Thermo Scientific ICP-MS User Manual

Thermo Scientific iCAP TQe ICP-MS
Redefining triple quadrupole ICP-MS with unique ease of use
iCAP TQe ICP-MS
Overcome unexpected interferences, reduce detection limits for critical contaminants and improve data quality
Leverage superior interference removal using triple quadrupole (TQ) ICP-MS for uncomplicated analysis with incredible accuracy. Expand your applications and enhance your laboratory eciency with this breakthrough technology, which is so easy to use that it can be operated by any analyst.
• Reaction Finder method development assistant enables you to tackle challenging matrices without complex, time-consuming method development
• Common Thermo Scientific™ Qtegra™ Intelligent Scientific Data Solution™ (ISDS) software platform allows analysts to switch easily between ICP techniques
• Minimal installation and bench space requirements
The Thermo Scientific optimal solution for future-proofing elemental analysis in your laboratory, explore developing markets, increase productivity and meet the requirements of evolving legislation.
• Right-first-time analysis with powerful interference removal, even in the toughest matrices
• Reduced re-runs in the daily workload with assured accuracy and repeatability
• Maintained flexibility of single quadrupole (SQ) mode for less challenging analyses
iCAP™ TQe ICP-MS is the
2
For applied testing
Robust and easy to use, the iCAP TQe ICP-MS is a compact and low maintenance instrument. Daily analysis is elevated to a new level and the high matrix tolerance and exceptional interference removal, even in challenging sample matrices, open up new applications. Simplified operation from Qtegra ISDS software means operators do not need to be specialists.
For research
Improved interference removal leads to the lower detection limits that are essential for new scientific breakthroughs. Find out what is possible with the advanced performance of TQ-ICP-MS technology.
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Inside TQ technology
Highly eective interference removal for accurate and reliable results
• The iCAP TQe ICP-MS achieves consistent interference removal regardless of the sample composition using just helium and oxygen as the collision/reaction cell gases. This simplifies operation and eliminates the need for special gas installation in the laboratory.
• If SQ analysis is required, switching between preset Kinetic Energy Discrimination (KED) mode and TQ modes is possible in a single sample analysis for rapid and reliable results.
• The Reaction Finder Method Development Assistant dramatically simplifies method development. No requirement for advance knowledge of complex reaction chemistry is necessary—Reaction Finder does it for you!
91
[AsO]⁺
Q3 set to product
ion mass (m/z 91)
150
40Ar35
Nd⁺⁺,
Cl⁺
150
Sm⁺⁺
Let Reaction Finder select the right mode for your analysis
SQ mode: Comparable to SQ-ICP-MS instruments, Q1 transmits all masses
TQ on mass mode: Q1 and Q3 set to the same mass
TQ mass shift mode: Q1 and Q3 set to dierent masses
111
Cd⁺
Q3 set to product
ion mass (m/z 111)
MoO2⁺
reactive gas (O
Q1 set to analyte
mass (m/z 75)
4
Q2 filled with
2
75
150
As⁺,
)
150
Nd⁺⁺,
"Mass Shift"
75
As⁺
into
150
N d ⁺,
Sm⁺⁺, 40Ar35Cl⁺
is converted
75As16
O⁺
150
S m⁺, 91Zr⁺
Q2 filled with
reactive gas (O
Q1 set to analyte
mass (m/z 111)
2
)
111
Cd⁺, 95Mo16O⁺
"On Mass"
95Mo16O⁺
oxide products such as MoO
95
Mo⁺
forms higher
2
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