Thermo Scientific SL16R, Thermo Scientific SL16 Instruction Manual

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Thermo Fisher Scientific
Thermo Scientific SL16 Thermo Scientific SL16R
Instruction Manual
50120986-1 June 2009
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© 2009 Thermo Fisher Scientific Inc. All rights reserved.
BIOLiner
TM
, BIOShieldTM, HIGHPlateTM, HIGHConicTM, AutoLockTM, FIBERLite TM and CLINIConic
TM
re either registered trademarks or trademarks of Thermo Fisher Scientific..
Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the product operation. This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.
The contents of this document are subject to change without notice. All technical information in this document is for reference purposes only. System configurations and specifications in this document supersede all previous information received by the purchaser.
Thermo Fisher Scientific Inc. makes no representations that this document is complete, accurate or error-free and assumes no responsibility and will not be liable for any errors, omissions, damage or loss that might result from any use of this document, even if the information in the document is followed properly.
This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of Sale shall govern all conflicting information between the two documents.
Release history: 50120986-1 printed in June 2009.
For Research Use Only. Not for use in diagnostic procedures.
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WEEE Conformity
This product is subject to the regulations of the EU Waste Electrical & Electronic Equipment (WEEE) Directive 2002/96 It is marked by the symbol opposite:
Thermo Fisher Scientific has entered into agreements with recycling and disposal companies in all EU Member States for the recycling and disposal of this device. For information on recycling and disposal companies in Germany and on the products of Thermo Fisher Scientific, which fall under the RoHS Directive (Restriction of the use of certain hazardous substances in electrical and electronic equip­ment), please visit the website www.thermo.com/WEEERoHS.
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Table of Contents
Preface .......................................................................................................................................iii
Scope of supply ........................................................................................................................iii
Proper use .................................................................................................................................iii
Accident Prevention ................................................................................................................ iv
Precautions ............................................................................................................................... iv
Chapter 1 Introduction and Description ...............................................................................................1-1
Characteristics ..........................................................................................................1-2
Technical Data .........................................................................................................1-3
Directives, standards and guidelines ......................................................................................... 1-4
Functions and features ............................................................................................................. 1-5
Mains Supply ...........................................................................................................1-5
Rotor selection .........................................................................................................1-6
T
Chapter 2 Before use ................................................................................................................................2-1
Before setting up ......................................................................................................2-2
Transporting the centrifuge ......................................................................................2-2
Location ...................................................................................................................2-2
Aligning the centrifuge .............................................................................................2-3
Mains connection .....................................................................................................2-3
Storage .....................................................................................................................2-4
Chapter 3 Control panel ...........................................................................................................................3-1
Keys .........................................................................................................................3-2
Control panel ...........................................................................................................3-2
Chapter 4 Operation .................................................................................................................................4-1
Switch on centrifuge .................................................................................................4-2
Lid Opening .............................................................................................................4-2
Close lid ...................................................................................................................4-2
Rotor installation ......................................................................................................4-2
Entering parameters ..................................................................................................4-3
Saving programs .......................................................................................................4-6
Centrifuging .............................................................................................................4-7
Temperature adaptation during standstill .................................................................4-8
Short-term centrifuging ............................................................................................4-8
Removing the rotor ..................................................................................................4-8
Aerosol-tight rotors ...................................................................................................4-9
Switching the centrifuge off ......................................................................................4-9
Thermo Scientific SL 16 / 16R i
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Table of Contents
Chapter 5 System menu ...........................................................................................................................5-1
Chapter 6 Maintenance and care .......................................................................................................... 6-1
Intervals ................................................................................................................... 6-2
Cleaning .................................................................................................................. 6-2
Disinfection ............................................................................................................. 6-3
Disinfection with bleaching agents ........................................................................... 6-4
Decontamination ..................................................................................................... 6-4
Autoclaving .............................................................................................................. 6-4
Service of Thermo Fisher Scientific .......................................................................... 6-4
Chapter 7 Troubleshooting ..................................................................................................................... 7-1
Mechanical emergency lid release ............................................................................. 7-2
Troubleshooting by user .......................................................................................... 7-3
When to contact customer service ............................................................................ 7-6
Chemical Compatibility Chart ..............................................................................A-1
Warranty ...................................................................................................................B-1
Contact Information ................................................................................................C-1
ii SL 16 / 16R Thermo Scientific
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Preface
P
Before starting to use the centrifuge, read through this instruction manual carefully and follow the instructions.
The information contained in this instruction manual is the property of Thermo Fisher Scientific; it is forbidden to copy or pass on this information without explicit approval.
Failure to follow the instructions and safety information in this instruction manual will result in the expiration of the sellers warranty.
Scope of supply
If any parts are missing, please contact the nearest Thermo Fisher Scientific representative.
Proper use
This centrifuge is an IVD accessory, and therefore subject to the Directive 98/79/EC of the
European Parliament and the Council of October 27, 1998 on in vitro diagnostic medical devices.
Article Number Quantity Check
Centrifuge Thermo Scientific SL16 1
Power supply cable 1
50120986 Instruction manual 1
70009824 Anti-corrosion oil 1
This centrifuge is a laboratory product designed to separate components by generation of Relative
Centrifugal Force. It separates human samples (e.g. blood, urine and other body fluids) collected in appropriate containers, either alone or after addition of reagents or other additives.
As general-purpose centrifuge, it is designed to also run other containers filled with chemicals,
environmental samples and other non-human body samples.
This centrifuge should be operated by trained specialists only.
Thermo Scientific SL 16 / 16R iii
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Accident Prevention
Accident Prevention
Prerequisite for the safe operation of the Thermo Scientific SL16 / 16R is a work environment in compliance with standards, directives and trade association safety regulations and proper instruction of the user:
The safety regulations contain the following basic recommendations:
Maintain a radius of at least 30 cm around the centrifuge.
Implementation of special measures which ensure that no one can approach the centrifuge for
longer than absolutely necessary while it is running.
The mains plug must be freely accessible at all times. Pull out the power supply plug or
disconnect the power supply in an emergency.
Precautions
In order to ensure safe operation of the Thermo Scientific SL16 / 16R, the following general safety regulations must be followed:
Do not manipulate the safety devices.
The centrifuge should be operated by trained specialists only.
The centrifuge is to be used for its intended purpose only.
Plug the centrifuge only into sockets which have been properly grounded.
Do not move the centrifuge while it is running.
Use only rotors and accessories for this centrifuge which have been approved by Thermo Fisher
Scientific. Exceptions to this rule are commercially available glass or plastic centrifuge tubes, provided they have been approved for the speed or the RCF value of the rotor.
Do not use rotors which show any signs of corrosion and/or cracks.
Do not touch the mechanical components of the rotor and do not make any changes to the
mechanical components.
Use only with rotors which have been properly installed. Follow the instructions on the Autolock
in section “Rotor installation” on page 4-2.
Use only with rotors which have been loaded properly. Follow the instructions given in the rotor
manual.
Never overload the rotor. Follow the instructions given in the rotor manual.
Never start the centrifuge when the lid is open.
Never open the lid until the rotor has come to a complete stop and this has been confirmed in
the display.
iv SL 16 / 16R Thermo Scientific
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Precautions
The lid emergency release may be used in emergencies only to recover the samples from the
centrifuge, e.g. during a power failure (see section “Mechanical emergency lid release” on
page 7-2).
Never use the centrifuge if parts of its cover panels are damaged or missing.
Do not touch the electronic components of the centrifuge or alter any electronic or mechanical
components.
Please observe the safety instructions.
Please pay particular attention to the following aspects:
Location: well-ventilated environment, set-up on a level and rigid surface with adequate load-bearing
capacity.
Rotor installation: make sure the rotor is locked properly into place before operating the
centrifuge.
Especially when working with corrosive samples (salt solutions, acids, bases), the accessory parts and
vessel have to be cleaned carefully.
Always balance the samples.
Centrifuging hazardous substances:
Do not centrifuge explosive or flammable materials or substances which could react violently with
one another.
The centrifuge is neither inert nor protected against explosion. Never use the centrifuge in an
explosion-prone environment.
Do not centrifuge inflammable substances.
Do not centrifuge toxic or radioactive materials or any pathogenic micro-organisms without
suitable safety precautions.
When centrifuging microbiological samples from the Risk Group II (according to the "Laboratory Bio-safety Manual" of the World Health Organization WHO), aerosol-tight biological seals have to be used.
For materials in a higher risk group, extra safety measures have to be taken.
If toxins or pathogenic substances have gotten into the centrifuge or its parts, appropriate
disinfection measures have to be taken (see “Disinfection” on page 6-3).
Highly corrosive substances which can cause material damage and impair the mechanical stability
of the rotor, should only be centrifuged in corresponding protective tubes.
IF A HAZARDOUS SITUATION OCCURS, TURN OFF THE POWER SUPPLY TO THE CENTRIFUGE AND LEAVE THE AREA IMMEDIATELY.
Normal use
The centrifuge is to be used for separating materials of different density or particle size suspended in a liquid.
g
Maximum sample density at maximum speed: 1,2
Thermo Scientific SL 16 / 16R v
---------- -
cm
3
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Precautions
The symbol on the left refers to general hazards. ATTENTION means that material damage could occur. WARNING means that injuries or material damage or contamination could occur.
The symbol on the left refers to biological hazards. Observe the information contained in the instruction manual to keep yourself and your environment safe.
vi SL 16 / 16R Thermo Scientific
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Introduction and Description
“Characteristics” on page 1-2
“Technical Data” on page 1-3
“Functions and features” on page 1-5
“Rotor selection” on page 1-6
1
Thermo Scientific SL 16 / 16R 1-1
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1
Introduction and Description
Characteristics
Characteristics
The Thermo Scientific SL16 / 16R is an in-vitro diagnostics device according to the In-Vitro Diagnostics Directive 98/79/EC.
Several rotors with commercial tubes can be used.
The set speed is reached in seconds. The maintenance-free induction motor ensures quiet and low-vibration operation even at high speeds, and guarantees a very long lifetime.
The user-friendly control panel makes it easy to pre-set the speed, RCF value, running time, temperature, and running profile (acceleration and braking curves). You can choose between the display of speed and RCF or the entry mode.
These settings can be changed even while the centrifuge is running.
With the help of the "Pulse"-key , you can also centrifuge a sample for just a few seconds, if called for.
The Thermo Scientific SL16 / 16R is equipped with various safety features:
The housing and rotor chamber consist of steel plate, the interior of armour steel, while the front
panel is made of high-impact resistant plastic.
The lid is equipped with a view port and a lock.
The lid of the centrifuge can only be opened while the centrifuge is switched on and the rotor
has come to a complete stop. The centrifuge cannot be started until the lid has been closed properly.
The integrated rotor detection systems ensures that no inadmissible speed settings can be
preselected.
Electronic Imbalance recognition
Lid emergency release: For emergencies only, e.g. during power failures (see “Mechanical
emergency lid release” on page 7-2
1-2 SL 16 / 16R Thermo Scientific
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1
Introduction and Description
Technical Data
The technical data of the Thermo Scientific SL16 / 16R is listed in the following table.
Table 1- 1 . Technical Data Thermo Scientific SL16 / 16R
Feature Value
Environmental conditions - use in interior spaces
- altitudes of up to 2,000 m above sea level
- max. relative humidity 80% up to 31 °C; decreasing linearly up to 50% relative humidity at 40 °C.
permissible ambient temperature +2° C to +35° C +2° C to +35° C
Overvoltage category II II
Pollution degree 2 2
Heat dissipation refrigerated ventilated
230V 120V 230V 120V
4778 BTU/h 4096 BTU/h 3447 BTU/h 3901 BTU/h
Technical Data
IP 20 20
running time unlimited unlimited
maximum speed n
minimum speed n
maximum RCF value at n
maximum kinetic energy <62,5 kJ <51,7 kJ
noise level at maximum speed <63 dB(A) <63 dB(A)
temperature setting range -10 °C to +40 °C
Dimensions refrigerated ventilated
Height Height lid open Width Depth Table top height
weight without rotor 91,5 kg 57,5 kg
max
max
max
15200 rpm 15200 rpm
300 rpm 300 rpm
25701xg 25701xg
360 mm 870 mm 623 mm 605 mm 310 mm
360 mm 870 mm 440 mm 605 mm 310 mm
Thermo Scientific SL 16 / 16R 1-3
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1
Introduction and Description
Directives, standards and guidelines
Directives, standards and guidelines
Table 1-2. Directives, standards and guidelines
Tension / Frequency
230V 50/60Hz 2006/95/EC Low Voltage Directive:
2006/42/EC & 98/37/EC Machine Directive:
2004/108/EC EMC Directive
98/79/EC In-vitro-Diagnostika (IvD)
Produced and inspected according to the following standards and guidelines
EN 61010-1, 2
EN 61010-2-020, 2
EN 61010-2-101
EN 61326-1
EN 61326-2-6
EN 55011B
EN 61000-6-2
EN ISO 13485
230V 60Hz
120V 60Hz
100V 60Hz
The centrifuges are produced and inspected according to the following standards and guidelines
UL 61010-1, 2
CAN/CSA-C22.2 No. 61010-1, 2
IEC 61010-2-20, 2
(Pollution degree 2, Overvoltage category II)
EN 61010-2-101
Emitted interference FCC Part 15 CLASS A
NOTE: This equipment has been tested and found to comply with the limits for a Class A digital device, pursuant to Part 15 of the FCC Rules. These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment. This equipment generates, uses, and can radiate radio frequency energy and, if not installed and used in accordance with the instruction manual, may cause harmful interference to radio communications. Operation of this equipment in a residential area is likely to cause harmful interference in which case the user will be required to correct the interference at his own expense.
100V 50Hz IEC 61010-1 2
IEC 61010-2-020 2
IEC 61010-2-101
EN 61326-1
EN 61326-2-6
EN 55011A
EN 61000-6-2
EN ISO 13485
nd
Edition
nd
Edition
nd
Edition
nd
Edition
nd
Edition
nd
Edition
nd
Edition
1-4 SL 16 / 16R Thermo Scientific
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1
Introduction and Description
Functions and features
Functions and features
The following table gives an overview of the important functional and performance characteristics of the Thermo Scientific SL16 / 16R.
Table 1- 3 . Functions and features
Component / Function Description / Features
Structure / Housing Galvanized steel chassis with armoured plating.
Chamber Stainless steel
Drive Induction drive without carbon brushes
Keys and display Easy-to-clean keypad and display surface
Controls Microprocessor-controlled
Internal memory The most recent data is saved
Functions RCF-selection, temperature control, pretemp with cooling equipped devices
Acceleration / braking profiles 9 acceleration and 10 braking curves
Rotor recognition Automatic
Imbalance recognition Electronic, contingent on rotor and speed
Lid lock Automatic lid closing and locking starting from an initial hold position
Mains Supply
The following table contains an overview of the electrical connection data for the Thermo Scientific SL16 / 16R. This data is to be taken into consideration when selecting the mains connection socket.
Table 1- 4 . Electrical connection data of the Thermo Scientific SL16 / 16R
Cat. No.
7500 4030 refrigerated 230 V 50 / 60 Hz 8 A 1400 W 15 AT 16 AT
7500 4031 refrigerated 120 V 60 Hz 12 A 1200 W 15 AT 15 AT
7500 4000 ventilated 230 V 50 / 60 Hz 6 A 1010 W 15 AT 16 AT
7500 4001 ventilated 120 V 60 Hz 9,5 A 850 W 15 AT 15 AT
Mains voltage
Frequency Rated current
Power consumption
Equipment fuse
Building fus e
Thermo Scientific SL 16 / 16R 1-5
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1
Introduction and Description
Rotor selection
Rotor selection
The Thermo Scientific SL16 / 16R is supplied without a rotor. Various rotors are available to choose from.
TX-400 7500 3629
with round buckets 7500 3655
TX-200 7500 3658
with round buckets 7500 3659
BIOShield
M-20 7500 3624
Microliter rotor 30x2 sealed 7500 3652
CLINIConic
8x50 sealed 7500 3694
FIBERLite
HIGHConic
TM
720 7500 3621
TM
30x15 7500 3623
TM
F15-6x100 7500 3698
TM
II 7500 3620
The technical data of the rotors and the corresponding adapters and reduction sleeves for various commercially available containers can be found in the corresponding rotor operating manuals.
For more information visit our website at: http://www.thermo.com
1-6 SL 16 / 16R Thermo Scientific
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Before use
“Before setting up” on page 2-2
“Transporting the centrifuge” on page 2-2
“Location” on page 2-2
“Aligning the centrifuge” on page 2-3
“Mains connection” on page 2-3
“Storage” on page 2-4
2
Thermo Scientific SL 16 / 16R 2-1
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2
Before use
Before setting up
Before setting up
1. Check the centrifuge and the packaging for any shipping damage. Inform the shipping company and Thermo Fisher Scientific immediately if any damage is discovered.
2. Remove the packaging.
3. Check the order for completeness (see “Scope of supply” on page iii.). If the order is incomplete, please contact Thermo Fisher Scientific.
Transporting the centrifuge
Due to its weight (see “Technical Data” on page 1-3), the centrifuge should be carried by several
people.
Always lift the centrifuge at both sides.
Location
Figure 2-1. Lifting the centrifuge at both sides.
The centrifuge can be damaged by impacts.
Transport the centrifuge upright and if at all possible in its packaging.
WARNING Always lift the centrifuge on both sides. Never lift the centrifuge by its front or the back panel. Always remove the rotor before moving the centrifuge.
The centrifuge should only be operated indoors.
The set-up location must fulfil the following requirements:
A safety zone of at least 30 cm must be maintained around the centrifuge.
People and hazardous substances must be kept out of the safety zone while centrifuging.
2-2 SL 16 / 16R Thermo Scientific
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The supporting structure must be stable and free of resonance, for example a level laboratory
bench.
The supporting structure must be suitable for horizontal setup of the centrifuge.
The centrifuge should not be exposed to heat and strong sunlight.
WARNING UV rays reduce the stability of plastics. Do not subject the centrifuge, rotors and plastic accessories to direct sunlight.
The set-up location must be well-ventilated at all times.
Aligning the centrifuge
The alignment of the centrifuge must be checked every time after moving it to a different location. The supporting structure must be suitable for horizontal setup of the centrifuge.
2
Before use
Aligning the centrifuge
VORSICHT If the centrifuge isn’t level, imbalances can occur and the centrifuge can be damaged. Do not place anything under the feet to level the centrifuge.
Mains connection
Main Power Switch
Mains plug
Figure 2-2. Mains connections
1. Turn off the power supply switch on the back (press "0").
2. Plug the centrifuge into grounded electrical sockets only.
3. Check whether the cable complies with the safety standards of your country.
Thermo Scientific SL 16 / 16R 2-3
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2
Before use
Storage
4. Make sure that the voltage and frequency correspond to the figures on the rating plate.
Figure 2-3. Rating plate of the Thermo Scientific SL16R
5. Establish the connection to the power supply with the connecting cable.
Storage
Store the centrifuge in a clean, dust-free location.
Be sure to place the centrifuge on its feet.
Avoid direct sunlight.
2-4 SL 16 / 16R Thermo Scientific
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Control panel
“Control panel” on page 3-2
“” on page 3-3
3
Thermo Scientific SL 16 / 16R 3-1
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3
Control panel
Keys
Keys
The keys allow user intervention for controlling the operating mode as follows:
key display contents
Start
Stop
Open lid
Pulse
Change value
Snow symbol
Changing the display mode
Normal start of the centrifuge
End run manually
Release (possible only when device is switched on). Release during power failure: see
“Mechanical emergency lid release” on page 7-2)
By pressing the "PULSE" key the centrifuge starts immediately and accelerates up to the end speed. Releasing the key initiates a stopping process at the highest braking curves.
Use the arrow buttons in order to modify the displayed value.
Press the snow symbol key for prewarming or precooling the centrifuge.
Use the CHANGE key to change the display mode. (Speed / RCF-value)
Control panel
The control panel contains the keys and displays of the centrifuge (only the power switch is located on the back of the device). All parameters can be selected and changed during operation.
3-2 SL 16 / 16R Thermo Scientific
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3
Control panel
Control panel
Acceleration profile
PULSE-key
Bucket selection
Braking profile
OPEN key
Stop key
Start key
Bucket selection key
Temperature
Prewarming or precooling
Running time
Speed
RCF-value
Changing the display mode
Speed / RCF-value
Program selection keys
Thermo Scientific SL 16 / 16R 3-3
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3
Control panel
Control panel
3-4 SL 16 / 16R Thermo Scientific
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Operation
“Switch on centrifuge” on page 4-2
“Lid Opening” on page 4-2
“Close lid” on page 4-2
“Rotor installation” on page 4-2
“Entering parameters” on page 4-4
“Saving programs” on page 4-6
“Centrifuging” on page 4-7
4
“Temperature adaptation during standstill” on page 4-8
“Short-term centrifuging” on page 4-8
“Removing the rotor” on page 4-8
“Switching the centrifuge off” on page 4-9
Thermo Scientific SL 16 / 16R 4-1
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4
Operation
Switch on centrifuge
Switch on centrifuge
6. Turn on the power switch on the back of the device. The device performs a self-check of its software.
a. When the centrifuge lid is closed the following display shows:
The speed and time displays read 0. The temperature indicator displays the current temperature inside the rotor chamber. The preset acceleration and braking curves and the selected bucket are also displayed.
b. When the centrifuge lid is open the following display shows:
The speed and time displays show the preset values. The temperature indicator displays the current temperature inside the rotor chamber. The preset acceleration and braking curves and the selected bucket are also displayed.
Lid Opening
1. Press the "OPEN" key .
WARNING Do not reach into the crack between the lid and the housing. The lid is drawn shut automatically. Use the emergency release only for malfunctions and power failures (see “Mechanical
emergency lid release” on page 7-2).
Close lid
Close the lid by pressing down on it lightly in the middle or on both sides of it. One lock closes the lid completely. The lid will close automatically.
WARNING Do not reach into the crack between the lid and the housing. The lid is drawn shut automatically.
Note The lid should audibly click into place.
Rotor installation
The approved rotors for the Thermo Scientific SL16 / 16R are listed in section “Rotor selection” on
page 1-6. Use only the rotors and accessories from this list in the centrifuge.
CAUTION Unapproved or incorrectly combined accessories can cause serious damage to the centrifuge.
4-2 SL 16 / 16R Thermo Scientific
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4
Operation
Rotor installation
The rotors are equipped with an AutoLockTM locking system.
This system is used to automatically lock the rotor to the centrifuge spindle. The rotor does not have to be bolted onto the centrifuge spindle.
Proceed as follows:
1. Open the lid of the centrifuge and if necessary remove any dust, foreign objects or residue from the chamber. AutoLock
TM
and o-ring must be clean and undamaged.
AutoLock
TM
O-ring
Figure 4-4. AutoLock
2. Hold the rotor over the shaft and let it slide slowly down the centrifuge spindle. The rotor clicks automatically into place.
CAUTION Do not force the rotor onto the centrifuge spindle. If the rotor is very light, then it may be necessary to press it onto the centrifuge spindle with a small amount of pressure.
TM
3. Check if the rotor is properly installed by lifting it slightly on the handle. If the rotor can be pulled up, then it must be reclamped to the centrifuge spindle.
WARNING If the rotor cannot be properly locked in place after several attempts, then the AutoLock
TM
is defective and you are not permitted to operate the rotor. Check for any damage to the rotor: Damaged rotors must not be used. Keep the hub area clear of objects.
CAUTION Check that the rotor is properly locked on the centrifuge spindle before each use by pulling it a its handle.
4. Place the rotor lid onto the rotor.
Be sure to check all sealings before starting any aeorsol-tight applications. See the information in the rotor instruction manual.
5. Close the centrifuge lid.
Thermo Scientific SL 16 / 16R 4-3
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4
Operation
Entering parameters
Entering parameters
The Thermo Scientific SL16 offers you a total of 9 acceleration and 10 braking curves with which samples and gradients can be centrifuged.
After the centrifuge is turned on, the last running profile selected is shown.
Acceleration curve
1. Press the key below the ACC display in order to open the acceleration profile selection menu. The display shows the message "Acceleration"
2. Select the profile by pressing the key, until the desired acceleration curve shows.
Braking profile
1. Press the key below the DEC display in order to open the braking profile selection menu. The display shows the message "Set Deceleration“
2. Select the profile by pressing the key, until the desired deceleration curve shows.
Preselecting Speed / RCF
1. Press the key below the “SPEED” display. The display shows the "RPM“ or the "RCF"-value depending on the display setting. Press the
key to toggle between the two values.
2. Enter the desired value by pressing the key repeatedly, until the desired value shows.
Note If an extremely low RCF value has been selected, it will be corrected automatically if the resulting speed is less than 300 rpm.
4-4 SL 16 / 16R Thermo Scientific
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4
Operation
Entering parameters
Explanation of RCF value
The relative centrifugal force is given as a multiple of the force of gravity g. It is a unitless numerical value which is used to compare the separation or sedimentation capacity of various devices, since it is independent of the type of device. It simply involves the rotational radius and the rotating speed:
2
n
RCF 11 18,
r = Rotational radius in cm
n = Speed in rpm
The maximum RCF value is related to the maximum radius of the tube.
Remember that this value is reduced depending on the tubes and adapters used.
This can be accounted for in the calculation above if required.
-------------
〈〉
1000
r××=
Running time preselection
1. Press the key below the TIME display in order to open the runtime selection menu. The display shows the message "Set Time“. Enter the desired runtime in hh:mm
2. Enter the desired value by pressing the key repeatedly, until the desired value shows.
Continuous operation
1. Press the "START" key . During continuous operation, the centrifuge will continue running until you stop it manually.
Preselecting the temperature
You can preselect temperatures between -10 °C and +40 °C.
To set the temperature, proceed as follows:
1. Press the key below the TEMPERATURE display in order to open the temperature selection menu. The display shows "Set temp".
2. Enter the desired value by pressing the key repeatedly, until the desired value shows.
Thermo Scientific SL 16 / 16R 4-5
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4
Operation
Saving programs
Prewarming or precooling the centrifuge
For setting the pretemp value for the centrifuge proceed as follows:
1. Press the key below the TEMPERATURE display in order to open the temperature selection menu. The display shows the message "Set PreTemp "
2. Enter the desired value by pressing the key repeatedly, until the desired value shows.
3. Close the centrifuge lid.
The display shows the current temperature inside the rotor chamber.
4. Press the "START" key .
The rotor chamber is cooled down or heated up to the preset temperature.
5. Press the "STOP" key . The display shows the current temperature inside the rotor chamber.
Bucket selection
Bucket selection is only possible for swing-out rotors. The bucket code corresponds to the last four digits of the bucket catalog number.
1. Press the "BUCKET" key. The display shows the following message:
2. Press the BUCKET key repeatedly until the bucket being used is displayed.
Saving programs
1. Enter the program parameters.
2. Press any of the program store keys for 5 seconds.
4-6 SL 16 / 16R Thermo Scientific
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Centrifuging
Once the rotor has been properly installed, the main switch has been turned on and the lid has been closed, you can start centrifuging.
Starting centrifuge program
Press the START key on the control panel. The centrifuge accelerates to the pre-set speed with the time display active.
If the speed setting is higher than the maximum permissible speed or RCF-value for the particular rotor, then the display will show the message max. 4,700 rpm once the centrifuge has been started.
Within 15 seconds you can apply this value by pressing the "START" key again, and the centrifug­ing program will continue. Otherwise the centrifuge will stop and you will have to enter a valid num­ber.
You cannot open the lid as long as the centrifuge is running.
4
Operation
Centrifuging
Imbalance indicator
If a load is imbalanced, this will be indicated at speed higher than approx. 300 rpm by the message "Imbalanced load".
The run will terminate.
Check the loading and start the centrifuge once again. See the information on proper loading in the rotor instruction manual. For information on troubleshooting, see section “Troubleshooting by user” on page 7-3.
Stopping the centrifuging program
With preset running time
Usually the running time is preset and you only have to wait until the centrifuge stops automatically when the preset time limit expires.
As soon as the speed drops to zero, the message "END" will appear in the display. By pressing the OPEN key , you can open the lid and remove the centrifuged material.
You can also stop the centrifuging program manually at any time by pressing the "Stop" key.
Continuous operation
If you selected continuous operation (see “Continuous operation” on page 4-5), you will have to stop the centrifuge manually. Press the STOP key on the control panel. The centrifuge will be deceler­ated at the designated rate. The message "END" will illuminate, and after pressing the OPEN key , the lid will open and you can remove the centrifuged material.
Thermo Scientific SL 16 / 16R 4-7
Page 32
4
Operation
Temperature adaptation during standstill
Temperature adaptation during standstill
The temperature cannot be adapted until the rotor has been positively identified; the speed display will then show "END".
When the rotor is not recognized (lid closed and START key not yet pressed, speed display "0"), the centrifuge responds by ensuring that the sample cannot freeze regardless of the rotor being used.
Short-term centrifuging
For short-term centrifuging, the Thermo Scientific SL16 / 16R has a "Pulse"- function.
By holding down the PULSE key , spinning will start and continue until the key is let go.
The centrifuge accelerates and brakes at maximum power. Any rpm or RCF entered beforehand is overridden.
Note The centrifuge accelerates to maximum speed, regardless of which rotor was installed.
Check carefully whether you have to maintain a certain speed for your application.
During the acceleration process, time is counted forwards in seconds. The reading stays displayed until the centrifuge lid is opened.
Removing the rotor
To remove the rotor, proceed as follows:
1. Open the centrifuge lid.
2. Grab the rotor handle with both hands and press against the green AutoLock time, pull the rotor directly upwards with both hands and remove it from the motor shaft. Make sure not to jam the rotor while doing this.
TM
key. At the same
4-8 SL 16 / 16R Thermo Scientific
Page 33
Aerosol-tight rotors
When using a lid sealed against aerosols, you can only remove the rotor with the rotor lid closed! This is for your personal safety and to ensure the integrity of the samples.
4
Operation
Aerosol-tight rotors
CAUTION Rotors supplied with a lid for aerosol-tight applications come with a mandril, which belongs to the AutoLock prevent it from being damaged.
Figure 4-5. AutoLock
WARNING Mind the AutoLockTM-mandril inside the lid. Do not touch.
TM
-lid for aerosol-tight rotors
Switching the centrifuge off
TM
. Be sure not to place the lid onto this mandril to
1. To turn off the centrifuge put the mains switch to "0".
Thermo Scientific SL 16 / 16R 4-9
Page 34
4
Operation
Switching the centrifuge off
4-10 SL 16 / 16R Thermo Scientific
Page 35
System menu
To enter the system menu hold down any of the keys when switching the centrifuge on.
To modify setting, use the UV keys.
Use the UV keys for the speed fields to navigate in the system menu.
Use the UV keys for the bucket field to navigate from one system menu item to the next.
5
Thermo Scientific SL 16 / 16R 5-1
Page 36
5
System menu
Enter system menu?
Z
Z
Start
Start
Stop
Stop
Press the STOP key to quit the system menu.
Language
V
V
End of run beep?
V
V
Keypad beep?
V U
V U
LCD powersave?
V
V
Auto lid open?
V
V
English
U
U
no
U
U
U
U
U
U
no
no
no
English
Deutsch
Francaise
Español
Italiano
.
yes
no
Software ID:
V
V
Cycle count:
V
V
0547V01
U
U
2368
U
U
0547V01
4641V05
*
Software and NVRAM identification exam-
ple values.
*
5-2 SL 16 / 16R Thermo Scientific
Page 37
Maintenance and care
“Intervals” on page 6-2
“Cleaning” on page 6-2
“Disinfection” on page 6-3
“Handling and care of rotors and accessories made of aluminium” on page 6-6
“Disinfection with bleaching agents” on page 6-4
“Decontamination” on page 6-4
“Autoclaving” on page 6-4
6
“Service of Thermo Fisher Scientific” on page 6-4
Thermo Scientific SL 16 / 16R 6-1
Page 38
6
Maintenance and care
Intervals
Intervals
For the sake of personal, environmental, and material protection, it is your duty to clean and if necessary disinfect the centrifuge on a regular basis.
Maintenance Recommended interval
Clean rotor chamber daily or when polluted
Clean rotor daily or when polluted
Accessories daily or when polluted
Cabinet Once per month
Ventilation holes Every six months
CAUTION Refrain from using any other cleaning or decontamination procedure than those recommended by Thermo Fisher Scientific, if you are not entirely sure that the intended procedure is safe for the equipment. Contact Thermo Fisher Scientific for further advice. Use only approved cleansers. If in doubt, contact Thermo Fisher Scientific
Cleaning
1. Open the centrifuge.
2. Turn off the centrifuge.
3. Pull out the power supply plug.
4. Unscrew the rotor holder.
5. Grasp the rotor with both hands and lift it vertically off the centrifuge spindle.
6. Remove the centrifuge tubes and adaptors.
7. Use a neutral cleaning agent with a pH value between 6 and 8 for cleaning.
8. Dry all of the aluminum parts after cleaning with a cloth or in a warm air cabinet at a maximum temperature of 50°C.
Clean the housing of the centrifuge as needed.
Caution When cleaning, do not allow liquids, especially organic solvents, to get on
the drive shaft, the bearings, the AutoLockTM or the locks. Organic solvents break down the grease in the motor bearing. The drive shaft could freeze up.
Drain off any melted ice from the rotor chamber.
CAUTION Before using any cleaning or decontamination methods except those recommended by the manufacturer, users should check with the manufacturer that the proposed method will not damage the equipment.
6-2 SL 16 / 16R Thermo Scientific
Page 39
Disinfection
Disinfect the centrifuge immediately whenever infectious material has spilled during centrifuging.
Use a sprayer whenever possible so that all surfaces are covered evenly.
The rotor chamber and the rotor should be treated preferably with a neutral disinfectant. A disinfectant spray would be most suitable for this purpose so that the rotor and accessory surfaces are covered evenly.
6
Maintenance and care
Disinfection
WARNING Infectious material can get into the centrifuge when a tube breaks or as a result of spills. Keep in mind the risk of infection when touching articles and take all necessary precautions. In case of contamination, make sure that others are not put at risk. Decontaminate the affected parts immediately. Take other precautions if need be.
WARNING Observe the safety precautions and handling instructions for the cleaning agents used.
Contact the service department of Thermo Fisher Scientific for questions regarding the use of other disinfectants!
Disinfect the rotor and accessories as follows:
1. Open the centrifuge.
2. Turn off the centrifuge.
3. Pull out the power supply plug.
4. Unscrew the rotor holder.
5. Grasp the rotor with both hands and lift it vertically off the centrifuge spindle.
6. Remove the centrifuge tubes and adaptors and dispose of them or disinfect them.
7. Treat the rotor and rotor lid according to the instructions for the disinfectant (spray or soak in solution). Adhere strictly to the given application times.
8. Be sure the disinfectant can drain off the rotor.
9. Rinse the rotor and rotor lid thoroughly with water and then rub down.
10. Dispose of the disinfectant according to the applicable guidelines.
11. Treat aluminum rotors afterwards with an anti-corrosion oil (7000 9824). Apply a thin layer of oil using a soft cloth.
Thermo Scientific SL 16 / 16R 6-3
Page 40
6
Maintenance and care
Disinfection with bleaching agents
Disinfection with bleaching agents
Never use bleaching agents when disinfecting.
CAUTION Bleaching agents contain highly aggressive hypochlorites and should not be used on aluminum rotors.
Decontamination
For general radioactive decontamination use a solution of equal parts of 70% ethanol, 10% SDS and water. Rinse the rotor first with ethanol and then with de-ionized water. Dry off the rotor with a soft cloth.
Dispose of all rinsing solutions in a container suitable for radioactive waste.
CAUTION Before using any cleaning or decontamination methods except those recommended by the manufacturer, users should check with the manufacturer that the proposed method will not damage the equipment.
Autoclaving
Rotors and adapters can be autoclaved at 121 °C.
The maximum permissible autoclave cycle is 20 minutes at 121 °C.
Clean the rotor before autoclaving and rinse it with distilled water. Remove all accessories (tubes, adapters) from the rotor. Place the rotor on a flat surface.
Note No chemical additives are permitted in the steam.
Caution Never exceed the permitted temperature and duration when autoclaving.
If the rotor shows signs of corrosion or wear, it must be replaced.
Service of Thermo Fisher Scientific
Thermo Fisher Scientific recommends having the centrifuge and accessories serviced once a year by an authorized service technician. The service technicians check the following:
the electrical equipment
the suitability of the set-up site
the lid lock and the safety system
the rotor
the fixation of the rotor and the drive shaft
6-4 SL 16 / 16R Thermo Scientific
Page 41
Service of Thermo Fisher Scientific
Thermo Fisher Scientific offers inspection and service contracts for this work.
6
Maintenance and care
Thermo Scientific SL 16 / 16R 6-5
Page 42
6
Maintenance and care
Service of Thermo Fisher Scientific
6-6 SL 16 / 16R Thermo Scientific
Page 43
Troubleshooting
“Mechanical emergency lid release” on page 7-2
“Troubleshooting by user” on page 7-3
“When to contact customer service” on page 7-6
7
Thermo Scientific SL 16 / 16R 7-1
Page 44
7
Troubleshooting
Mechanical emergency lid release
Mechanical emergency lid release
During a power failure, you will not be able to open the centrifuge lid with the regular electric lid release. A mechanical override is provided to allow sample recovery in the case of an emergency. However, this should be used only in emergencies and after the rotor has come to a complete stop.
WARNING The rotor can still be spinning at high speed. If touched, it can cause serious injuries.
Always wait a few minutes until the rotor has come to a stop without braking. The brake does not work when there is no current. The braking process lasts much longer than usual.
Proceed as follows:
1. Make sure the rotor has stopped (view port in the lid).
WARNING Never use your hand or other tools to brake the rotor.
2. Pull out the power supply plug.
3. On the left side of the housing is one white plastic plugs which you can pry out of the side plate with a screwdriver or a knife. Pull the release cord attached to it to trigger the mechanical lid release. The lid will open and the samples can be removed.
Emergency lid release
Figure 7-6. Emergency lid release
4. Push the cord back into the centrifuge and mount the plugs.
Reconnect the centrifuge once the power has been restored. Switch on the centrifuge. Press the OPEN key
7-2 SL 16 / 16R Thermo Scientific
to have the lid locks operative again.
Page 45
Troubleshooting by user
If problems occur other than those listed in this table, the authorized customer service representative must be contacted.
Failure message Problem with centrifuge Possible causes and cures
7
Troubleshooting
Troubleshooting by user
Overtemperature The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Incorrect bucket ID The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Unapproved rotor The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Rotor ID failure The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Overheating in chamber. Check the function of the refrigeration unit. Clean the air inlet for the condenser.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Bucket code is undefined for the rotor detected, check the set points for the given bucket code. Is it permitted to use the current bucket in the rotor currently mounted?
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Rotor code is not in the rotor table. Is it permitted to use the rotor currently mounted in this device?
Restart the centrifuge.
If an error message appears again, inform Customer Service.
The rotor could not be identified.
Check to see if the rotor is properly installed.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Lid blocked Centrifuge does not open Restart the centrifuge.
The emergency lid release enables you to retrieve your samples.
If an error message appears again, inform Customer Service.
Motor overtemp. The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
PCB overtemp. The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Emergency release The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Thermo Scientific SL 16 / 16R 7-3
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
The lid opens while the device is running.
Close the lid and restart the centrifuge.
If an error message appears again, inform Customer Service.
Page 46
7
Troubleshooting
Troubleshooting by user
Failure message Problem with centrifuge Possible causes and cures
Imbalanced load The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Check Set Speed The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-01 - E-12 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-13 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-15 - E-16 Temperature sensor broken / controller
defective
Imbalance detected.
Check the load placed in the rotor.
Check that the rotor cross bolts are well greased.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
The set point speed is higher than the maximum rotor speed.
Correct the value.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Error during the self-test of the centrifuge program and the electronics.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
The check sum in the data memory is incorrect. The software corrects errors automatically. Check the values of the set point settings, etc.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Malfunction in the temperature detection.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
E-17 Speed for rotor detection exceeded Restart the centrifuge.
If an error message appears again, inform Customer Service.
E-21 - E-22 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
The rotor could not be identified.
Check to see if the rotor is properly installed.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
E-23 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-25-E-27 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-28 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
The speed control measurement returned a different result.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Time has expired for the lid lock drive while opening the lid.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Error during the self-test of the centrifuge program and the electronics.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
7-4 SL 16 / 16R Thermo Scientific
Page 47
Failure message Problem with centrifuge Possible causes and cures
7
Troubleshooting
Troubleshooting by user
E-29 The centrifuge cannot be operated.
The run will not be started.
E-30 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-33 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-34-E-36 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
E-40 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Is the rotor properly installed? Is it easy to turn the rotor when the lid is open? Does the rotor rub against the device?
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Overpressure in the refrigeration unit.
Clean the air inlet for the condenser.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Error during the self-test of the centrifuge program and the electronics.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
The centrifuge accelerates too slowly.
Is the rotor properly installed? Check wether you selected the right bucket. Is it easy to turn the rotor when the lid is open? Does the rotor rub against the device?
Restart the centrifuge.
If an error message appears again, inform Customer Service.
E-41-E-74 The centrifuge cannot be operated.
The run does not start or the centrifuge runs down without being braked.
Error during the self-test of the centrifuge program and the electronics.
Restart the centrifuge.
If an error message appears again, inform Customer Service.
Thermo Scientific SL 16 / 16R 7-5
Page 48
7
Troubleshooting
When to contact customer service
When to contact customer service
If you need to contact customer service, please provide the order no. and the serial no. of your device. This information can be found on the back near the inlet for the power supply cable.
To identify the software version, proceed as follows:
1. Hold down any of the keys and then switch on the centrifuge. You enter the system menu.
2. Press the START key .
3. Press and hold the ENTER key , until the following message is displayed:
Software ID:
4. Communicate the software version to the service technician.
XXXXXXXX
7-6 SL 16 / 16R Thermo Scientific
Page 49
Chemical Compatibility Chart
Table A-1. Chemical Compatibility Chart
A
®
CCCLEARCRIMP
®
CHEMICAL
2-mercaptoethanol
Acetaldehyde
Acetone
Acetonitrile
®
Alconox
Allyl Alcohol
Aluminum Chloride
Formic Acid (100%)
Ammonium Acetate
Ammonium Carbonate
Ammonium Hydroxide (10%)
Ammonium Hydroxide (28%)
Ammonium Hydroxide (conc.)
Ammonium Phosphate
Ammonium Sulfate
Amyl Alcohol
Aniline
Sodium Hydroxide (<1%)
Sodium Hydroxide (10%)
Barium Salts
Benzene
MATERIAL
ALUMINUM
ANODIC COATING for ALUMINIUM
BUNA N
,CLEARCRIMP
®
, POLYCLEAR
CELLULOSE ACETATE BUTYRATE
POLYURETHANE ROTOR PAINT
COMPOSITE Carbon Fiber/Epoxy
DELRIN®ETHYLENE PROPYLENE
GLASS
NEOPRENE
NORYL®NYLON
1
PET
POLYALLOMER
POLYCARBONATE
POLYESTER, GLASS THERMOSET
POLYTHERMIDE
POLYRTHYLENE
POLYPROPYLENE
POLYSULFONE
®
, TEFLON
®
POLYVINYL CHLORIDE
RULON A
SILICONE RUBBER
STAINLESS STEEL
TITANIUM
TYGON®VITON
SSU- SMS- SUSSUSS- SSSSUSSSSSS
S-UU---M-U---MU U U MM- MS U - S - U
MSUUSUMSSUUSUSUUUS SUUSMMSUU
SSU- SMS- SSUSUMUU- SMUUSSSSUU
UUS- SSS- SSSSSSMSSSSSSSSSSSU
---U--S----S-SSMSSS- MS- - S- -
UUSSSSUSSSSMSSSS- SSSSSMUUSS
-SMU--U----U-SMUUSS-US-US-U
SSU- SSS- SSSSSSSU- SSSSSSSSSS
MSUSSSSSSSSSSSUU- SSSSSSMSSS
UUSUSSMSSSSS- SUMSSSSSSSSSMS
UUSUSUMSSSSSUSUMSSSSSSSSSMS
UUUUSUMS- S- SUSUUSSS- MSSSS- U
U- S- SSSSSSSS- SSM- SSSSSSMSSS
UMS- SSUSSSSSSSSS- SSSSSSUSSU
S- MU- - SS- M- S- MSSSSM---U-S-M
SSUUSUSMSUUUUUUU- SMUUSSSSUS
U- MSSS- - SMSS- SMMSSSSSSMSS- U
U- MU- - U- MMSSUSUUSSSSSSMSS- U
MUS- SSSSSSSSSSSM- SSSSSSMSSS
SSUUSUMUSUUSUUUMUMUUUSUUSUS
®
Thermo Scientific SL 16 / 16R A-1
Page 50
A
Chemical Compatibility Chart
Table A-1. Chemical Compatibility Chart
®
CCCLEARCRIMP
®
CHEMICAL
Benzyl Alcohol
Boric Acid
Cesium Acetate
Cesium Bromide
Cesium Chloride
Cesium Formate
Cesium Iodide
Cesium Sulfate
Chloroform
Chromic Acid (10%)
Chromic Acid (50%)
Cresol Mixture
Cyclohexane
Deoxycholate
Distilled Water
Dextran
Diethyl Ether
Diethyl Ketone
Diethylpyrocarbonate
Dimethylsulfoxide
Dioxane
Ferric Chloride
Acetic Acid (Glacial)
Acetic Acid (5%)
Acetic Acid (60%)
Ethyl Acetate
Ethyl Alcohol (50%)
Ethyl Alcohol (95%)
Ethylene Dichloride
MATERIAL
ALUMINUM
ANODIC COATING for ALUMINIUM
BUNA N
,CLEARCRIMP
®
, POLYCLEAR
CELLULOSE ACETATE BUTYRATE
POLYURETHANE ROTOR PAINT
COMPOSITE Carbon Fiber/Epoxy
DELRIN®ETHYLENE PROPYLENE
GLASS
NEOPRENE
NORYL®NYLON
1
PET
POLYALLOMER
POLYCARBONATE
POLYESTER, GLASS THERMOSET
POLYTHERMIDE
POLYRTHYLENE
POLYPROPYLENE
POLYSULFONE
®
, TEFLON
®
POLYVINYL CHLORIDE
RULON A
SILICONE RUBBER
STAINLESS STEEL
TITANIUM
TYGON®VITON
S- UU- - MM- M- SUUUUUUU- MSM- S- S
USSMSSUSSSSSSSSSUSSSSSSSSSS
M- S- SSS- SSSS- SS- - SSSSSSMSSS
MSS- SSS- SSSSSSS- - SSSSSSMSSS
MSSUSSS- SSSSSSS- - SSSSSSMSSS
MSS- SSS- SSSSSSS- - SSSSSSMSSS
MSS- SSS- SSSSSSS- - SSSSSSMSSS
MSS- SSS- SSSSSSS- - SSSSSSMSSS
UUUUSSMUSUUMUMUUUMMUUSUUUMS
U- UUSUU- SSSUSSMUMSSUMSMUSSS
U-UU-UU---SUUSMUMSSUMS-UM-S
SSU---S-SUUUUUU- - UU- USSSSUS
SSS- SSSUSUSSUUUMSMUMMSUMMUS
SSS- SSS- SSSSSSS- - SSSSSSSSSS
SSSSSSSSSSSSSSSSSSSSSSSSSSS
MSSSSSS- SSSSSSSSSSSSSSSMSSS
SSUUSSSUSUUSUUUUUUUUUSSSSMU
S- UU- - M- SU- S- MUUUMM- US- - SUU
SSU- SSS- SSUSUSU- - SSSMSSSSSS
SSUUSSS- SUSSUSUU- SSUUSSSSUU
MS U U S S MMS U U S U MU U - MMMU SSSSUU
UUS---MS-M-S-S---SS---MUS-S
SSUUSSUMSUSUUUUUMS UMUSUUS- U
SSMSSSMSSSSSMSSSSSSSMSSMSSM
S S U U S S U - S MS U U MU S MS MS MS MU S MU
MMUUSSMMSSUSUMUU- SSUUSMMSUU
SSSSSSMSSSSSUSUSSSSSSSSMSMU
SSSUSSMSSSSSUSU- SSSMSSSUSMU
S- UU- - SM- UUSUUUUUUU- USU- S- S
®
A-2 SL 16 / 16R Thermo Scientific
Page 51
Table A-1. Chemical Compatibility Chart
A
Chemical Compatibility Chart
®
CCCLEARCRIMP
®
CHEMICAL
Ethylene Glycol
Ethylene Oxide Vapor
Ficoll-Hypaque
Hydrofluoric Acid (10%)
Hydrofluoric Acid (50%)
Hydrochloric Acid (conc.)
Formaldehyde (40%)
Glutaraldehyde
Glycerol
Guanidine Hydrochloride
Haemo-Sol
Hexane
Isobutyl Alcohol
Isopropyl Alcohol
Iodoacetic Acid
Potassium Bromide
Potassium Carbonate
Potassium Chloride
Potassium Hydroxide (5%)
Potassium Hydroxide (conc.)
Potassium Permanganate
Calcium Chloride
Calcium Hypochlorite
Kerosene
Sodium Chloride (10%)
Sodium Chloride (sat'd)
Carbon Tetrachloride
Aqua Regia
Solution 555 (20%)
®
®
MATERIAL
ALUMINUM
ANODIC COATING for ALUMINIUM
BUNA N
,CLEARCRIMP
®
, POLYCLEAR
CELLULOSE ACETATE BUTYRATE
POLYURETHANE ROTOR PAINT
COMPOSITE Carbon Fiber/Epoxy
DELRIN®ETHYLENE PROPYLENE
GLASS
NEOPRENE
NORYL®NYLON
1
PET
POLYALLOMER
POLYCARBONATE
POLYESTER, GLASS THERMOSET
POLYTHERMIDE
POLYRTHYLENE
POLYPROPYLENE
POLYSULFONE
®
, TEFLON
®
POLYVINYL CHLORIDE
RULON A
SILICONE RUBBER
STAINLESS STEEL
TITANIUM
TYGON®VITON
SSSSSSSSSSSS- SUSSSSSSSSMSMS
S- U- - U- - SU- S- SM- - SSSUSUSSSU
MSS- SSS- SSSS- SS- SSSSSSSMSSS
UUUM- - U- - UUS- SMUSSSSMSUUU- -
UUUU- - U- - UUUUSUUUSSMMSUUU- M
UUUU- UUM- UMUUMUUU- S- USUUU- -
MMMSSSSMSSSSMSSSUSSMSSSMSMU
SSSS- - S- SSSSSSS- - SSS- - SSS- -
MSS- SSSSSSSSSSSS- SSSSSSSSSS
UUS- SSS- SSSSSSS- - SSSSSSUSSS
SSS---S-SSSSSSS- - SSSSSSSSSS
SSS- SSS- SSUSUMUSSUSSMSUSSUS
- - MU- - SS- U- SUSSMSSS- SSS- S- S
MMMU SSSSSUSSUSUMSSSSSSSMMMS
SSM- SSS- SMSSMSS- MSSSSSMSSMM
USS- SSS- SSSSSSSSSSS- SSSMSSS
MUSSSSS- SSSSSSUSSSSSSSSSSSS
USS- SSSSSSSSSSS- SSSSSSSUSSS
UUSSSSM- SSSS- SUSSSSSSSMUMSU
UUMU- - M- MSS- UMUUUSM- MU- UU- U
SSS- SSS- SSSUSSSM- SMSUSSMSUS
MUSSSSSSSSSSSSMS- SSSSSSMSSS
M- U- SMMS- M- S- SMS- SSSMSMUS- S
SSS- SSSUSMUSUMMS- MMMSSUSSUS
S- SSSSSS- - - SSSSS- SSSS- SSM- S
U-SUSSS----SSSSS- SS- S- SSM- S
U U MS S U MU S U U S U MU S S MMS MMMMU S S
U-UU--U-----UUUUUUU-----S-M
SSS---S-SSSSSSS- - SSS- SSSSSS
®
Thermo Scientific SL 16 / 16R A-3
Page 52
A
Chemical Compatibility Chart
Table A-1. Chemical Compatibility Chart
®
CCCLEARCRIMP
®
CHEMICAL
Magnesium Chloride
Mercaptoacetic Acid
Methyl Alcohol
Methylene Chloride
Methyl Ethyl Ketone
Metrizamide
Lactic Acid (100%)
Lactic Acid (20%)
N-Butyl Alcohol
N-Butyl Phthalate
N, N-Dimethylformamide
Sodium Borate
Sodium Bromide
Sodium Carbonate (2%)
Sodium Dodecyl Sulfate
Sodium Hypochlorite (5%)
Sodium Iodide
Sodium Nitrate
Sodium Sulfate
Sodium Sulfide
Sodium Sulfite
Nickel Salts
Oils (Petroleum)
Oils (Other)
Oleic Acid
Oxalic Acid
Perchloric Acid (10%)
Perchloric Acid (70%)
Phenol (5%)
®
MATERIAL
ALUMINUM
ANODIC COATING for ALUMINIUM
BUNA N
,CLEARCRIMP
®
, POLYCLEAR
CELLULOSE ACETATE BUTYRATE
POLYURETHANE ROTOR PAINT
COMPOSITE Carbon Fiber/Epoxy
DELRIN®ETHYLENE PROPYLENE
GLASS
NEOPRENE
NORYL®NYLON
1
PET
POLYALLOMER
POLYCARBONATE
POLYESTER, GLASS THERMOSET
POLYTHERMIDE
POLYRTHYLENE
POLYPROPYLENE
POLYSULFONE
®
, TEFLON
®
POLYVINYL CHLORIDE
RULON A
SILICONE RUBBER
STAINLESS STEEL
TITANIUM
TYGON®VITON
MSS- SSSSSSSSSSSSSSSSSSSMSSS
USU- SMS- SMSUUUU- SUUSMSUSSSS
SSSUSSMSSSSSUSUMSSSSSSSMSMU
UUUUMSSUSUUSUUUUUMUUUSSMUSU
SSUUSSMSSUUSUSUUUSSUUSSSSUU
MSS- SSS- SSSS- SS- - SSSSSSMSSS
--S------MSU-SSSMSS- MSMSS- S
--SS-----MSM-SSSSSSSMSMSS- S
S- SU- - S- - SM- USMSSSSMMSM- S- S
SSU- SSS- SUUSUUUM- UUSUS MMSUS
SSSUSMS- SSUSUSUU- SSUUSMSSSU
MSSSSSSSSSSUSSSS- SSSSSSMSSS
USS- SSS- SSSSSSSS- SSSSSSMSSS
MUSSSSSSSSSSSSUSSSSSSSSSSSS
SSS- SSS- SSSSSSS- SSSSSSSSSSS
UUMSSMUSSMSSSMSSSSMSSSMUSMS
MSS- SSS- SSSSSSS- - SSSSSSMSSS
SSS- SSSSSSSSSSSS- SSSSSUSSSS
USS- SSSSSSSSSSSSSSSSSSSMSSS
S-SS---S---SSSUU--S---SSM-S
SSS- SSSSMSSSSSSM- SSSSSSSSSS
USSSSS- SSS- - SSSS- SSSSSSMSSS
SSS---SUSSSSUUMSMUUSSSUSSSS
S-S---SMSSSSUSSSSUSSSS- SSMS
S- USSSUUSUSSMSSSSSSSSSMUSMM
UUMSSSUSSSSSUSUSSSSSSSSUMSS
U- U- SUU- SMM- - MUMSMM- MSU- S- S
UUU- - UU- SUMUUMUUUMMUMSUUSUS
U S U - S MM- S U MU U S U MS MS U U S U MMMS
®
A-4 SL 16 / 16R Thermo Scientific
Page 53
Table A-1. Chemical Compatibility Chart
A
Chemical Compatibility Chart
®
CCCLEARCRIMP
®
CHEMICAL
Phenol (50%)
Phosphoric Acid (10%)
Phosphoric Acid (conc.)
Physiologic Media (Serum, Urine)
Picric Acid
Pyridine (50%)
Rubidium Bromide
Rubidium Chloride
Sucrose
Sucrose, Alkaline
Sulfosalicylic Acid
Nitric Acid (10%)
Nitric Acid (50%)
Nitric Acid (95%)
Hydrochloric Acid (10%)
Hydrochloric Acid (50%)
Sulfuric Acid (10%)
Sulfuric Acid (50%)
Sulfuric Acid (conc.)
Stearic Acid
Tetrahydrofuran
Toluene
Trichloroacetic Acid
Trichloroethane
Trichloroethylene
Trisodium Phosphate
Tris Buffer (neutral pH)
Triton X-100
Urea
®
MATERIAL
ALUMINUM
ANODIC COATING for ALUMINIUM
BUNA N
,CLEARCRIMP
®
, POLYCLEAR
CELLULOSE ACETATE BUTYRATE
POLYURETHANE ROTOR PAINT
COMPOSITE Carbon Fiber/Epoxy
DELRIN®ETHYLENE PROPYLENE
GLASS
NEOPRENE
NORYL®NYLON
1
PET
POLYALLOMER
POLYCARBONATE
POLYESTER, GLASS THERMOSET
POLYTHERMIDE
POLYRTHYLENE
POLYPROPYLENE
POLYSULFONE
®
, TEFLON
®
POLYVINYL CHLORIDE
RULON A
SILICONE RUBBER
STAINLESS STEEL
TITANIUM
TYGON®VITON
USU- SUM- SUMUUUUUSUMUUSUUUMS
UUMSSSUSSSSU- SSSSSSSSSUMUSS
UUMM- - US- MSUUMMSSSMSMSUMU- S
MSSS- - S- SSSSSSSSSSSSSSSSSSS
SSU- SMSSSMSUSSSUSSSSUSUMSMS
USUUSUU- USSUUMUU- USMUSSUUUU
MSS- SSS- SSSSSSS- - SSSSSSMSSS
MSS- SSS- SSSSSSS- - SSSSSSMSSS
MSS- SSSSSSSSSSSSSSSSSSSSSSS
MSS- SSS- SSSSSSUSSSSSSSSMSSS
UUSSSSS- SSSUSSS- SSS- SSSUSSS
USUSSUU- SUSU- SSSSSSSSSMSSSS
USUMSUU- SUSUUMMUMMMSSSUSSMS
U- UU- UU- - UUUUMUUUUMUUSUSS- S
UUMSSSU- SSSUUSUSSSSSSSSUMSS
UUUUSUU- SMSUUMUUSSSSMSMUUMM
MUUSSUU- SSMUSSSSSSSSSSUUUSS
MUUUSUU- SSMUUSUUMSSSSSUUUMS
MUUU- UUM- - MUUSUUUMSUMSUUU- S
S-S---SMSSSS- SSSSSSSSSMMSSS
SSUUSUUMSUUSUUU- MUUUUSUSSUU
SSUUSSMUSUUSUUUSUMUUUSUSUUM
UUU- SSUMSUSUUSM- MSSUUSUUUMU
S-U---MU-U-SUUUUUUUUUSU- S- S
--UU---U-U-SUUUUUUUUUSU- U- S
---S--M------S--SSS--S--S-S
USSSSSS- SSSSSSSSSSSSSSSSSSS
SSS- SSS- SSSSSSSSSSSSSSSSSSS
S- USSSS----SSSMSSSS- SSSMS- S
®
Thermo Scientific SL 16 / 16R A-5
Page 54
A
Chemical Compatibility Chart
Table A-1. Chemical Compatibility Chart
®
CCCLEARCRIMP
®
CHEMICAL
Hydrogen Peroxide (10%)
Hydrogen Peroxide (3%)
Xylene
Zinc Chloride
Zinc Sulfate
Citric Acid (10%)
1
Polyethyleneterephthalate
Key
S Satisfactory
M M = Moderate attack, may be satisfactory for use in centrifuge depending on length
U U = Unsatisfactory, not recommended.
-- No data available. Because no organized chemical resistance data exists for materials
,CLEARCRIMP
®
, POLYCLEAR
MATERIAL
ALUMINUM
ANODIC COATING for ALUMINIUM
BUNA N
CELLULOSE ACETATE BUTYRATE
POLYURETHANE ROTOR PAINT
COMPOSITE Carbon Fiber/Epoxy
DELRIN®ETHYLENE PROPYLENE
GLASS
NEOPRENE
NORYL®NYLON
1
PET
POLYALLOMER
POLYCARBONATE
POLYESTER, GLASS THERMOSET
POLYTHERMIDE
POLYRTHYLENE
UUMSSUU- SSSUSSSMUSSSSSSMSUS
SMSSS- S- SSSSSSSSMSSSSSSSSSS
SSUSSSMUSUUUUUUMUMUUUSUMS US
UUSSSSUSSSSSSSSSSSSSSSSUSSS
USS- SSSSSSSSSSSSSSSSSSSSSSS
MSSMSSMSSSSSSSSSMSSSSSSSSSS
of exposure, speed involved, etc.; suggest testing under actual conditions of use.
under the stress of centrifugation, when in doubt we recommend pretesting sample lots. suggest testing, using sample to avoid loss of valuable material.
POLYPROPYLENE
POLYSULFONE
®
, TEFLON
®
POLYVINYL CHLORIDE
RULON A
®
SILICONE RUBBER
STAINLESS STEEL
TITANIUM
TYGON®VITON
Chemical resistance data is included only as a guide to product use.
A-6 SL 16 / 16R Thermo Scientific
Page 55
Warranty
Thermo Fisher Scientific warrants that the Products will operate substantially in conformity with Thermo Fisher Scientific s published specifications, when subjected to normal, proper and intended usage by properly trained personnel, for a period of 12 MONTHS after shipment to the Customer (the “Warranty Period”). Thermo Fisher Scientific agrees during the Warranty Period, provided it is promptly notified in writing upon the discovery of any material defect and further provided that all costs of returning the defective Goods to the Thermo Fisher Scientific are pre-paid by the Customer, to repair or replace, at Thermo Fisher Scientific s option, defective Goods so as to cause the same to oper­ate in substantial conformance with the said specifications. Replacement parts may be new or refur­bished, at the election of Thermo Fisher Scientific. All replaced parts shall become the property of Thermo Fisher Scientific. All consumable or expendable items are expressly excluded from the war­ranty under this Clause. Thermo Fisher Scientific s sole liability with respect to equipment, materials, parts or software furnished to Thermo Fisher Scientific by its third party suppliers shall be limited to the assignment by Thermo Fisher Scientific to the Customer of any such third party supplier s war­ranty, to the extent the same is assignable. In no event shall Thermo Fisher Scientific have any obliga­tion to make repairs, replacements or corrections required, in whole or in part, as the result of (i) normal wear and tear, (ii) accident, disaster or event of force majeure, (iii) misuse, fault or negligence of or by or on behalf of the Customer, (iv) use of the Goods in a manner for which they were not designed, (v) causes external to the Goods such as, but not limited to, power failure or electrical power surges or (vi) use of the Goods in combination with equipment or software not supplied by Thermo Fisher Scientific. If Thermo Fisher Scientific determines that Goods for which the Customer has requested warranty services are not covered by the warranty hereunder, the Customer shall pay or reim­burse Thermo Fisher Scientific for all costs of investigating and responding to such request at Thermo Fisher Scientific s then prevailing time and material rates. If Thermo Fisher Scientific provides repair services or replacement parts that are not covered by the warranty provided in this Clause, the Cus­tomer shall pay Thermo Fisher Scientific therefor at Thermo Fisher Scientific s then prevailing time and materials rates. Any installation, maintenance, repair, service, relocation or alteration to or of, or other tampering with, the Goods, performed by any person or entity other than Thermo Fisher Scien­tific without Thermo Fisher Scientific s prior written approval, or any use of replacement parts not supplied by Thermo Fisher Scientific, shall immediately void and cancel all warranties with respect to the affected Goods.
B
Thermo Scientific SL 16 / 16R B-1
Page 56
B
Warranty
B-2 SL 16 / 16R Thermo Scientific
Page 57
Contact Information
United States 866-9-THERMO
Canada +1 866 984 3766
C
+1 866 984 3766
Austria +43 1 801 400
Belgium +32 2 482 30 30
Germany 08001 536 376
+49 6184 90 6940
France +33 2 2803 2180
+33 2 2803 2000
Italy +39 02 02 95059 341
Netherlands +31 76 571 4440
Nordic / Baltic Countries +35 89 329 100
Russia +7 (812) 703 42 15
Thermo Scientific SL 16 / 16R C-1
Page 58
C
Contact Information
Spain +34 932 23 09 18
Portugal +34 932 23 09 18
Switzerland +41 44 454 12 12
UK / Ireland +44 870 609 9203
China +86 21 6865 4588
+86 10 8419 3588
India +91 22 6716 2200
Japan +81 45 453 9220
Other Asian Countries +852 2885 4613
Latin America +1 866 984 3766
Other Countries +49 6184 90 6940
+33 2 2803 2180
C-2 SL 16 / 16R Thermo Scientific
Page 59
Index
I
A
Acceleration curve ................................................ 4-4
Accident Prevention ............................................... iv
Aerosol-proof rotors ............................................. 4-9
Aligning the centrifuge ..........................................2-3
Autoclaving ........................................................6-4
B
Bleaching agents ..................................................6-4
Braking profile .................................................... 4-4
Bucket selection ...................................................4-6
C
Care ................................................................. 6-1
Centrifuging ....................................................... 4-7
Cleaning ............................................................ 6-2
Cleaning agents ................................................... 6-2
Close lid ............................................................ 4-2
Contact Information ........................................... C-1
Continuous operation ........................................... 4-5
Control panel ......................................................3-2
D
Decontamination .................................................6-4
Disinfection ........................................................6-3
E
Emergency lid release ............................................ 7-2
Entering parameters ..............................................4-3
Explanation of RCF value ......................................4-5
K
Keys ..................................................................3-3
L
Lid Opening .......................................................4-2
M
Mains connection ................................................2-3
Mains Supply ......................................................2-4
Maintenance .......................................................6-1
O
Operation ..........................................................4-1
P
Precautions ........................................................... iv
Preselecting speed ................................................ 4-4
Preselecting the temperature ...................................4-5
Prewarming or precooling ......................................4-6
Prewarming or precooling the centrifuge ...................4-6
Proper use ............................................................. v
R
Rating plate ........................................................2-4
Removing the rotor ..............................................4-8
Rotor installation .................................................4-2
Rotor selection .................................................... 1-6
Running time preselection .....................................4-5
S
F
Failure message ....................................................7-3
Failures ..............................................................7-1
Features ............................................................. 1-5
Foreword ............................................................. iii
I
Imbalance indicator .............................................. 4-7
Installation location ..............................................2-2
Thermo Scientific SL 16 / 16R I-1
Safety area ..........................................................2-2
Safety features .....................................................1-2
Service technician ..........................................6-4, 7-6
Short-term centrifuging .........................................4-8
Starting centrifuge program ....................................4-7
Stopping the centrifuging program ...........................4-7
Storage ..............................................................2-4
Switch on centrifuge ............................................. 4-2
T
Technical Data ....................................................1-3
Page 60
Index:
Temperature adaptation ........................................4-8
Transporting the centrifuge ....................................2-2
I-2 SL 16 / 16R Thermo Scientific
Page 61
Page 62
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