Thermo Scientific Barnstead Smart2Pure 12 UV/UF Operating Instructions Manual

Operating instructions
Thermo Scientific Barnstead Smart2Pure 12
Water Purification System
with external tank
  Art. no.: 50129888 (Standard)   Art. no.: 50129890 (UV)   Art. no.: 50129889 (UF)   Art. no.: 50129845 (UV/UF)
Serial no.: ................................
These instructions are to be read prior to starting installation and start-up!
50129897; Status: 04.12 Rights to technical changes reserved
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
2
EC Declaration of Conformity
according to EC Machines Directive 2006/42/EG, Appendix II A
We herewith declare that the design and construction of the machine named below and the
types of it that we have introduced into the market conform to the fundamental safety and
health requirements of EC Directive 2006/42/EC.
This declaration loses its validity when changes which were not agreed to by us are made to
the machine.
Manufacturer: Thermo Electron LED GmbH Robert-Bosch-Straße 1 D-63505 Langenselbold Germany
Description of the machine:
Function: Ultrapure water system
Types: Smart2Pure 12, Smart2Pure 12 UF, Smart2Pure 12 UV, Smart2Pure 12 UV/UF,
Article nos.: 50129888, 50129889, 50129890, 50129845
We also declare that the product complies with the following applicable Guide­lines/Directives:
Electromagnetic Compatibility Directive (2004/108/EG)
Harmonized standards applied:
DIN EN ISO 12100-1 Safety of machines, Part 1: Principles DIN EN ISO 12100-2 Safety of machines, Part 2: Technical Guidelines DIN EN ISO 14121-1 Safety of machines, Part 1: Risk Assessment DIN EN 61326-1
Authorized person for documentation:
Detlef Opp Stockland 3 D-56412 Niederelbert
Niederelbert, 1 April 2011
Detlef Opp, Technical documentation manager Signature
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
3
Preface
Dear Sir or Madam,
With your decision for this ultrapure water system from the Smart2Pure series, you have se­lected a high-quality product.
Thank you for the confidence you have placed in us.
Before you start to install and operate this ultrapure water system, please carefully read the in­formation on how it is to be properly installed and operated that is given in these operating in­structions.
This is particularly important, as we, the manufacturer, cannot accept liability for any damage occurring as a result of improper operation of the system, or from use of it for other than the in­tended purpose.
Niederelbert, 15.04.2011
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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1. Contents
Preface ......................................................................................................... 3
1. Contents .................................................................................................. 4
2. Explanatory notes on the operating instructions ..................................... 6
3. Transport and packaging ........................................................................ 7
3.1 Examination on receipt ....................................................................................................... 7
3.2 Complaints ......................................................................................................................... 7
3.3 Packaging and return shipment .......................................................................................... 7
4. Extent of delivery .................................................................................... 8
5. Safety precautions .................................................................................. 9
6. Intended application .............................................................................. 11
6.1 Application areas .............................................................................................................. 11
7. Technical specifications ........................................................................ 12
8. How Smart2Pure functions ................................................................... 14
8.1 Flow chart, Smart2Pure 12 Standard ............................................................................... 15
8.2 Flow chart, Smart2Pure 12 UF ......................................................................................... 16
8.3 Flow chart, Smart2Pure 12 UV ......................................................................................... 17
8.4 Flow chart, Smart2Pure 12 UV/UF ................................................................................... 18
9. Installation of the system ...................................................................... 19
9.1 Installation location ........................................................................................................... 19
9.2 Installation ........................................................................................................................ 20
9.3 Mounting the power pack (voltage supply) ....................................................................... 22
10. Start-up ............................................................................................... 24
11. Brief operating instructions ................................................................. 25
12. Operating elements ............................................................................. 26
13. System control .................................................................................... 27
13.1 Menu .............................................................................................................................. 27
13.2 Setting the limiting value for the conductivity ................................................................. 27
3.3 Setting the limiting value for temperature ......................................................................... 28
13.4 Communication .............................................................................................................. 28
14. Maintenance ....................................................................................... 29
14.1 Maintenance intervals .................................................................................................... 30
14.2 Replacing the pretreatment cartridge ............................................................................. 31
14.3 Replacing the filter cartridge ........................................................................................... 32
14.4 Disinfection ..................................................................................................................... 33
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Ultrapure water system
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15. Waste disposal ................................................................................... 34
16. Trouble shooting ................................................................................. 35
17. Replacement pats and consumable materials ................................... 37
18. Accessories ........................................................................................ 39
19. Terminal assignment .......................................................................... 41
20. Maintenance record ............................................................................ 43
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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2. Explanatory notes on the operating instructions
EU Mark of Conformity
CSA - admission
Important operating and/or maintenance instructions! Read the oper­ating instructions with due care
.
Risk of electric shock! Electrical work on the system is only to be car­ried out by qualified personnel.
General information! Particularly important notes are marked with this information sign.
Protective conductor connection
Connect the power supply to an electrical socket with a protective connection.
The information provided in these operating instructions is only valid for the system which has the serial number which is to be entered on the front page.
Please enter the serial number* of your Smart2Pure system in the space provided on the front page.
* Read the serial number of your ultrapure water system from the type plate.
For quick and correct service, please include the following information on all inquiries and re­placement parts orders which relate to your system:
- The serial number
- The article number
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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3. Transport and packaging
Ultrapure water systems are carefully controlled and packed prior to dispatch, but damage could nevertheless still occur during transport.
3.1 Examination on receipt
- Check the completeness of delivery against the delivery note.
Is the packaging damaged?
- Inspect the system for damage.
3.2 Complaints
If damage has occurred to the system during transport:
- Immediately contact the post, railway or forwarding agent*.
- Keep the packaging and outer cardboard box for possible examinations and return
shipment.
3.3 Packaging and return shipment
Whenever possible, use the original cardboard box and packaging material.
Should these no longer be available:
- Pack the system in packing film and a strong cardboard box
- Protect the system against damage from shock.
* The time limit for complaints is 6 days (after receipt of the goods). The right to claim for damages expires when this time has elapsed.
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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4. Extent of delivery
The following Smart2Pure ultrapure water system versions, each with a performance of 12 L/h, are available:
50129888 Smart2Pure 12 (Standard system) 50129889 Smart2Pure 12 UF (Standard system + Ultrafiltration module) 50129890 Smart2Pure 12 UV (Standard system + UV-Photooxidation) 50129845 Smart2Pure 12 UV/UF (Standard system + UV-Photooxidation + Ultrafiltration module)
(Please compare the article number of your wanted version with the article number given on the delivery note.)
1x Smart2Pure 12 (acc. to version) Article no. 50129xxx 1x Pure water tank 30 or 60 litres Article no. 06.50xx
and an assembly kit consisting of:
Pretreatment cartridge Article no. 09.2012 Filter cartridge Article no. 09.1020 Sterile filter capsule, 0.2 µm Article no. 09.1003 Feedwater connecting kit, R 3/4" Article no. 25.0071 Connecting hose, o.d. 1/4", 6 m Article no. 18.0137 Ball valve, dia. 1/4" Article no. 15.0112 Tabletop power pack, 24 VDC Article no. 50133713 Universal adapter Article no. 21.1006 Universal holder Article no. 21.1007 Connecting cord (rubber connector to nema plug connector) Article no. 50132200 Connecting cord (rubber connector to british ST plug connector) Article no. 50132203 Connecting cord (rubber connector to euro plug connector) Article no. 50132215 Operating instructions Article no. 50129897 Put in angle connector d1/4” Article no. 14.0361 T-connector d1/4” Article no. 14.0362
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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5. Safety precautions
Observe these safety precautions for your own safety!
The Smart2Pure version that you have selected is a state-of-the-art ultrapure water
system, the intended purpose of which is to purify tap water of drinking water quality.
Please do not start to install and operate the system until you have read through the
information that is given in these operating instructions.
Please note that the use of the system for other than the intended purpose and/or im-
proper operation of it release the manufacturer from all liability.
Lifting and carrying the ultrapure water system, e.g. to the installation location, should
be carried out by two people. To lift it, each takes hold of it under the base plate at two corners.
The CE-mark is invalidated when constructional changes are made to the system or
foreign products are installed in it.
Protect the system from frost. The temperature at the installation area must be at least
+ 2°C.
Observe all general rules and regulations that are valid at the installation location, in-
cluding the relevant current accident prevention regulations.
Feedwater pressure min. 1 bar and max. 6 bar. Should it be higher, then an additional
pressure reducer must be installed.
According to DIN EN 1717, water purification systems must be equipped with a device
that safeguards the tap water against contamination.
A suitable electric socket must be made available for the system (see Technical speci-
fications).
The installation area must have a drain at floor level with at least DN 50 pipe and
which allows free run off.
When the system is to be wall-mounted please check that the wall has sufficient load
bearing capacity (see Technical specifications for the weight).
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Ultrapure water system
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The maximum operating temperature is 40°C.
Proceed as follows during longer system standstills (e.g. long holidays) when neither a
floor drain nor a water watcher is available,:
Switch the system off (unplug the mains plug). Close off the supply of water to the ultrapure water system.
Do not start the system up again with the water supply closed off, as the pump would then suffer damage. The manufacturer accepts no liability should this occur.
When installing the ultrapure water system, ensure that there is sufficient working
room around it for problem-free usage (e.g. filter replacement, connections etc.).
The guarantee is valid for a period of 12 months!
Never look directly at a switched-on UV-lamp, as the UV light would endanger your
eyesight! The UV-lamp is only to be replaced by personnel from a authorised com­pany.
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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6. Intended application
The continually increasing requirements that ultrapure water quality must fulfil, the ever stricter demands resulting from technological advances and increasingly lower detection limits in labo­ratories, together with the need for user-friendly systems and complete solutions, were the basis for the development of the novel Smart2Pure ultrapure water systems.
Smart2Pure systems have been specifically designed to produce sterile filtered ultrapure water that is free of particles, salts and organic compounds.
6.1 Application areas
- Analytical techniques in laboratories:
- HPLC (
High Performance Liquid Chromatography )
- IC (
Ion Chromatography )
- ICP (
Inductive Coupled Argon Plasma )
- AAS (
Atomic Absorption Spectrophotometry )
- TOC-Analyse (
Total Organic Carbon )
- etc.
- Reagent and solution preparation:
- Cell culture media
- Tissue culture media
- Make up water for reagents used in on-line analytical systems
- Water for high-purity rinsing in laboratories
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Ultrapure water system
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7. Technical specifications
Demands made on the feedwater
Source Drinking water acc. to DIN 2000. Blocking index (SDI) max. < 3 for all versions. With higher values, a prefilter
must be installed upstream. Free chlorine concentration < 0.1 mg/L Manganese content < 0.05 mg/L Iron content < 0.05 mg/L pH-Range 4 - 11 Temperature 2 - 35 °C Pressure 1 - 6 bar
Product water of quality ASTM I (dispensing valve)
Standard UV UF UV/UF
Conductivity µS/cm 0.055 0.055 0.055 0.055 Resistance Mxcm at 25°C 18.2 18.2 18.2 18.2 TOC ppb 5 - 10 1 - 5 5 - 10 1 - 5 Bacteria CFU/ml < 1 < 1 < 1 < 1 Bacterial endotoxines
EU/ml
-- --
< 0.005* < 0.005*
Particles > 0,2 µm < 1/ml < 1/ml < 1/ml < 1/ml Flow rate l/min 1.0 1.0 0.6 0.6 Typical amount withdrawn
up to 30 litres per day
* Dependent on feedwater and disinfection
Product water of quality ASTM II
Standard UV UF UV/UF
Conductivity µS/cm 0.067 - 0.1 0.067 - 0.1 0.067 - 0.1 0.067 - 0.1 Resistance Mxcm at 25°C 10 - 15 10 - 15 10 - 15 10 - 15 Retention quota for bacteria and particles
Ø 99 % Ø 99 % Ø 99 % Ø 99 %
Permeate performance
L/h 12 12
12 12
Dimensions
Height: 545 mm Width: 305 mm Depth: 300 mm Weight: Smart2Pure 12 Standard 20 kg Smart2Pure 12 UF 20 kg Smart2Pure 12 UV 21 kg Smart2Pure 12 UV/UF 21 kg
Airborne sound emission
Sound-pressure level 49 db(A)
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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Water connections
Feedwater Hose, 1/4" o.d. Concentrate Hose, 1/4" o.d. Tank water supply Hose, 1/4" o.d. Tank water return Hose, 1/4" o.d. Pure water Hose, 1/4" o.d. Dispensing valve outlet Hose, 8 - 10 mm o.d.
Electrical connections / external switched mode power supply
Input voltage AC 100 – 240 V, 50 – 60 Hz, 5 – 3.8 A Output voltage DC 24 V, 3.8 A System connection DC 24 V, 80 W Serial interface RS 232 Potential-free contact max. 30V, 2A Protection Class Class II (external SMPS certified as Class I)
Ambient conditions (DIN EN 61010-1 (VDE 0411-1):2011-02)
Usage Indoor rooms Height Up to 2000 m Temperature range From 5° C to 40° C Relative humidity Maximum relative humidity 80 % at temperatures of
up to 31° C, linearly decreasing to 50 % relative hu­midity at 40° C
Line-voltage variation
Not more than
± 10 % of the line voltage
Transient overvoltages As usually occur in the supply network (overvoltage
category II acc. to IEC 60364-4-443). Note
: The rated level of transient overvoltage is the withstand impulse voltage acc. to overvoltage cate­gory II of IEC 60364-4-443
Ventilation requirements There are no special requirements with regard to ven-
tilation.
Degree of pollution 2
Materials of parts that contact water
Pump head Nylon with glass fibre UV-Lamp High-purity quartz UV Housing Stainless steel Filter cartridge PP UF Housing Polycarbonate Raw water Solenoid valve PA Recirculation Solenoid valve PA Rinsing solenoid valve PA Pressure hold valve Brass, chemically nickel-plated Dispensing valve POM Conductivity measuring cell PVC, stainless steel Connectors POM Hoses PE Gaskets EPDM RO-Membrane PA
Thermo Scientific Barnstead Smart2Pure
Ultrapure water system
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8. How Smart2Pure functions
Raw water solenoid valve V1 is closed during Stand-by and standstills. This prevents raw water from flowing into the system when it is not in operation and so protects the external tank B1 from overflowing.
In normal operation, tap water having a maximum pressure of 6 bar flows into the system and is pumped by pressure booster pump P1 through the subsequent pretreatment F1 and reverse osmosis membrane F2. The latter retains all salts dissolved in the incoming water to the extent of the given retention quota and, because of the molecular size of the membrane pores, also bacteria, pyrogens and particles to Ø 99%.
The permeate flows through the downstream purification stages, such as UV-photooxidation UV1, the 185 nm and 254 nm wavelengths of which reduce organic compounds (only with Smart2Pure versions UV and UV/UF), filter cartridge F3 and ultrafilter F6 with automatic rinsing (only with Smart2Pure versions UF and UV/UF) to the tank.
The retained water constituents are led away in the remaining concentrate. The special conductivity measuring probe QISA 300 (with temperature compensation) and tem­perature probe TIA 500 permanently monitor the conductivity and temperature of the ultrapure water and the values of these are shown in the display.
To ensure a constantly high water quality, the water in the storage tank is recirculated at regular intervals by recirculation pump P2. Float switch LS 100 monitors the water level inside the tank..
Pressure hold valve V2 is factory adjusted. A change in this adjustment could lead to damage to the reverse osmosis membrane. Fluctuations in the temperature and pressure of the feedwater make it necessary for the adjustment of the pressure hold valve, and of the concentrate flow that is
linked to it, to be checked and re-adjusted at regular intervals by Service or service personnel from a authorised company.
Concentrate flows for Smart2Pure 12
to be checked/adjusted every 3 months
Permeate flow
[L/h]
Concentrate flow
[L/h]
12 60
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