yesyes

yes and no

nono

no.

3. Choose Yes to clear, press the ENTER key to

confirm.

Press the SELECT key up for next setting.

Unt

- TEMPERATURE UNIT OF MEASUREMENT

This setting allows you to set the unit of measurement for temperature between Celcius and Fahrenheit. Factory preset is in Celcius.

1. Press the ENTER key to set; display will show C

C C

blinking.

2. Press the SELECT key up or down to choose

between CCCC and F

F F

3. Press the ENTER key to confirm.

Press the SELECT key up for next setting.

Avto off

- AUTO-OFF TIME SETTING

This setting allow you set the time to automatically shutoff the unit to power save. This feature is good if you want the meter to make prolong measurement or continuous display.

1. Press the ENTER key to set; display will show 15

15 15

blinking.

2. Press the SELECT key up or down to scroll between

nono

no,15

1515

15minutes, 30

3030

30 minutes or 60

6060

60 minutes.

3. Select no

nono

no will disable auto-shutoff feature.

4. Press the ENTER key to confirm.

5. Press the SELECT key up for next setting.

CLr

Memory

SETUP ENTER

SELECT

EXIT

UNt

°C

SETUP ENTER

SELECT

EXIT

Avto

SETUP ENTER

SELECT

EXIT

Page 8

Rtc

- REAL TIME CLOCK

This setting allows you to change the date and time on the meter.

1. Press the ENTER key to begin setting; display will

show clock with hour digit blinking.

2. Press the SELECT key up or down to scroll digit.

3. Press the ENTER key to confirm or move to set

Minute then Day, Month and Year on each instance. While digit is blinking, repeat step 2~3 to set digit.

4. After setting Year and ENTER , clock is up to date.

5. Press the SELECT key up for next setting.

RST

- MASTER RESET

This setting allows you to reset the unit to the original factory’s default.

Original factory default:

Buffer Standard = IIIISO

SOSO

Auto Shutoff =1s

1s1s

1s minutes

1. Press the ENTER key to set; display will show no

no no

blinking.

2. Press the SELECT key up or down to choose

between yes

yesyes

yes and no

no no

3. Press the ENTER key to confirm.

4. Press the SELECT key up to repeat from beginning or

EXIT key to return to measuring mode.

rtc

2 : 04

SETUP ENTER

SELECT

EXIT

rSt

SETUP ENTER

SELECT

EXIT

Page 9

7. CALIBRATION:

7.1 Prepare standard solutions of at least 2 calibration points. If measurements are to be made in the acidic range, select 2 points between pH-2 to 7. If measurements are made in the alkaline range, then select between pH7 to 16. If full range is required, calibrate at least 3 to 5 calibration points between pH-2 to 16.

7.2 Buffer standard must be set during SETUP in page 6, BuF

BuFBuF

BuF.

7.3 Standard solutions are in 3 groups of standards – ISO, Nist and custom standards.

ISO buffer standards are pH1.68, 7.00, 4.01, 10.01 and 12.45

NIST buffer standards are pH1.68, 4.01, 6.86, 9.18 and 12.45

Custom standards are defines manually for each buffer standard.

7.4 Do keep in mind that buffer all standards are specifies at 25°C. Calibration value should set to the exact value as the buffer’s solution value correlate to its current temperature.

Calibration with ISO Standard

7.5 Make sure the unit is properly installed and electrode connected.

7.6 This meter can automatically recognize the ISO Standard buffer solution. You will need at least 2 buffer solutions. Always begin with “Offset” calibration first.

7.7 Rinse the pH electrodes and temperature probe in distilled-water then dip it in the buffer solution, first in the offset buffer (pH7.00) then subsequently each of the slope buffer solution.

7.8 Press CAL key for 2 seconds and display will show the

7.00

and CAL

blinking, indicating it is in calibration mode.

* Calibration should be performed as frequently as possible

to ensure accurate measurement, depending on the

frequency of tests performed. Additional calibration

solution should be purchased for future needs.

Always rinses the electrode with distilled water before and after each

test. This is to prevent solution carry over or cross contamination.

Standard solutions must maintain highest purity; otherwise the

meter’s accuracy could be compromised.

Page 10

7.9 Value will vary according to solution’s temperature listed below:

ISO standard buffer solution Temperature

(°C)

Slope

1.68

Offset

7.00

Slope

4.01

Slope

10.01

Slope

12.45

0 1.67 7.11 4.00 10.32 13.43

5 1.67 7.08 4.00 10.25 13.21 10 1.67 7.06 4.00 10.18 13.00 15 1.67 7.03 4.00 10.12 12.81 20 1.68 7.01 4.00 10.06 12.63

25 1.68 7.00 4.01 10.01 12.45

30 1.69 6.98 4.02 9.97 12.29 35 1.69 6.98 4.02 9.93 12.13 40 1.70 6.97 4.03 9.89 11.99 45 1.70 6.97 4.04 9.86 11.84 50 1.71 6.97 4.05 9.83 11.70 55 1.72 6.97 4.06 11.57 60 1.72 6.97 4.08 11.45 65 1.73 6.97 4.10 70 1.74 6.98 4.12 75 1.75 6.99 4.14 80 1.77 7.00 4.16 85 1.78 7.02 4.18 90 1.80 7.03 4.21 95 1.81 7.05 4.24

7.10 If the meter does not recognize the buffer, it means the electrode could be defective or the buffer solution is wrong. Calibration cannot proceed until they are rectified.

7.11 When the meter beeps, Offset point is established.

7.12 Now 1.68, 4.01, 10.01 and 12.45 will alternate on main display.

7.13 Rinse the pH electrodes and temperature probe in distilled water, blot or shake dry then dip into next slope buffer solution.

7.14 When the meter recognizes the buffer, it displays in blinking mode.

7.15 If the value is different from that of the buffer solution then the electrode could be damage.

7.16 When the meter starts beeping, a Slope point is established. The remaining slope values will alternate on the main display.

7.17 Repeat step 7.13 to 7.16 sequentially up to 4 slope points.

7.18 At least 2 calibration points (offset & slope) must be established in each session of calibration. Otherwise, the whole calibration will not register.

7.19 When calibration is completed, press ENTER to store all calibrated points and to return to normal measuring mode.

7.20 Anytime during calibration, press EXIT for 2 seconds will abort all.

Page 11

Calibration with Nist Standard (if you have NIST buffer solution)

7.21 Make sure the unit is properly installed and electrode connected.

7.22 This meter can automatically recognize the Nist Standard buffer

solution. You will need at least 2 buffer solutions. Always begin with “Offset” calibration first.

7.23 Rinse the pH electrodes and temperature probe in distilled water

then dip in the buffer solution, first on the Offset buffer (pH6.86) then subsequently on each slope buffer.

7.24 Press CAL key and display will show the 6.86 and CAL blinking,

indicating it is in calibration mode.

7.25 Value will vary according to temperature listed below table:

NIST standard buffer solution Temperature

(°C)

Slope

1.68

Slope

4.01

Offset

6.86

Slope

9.18

Slope

12.45

0 1.67 4.01 6.98 9.47 13.43

5 1.67 4.00 6.95 9.38 13.21 10 1.67 4.00 6.92 9.32 13.00 15 1.67 4.00 6.90 9.27 12.81 20 1.68 4.00 6.88 9.22 12.63

25 1.68 4.01 6.86 9.18 12.45

30 1.69 4.01 6.85 9.14 12.29 35 1.69 4.02 6.84 9.10 12.13 40 1.70 4.03 6.84 9.07 11.99 45 1.70 4.04 6.83 9.04 11.84 50 1.71 4.06 6.83 9.01 11.70 55 1.72 4.06 6.83 8.99 11.57 60 1.72 4.08 6.84 8.96 11.45 65 1.73 4.10 6.84 8.94 70 1.74 4.12 6.85 8.92 75 1.75 4.14 6.85 8.90 80 1.77 4.16 6.86 8.88 85 1.78 4.18 6.87 8.87 90 1.80 4.21 6.88 8.85 95 1.81 4.24 6.89 8.83

Always rinses the electrode with distilled water before and after each

test. This is to prevent solution carry over or cross contamination.

Standard solutions must maintain highest purity; otherwise the

meter’s accuracy could be compromised.

Page 12

7.26 If the meter does not recognize the buffer, it means the electrode could be defective or the buffer solution is wrong. Calibration cannot proceed until they are rectified.

7.27 When the meter beeps, Offset point is established.

7.28 Now 1.68, 4.01, 9.18 and 12.45 will alternate on main display.

7.29 Rinse the pH electrodes and temperature probe in distilled water, blot or shake dry then dip into next slope buffer solution.

7.30 When the meter recognizes the buffer, it will appear blinking.

7.31 If the value is different from the buffer solution then the electrode could be damage.

7.32 Wait for meter to beep, Slope point is established.

7.33 The remaining buffer values will alternate on the main display.

7.34 Repeat step 7.29 to 7.33 sequentially up to 4 slope points.

7.35 At least 2 calibration points (offset & slope) must be established in each session of calibration. Otherwise, calibrated point will not register.

7.36 When calibration is completed, press ENTER to store all calibrated points and return to normal reading mode.

7.37 Anytime during calibration, press EXIT for 2 seconds will abort all.

Calibration with Custom Standard

7.38 Make sure the unit is properly installed and electrode connected.

7.39 Rinse the pH electrodes and temperature probe in distilled water and dip in the buffer solution. You will need at least two (2) buffers. Always begin with “Offset” calibration first.

7.40 Press CAL and display will show 7777.00

0000

00 while CAL blinking, indicating

it is in calibration mode.

7.41 Press the SELECT button up / down to adjust the value.

7.42 When the meter beeps, it means reading has stabilized and ready for calibration. Press ENTER to confirm to calibrate to the point.

7.43 A preset value of 1111.40

4040

40, 3333.80

8080

80, and 12

1212

12..60

.60.60

.60 will now alternate

requesting for a slope value.

7.44 Rinse the pH electrodes and temperature probe in distilled water, blot or shake dry then dip into next slope buffer solution.

7.45 The meter will recognize the nearest buffer value and will appear blinking while it beeps in wait of a complete action.

Always rinses the electrode with distilled water before and after each

test. This is to prevent solution carry over or cross contamination.

Standard solutions must maintain highest purity; otherwise the

meter’s accuracy could be compromised.

Page 13

7.46 Press the SELECT button up or down to adjust to the Slope value of the solution.

7.47 Press ENTER to confirm set value, wait a while for an endpoint reading to establish and press it again to calibrate to the point.

7.48 The remaining slope values will alternate on the main display.

7.49 Repeat step 7.43 to 7.47 in sequence. You can calibrate up to 4 slope points.

7.50 At least 2 calibration point (offset & slope) must be established in each session of calibration. Otherwise, calibrated point will not register.

7.51 When calibration is completed, press EXIT to resume measuring mode.

8 MAKING PH MEASUREMENT:

Measurement with Auto-Lock feature enabled:(see Page 4)

8.1 Always rinse the pH electrode and temperature probe with distilled-water before and after each test.

8.2 Dip the pH electrode and temperature probe in the test sample and press the READ button once.

8.3 Display will show current pH reading with AutoLock symbol blinking.

8.4 When the AutoLock sign stops with short beep, an endpoint reading is established. You can now record the reading.

8.5 Press the READ button for each new measurement.

Measurement with Auto-Lock feature disabled: (see Page 4)

8.6 When feature is disabled, meter will display readings continuously.

8.7 Press the READ button once to freeze displayed reading.

8.8 The HOLD symbol will appear. Press again will release display and resume continuous measurement.

pH measurement without ATC (Manual temperature compensation on sensor error)

8.9 If ATC is not required, disconnect the temperature probe. ATC symbol will not appear on screen and display will show the default temperature of 25ºC.

8.10 You can also manually set the solution’s temperature as follow:

8.11 Press the READ button start measuring, then press and hold down

MODE button until temperature reading appears blinking.

Note on Measurements and Analysis:

Each type of liquid has its own pH value varies at different temperature. ATC

measurement only compensates for the pH sensor’s error, it does not compensate

for the pH variation due to temperature fluctuation in the liquid. Therefore, each

test should be made at the same temperature if possible or recorded with

temperature reading for a comprehensive analysis.

Page 14

8.12 While temperature digit is blinking. Press the SELECT button up or down to adjust the value to that of the solution.

8.13 Press ENTER to confirm the set value or EXIT to abort. Display will resume measuring mode.

9 MAKING REDOX(ORP) MEASUREMENT:

9.1 Disconnect and remove the pH electrode and temperature probe. Connect with a Redox/ORP electrode. Temperature has no effect on ORP readings and therefore is not require during measurement.

9.2 Rinse the sensor in distilled water then in the test liquid. Stir to remove bubbles and wait for a stabilized reading.

9.3 Press the MODE button once to switch display to mV reading.

9.4 Press the READ button once and display will show AutoLock symbol blinking, indicating meter is sensing an endpoint reading.

9.5 When the AutoLock sign stops with short beep, an endpoint reading is established. You can now record the reading.

9.6 Depend on the liquid that is measured, some volatile liquid may take up to 20 minutes or even longer time to stabilize. Disable the Auto-lock (Page4) and Auto-Off (Page6) features. Then endpoint reading should determine by individual experience in each case.

DATA MEMORY:

9.7 This meter can save up to 99 data with time and clock with either pH or ORP measurements.

STORE MEMORY:

9.8 After a reading has established, press the M+ . button to save data into memory. Display will show Stor

StorStor

Stor and memory counter blink briefly.

9.9 Data is stored and measuring mode resumes.

9.10 When memory is above 99, display will show “FULL” and data will not be saved. Please download data and clear memory to resume.

9.11 It is a good practice to download data daily.

RECALL MEMORY:

9.12 To review the saved data, press the SELECT button then press RECALL button.

9.13 Press the SELECT button up or down to review each saved data. Time and date will alternate.

9.14 When finish reviewing, press EXIT to return to normal measuring mode.

7.08

25.0

Memory

2 8:

RECALL

SELECT

EXIT

stor

Memory

Page 15

ONLINE DATA LOGGING TO PC: (SOLD SEPARATELY)

The USB Connection kit is sold separately. Full instruction is in the Readme.txt file of the attached CD.

MAINTENANCE:

11.1

The pH electrode is a vital part of the pH measuring system. Keeping the electrode in good condition will ensure higher accuracy. Follow the maintenance instructions attached with each type of electrode.

11.2

Always review the pH electrode status after calibration to determine if the electrode is suitable for the measuring requirements.

11.3

When the battery sign appear permanently on the screen, it means the battery should be replace. Removed the battery cover and replace with 4 “AAA” batteries according to polarity.

11.4 If the battery sign appear blinking, it means the back-up battery should be replace. Return meter to your local agent for battery replacement.

TROUBLESHOOTING:

Error Code Reason or cause Remedy

----

--------

----

Inputs exceed measuring range

Measure liquid within specified range

ErLc Prob

Readings drift or unstable, cannot auto-lock during Read or Cal.

1. Ground loop in solution

2. Electrode is clog or expired.

3. Electromagnetic interference

4. ORP measurement

1. Make measurement in a cup or container.

2. Check % of slope >75% or <115%, otherwise, replace electrode.

3. Move to another location to perform test.

4. Disable auto-lock (see 9.6)

Er T Prob

Temperature out of the buffer solution range during calibration

1. Measure liquid within specified range

2. Replace temperature probe.

Er 6 Prob Er 7 Prob

Offset calibration error

1. Wrong buffer type

2. Sensor damaged or expired

1. Use only pH7.00 or 6.86 solution.

2. Check Offset status to be within ±15mV. Replace with new electrode

Er 1 Prob Er 4 Prob Er 9 Prob Er10 Prob Er12 Prob

Slope calibration error

1. Sensor damaged, clogged or expired.

1. Check % of slope status to be within 75 to115%. Replace with new electrode.

Reading does not change

1. Broken pH glass sensor.

2. Hold function is activated.

1. Change new electrode.

2. Press READ button to release.

Wrong date & time

Backup battery has expired.

Contact your dealer to replace new ones.

Page 16

WARRANTY:

Trans Instruments (Singapore) Pte. Ltd., warranties this product for a period

of 12 months for main unit and 3 months for electrode, probe or sensors from date of purchase; against all defects in material and workmanship.

This warranty does not apply to the abuse or misuse of the instrument. If repairs or adjustments are required, please return the defective product freight prepaid. Instrument within warranty will be repaired at no charge.

Make sure that the product is properly packed and insured against possible damage or loss in shipment. Purchase invoice MUST be accompanied in returned product or else warranty is considered void.

Please obtain authorization from Trans Instruments (Singapore) Pte Ltd. directly or through your local sales representatives prior to returning the product. Trans Instruments staff can be contacted at the following email address or through our webpage contacts:

[email protected] http://www.transinstruments.com

(Singapore) Pte Ltd

email: [email protected]

Website: www.transinstrumnets.com

ISO9001 Certified Firm

Rev-4 Sep2015

PRINTED IN SINGAPORE

Quality checked in Singapore

CALIBRATION CERTIFICATE

Product: WalkLAB pH meter HP9010 Measuring range: 0 to 14 pH Calibration point(s): 7.00, 4.01, 10.01 Test point(s): 7.00, 4.01, 10.01 Accuracy achieved: ±0.02 (Complete system, meter + probe)

CL Teh

Trans Instruments (S) Pte. Ltd.

certified that the above products underwent stringent

calibration in accordance with Trans Instruments product manufactu

ring standards

and work procedures and the result of inspection or testing for calibration meets the

product specifications above. The standard solutions use for the calibration

procedure was tested by instrument which is traceable to the US National Inst

itute

for Standards & Technology standard, under ambient conditions.

This certificate validates the product at the point of production. A complete pH

system will require regular calibration from time to time. A traceable pH Buffer

solutions should be used for continual re-calibration.