Teledyne IR-7000 User Manual

OPERATING INSTRUCTIONS FOR
IR7000
NDIR Gas Analyzer
REV. 3
NDIR Gas Analyzer Safety
Copyright © 2000 Teledyne Analytical Instruments.
All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed, stored in a retrieval system, or translated into any other language or computer language in whole or in part, in any form or by any means, whether it be electronic, mechanical, magnetic, optical, manual, or otherwise, without the prior written consent of Teledyne Analytical Instruments, 16830 Chestnut St. City of Industry, Ca. 91748
Warranty
This equipment is sold subject to the mutual agreement that it is warranted by us to be free from defects of material and of construction, and that our liability shall be limited to replacing or repairing at our factory (without charge, except for transportation), or at customer plant at our option, any material or construction in which defects become apparent within one year from the date of shipment, except in cases where quotations or acknowledgments provide for a shorter peri o d. C omponents manufactured by others bear the warranty of their manufacturer. This warranty does not cover defects caused by wear, accident, misuse, neglect or repairs other than those performed by Liston or an authorized service center. We assume no liability for direct or indirect damages of any kind and the purchaser by the acceptance of the equipment will assume all liability for any damage which may result from its use or misuse.
We reserve the right to employ any suitable material in the manufacture of our apparatus, and to make any alterations in the dimensions, shape or weight of any parts, in so far as such alterations do not adversely affect our warranty.
Important Notice
This instrument provides measurement readings to its user, and serves as a tool by which valuable data can be gathered. The information provided by the instrument may assist the user in eliminating potential hazards caused by his process; however, it is essential that all personnel involved in the use of the instrument or its interface be properly trained in the process itself, as well as all instrumentation related to it.
The safety of personnel is ultimately the responsibility of those who control process conditions. While this instrument may be able to provide early warning of imminent danger, it has no control over process conditions, and it can be misused. In particular, any alarm or control systems installed must be tested and understood, both as to how they operate and as to how they can be defeated. Any safeguards required such as locks, labels, or redundancy, must be provided by the user or specifically requested of Teledyne Analytical Instruments at the time the order is placed.
Therefore, the purchaser must be aware of the hazardous process conditions. The purchaser is responsible for the training of personnel, for providing hazard warning methods and instrumentation per the appropriate standards, and for ensuring that hazard warning devices and instrumentation are maintained and operated properly.
Teledyne Analytical Instruments cannot accept responsibility for conditions beyond its knowledge and control. No statement expressed or implied by this document or any information disseminated by the manufacturer or its agents, is to be construed as a warranty of adequate safety control under the user’s process conditions.
Teledyne Analytical Instruments, - Rev. 3
Table of Contents
Important Safety Information....................................................S-1
S.1 General Format.............................................................S-1
S.2 Specific Hazards...........................................................S-2
Introduction....................................................................................1
1.0 Overview .......................................................................... 2
1.1 Standard Features........................................................... 4
1.2 Optional Features............................................................ 4
1.3 IR Detection ..................................................................... 6
1.4 Operator Interface........................................................... 6
Operational Theory........................................................................8
2.1 Introduction ..................................................................... 8
2.2 Optical Bench.................................................................. 8
2.3 Electronics..................................................................... 11
2.3.1 Power Supply Board........................................... 11
2.3.3 Main Board.......................................................... 12
2.3.4 Display Board...................................................... 14
2.3.5 I/O Board ............................................................. 14
2.4 Sample System.............................................................. 14
2.5 Internal Gas Handling System...................................... 16
Installation....................................................................................18
3.1 Overview ........................................................................ 18
3.2 Unpacking and Installation........................................... 18
3.3 Mounting the Analyzer.................................................. 18
3.4 Gas Connections........................................................... 19
3.5 Sample System Considerations................................... 20
3.6 Electrical Connections.................................................. 21
3.6.1 Analog Output..................................................... 22
3.6.2 Analog Output Connections.............................. 25
3.6.3 Solenoid Valve Connections.............................. 25
3.6.4 Optional Relay Outputs...................................... 26
3.6.5 Digital I/O Option ................................................ 27
3.6.6 RS-232 Cable....................................................... 28
3.6.7 Power Connections............................................ 29
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NDIR Gas Analyzer Safety
Operation......................................................................................31
4.1 Overview ........................................................................ 31
4.2 The SETUP Menu........................................................... 31
4.3 The MODE Menu............................................................ 39
Calibration....................................................................................46
5.1 Overview ........................................................................ 46
5.2 Typical Sample System ................................................ 46
5.3 Manual Calibration........................................................ 47
5.3.1 Manual Zero Calibration..................................... 47
5.3.2 Manual Span Calibration.................................... 48
5.4 AUTO Calibration .......................................................... 50
5.5 Calibration Issues ......................................................... 51
Maintenance.................................................................................53
6.1 Scheduled Maintenance ............................................... 53
6.1.1 Cleaning .............................................................. 53
6.1.2 Particle Filter....................................................... 53
6.2 Service ........................................................................... 55
6.2.1 Removing the Optical Bench............................. 55
6.2.2 Cleaning the Sample Cell................................... 58
6.2.3 Replacing the IR Source .................................... 59
6.2.4 Replacing the Battery (Portable Model Only)... 59
6.2.5 Changing the Fuse ............................................. 60
6.3 Display Messages ......................................................... 61
6.3.1 Error Messages................................................... 62
6.3.2 Normal Operation Messages ............................. 65
6.3.3 Normal Operator Induced Messages ................ 66
Appendix ......................................................................................69
A-1 Specifications.................................................................... 69
A-2 Recommended Spare Parts List .................................. 71
A-3 RS-232 Communication Protocol .................................... 72
A-3.1 Codes for "e" Type Messages........................... 76
A-3.2 Codes for "s" Type Messages........................... 77
A-3.3 Codes for "c" Type Messages........................... 77
A-3.4 Codes for “m” Type Messages.......................... 78
A-3.5 Codes for “a” Type Messages........................... 78
Addendum A……………………………………………………………..
Configuration and Compliance Certificates
Addendum B…………………………………………………………….. Automatic Calibration Electrical Connection Diagram
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Important Safety Information
S.1 General Format
Important information relating to health and safety of personnel, possible equipment damage and special instructions regarding instrument setup and operation are setoff and highlighted within this manual. The following format will be used in this manual to indicate safety hazards and special instructions:
Symbol Heading Typeface and
Description
WARNING 12 poi nt bol d t ypefa ce.
Contains important informa tion w hi ch i f ignored could result in persona l in jury or dea th.
CAUTION 12 poi nt bol d t ypefa ce.
Contains important informa tion w hi ch i f ignored could result in dam ag e t o t h e syst em.
NOTE
No Symbol
12 point Italic typeface. Contains important or helpful information relating to the setup and/or operation of the system.
Read this instruction manual carefully and familiarize yourself
thoroughly with its contents. Do not ignore any warnings or cautions or operate this equipment with any safety feature
Safety IR7000
defeated or inoperable. Failure to heed warnings or cautions can result in injury or death as well as damage to the instrument.
S.2 Specific Hazards
WARNING: ELECTRICAL HAZARD! Hazardous voltage is present inside. Keep
away from Live Circuits. Under no circumstances should untrained personnel open any panel or remove any cover, lid or wiring harness without proper guidance and supervision.
Component replacement, internal adjustments and electrical service must be made by qualified maintenance personnel. Always disconnect the power cable and discharge circuits before servicing the equipment. To avoid accidental power up, Liston recommends using an electrical lock­out device whenever maintenance is to be performed. Disconnect power to any other equipment connected to the instrument to avoid the possibility of component failure and transmission of dangerous voltage through signal connections.
WARNING: FLAMMABLE GAS HAZARD! EXPLOSION HAZARD! TOXIC GAS
HAZARD! Do not operate this instrument in an explosive atmosphere. Read all documentation that comes with this instrument especially any application notes or addenda which, among other important details, may specify the nature and properties of the gas to be analyzed.
Unless specifically designed for hazardous environment application, this instrument is not designed to handle explosive or flammable gases. Exposed electrical terminals pose a substantial risk of ignition if powered in the presence of flammable gas. The sample system is not appropriate for handling toxic, flammable or explosive gases!
If your application requires using toxic, flammable or explosive gases for analysis or calibration, please consult the factory. An explosion proof instrument with enhanced sample system is available as an option.
WARNING: ELECTRICAL HAZARD! This instrument must be properly
grounded.
To avoid shock hazard, the instrument chassis and cabinet must be connected to an electrical ground. The instrument is equipped with a three conductor AC power cable. This cable must be plugged into an approved three-contact electrical outlet. The power jack and plug of the power cable meet International Electro-Technical Commission (IEC) safety standards. When replacing this cable, use only the proper replacement cable as listed in the Spare Parts Listing in the Appendix.
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NDIR Gas Analyzer Safety
WARNING: Do not attempt to service or make adjustments to this equipment
while working alone.
Whenever servicing or adjusting this equipment, notify your supervisor and have another person capable of rendering first aid standby in case of an accident.
WARNING: Do not substitute parts or modify this instrument.
The IR7000 was designed and tested at the factory. The quality, safety and workmanship inherent in this product is a result of careful design, selection and assembly of components. Any use of non-authorized replacement parts can impair the functioning of this system. In addition to voiding your warranty, any substitution of non-authorized replacement parts or unauthorized modifications to the instrument can create an unnecessary risk of harm. Return the analyzer to Teledyne Analytical Instruments for service and repair to ensure proper functioning of the unit.
WARNING: Do not operate a damaged instrument.
If any of the built-in safety features of this instrument is impaired, either through physical damage, excessive moisture, or any other reason, IMMEDIATELY REMOVE POWER. Do not use the instrument until safe operation can be verified by service-trained personnel. If necessary, return the instrument to Teledyne Analytical Instruments. for service and repair.
DANGER
HIGHLY TOXIC AND/OR FLAMMABLE LIQUIDS MAY BE PRESENT IN THIS MONITORING SYSTEM PERSONAL PROTECTIVE EQUIPMENT MAY BE REQUIRED WHEN SERVICING THIS SYSTEM. HAZARDOUS VOLTAGES EXIST ON CERTAIN COMPO NENT S INTERNALLY WHIC H MAY
PERSIST FOR A TIME EV EN AFTER THE POWER IS TURNED OFF AND DISCONNECTED. ONLY AUTHORIZED PERSONNEL SHOULD CONDUCT MAINTENANCE AND/OR SERVICING.
BEFORE CONDUCTING ANY MAINTENANCE OR SERVICING CONSULT WITH AN AUTHORIZED SUPERVISOR OR MANAGER.
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Safety IR7000
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Introduction
Introduction 1 IR7000
1.0 Overview
The Teledyne analytical Instruments Model IR7000 Non-Dispersive Infrared Gas Analyzer is a versatile microprocessor based analyzer for measuring or monitoring a gas stream. The IR7000 analyzer is available in a variety of configurations to suit most applications.
The IR7000 series analyzer is designed for rapid monitoring of a process gas stream. Four user definable chart ranges are available for accurate monitoring over the full range of the process gas composition. A trace analysis unit is available for analysis at low ppm levels. This manual describes the setup and operation of the Model IR7000. It also covers particular features of the other analyzers in the IR7000 series where setup and operation differs from the standard unit.
MODEL DESCRIPTION
IR7000 Panel/19” Rack Mount – CE Mark IR7010 Split Architecture, Analysis Unit – Explosion Proof IR7000P Portable Battery Operated with AC Charger IR7000T Similar to IR7000 for Trace Analysis
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NDIR Gas Analyzer Introduction 1
IR7000D Dual Optical Bench for Monitoring 2 Gases IR7000B Wall Mount Unit
The standard rack mount model IR7000 is shown in Figure 1-1 and the portable IR7000P is shown in Figure 1-2. The explosion proof models have the analysis unit installed in an explosion proof housing and employ steel tubing and fittings in the sample system. The control unit on these models is separate from the analyzer and generally located outside the hazardous environment.
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Introduction 1 IR7000
1.1 Standard Features
The following features are standard on the IR7000 series of analyzers:
User selected automatic zero and span calibration
Linearized output over the entire full scale range eliminating the need for separate instrument ranges to achieve full span
Closed sample path is not exposed to ambient air eliminating the need for purging of the cell compartment
Four user-definable chart ranges plus auto-ranging
Selectable analog output: 0–1, 0–5, or 0–10V or optionally, a 4–20mA non-isolated or isolated current output
High and low alarms or limits with adjustable setpoints. The alarms are configured at the factory for either latching or non­latching operation
Modular design for easy maintenance
Configured to easily accommodate an optional oxygen channel for simultaneous oxygen analysis at either 0–25% or 0–100%
Patented IR detector uses a sensitive mass flow sensor and a dual chamber for rapid analysis of IR absorption in a sample flow
Unique optical bench design eliminates mechanical chopping of IR source
IR bench does not require tuning for maximum signal like other optical NDIR systems
• Self-diagnostic software installed
Easy setup and maintenance
Easy to operate with all user controls accessible from the front panel
CE Mark (IR7000 Rack and battery portable)
1.2 Optional Features
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NDIR Gas Analyzer Introduction 1
To extend the versatility of the Ir7000 series of analyzers, many
options are available.
Dual optical bench for simultaneous monitoring of 2 gases
Oxygen channel (0–25% or 0–100%). The IR7000 series easily accepts Teledyne analytical Instruments oxygen electrochemical cell for measuring oxygen levels in the process gas.
RS-232 port for control input and data output via a remote computer
4–20ma analog current output either isolated or non-isolated
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Introduction 1 IR7000
Relay outputs. Single pole double throw (SPDT) relays driven off the status signal, high, and low limit alarms can be installed for triggering status alarms, indicators, or other customer supplied peripherals.
External sample system. The instrument can be supplied with a sample handling system ensuring safe delivery of conditioned sample gas to the analyzer.
Z-Purge system. The split-architecture models can be fitted with a Z-Purge system for automatic purging of the NEMA-4 enclosure.
1.3 IR Detection
Central to the IR7000 analyzer is the unique patented IR detector. It incorporates 2 chambers in optical series at the end of a gold-coated sample cell. The chambers are connected through a tiny orifice. IR is differentially absorbed in the 2-chambered detector and causes a mass flow between the chambers. The modulation of the IR signal causes the chambers to quickly readjust and the flow reverses. A sensitive mass flow sensor located in the tiny orifice between the 2 chambers senses the flow in both directions and outputs a signal related to the concentration. A high-resolution electronic circuit is employed to provide synchronous detection of the flow sensor’s signal. This circuit allows the IR7000 to measure gas compositions over a wider range of the infrared spectrum than conventional photon-based IR analyzers.
1.4 Operator Interface
Except for the split architecture models (Explosion Proof), the analysis and control sections are housed together in a single compact metal housing. A NEMA-4 enclosure is used on the IR7000B wall mountable model.
All operator input and display of process information takes place from the panel (or on the control section panel for the split architecture instruments). There are minor differences in the location of some of the components among the different models within the IR7000 series but each instrument has the following front panel components:
Display—vacuum fluorescent with 2 lines of 16 characters.
The display sends data and information to the user about the process and guides the operator through the calibration and operation.
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NDIR Gas Analyzer Introduction 1
Input Buttons—4 push buttons are installed on the front panel
and are used to enter data and set operational modes.
Flowmeter—an integral flowmeter is mounted on the front
panel for monitoring the sample flow through the instrument.
Power Switch—an off/on switch is mounted on the front panel
for powering up the instrument.
Sample Pump Switch (IR7000P only)—this switch controls
the operation of the sample pump on portable models.
Sample Pump Connector (IR7000P only)—a quick
disconnect nylon fitting is mounted on the front panel of portable models for attaching the sample probe to the instrument.
.
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Operational Theory
2.1 Introduction
The IR7000 is a microprocessor controlled, single beam infrared analyzer that employs an electronically modulated IR source with no moving parts.
The analyzer is composed of 2 subsystems:
• Optical Bench
• Electronics
2.2 Optical Bench
At the heart of the IR7000 NDIR Gas Analyzer is the patented dual chambered balanced detector. The advanced detector design offers higher sensitivity and selectivity with a greater dynamic range compared to other IR detectors in the marketplace.
The optical bench is shown in Figure 2-1. It consists of:
• Sample cell
• Detector
• IR source
• Filter cell
Windows and seals
The sample cell is a gold coated glass tube (metal Tube Optional) through which the sample gas flows. At one end of the sample cell, infrared energy is generated by a modulated IR source. The modulation is achieved electronically by feeding the IR source a 4 Hz square wave generated by the source control circuit on the main PC board. The electronic modulation is very stable and eliminates the need for mechanical choppers and motors routinely used in other IR systems. At the other end of the optical bench is the detector and filter cell.
NDIR Gas Analyzer Operational Theory 2
Figure 2-1: Optical Bench Components
The detector consists of 2 chambers filled with the gas of interest in optical series with a sensitive mass flow sensor. The sensor measures a fluctuating mass flow between the 2 chambers due to a differential in infrared absorption between the chambers.
The 2 chambers of the detector are of unequal volume, the first chamber, called the primary chamber, is much smaller than the trailing chamber, or secondary chamber. A small passageway connects the 2 chambers and contains the mass flow sensor. During assembly at the factory, both chambers are filled with the gas of interest and due to the unequal volume, a vastly different optical path length exists between the chambers.
Initially, with only nitrogen (zero gas) passing through the sample cell, pulsed IR radiation from the source passes through the cell. Since this is the zero gas, no differential absorption takes place. At the rear of the sample cell an IR transparent window (typically sapphire but may be some other material depending on the application) allows the radiation to pass into the primary detector chamber. Due to the heteroatomic nature of the gas contained within the chambers (identical to the gas to be monitored), IR absorption takes place at a few characteristic wavelengths corresponding to the most strongly absorbed lines for that particular gas in the IR spectrum. The remaining radiation passes through to the secondary chamber.
The secondary chamber has a much greater path length and therefore additional absorption takes place but at different energies. Due to the longer residence time of the optical beam in this chamber, absorption occurs at weaker absorption bands in the IR and accounts for the less intense absorption relative to the primary chamber. The remaining unabsorbed energy is eventually dissipated.
Essentially, the front chamber absorbs IR differentially at specific wavelengths characteristic of the gas of interest within the detector
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Operational Theory 2 IR7000
chamber while the rear chamber absorbs radiation at primarily weaker absorption bands. The absorption causes the gas to heat up and the differential nature of the absorption process causes the front chamber to heat up more than the rear chamber. Since the chambers are charged with gas, the pressure in the primary chamber becomes higher than in the secondary chamber. This pressure differential causes a net flow of gas from the primary chamber to the secondary chamber through a tiny orifice connecting the 2 chambers. The gas cools in quick order and the flow reverses until the pressures are once again equal.
A mass flow sensor is placed in the orifice between the 2 chambers and senses the mass transport between them. It is designed in such a manner as to be able to sense minute flows in either direction. The sensor produces a signal resulting from an electronic imbalance each time mass flow is detected (in either direction) through the orifice. The signal is passed along to a preamplifier and then to a voltage to frequency converter for enhanced signal processing. The microcontroller retains this information as a zero gas reading for calibration and offset in real measurements.
When the process is repeated and a span gas is introduced into the sample cell, a slightly different condition exists. Now IR absorption takes place within the sample cell. Less energy is received at the detector. But since the primary chamber is smaller than the secondary chamber and differential absorption takes place at predominately strongly absorbing wavelengths within the primary chamber, the difference in energy of the gas in the primary chamber is less than when there is no IR absorption in the sample cell. The energy of the gas in the secondary chamber is also less but the change is not as dramatic. Hence the patented balanced design detector produces a different signal when an IR absorbing gas is introduced in the sample cell. The resulting signal is inversely related to the concentration of the gas of interest in the sample cell.
Between the IR window and the detector is the filter cell. Depending on the nature of the sample gas, some applications could experience interference in the absorption band spectra. For instance, both CO and CO
absorb at wavelengths in the IR very close to each other. The presence of CO2 could produce a measurement error in a system designed to detect
CO. The filter cell is a sealed volume of gas specifically designed to “comb out” the offending absorption line or lines before the radiation reaches the detector. The filter cell in some cases acts as a thermal barrier to keep the detector from experiencing sudden temperature fluctuations.
2
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NDIR Gas Analyzer Operational Theory 2
2.3 Electronics
The IR7000 uses a sophisticated microprocessor to control the signal processing, I/O, and display functions within the analyzer. Custom EPROMs are installed with permanently stored data and routines specific to the customer’s application. Depending on what options are installed, 2 or more PCB’s are used in the electronic subsystem. Figure 2-2 shows the location of the boards in the portable model. Other models are similar but mount the boards differently.
2.3.1 Power Supply
This unit is externally powered by either 120 or 230 VAC. Fuses are located on the back panel for circuit protection.
Figure 2-2: PC Board Identification and Location
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Operational Theory 2 IR7000
2.3.3 Main Board
In effect, the main board imports an analog signal from the preamplifier and outputs a digital signal. A lot of signal conditioning and processing is performed along the way. Major functions of this board include:
• Amplification The signal from the detector is amplified
• Filter The analog signal is filtered and conditioned
A to D Converter The analog signal is digitized using a voltage to frequency
converter
• Microprocessor Encodes both the amplitude and phase of the digital signal
Counts, integrates, and stores the signal Handles input and output to and from the main board
• Linearizer Scales and linearizes the signal using data and algorithms
permanently stored in the microprocessor
• Filter De-spikes, pre-filters and filters the signal again with a
filter rate chosen by the operator
The main board receives the raw signal from the detector and amplifies it. In the analog circuit portion of the main board, the signal is filtered to remove any electrical interference before passing it along to the digital section as a relatively clean sine wave of several volts.
The sine wave is digitized using an onboard voltage to frequency converter. In this process, both the amplitude and phase of the digital signal are encoded and integrated. The microprocessor counts the digital pulses and linearizes it using a 7th order polynomial whose coefficients were determined at the factory based on the particular detector.
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NDIR Gas Analyzer Operational Theory 2
The data is linearized over the entire instrument range. This linearization is inherently more accurate than the conventional process of segmenting and optimizing the data over a narrow range.
Before being sent to the read out display or output as a voltage, the result is de-spiked and filtered then scaled for the appropriate chart output range. Filtering uses a selectable algorithm to damp sudden value changes. The amount of filtering applied is determined by the operator and generally depends on the process. Large filter values yield a correspondingly lower instrument response but higher sensitivity.
The de-spiking filter is a software routine used to clean up the signal. Essentially it looks at the last 5 instrument readings and discards a reading if it varies significantly over the average. A “rolling average” method of filtering is also applied through the software. This filtering process depends on the filter value set by the user. Increasing the filter number gives more weight to the last entry into the instrument reading buffer, hence the “rolling average” is influenced to a greater degree by the last input.
Figure 2-3 is a system block diagram which shows the functional relationship between the electronics and the optical bench.
Figure 2-3: System Block Diagram
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Operational Theory 2 IR7000
During calibration, the microcontroller on the main board stores information regarding zero and full span values. Specifically, the microprocessor takes a series of consecutive readings and calculates the difference between pairs of consecutive readings. The embedded software analyzes the resulting differences and tests for discrepancies in the result. The microprocessor uses this information to test for drift during calibration.
The absolute difference between a true zero and 100% span gas is determined at the factory and permanently stored in memory. The software compares this value with collected data during a calibration or measurement to determine the validity of the reading. If the calibration or sample gas measurement falls outside a predetermined range based on the known good values in memory, error routines are called and signals are sent to the display board to generate appropriate messages. See Section 5 Calibration for more information.
2.3.4 Display
The display contains the 2-line 16 character vacuum fluorescent display on the front panel. Signals are transferred to and from the main board via a ribbon cable.
2.3.5 I/O Board
The standard I/O board is responsible for taking a analog signal from the main board and converting it to a 0–1, 0–5 or 0–10 V analog output. An optional 4–20 mA isolated current ouput may be installed depending on the options selected by the customer. See Section 3.7.1.
2.4 Sample System
If a sample system is not provided by LSC, the customer will be responsible for providing a suitable sample system. A custom sample system can be designed and fabricated by LSC based on the particular application. Contact Teledyne Analytical Instruments for details.
In order to achieve maximum results from the analyzer, some consideration must be given to the sample system design. The sample system is responsible for supplying properly conditioned sample and calibration gases to the analyzer at a pressure and flow rate commensurate with the analyzer. The sample system provided by the customer must be capable of delivering clean and moisture free (non-condensing) sample to
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NDIR Gas Analyzer Operational Theory 2
the instrument with a flow rate between 0.2–2.0 liters per minute (2.0 to
5.0 liters per minute for low level optical bench) at 5 psig or less. For samples greater than 5 psig contact factory. The sample temperature must be in the range of -10 to 50°C (14–122)°F.
WARNING: The maximum rated pressure of the sample cell is 5 psig.
Exceeding this pressure at any time may cause the sample cell to fail. This could result in harmful release of sample gas.
The following are items to be provided by the customer:
• Calibration gases
• Nitrogen (N
) for zero calibration
2
Span calibration gas Use a span gas with a concentration of the gas of
interest greater than 50% of the largest desired measurement. The span gas should be between 10% and 100% of the instrument’s full scale, preferably around 80%. For example, if the largest expected reading is 3000 ppm, then the calibration gas should be at least 1500 ppm.
The balance of the span gas should be N2. If the instrument has a dual optical bench (Model
IR7000B or IR7000D), the span gas must contain calibration values for both species being measured.
If an optional oxygen (O2) sensor is installed, the span
gas must contain a calibration value for O2. If the 0– 25% O
sensor is installed, use a calibration gas
2
containing 20% O2.
Pressure regulator, flow adjustment valves, tubing and fittings for delivering properly conditioned sample gas to the instrument. The sample gas pressure must be less than 5 psig. For pressures above 5 psig contact factory.
• Pressure regulator, flow adjustment valves, tubing and fittings for delivering calibration (zero and span) gas to the instrument.
If the automatic calibration feature is to be used, the customer must also supply 2 solenoid valves. The split architecture versions of this instrument are capable of handling 3 solenoid valves. Refer to Section 3 Installation and Setup for details regarding the installation of these components.
• The sample gas should be vented to atmospheric pressure. If the
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Operational Theory 2 IR7000
sample gas is to be returned to the process or flare, suitable back
pressure controls should be employed to ensure the analyzer vents at a constant pressure.
2.5 Internal Gas Handling System
The gas handling system inside the analyzer is similar in principle for all models. The following information describes the internal gas handling system for the IR7000 model. Variations for other models will be noted.
Figure 2-4 is a diagram of the internal components and plumbing for directing calibration or sample gas through the analyzer.
Figure 2-4: Sample Path Through Analyzer – Sta ndard Model
Either sample or calibration gas is delivered under pressure to the analyzer by the customer or LSC supplied sample system. The gas enters the analyzer and passes through a 0.3-micron disposable filter to remove any particulate matter. If an O2 channel has been incorporated, the O
2
sensor is installed in series with the sample cell. The gas passes first through the O2 sensor and then through the sample cell and out to the
sample return.
In the portable model, a 12V DC mini-pump is installed between the disposable filter and the sample cell. Otherwise the internal plumbing is the same.
The internal gas handling systems installed in the split-architecture and explosion proof models vary according to the specific application. In general, the plumbing is the same as the standard models with the following exceptions:
Metal tubing and fittings replace Teflon lined PVC tubing
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NDIR Gas Analyzer Operational Theory 2
Stainless steel, brass or copper fittings are installed for mating to the customer’s sample system or throughout the system for a LSC supplied sample system.
A different filter and a filter housing is used
NOTE: Because these models are often supplied for custom applications,
please check the front of this manual for any included Addendum which will describe features, notes and warnings that specifically apply to your instrument.
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Installation
3.1 Overview
Installing the Model ir7000 consists of:
Unpacking and Inspection
• Mounting
• Gas Connections
• Electrical Connections
• Calibrating the System
3.2 Unpacking and Installation
The analyzer is shipped ready for installation. You should have received a single carton containing the analyzer and power cord (except 230 VAC versions). If you have ordered an instrument with the optional O2 sensor channel, the electrochemical cell will have been installed at the
factory.
Carefully unpack the instrument and inspect it for any damage or missing components. Signs of damage would include dents, scratches, broken glass inside the casing etc. Check that you have received the power cord or battery charger for the portable model. Contact the shipper immediately to report shipping damage. Contact the factory for missing parts.
3.3 Mounting the Analyzer
The ir7000 series of analyzers are designed to be used indoors and in a general-purpose area. The split-architecture models (explosion proof) are designed to have the analysis unit operate in a hazardous environment with the control unit remotely located in a general-purpose area.
The instrument must be kept dry and protected from:
• Direct sunlight
Direct air currents which could affect the temperature of the sensors
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