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Revision A (Document Number 82WIN-900-01)...............................................................April 1997
Revision B (Document Number 82WIN-900-01).................................................................October 1999
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S
afety Precautions
The following safety precautions should be observed before using this product and any associated instrumentation. Although
some instruments and accessories would normally be used with non-hazardous voltages, there are situations where hazardous
conditions may be present.
This product is intended for use by qualified personnel who recognize shock hazards and are familiar with the safety precautions
required to avoid possible injury. Read and follow all installation, operation, and maintenance information carefully before using the product. Refer to the manual for complete product specifications.
If the product is used in a manner not specified, the protection provided by the product may be impaired.
The types of product users are:
Responsible body
ment is operated within its specifications and operating limits, and for ensuring that operators are adequately trained.
Operators
instrument. They must be protected from electric shock and contact with hazardous live circuits.
Maintenance personnel
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A good safety practice is to expect that hazardous voltage is present in any unknown
no conductive part of the circuit may be exposed.
5/02
bles or jumpers, installing or removing switching cards, or making internal changes, such as installing or removing jumpers.
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!
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ranty.
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User’s Guide
Model 82~WIN
Simultaneous C-V
Measurement
Keithley instruments, Inc.
Release Date: April 1997
Accumulation
I-
Depletion
if-
\
ligh-Frequenqd .
he0 Deoletion
. .
V substrate
Inversion
Quasistatic
High Frequency
l
Contents
C-V Measurement
Introduction
Typical Measurement Sequence
First Time System Testing and
Measurement Procedures
Choose the Right Parameters .................................................................................................. .18
This chapter provides detailed information on using Metrics ICS
software with Keithley Model 82-WIN to set up C-V
measurements and acquire C-V data. A quicker and easier
approach is to use Keithley libraries, which contain typical
measurement setup parameters and analysis algorithms to
extract many parameters from basic C-V measurements. The
next chapter provides detailed information on how to use
Keithley libraries.
This chapter is organized as the following:
Typical Measurement Sequence: Outlines the basic
measurement sequence that should be followed to ensure
accurate measurements and analysis.
First Time System Testing and Cable Correction: Describes
the procedure to test the complete system for the presence of
unwanted characteristics such as leakage resistance, leakage
current, and stray capacitance. It also details the cable correction
procedure that must be performed in order to ensure accuracy of
high-frequency C-V measurement.
Measurement Procedures: Describes basic procedures for
making C-V measurement. A simultaneous C-V measurement
example is included to illustrate the procedures.
User’s Guide Model 82-WIN Simultaneous C-V
C-V Measurement l 1
Choosing the Right Parameters: Briefly discusses the
considerations in choosing right measurement parameters to
achieve accurate
C-V
measurements. It also describes a
procedure to determine the correct delay time to optimize C-V
measurements.
Additional C-V Measurement Features: Includes a
description of squarewave, single staircase, double staircase,
and capacitance vs. delay time measurements.
Measurement Considerations: Outlines numerous factors that
should be taken into account in order to maximize measurement
accuracy and minimize errors.
2 0 C-V Measurement User’s Guide Model 824MN Simultaneous C-V
Typical Measurement Sequence
Measurements should be carried out in the proper sequence in
order to ensure that the system is optimized and error terms are
minimized. The basic sequence is outlined below. If your
system is properly set up, tested, and calibrated, you may skip
Steps 1 and 2. Otherwise you must perform the testing and
calibration procedures.
Step 1: Test and
Correct for System Leakage and Strays
Initially, you should test and determine if any problems, such as
excessive leakage or unwanted stray capacitance, are present.
You should correct these problems before making C-V a
measurement. Refer to your system manuals for proper
installation and testing procedures. After initial testing, the
system need be tested only when you have changed some
aspects of its configuration, such as connecting cables or test
futures.
Probe-up suppression should be performed before each
measurement to ensure accuracy. This procedure is discussed in
the measurement section in detail.
Step 2: Correct for Cabling Effects
Cable correction is necessary to compensate for transmission
line effects through the connecting cables and remote input
coupler. Transmission line effects are more significant at higher
frequencies and with longer cables, or with switches in the
system. Failure to perform cable correction will result in
substantially reduced accuracy of high-f?equency C-V
measurement. In order to perform correction, you must connect
the Model 5909 calibration capacitors to the system, and
perform the correction procedure under Metrics ICS. Cable
correction must be performed the first time you use your
User’s Guide Model 82-WIN Simultaneous C-V
C-V Measurement * 3
system. After that, it needs to be performed only if the system
configuration
is
changed in
some
manner, or if the ambient
temperature changes by more than 5’C.
Step 3: Configure Your System with Metrics ICS
If you are not using the Keithley library setup to make C-V
measurement, it will be necessary for you to properly configure
your system under Metrics ICS, including GPIB, instrument,
switching matrices, measurement parameters, etc. You should
refer to the Metrics ICS and Keithley C-V Driver manuals for
detailed information regarding configuration of your system.
Step 4: Make a C-V Measurement
Before you can actually make measurements, you must select
measurement parameters such as sweep mode, range, frequency,
and voltage values. As the sweep is performed, measured values
are stored in data arrays for analysis and later retrieval.
Step 5: Analyze C-V Data
4. C-V Measurement
Besides Metrics ICS and Keithley C-V drivers, the Keithley
C-V system includes libraries for setup and data analysis.
Depending on the options you choose, you will be able to
extract a large amount of useful information from your C-V
measurement data. Available analysis features include doping
profile, flatband capacitance and voltage, interface trap density,
and mobile ion density, etc.
User’s Guide Model 82-WIN Simultaneous C-V
First Time System Testing and Cable Correction
Leakage Test
Before using the system, it is necessary to check system
leakage. Zero suppress in Metrics ICS is intended to correct for
small system leakage current and stray capacitance. Any
excessive leakage problem must be solved before attempting a
measurement. Procedures are outlined below.
You should run a probe-up test sweep to determine if there is
excessive system or voltage-dependent leakage and stray
capacitance. You may also load the Keithley standard system
leakage check library. Refer to the C-V Libraries and Analysis
chapter for information on using the leakage check library. Note
that setup parameters should be same as those used for your
measurement.
Once leakage check setup is loaded and properly configured,
click on Single on the Meas button. After the sweep, you may
view the capacitance and Q/t vs. voltage plots. There are two
key items to note when performing this procedure. For a typical
system, capacitance and Q/t values should be as small as
possible. Ideally, the stray capacitance should be less than 1%
of the expected capacitance values for optimal accuracy, and
leakage current should be very small as well. Typically, leakage
current should be less than 0.5 pA on the 200pF range, while on
the 2nP range, leakage current should be less than 2pA. In
addition, stray capacitance or leakage current should not display
any voltage-dependent features.
User’s Guide Model 824MN Simultaneous C-V C-V Measurement l 5
Make sure proper cables are installed in the correct
1.
places. Be certain you have not interchanged Model
4801 (low noise) cables with the Model 705 1 (50R)
cables or other regular cables.
Make sure all connecting jacks and connectors are f?ee
2.
of contamination. Clean any dirty connectors with
methanol, and allow them to dry thoroughly before
use.
Be certain that you are making a probe-up
3.
measurement.
Check to see that no leakage paths are present in the
4.
test future.
If necessary, tie down cables to avoid noise currents
5.
caused by cable flexing. Also avoid vibration during
testing.
6 l C-V Measurement
Verify that all cables are of the proper type and not of
1.
excessive length.
Verify the integrity of all cable shields, and that the
2.
shield connections are carried through to the
connectors.
Again, make sure the procedure is being performed in
3.
the probe-up configuration.
User’s Guide Model 824VlN Simultaneous C-V
Cable Correction
The Keithley library disk includes a standard cable calibration
file with typical cable compensation for the Keithley
simultaneous C-V system; the tile name is STANDARDCAL.
This file maybe be copied to the UCS sub directory of the hard
disk for initial use.
For optimal accuracy, system cables must be compensated, and
you should perform a new cable calibration on your system.
You may load the Keithley leakage check library for cable
calibration purposes. Click on the Setup Editor button, then
click on the Opts option button. If you have performed cable
calibration, you may load the calibration file. Otherwise, you
must perform cable calibration to assure measurement accuracy.
4. Use a test fixture of good, low capacitance design. Use
low-noise, coaxial, or triaxial probes.
5. Make certain the test fucture shield is in place when
characterizing the system. The same precaution holds
true when characterizing or measuring a device.
6. If problems persist, see Measurement Considerations at
the end of this chapter.
In order to perform cable calibration, you will need the Model
5909 calibration capacitors. Disconnect your test future and
connect each calibration capacitor in its place when prompted to
do so. Use the supplied female-to-female BNC adapters to
connect the sources to the cables. Calibration capacitors should
be connected to the end connecting to the probe station. When
making the connection, be sure not to handle the cables and
capacitors excessively, since the resulting temperature rise will
change the capacitance values. Refer to Figure 1 for
connections.
User’s Guide Model 82WlN Simultaneous C-V
C-V Measurement l 7
5951
Remote Input Coupler
to sa%rssmElNFvrauRER
Figure 1
Cable Correction Capacitor Connecfions
Performing Cable Correction
1.
Click on the Calibration button, and the cable
calibration window shown in Figure 2 will be
displayed.
2.
Select the frequency and range you want to calibrate,
then follow the prompts to connect the calibration
capacitors to the cable.
3.
Once calibration is finished, the screen should appear
as shown in Figure 3.
8 l C-V Measurement
User’s Guide Model 82-WIN Simultaneous C-V
4. Save this file as CABLE.CAL or the name you prefer.
Note that the file extension must be .CAL.
5. Now load the calibration file, then exit the Opts
window. You should now be in the Setup editor.
6. Click the Done button to exit SetuD.
Current calibration filename
Calibration file
Low CAP @f) :
High CAP
KO, Real
KO,
Kl, Real :
Kl, lmag :
hag
(~9 :
:
:
595 Display
Figure 2
1.
1 kHr -: rjl oakliz
fas1.933 I 1461.97 I 1462.4 1
Options Setup window
”
;,.,, I <..i^ ‘.:
I
,nlMht
Figure 3
User’s Guide Model 82-WIN Simultaneous C-V
System Cable Calibration window
C-V Measurement l 9
Measurement Procedures
Detailed information about properly configuring your system
can be found in Metrics ICS and Keithley Instruments C-V
driver manuals. Here, only a brief summary related to Keithley
C-V system is provided. An example of making a simultaneous
C-V measurement is outlined.
GPIB Configuration
Once the GPIE3 board is properly installed and tested, click on
the GPIB button on the menu strip. You should select the GPIB
card installed in your computer (see Figure 4). Note that the
GPIB Timeout option must be set to at least two times the
expected maximum sweep delay time, or a GPIB timeout error
may occur.
WPE
.
:
-“‘I
IO. C-V Measurement
Sub-Type
IKI KMCX38.2
Oj#i 0 ns:
Timeout
30 sect
Delay
No Delay
Figure 4
q
Iail
@!I
ED &ddr
]
I
Cl Show Messages
q
Show bog
Communicafions Setup Window
User’s Guide Model 824VlN Simultaneous C-V
Instrument Selection
You may have installed several Keithley instrument drivers with
your Metrics core. You can make a selection here, such as a
K182 Simultaneous C-V system. Alternatively, you can select
KI23x I-V, KU90 High Frequency C-V, and KI595 Quasistatic
C-V instruments.
Instrument Setup
1.
Click the Connect button to select the K182 driver.
GPIB bus address menu appears when you click the
Configuration button.
2.
Type in the corresponding primary address for each
instrument.
3.
Click the Verify button to test if instruments are
correctly configured. If they are not correctly
configured, an error message will appear. Otherwise,
the following message will be displayed: “The system
is correctly configured.”
4.
Once the system is correctly configured, ICS will
automatically store the configuration. After this
procedure, the configuration step need not be run again
unless the instrument configuration changes.
1. Click on the Setup button; the instrument setup editor
window will appear. (See Figure 5.)
The
2. Click on New, and the program will prompt you to
type in the Setup name.
User’s Guide Model 824MN Simultaneous C-V
C-V Measurement l 11
You may
select many different devices. For this
example, select the MOSFET icon.
Click on Source Unit, then click on K182 IN to select
the input.
Click on the G (gate) on the MOSFET symbol to
connect the input to the gate.
Similarly, click on KI82.OUT to select the output,
then click on the B (substrate) symbol of the MOSFET
to connect the output to the substrate.
Click on the W82 OUT icon; the measurement
parameter setup window will appear. (See Figure 6.)
You may now select the proper measurement
parameters. The parameter window should appear like
the one shown in the Figure 6. Refer to the Metrics ICS
and Keithley C-V driver manuals for full details on all
setup parameters.
12 * C-V Measurement
Before you make a measurement, be sure to load the
cable correction and calibration file. To do so, click on
the Opts. button in the Setup Editor, then click on
Load option to select the calibration file for your test
fucture.
Exit from the Opts. window and the Setup Editor
window.
. The zero cancel procedure described below will correct
system leakage and stray capacitance. Note that large
leakage current or stray capacitance should not be
suppressed. Determine the source of the problems, and
correct them before using your system.
!. Click on the Meas. button, and note there are several
options from which to choose. (See Figure 7.)
;. Before you make measurements, you should do a
probe-up zero suppress by clicking on the Zero Cancel
button and following the instructions.
C. After the zero cancel procedure, the message “Please
lower your probe” will be displayed on the screen.
During this period, the Model 590 C-V meter is in its
active reading mode, and you may lower your probe to
contact the DUT while at same time observing the
Model 590 display reading. Doing so ensures proper
electrical contact between the probe and DUT.
14 0 C-V Measurement
i. You are now ready to make a C-V measurement. For
this example, click on the Single button to make a
single-sweep measurement. You may observe that
when instrument finishes data taking, the data screen
will flicker a few times. This situation is normal while
ICS is updating the data. If the analysis package has
been loaded, it make take some time to perform the
calculations and display the data, depending on the
amount of data and the speed of your computer.
User’s Guide Model 824VlN Simultaneous C-V
Analyzing Data
Before you attempt to analyze data, you should plot raw dam
and determine if there are any obvious measurement problems.
Keep in mind that no analysis will compensate for substandard
system-related problems and select better measurement
parameters. If a large amotmt of noise is present, analysis results
will not be dependable and may even be meaningless. Repeat
the measurement procedure to determine the root cause of the
problems, and correct them before proceeding.
Figure 7
Measurement Selection Window
data caused by measurement problems. At this time, you may
find it necessary to make a few adjustments to compensate for
The first step is to transfer the analysis constants to
Metrics. Click on the Transform Editor button, then
the name, value, unit, and comments into the fields.
User’s Guide Model 82WlN Simultaneous C-V
C-V Measurement 0 15
2.
Click on the New Plot button to draw a new graph.
The Setup Plot window will pop up. (See Figure 8.)
3.
Select the data option you wish to plot. For our
example, select Vsm as the X-Axis data parameter. Fo:
a simultaneous C-V measurement, plot both Cn and Cc
on the y-axis.
t.
You may select one data set to plot on the y axis.
Select the data you wish to plot on the Y l-Axis
column. If you wish to plot another data set on a
different scale but on the same graph, select that data
set for the Y2-Axis column.
j.
If you wish to plot two sets of dam on the same scale
you may use the Build Group feature. Click on the
Build Group button, and add both Cu and Co to the
group, for example Sim-CV. (See Figure 9.) After you
close this window, you will notice a Sim-CV group is
available under the y-axis sub-menu selection. Choose
Sim-CV for the y-axis.
18
l C-V
Measurement
i.
Click on Apply and then Done. You should see both
Co and C, curves plotted on the graph. By using the
Build Group feature of Metrics ICS, you can put many
curves on the same graph. Also notice that you can set
up a second y-axis with different scale and different
data set.
User’s Guide Model 82WlN Simultaneous C-V
Plot Definition:
Axis Options:
Data Group:
Scale Type:
Min Value:
Max Value: 11.981
Setup Name: -1
Data Orientation:
Q Column Vectors
*
m-o]
-1
piz--l
Figure 8
Setup PIof View Mlindow
q
lAEpend data only to
View Vectors.
Data Vectors:
User’s Guide Model 82-WIN Simultaneous C-V
Figure 9
View Vectors:
Col 1: CH
Co12 CQ
Build Plot Group window
C-V Measurement. 17
Choose the Right Parameters
Optimal C-V Measurement Parameters
Simultaneous C-V measurement is a complicated matter.
Besides system considerations, you should carefully choose the
measurement parameters. Refer to the following discussion for
considerations when selecting these parameters.
Start, Stop, and Step Voltages
Most C-V data is derived from the steep transition, or depletion
region of the C-V curve. For that reason, start and stop voltages
should be chosen so that the depletion region makes up about
113 to 213 of the voltage range. (See Figure 10.)
Simultaneous CVvs. Vgs
18 l C-V Measurement
VGS (‘4)
Figure 10 Typical Simultaneous C-V Curve
User’s Guide Model 824MN Simultaneous C-V
The upper flat, or accumulation region of the high frequency
C-V curve defines the oxide capacitance, Cox. Since most
analysis relies on the ratio C/Cox, it is important that you
choose a start or stop voltage (depending on the sweep
direction) to bias the device into strong accumulation at the start
or the end of the sweep.
You should carefully consider the size of the step voltage. Start,
stop, and step size determine the total number of data points in
the sweep. Some compromise is necessary between having too
few data points in one situation, or too many data points in the
other.
For example, the complete doping profile is derived from data
taken in the depletion region of the curve by using a derivative
calculation. As the data point spacing decreases, the vertical
point scaling is increasingly caused by noise rather than changes
in the desired signal. Consequently, choosing too many points
in the sweep will result in increased noise rather than an
increased resolution in C-V measurement. It also takes more
time to perform a C-V sweep.
Many calculations depend on good measurements in the
depletion region, and too few dam points in this region will give
poor results. A good compromise results from choosing
parameters that will yield a capacitance change of
approximately ten times the percentage error in the signal.
Sweep Direction
For C-V sweeps, you can sweep either from accumulation to
inversion, or from inversion to accumulation. Sweeping from
accumulation to inversion will allow you to achieve deep
depletion-profiling deeper into the semiconductor than you
otherwise would obtain by maintaining equilibrium. When
sweeping from inversion to accumulation, you should use a
light pulse to achieve equilibrium more rapidly before the
sweep begins.
User’s Guide Model 82-WIN Simultaneous C-V
C-V Measurement l 19
Delay Time
For accurate measurement, delay time must be carefully chosen
to ensure that the device remains in equilibrium in the inversion
region during a sweep. With too fast a sweep the device will
remain in non-equilibrium, affecting Q/t (Figure 1 l), and also
resulting in skewed C-V curves (Figure 12).
Non-equilihrium Current Q-tvs.Vgs
20. C-V Measurement
Figure 11
Leakage Current Q/t 77mugh Device
User’s Guide Model 82WN Simultaneous C-V
Capacitance
T Delay T Delay
- Erroneous curve because - Erroneous curve because
maximum maximum delay time is delay time is
Figure 12 Figure 12
Choosing Optimum Delay Time Choosing Optimum Delay Time
Keithley Simultaneous C-V system has a built-in library to help
you determine optimal delay time quickly and easily. Refer to
the C-V Libraries and Analysis chapter for procedures, or use
the following procedure to determine optimal delay time.
Determining the Optimal Delay Time
For accurate interface trap density measurement, delay time
must be carefully chosen to ensure that the device remains in
equilibrium in the inversion region during a sweep.
1. Click on the Setup Editor button, then click on the
Source Units button.
2. Click on the IU82.OUT icon to open up the parameter
setup window. (See Figure 13.)
User’s Guide Model 82JMN Simultaneous C-V
C-V Measurement l 21
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