We warrant each of our products to be free
from defects in material and workmanship. Our
obligation under this warranty is to repair or
replace any instrument or part thereof which,
within a year after shipment, proves defective
upon examination. We will pay domestic
surface freight costs.
To exercise this warranty, call your local
field representative or the Cleveland factory,
DDD 216-248-0400. You will be given assist-
ance and shipping instructions.
REPAIRS AND RECALIBRATION
Keithley Instruments maintains a complete repair service and standards laboratory in Cleveland, and has an authorized field repair facility
in Los Angeles and in all countries outside the
United States having Keithley field representatives.
To insure prompt repair or recalibration service, please contact your local field representative or the plant directly before returning the
instrument.
Estimates for repairs, normal recalibrations,
and calibrations traceable to the National Bu-
*Yellow Change Notice sheet is included
only for instrument modifications affect-
ing the Instruction Manual.
MODEL 630 POTENTIOMETRIC ELECTROMETER
GENERAL DESCRIPTION
SECTION 1.
l-l.
potentiometer, It measures from 300 millivolts to 500 volts dc with 0.01% limit of error
from source resistances as high as lOlo ohms,
The upit need not be constantly calibrated or manually restandardized for a full year;
the limit of error is specified for one year.
in ut resistance of 1013 ohms,
10 5 ohms at 1% off null and to infinite resistance at null.
put resistance , .the Model 630 draws an absolute minimum of current to avoid loading and
polarizing the source.
lighted decimal points; one-volt,
ranges except the l-millivolt; input polarity switch;
off chassis ground; better than 60 db line-frequency rejection on the l-millivolt range.
Also, full guarding minimizes leakage problems.
l-2. OPERATING MODES. The Model 630 can be used as a five-dial potentiometer or as a
vibrating-reed electrometer.
500 volts full scale with *O.Ol% limit of error and from 1 millivolt full scale to 300
millivolts within 30 microvolts.
measure from 1 millivolt full scale to 500 volts within 23% full scale.
DESCRIPTION
The Keithley Model 630 Potentiometric Electrometer is a convenient, self-contained
a.
Using the guarded, vibrating-reed null detector,
F"'
Features for convenient use include:
c.
on the l-millivolt to l-volt ranges, increasing to over
one-milliampere output for full-scale deflection on all
As a potentiometer,
As a vibrating-reed electrometer, the Model 630 can
GENERAL DESCRIPTION
and below 300 millivolts within 30 microvolts.
the Model 630 has a minimum (slewing)
With this extremely high in-
5 in-line readout dials with automatically
floating operation up to 500 volts
it can measure from 300 millivolts to
1265R
FIGURE 1.
Keithley Instruments Model 630 Potentiometric Electrometer.
1
GENERAL DESCRIPTION
MODEL 630 PO'TENTIOMETRIC ELECTROMETER
l-3.
APPLICATIONS.
Due to its very high input resistance,
a.
the Model 630 is very useful in making accurate dc measurements from high resistance sources frequently encountered in electrochemical
and physical-chemical research.
It is especially useful for measuring potentials from
piezo-electric crystals, electro-chemical cells, grids and plates of tubes, biological
cells and pH electrodes.
fuel-cell studies,
silicon resistivity and capacitor charge measurements, and for mrasur-
The Model 630 is also ideally suited for making Hall-effect and
ing gate potentials of field effect transistors.
The null-detector output permits use with potentiometric recorders and digital volt-
b.
meters equipped with automatic print-out.
duct development,
inspection and production.
The Model 630 is
useful
in quality control, pro-
l-4. SPECIFICATIONS.
AS A POTENTIOMETRIC ELECTROMETER:
LIMIT OF ERROR:
ute warm-up.
LONG-TERM STABILITY:
TEMPERATURE COEFFICIENT:
?O.Ol% of reading or 30 microvolts, whichever is greater, after 30-min-
Accuracy is exclusive of null-detector drift.
Will operate within stated limit of error for one year.
Does not exceed 0.001% per OC.
REPEATABILITY:
MAXIMUM NULL SENSITIVITY:
INPUT RESISTANCE:
Within 0.0025% or 30 microvolts, whichever is greater.
1 millivolt full scale with 30-microvolt resolution.
Infinite at null, from 0 to 500 volts.
0 to 500 volts with DETECTOR INPUT Switch in OPEN position.
FLOATING OPERATION:
INPUT ISOLATION:
500 volts maximum off chassis ground.
Circuit ground to chassis ground: 108 ohms shunted by 0.05 microfarad.
AS A VIBRATING REED ELECTROMETER:
VOLTAGE RANGES:
NULL RANGES:
INPUT RESISTANCE:
O-5 volt full scale to 500 volts in four decade ranges.
1 millivolt full scale to 100 volts in six decade ranges.
1013 ohms or 1010 ohms selectable by switch, L-millivolt to l-volt
ranges; 1010 ohms, 5 to 500-volt ranges.
ELECTROMETER ACCURACY:
ZERO DRIFT:
Less than 2 millivolts per 24 hours after Z-hour warm-up.
f3% of full scale on all ranges, exclusive or noise and drift.
non-cumulative.
10 15
ohms at.l% off null frop
Long term drift is
RISE TIME (10% to 90%): Less than 2.5 seconds on any range with 1010 ohm source resistance.
LINE-FREQUENCY REJECTION:
Greater than 60 db on the l-millivolt range, decreasing to 35
db on the 500-volt range.
2
1067R
MODEL 630 POTENTIOMETRIC ELECTROMETER
GENERAL CHARACTERISTICS:
GENERAL DESCRIPTION
LINE STABILITY:
Better than 5 ppm for 10% change in line voltage.
RECORDER OUTPUT:
output:
1 volt, 1 milliampere for full-scale meter deflection on all ranges except on
l-millivolt range, where it is 10% less.
Noise:
30 microvolts peak-to-peak referred to input up to 1 cps.
Note: Recorder used must have fully isolated input, lOlo ohms minimum to ground.
POLARITY: Positive or negative, selectable by switch.
CONNECTORS: Input:
POWER:
105-125 or 210-250 volts (switch selected); 50, 60 or 400 cps; 50 watts.
DIMENSIONS, WEIGHT:
Special Triaxial. output: Banana jacks.
5-l/2 inches high x 17-l/2 inches wide x 13-l/2 inches deep; net
weight, 24 pounds.
ACCESSORIES SUPPLIED:
Model 6302 Input Cable consisting of a mating plug and 3-foot
triaxial cable.
l-5.
more conveniently.
ACCESSORIES.
Model 6301 Guarded Probe with 3-foot connecting cable allows measurements to be made
a.
Using the Probe does
not
affect any Model 630 specification.
Model 4000 Rack Mounting Kit, containing two brackets and a top cover, converts the
b.
Model 630 to fit standard 19-inch racks. Rack mounted,
the Model 630 is 5-l/4 inch&s
high x 19 inches wide x 13-l/2 inches deep. Section 6 has assembly instructions.
C. Model 6013 pH Electrode Adapter,which has a Z-foot cable and triaxial connector,
accepts Leeds & Northrop and Beckman pH electrode connectors.
The Adapter allows accurate
and convenient,pH potential measurements with the Model 630.
l-6.
EQUIPMENT SHIPPED. The Model 630 Potentiometric Electrometer is factory-calibrated
and is shipped with all components in place. All units are shipped for bench use. Model
4000 Kit may be ordered for rack mounting;
The shipping carton also contains the Instruction Manual and the Model 6302 Mating
refer to Section 6 for assembly instructions.
Connec-
tor with 3-foot triaxial cable.
016GR
3
OPERATION
s303
?4ODEL 630 POTENTIOMETRIC ELECTROMETER
Reference Voleage Dials
5304
s305
S-306 It381
-
DETECTOR INPUT
Swirch (5102)
Receptacle
FIGUKlc L.
.JlOl
5103 5104
Switch
(S101) (R122)
I'W~~L OJU rronr: .raneL wncrols and Terminals.
CO"tL-01
Replaceable Parts List and schematic diagram.
Switch
(5104)
SwFtch
(5301)
The designations refer to the.
4
FIGURE 3. Model 630 Rear Panel
Controls
and Tarminzlr.
1265
MODEL 630 POTENTIOMETRIC ELECTROMETER
OPERATION
SECTION 2.
2-1. FRONT PANEL CONTROLS AND TERMINALS.
a.
polarity.
POLARITY Switch.
The Switch reverses the polarity of the internal rc,Ccrcncc voltage supply so
The POLARITY Switch turns the instrument on and sclccts
OPERATION
(See Figure 2).
the
input
both positive and negative voltages may be measured; it does not reverse the meter polar-
ity.
DETECTOR INPUT Switch.
b.
A 3-position toggle switch allows selection of
the
Model
630 input resistance and also allows checking the meter zero.
1) Setting the Switch to 10 10 OIIMS sets the input resistance at 1010 ohms for all
ranges.
Setting the Switch to OPh'N sets the input resistance at 1013 ohms for the l-milli-
2)
volt through l-volt ranges.
The input resistance remains
at
1010 ohms for the ranges
above 1 volt.
3) Setting the Switch to ZERO CK internally disconnects the input from the vibrating
capacitor and shunts the capacitor to the amplifier low. This allows meter zeroing on
any range without removing the input signal.
'c . NULL Switch.
ranges from 1.0 millivolt full scale to 100 volts.
The NULL Switch sets the null detector sensitivity for six decade
When the Switch is in the VTVM posi-
tion, the Model 630 operates as a vibrating-reed electrometer for the four ranges of the
RANGE Switch.
RANGE Switch.
d.
0.5, 5, 50 and 500 volts full scale.
Varley divider and the position of the decimal point light
The RANGE Switch adjusts the sensitivity of the VTVM in four steps:
It also determines the voltage acrws the Kelvin-
- which also serves as a pilot
light - between the five Reference Voltage Dials.
Reference Voltage Dials. Five in-line dials at the top of the front panel set the
e.
reference voltage when the Model 630 is used as a potentiometer.
have decade steps as indicated on the dial.
METER ZERO Control. The METER ZERO Control adjusts the meter needle to zero. The
f.
The last dial is continuously adjustable.
The first four switches
Control allows precise meter zeroing on all ranges when the DETECTOR INPUT Switch is set
to ZERO CK.
Input Terminals. The Model 630 uses a special triaxial receptacle for its INPUT
g.
Receptacle.
Model 6302 Input Cable.
The Control has a. range of approximately 120 millivolts.
The Receptacle is similar to a bnc connector, but requires using the furnished
Using a standard bnc conmctor could damage the INPUT Receptacle.
A set of binding posts marked LO and GND is provided for grounding the LO input terminal
to the chassis when desired.
The LO terminal and the shell of the triaxial INPUT Recep-
tacle are internally connected.
2-2.
a.
REAR CONTROLS AND TERMlNALS.
Fuse.
For LOS-125 volt operation, the Model 630 uses a l-ampere 3 AG fuse.
(See Figure 3)
210-250 volt operation, the Model 630 uses a 0.5-ampere 3 AG fuse.
0166R
For
5
OPERATION
MODEL 630 POTmTIOMETRIC ELECTROMETER
Power Cord.
b.
less otherwise specified on the rear panel.
3-prong plug provides a ground connection for the cabinet. A 3:2 prong adapter is provided.
NULL DETECTOR OUTPUT.
C.
null detector.
COARSE ZERO Switch.
d.
tact potential of the vibrating-reed capacitor.
ten ZO-millivolt steps.
117-234 Switch.
e.
or 234volt ac power lines.
2-3.
power cord.
PRELIMINARY PROCEDURES.
Check the 117-234 Switch and the Fuse for the proper ac line voltage. Connect the
a.
Set the Model 630 front panel controls as follows:
b.
DETECTOR INPUT Switch
RANGE Switch
NULL Switch VTVM
Reference Voltage Dials
The Model 630 is designed for a 105-125 volt, 60-cps line source, un-
The 3-wire power cord with the NEMA approved
A screwdriver adjustment is provided for bucking out the con-
The screwdriver-operated slide switch sets the Model 630 for 117
POLARITY Switch
Two terminals, marked + and -,
The Switch has a i-100 millivolt span in
ZERO CK
500
-I.
ZWXJ
supply a dc signal from the
The decimal light between the third and fourth Dials will light. Allow the instrument
to'warm up 30 minutes to meet the specified accuracy on all ranges.
Set the NULL Switch to 1.0 MV.
c.
mally, using the COARSE ZERO Control on the rear panel is not necessary. Return the
NULL Switch to VTVM.
Check meter zero periodically.
per day,
DETECTOR INPUT Switch to ZERO CK disconnects the input signal source from the
instrument, avoiding polarization.
2-4. OPERATING PROCEDURES,
The Model 630 is used first as a voltmeter to determine the approximate value of
a.
the unknown voltage.
to 10.01%.
Vibrating capacitors are extremely sensitive to shock and vibration. when
making a measurement,place the Model 630 on a vibration free, rigid structure
or on some material which will minimize vibration.
the input cable and any attached circuitry; any cable flexure will generate
electrostatic charges which the Model 630 will detect.
which will cause inaccuracies in continuous readings.
It is then used in the potentiometric mode to determine the voltage
Zero the meter with the METER ZERO Control.
Null detector drift can be up to 2 millivolts
Setting the
It is not necessary to disconnect the input.
Also,
tightly tie down
Nor-
6
L265R
MODEL 630 POTENTIOMETRIC ELECTROMETER
OPERATION
FIGURE 4.
measuring at ground and for floating.
In A, the unknown voltage has one terminal at ground. The shorting Link is between
the LO and GND Posts of the Model 630.
In B, the unknown voltage has both terminals off ground potential. The floating or
off-ground potential must be less than 500 volts. Also note the shorting line is pe&
used.
The Model 630's high input resistance allows circuit measurements without causing
b.
circuit loading. (See paragraph 2-6.) On the l-millivolt to L-volt null ranges, the input resistance can be set to 1013 er 1010 ohms with the DETECTOR INPUT Switch. Use the
OPEN (1013 ohm input) setting for high source resistances; use the LOLO OHMS setting to
avoid pickup problems or to increase response speed.
resistance is 1010 ohms for either setting.
When making measurements on devices with high contact resistances (such as
silicon), completely isolate the power supply from ground to avoid measuring
the drop acress the contact resistance.
c. Voltmeter Operating Procedures.
1.
at VTVM, the RANGE Switch determines one of four full-scale ranges.
Reference Voltage Dials at zero,
six null ranges.
Input Connections to Model 630. The two diagrams show the input circuit for
On ranges above 1 volt, the input
NOTE
Ten full-scale ranges are available for VTVM operation. When the NULL Switch is
By putting the five
the Model 630 can then operate as a voltmeter on the
Connect the unknown voltage to the INPUT Receptacle, using the Model 6302 Input
2.
Cable or the Model 6301 Guarded Probe.
lead to the LO Terminal.
Switch the RANGE Switch to the most sensitive range for an on-scale meter deflec-
3.
tion.
When using the guarded probe, use a separate
7
OPERATION
Potentiometric Operating Procedures.
d.
NOTE
Avoid large overload voltages on the null detector. No damage occurs even
with 500~volt overloads, but some open circuit offset will be caused in the
null detector.
Leave the RANGE Switch at the last setting used in the voltmeter operation. If
1.
the voltmeter reading is negative, reverse the POLARITY Switch position.
Set the first two Reference Voltage Dials to the first two digits of the unknown
2.
voltage found in the voltmeter operation.
When switching between the 50-volt and SOO-volt ranges and when changing the
POLARITY Switch, the meter will sometimes temporarily read off-scale.
due to transients introduced when the circuit is interrupted and it does not
indicate a faulty instrument.
The offset will disappear after about 5 minutes.
NOTE
MODEL 630 POTENTIOMETRIC ELECTROMETER
This is
Set the NULL Switch to the initial
3.
null setting shown in Table 1. Adjust
the Voltage Reference Dials progressively for zero meter deflection while increasing the null detector's sensitivity
with the NULL Switch. Deflections to the
right indicate the voltage being measured
is more positive than the Reference Vol-
tage Dial setting.
NOTE
The most accurate resistors in the Kelvin-Varley divider are in the first
two Reference Voltage Dials. Therefore,
dings, use the first two dials as much as possible.
The value of the unknown voltage is read directly from the Reference Voltage Dials.
4.
The dial reading will be within the specified limit of error if the NULL Switch
a)
is at the most sensitive setting (Table 1) for the range used and if the meter indicates as close to null as possible.
b) When the first Reference Voltage Dial is used,
read to be within specifications (*O.Ol% of reading or 30 microvolts).
meter may be read as an approximation of a sixth digit,
RANGE
Switch
Setting Setting Setting
I
I
500 50 0.5 5v v v v 100 100 10 1.0 Mv v v v
I
TABLE 1. Recommended Model 630 Null Sensitivities and Settings.
to obtain the most accurate rea-
Initial
NULL Switch NULL Switch
only the five Dials need to be
Most Sensitive
1.0 1.0 10 1.0 Mv Mv Mv Mv
However, the
c) When the first Reference Voltage Dial is not used, read the voltage directly
from the remaining four dials.
d) Use the meter as a null indicator when balancing voltages. When the first Ref-
erence Voltage Dial is not used,
8
the meter approximates a fifth dial reading.
0166R
MODEL 630 POTENTIOMETRIC ELECTROMETER OPERATION
2-5. RECOFDER OUTPUT.
Recommended recorder for use with the Model 630 is the Keithley Model 370. Any re-
a.
corder used must be able to float 500 volts off ground and its input must be fully isolated
(1010 ohm minimum leakage resistance to ground).
before attaching the recorder, set all Reference Voltage Dials to zero. Disconnect
b.
The Model 370 meets these requirements.
the unknown voltage and short the Model 630 high input to the low. Set the NULL Switch
to 10 MV.
Connect the recorder to the OUTPUT Terminals on the Model 630 rear panel. The
370 Recorder mates directly with the Model 630 using the 3701 Cable.
Set the Reference Voltage Dials to 10 millivolts to apply an accurate lo-millivolt
c.
potential to the null detector on the lo-millivolt null range.
scale recorder output of 1 volt at 1 milliampere.
corder may load the Model 630 output. On this range,
On the l-millivolt null range, the re-
output resistance is 100 ohms.
This will provide a full-
To obtain accurate results and/or
d.
to
prevent ,damage to the instruments, the recorder
must be able to float off-ground with the Model 630. Leakage and pickup between the two
instruments should also be minimized.
The Model 370 meets these requirements.
NOTE
On the l-millivolt range there is a 10% loading error if the recorder draws
1 ma of current. Thus the output for full scale deflection will be .90 volt,
1 ma.
1. Make sure neither recorder terminal is grounded. Use a 3-wire grounded power line
for the recorder.
If a 2-wire line is used,
connect the recorder chassis and the Model
630 chassis with a separate lead.
2. Minimize all sources of leakage between the output terminals, the recorder and
ground. Use polystyrene or Teflon-insulated cable where possible. If the connecting
wires are shielded, connect the shield to the LO Post.
3. Avoid long leads between the Model 630 and the recorder.
Do not short either Model 630 output terminal to the case; this may damage the
Kelvin-Varley divider.
2-6.
EFFECTIVE INPUT RESISTANCE.
The Model 630 input resistance varies. It can be set either 1013 or 1010 ohms for
a.
the l-volt and lower ranges, and it is 1010 ohms for ranges above 1 volt.
are not the Model 630's effective input resistances.
higher due to the potentiometric principle of operation.
Its input resistance is considerably
When reference voltage (Refer-
ence Voltage Dial setting) is much greater than meter readings the value is
Ri* =
Rn( Ed )
Equation 1
v
Where Rin is the effective input resistance of the Model 630;
Ed is the setting of the Reference Voltage Dials in volts;
'Rn is the input resistance of the null detector in ohms;
V is the null detector meter reading in volts.
1067R
These, however,
9
OPERATION
To find the loading effect the Model 630 will have on a circuit, use Equation 1 to
b.
MODEL 630 POTENTIOMETRIC ELECTROMETER
compute its effective input resistance. At null, where V = 0, the input resistance is
infinite. Off null, the Model 630 input resistance is usually much greater than the
source resistance, and loading will not be enough to affect the measurement accuracy.
graph in Figure 6 shows the Model 630 effective input resistance for the l-millivolt to
l-volt null ranges with the DETECTOR INPUT Switch set to OPEN.
Note that the input resis-
tance for a reading 1.0% off null is 1015 ohms.
NOTE
The
For a ful.ler treatment of paragraphs 2-6 and 2-7,
Product Note,
0.6
zo.5
0
:,o.,
”
0.3
0.2
"The Effective Input Resistance of Potentiometric Voltmeters."
send for Keithley Instruments
0.L
18
FIGURE 6.
tance.
Model 630 Effective Input Res
The graph shows the effective input
resistance for the l-millivolt to l-volt
ranges when the DETECTOR INPUT Switch is
set to OPEN. Percent off null is 160 V/Ed
as defined in Equation 1.
10
~llrluw /. F,rrecr or xxlL^ce KeSlStnnCc on
Model 630 Null Sensitivity.
The graphs are
for the two null detector input resistance
settings.
in equation 2.
Ideally, V = Vs - Ed as defined
The graphs indicate the percent of the actual difference between the
source and reference voltages the meter
will indicate.
0266R
MODEL 630 POTENTIOMETRIC ELECTROMETER
OPERATION
2-7.
the Model 630 is less affected.
tiometric electrometer for accurate measurements from a high resistance source.
where V, is the source voltage in volts;
With no source resistance, the null detector meter will read exactly the difference be-
tween the reference voltage and the source voltage (V = V, - Ed).
resistance, the meter will indicate only a portion of the difference between the two
voltages.
ings for the Model ,630. The curves are the percent the meter reads the voltage difference. At loo%, V = V, - Ed.
indication as an absolute value becomes insignif+cant regardless of source resistance.
For instance, if the Model 630 is 0.1 millivolt off null on the l-millivolt range and the
source resistance is such that the meter indicates only 10% of actual value, the metier
will be within -09 millivolt. At .Ol millivolt off null, the meter will be within 9
microvolts.
NULL SENSITIVITY AND SOURCE RESISTANCE.
Source resistance affects null sensitivity. Because of its high input resistance,
a.
The following paragraphs show the value of using a poten-
The equation below gives the relationship of the meter reading to source resistance:
b.
Equation 2
R, is the source resistance in ohms;
V is the nuli detector meter reading in volts;
Ed is the setting of the Reference Voltage Dials in volts;
R,, is the input resistance of the null detector in ohms
For increasing source
This discrepancy becomes more important the more off null a reading is.
Figure 7 contains graphs showing the effect source resistance has on off-null read-
c.
Note that as the Model 630 approaches null, the meter
NOTE
When the Model 630 is as near to null as possible, the Reference Voltage Dial
setting is always correct within the instrument's specified limit of error.
2-8. AC EFFECTS ON MEASUREMENTS. The Model 630 has greater than 60 db line frequency re-
jection on its l-millivolt range.
sitivity and cause needle quiver or a zero shift.
the input. The component values depend on the source resistance.
might be a 109 resistor and a lOO-picofarad capacitor.
only about two seconds to the rise time.
Use a larger R or C if rise time is not important.
capacitor or one with as good an insulation resistance to avoid degenerating the
input resistance.
2-9. CURRENT MEASUREMENTS.
a. When used with a high-value precision resistor,
trometer can be used to accurately measure currents as low as lo-13 amperes.
Greater line frequency pickup may reduce off-null sen-
To reduce this, use an R-C filter at
A good compromise
ohm source, this adds
With a
NOTE
Always use a polystyrene
the Model 630 Potentiometric Elec-
1010
The choice
0266R
11
OPERATION MODEL 630 POTENTIOMETRIC ELECTROMETER
of the shunt resistor depends upon the
current to be measured and the setting of
the Model 630 (Refer to Table 2).
Current measuring procedure:
b.
Shunt the Model 630 input with a
seikcted resistor R. (See Table 2 for
resistor values).
Set the Reference Voltage Dial Set-
2.
ting to zero and the DETECTOR INPUT
Switch to OPEN.
Switch the Model 630 sensitivity
3.
to the lowest.setting to obtain an onscale reading.
4. The Meter reading is the voltage drop V across the shunt resistor R.
Use the Model 630 as a potentiometer and bring the meter to a null with the Re-
5.
ference Voltage Dials. Record the Reference Voltage Dial reading Ed.
Calculate the current I, using the equation,
6.
Current Range Shunt Resistor NULL Setting
in amperes in ohms
10-13
10-13
10-12
10-12
10-12
10-11
I
10-11 10-11 10-11
TABLE 2.
Use in Current Measurements.
Recommended Shunt Resistors for
10 10
1011
109
1010
1011
108
109 1010 1011
in millivolts
1
10
1
10
100
1
10
100
1000
I
I, =-
where I,
c.
the above procedure is followed.
of measurement may be *4% plus the accuracy of the shunt resistor.
calculate the current to compensate for the loading effect of the shunt resistor.
is the current to be measured in amperes;
R is the shunt resistance in ohms;
V is the meter reading (from step 4 above) in volts:
Ed is the setting of the Reference Voltage Dials in volts.
It is recommended that shunt resistors no larger than 1011 ohms be used
a larger resistor the response is extremely slow.
enough
The accuracy of the measurement is i3% plus the accuracy of the shunt resistor, if
to
affect accuracy may not show up immediately due to the slow response.
However, when using a 1011 shunt resistor the accuracy
1
R
NOTE
(-
Ed v
Ed - V
An offset which 1s largFth
It is necessary to
.
12
0266R
MODEL 630 POTENTIOMETRIC ELECTROMETER
CIRCUIT DESCRIPTION
3-1. GENERAL.
SECTION 3.
The Model 630 Potentiometric Electrometer measures voltage by the potentio-
CIRCUIT DESCRIPTION
metric (null) method. The variable known voltage is an ultra-stable 500-volt reference
supply used in conjunction with a precision 5-dial Kelvin-Varley divider.
Electronic
referencing of the 500-volt output to a zener diode standard maintains the reference supply's stability and accuracy. This method eliminates repeated manual standardization.
The difference between the divider output and the unknown voltage is indicated by the
null detector,
directly from the in-line dials of the Kelvin-Varley divider.
a vibrating-reed electrometer.
At null the unknown voltage can be read
The input and null detector
are fully guarded to avoid leakage.
NOTE
_.__ -_ __ l_..l...-__ - 1_1o ^-...
GUARDED,
VIBRATING-REED
NULL DETECTOR
INPUT
__-__- __.^ _~ _^..... -.
KELVIN-VARLEY
Guard
..,..,.. ..^. .
5.DIAL
DIVIDER
REFERENCE
VOLTAGE
SUPPLY
500 v
SUPPLY
Zener
Reference
Simplified Model 630 Circuit Diagram.
3-2.
FIGURE 8.
REFERENCE VOLTAGE SUPPLY.
Unregulated voltage from transformer T201 is rectified by a silicon half-wave
reziifier, D301, and is filtered by capacitors C302 and C303A.
to the regulator series pass tube, V3004.
Regulator tube V3005 is used to keep the
The voltage then is applied
screen of V3004 at a constant potential.
To obtain a stable, accurate voltage,
b.
divider network of wirewound resistors, R325 to R330.
justed with potentiometer R327 to better than 0.01%.
the 500-volt output of V3004 is sampled by a
The divider network ratio is ad-
Light modulator E302 compares the
sample voltage from the divider network to the voltage across zener diode, D302. Any difference between the
amplifier, V3001.
two
voltages is chopped by E302 and amplified by a 2-stage ac-coupled
'L"ne amplified output of V3001 is converted to a dc signal by light
modulator ~301 and then is amplified by the two-stage differential dc amplifier, V3002
and V3003.
1165
The amplifier output is applied to the grid of the series tube, ~3004, to
13
CIRCUIT DESCRIPTION MODEL 630 POTENTIOMETRIC ELECTROMETER
nullify input variations.
The temperature-compensated zener diode, D302, is used as the basic reference since
c.
typical variations are limited to less than 20 ppm per year and 5 ppm per oC.
Capacitor C305 is used in the ac feedback circuit.
Thus, a
highly stable reference which eliminates manual standardization is provided with respect
to both time and temperature.
The regulated 500-volt output of V3004 is either applied directly to the Kelvin-
d.
The zener diode will also withstand shock and vibration.
Varley divider or it is divided to 50, 5 or 0.5 volts by very stable wirewound resistor
networks. The RANGE Switch, S104, determines which network is used.
The 50-volt range
divider consists of resistors R333, R334, and R335; the 5-volt, or R333, R337 and R338;
and the 0.5-volt of R333, R339 and R340. Using potentiometers R334, R337 and R339
accurately sets the voltage division on each range.
3-3. KELVIN-VARLEY DIVIDER.
The Kelvin-Varley divider precisely divides the reference voltage for nulling an
a.
unknown voltage. It is, in effect, a constant input impedance decade potentiometer, consisting of resistors R341 through R381.
The resistors within each decade are matched;
the decades are matched for each instrument.
Each decade of the Kelvin-Varley divider, except the first, R341 through R346,
b.
parallels two resistors of the preceeding string.
Between the two contacts of the first
Reference Voltage Switch, S303, the total resistance is 40 kilohms (80 kilohms in parallel with the 80 kilohms total resistance of the four remaining strings).
With the RANGE
Switch set at 500, 100 volts dc will appear across the contacts of Reference Voltage
Switch S304, 10 volts across S305,
1 volt across 5306, and 0.1 volt across R381.
3-4.
The input signal is attenuated,
a specially constructed capacitor,
NULL DETECTOR.
The Model 630 uses a null detector which has a vibrating capacitor at the input.
a.
if necessary, and filtered. This signal is modulated by
VClOl, having one stationary plate and one moveable
plate. The signal is then amplified and applied to the meter.
b. Input resistance is greater than 1013
OPEN for the l-millivolt through l-volt ranges.
input signal is attentuated by resistors RlOl through R104.
input resistance is a constant lolo ohms.
ohms when the DETECTOR INPUT Switch is
set
For null ranges greater than 1 volt, the
Therefore,
above 1 volt, the
To maintain high resistance, switching with
the DETECTOR INPUT Switch (SlO2) is done using reed relays, KlOl to K103.
c. The null detector has full-scale sensitivity from 1 millivolt
volt, resistors RlOl through R104 divide the input by a 5OO:l ratio.
to
1 volt.
The full-scale
Above 1
sensitivity is determined by which of six feedback resistors, R147 through R152, is in
the circuit.
nents.
A twin-T filter, tuned for 94 cps, is connected between the plate and grid of
tube V1002.
negative feedback for frequencies other than 94 cps.
An R-C filter - R107 and capacitor Cl01 - decreases the ac input compo-
The filter, consisting of R130, R132, R133, CllO, Cl11 and C112, provides
The vibrating capacitor, VClOl, is
driven at 94 cps to further minimize ac pick-up effects.
The vibrating capacitor VClOl converts the difference between the input signal and
d.
the Kelvin-Varley divider output into an ac voltage, which is amplified by tubes VlOOl,
V1002, and half of V1003. The amplified voltage is demodulated by a bridge, diodes ~106
through D109,
and filtered by resistor R144 and capacitor Cl21.
The dc voltage is fed
to
14
0166R
MODEL 630 POTENTIOMETRIC ELECTROMETER
through a cathode follower, half of tube V1003, and drives the meter.
VClOl has a moveable plate driven by an electromagnet which varies the distance
1.
between the two plates. Since the capacitance varies in inverse proportion to the distance between the plates,
If a charge is placed on the capacitor its value is
2.
a time varying capacitance is produced.
CIRCUIT DESCRIPTION
Q = CE
where Q is the charge;
C is the capacitance;
E is the wltage across the capacitor.
In terms of the voltage, the equation becomes E = Q/C. If Q is constant and C varies
periodically,,E must also vary. Therefore, an ac voltage which is proportional to the
magnitude of the input voltage will be produced.
Resistors R147 through Rl52 form the feedback network, which divides the output
e.
voltage for all voltmeter and null ranges except the 500-volt and l-volt ranges.
output is fed back for these two ranges. The feedback voltage is returned to the low
end of the vibrating capacitor to provide stability.
The Model 630 uses a "driven guard" at its input:
f.
applied to the second conductor of the input cable. The potential between the input high
and low is the difference between the applied and feedback voltages.
capacitance charges only to the difference between the two voltages. This reduces the
effect of cable capacitance,
The zero-control network consists of a 1.35-volt mercury battery, BlOl, and resis-
g.
tors R109 through R123.
volts in 20-millivolt steps.
millivolt span.
providing faster response speed.
The rear panel COARSE ZERO Switch,
The front panel METER ZERO potentiometer, R112, has a 220
the feedback voltage is also
Therefore, the cable
S103, has a span of Cl00 milli.
Equation 3
Total
h. The recorder output is developed across the top end of meter MlOl. It is one volt
for a full-scale meter deflection for all ranges above 1 millivolt. However, using a recorder with a l-milliampere movement reduces the output to 0.9 volt on the l-millivolt
range since the output impedance is 100 ohms on this range.
3-5. OSCILLATOR.
The oscillator drives the vibrating capacitor and bridge demodulator and supplies
a.
the filament voltage for ,tubes VlOOl and V1002.
The output of transistor Q203,
b.
to zener diode D207. Any voltage difference is amplified by transistors Q235 and Q206,
operating as a differential voltage amplifier.
istors 4204, Q202, and 4201 and applied to the regulator, Q2U3.
A dc-to-ac converter forms the voltage to drive the vibrating capacitor, VClOl, and
c.
the bridge demodulator, diodes D106 through D109.
ing network to supply an interrupted dc voltage to transformer T202.
from the transformer supplies feedback to the network to sustain switching action.
sistor R213 determines the feedback magnitude.
0166R
connected as a regulator, is divided and compared
The signal is further amplified by trans-
Transistors Q207 and Q208 form a switch-
An extra winding
Re-
15
CIRCUIT DESCRIPTION
MODEL 630 POTENTIOMETRIC ELECTROMETER
3-6. GUARDING. Guarding is accomplished by floating the null detector and the input
circuitry at a voltage equal to the input voltage from a low impedance source.
This full
guarding eliminates leakage between the input terminal and ground. Such leakage in an
unguarded circuit is difficult to avoid, under laboratory conditions, and can result in
sizeable errors.
of 108
ohms will introduce 1% error. A guarded circuit eliminates this element of error.
For example, in an unguarded circuit with a 1-megohm source, leakage
16
OL66R
MODEL 630 POTENTIOMETRIC ELECTROMETER
SERVICING
SECTION 4.
4-1. GENERAL. Section 4 contains the maintenance and troubleshooting procedures for the
Model 630. Follow these procedures as closely as possible to maintain the accuracy and
stability of the instrument.
4-2. SERVICING SCHEDULE.
care required of high-quality electronic equipment. No part should need replacement under ordinary use except a pilot lamp, fuse or, occasionally, a vacuum tube.
4-3. PARTS REPLACEMmT.
The Replaceable Parts List in Section 7 describes the electrical components in the
a.
Model 630. Replace components only as necessary, and use only reliable replacements
which meet the specifications.
Replace resistors within any one of the first three Kelvin-Varley divider decades
b.
only as an assembly.
tors R341 to R368.
and resistors R329 and R330 are also parts of assemblies.
part number (see Section 7) and replace all resistors in the assembly.
portance in maintaining power supply stability,
Instruments, Inc.,
replace the zener.
Instruments, Inc.,
Refer to the Replaceable Parts List for the part number for resis-
Resistors R325, R326 and R328, resistors R333, R335, R338 and R340
or its representative.
If replacing the vibrating capacitor, VClOl, order only from Keithley
or its representative.
The Model 630 needs no periodic maintenance beyond the normal
SERVICING
Reorder using the Keithley
Because of its im-
order zener diode D302 only from Keithley
Refer to paragraph 4-6 for instructions
to
4-4.
63::
Table 3 lists equipment recommended for troubleshooting.
located or repaired, I contact Keithley Instruments, Inc. or its representative.
TROUBLESHOOTING.
The following procedures are for repairing troubles which might occur in the Model
Use these procedures to troubleshoot and use only specified replacement parts.
If the trouble cannot be readily
Instrument Use
Keithley Model 153 dc Microvolt-Ammeter,
3% accuracy, minimum 200 megohm input
resistance,
Keithley Model 610B Electrometer
Keithley Model 50211 Ohmmeter
Hewlett-Packard 200CD Oscillator
Tektronix Type 503 Oscilloscope
Grid-modulated tube tester
TABLi? 3. Equipment Recommended for Model 630 Troubleshooting. Use these instruments
or their equivalents.
1 volt to 500 volts.
Circuit checking
Check grid bias at cathode follower
Check resistance
Check frequency
Check wave forms
Test vacuum tubes
d
0166R
17
SERVICING
MODEL 630 POTENTIOMETRIC ELECTROMETER
I
eter rattle, drift, or er-
Excessive drift on most
sensitive range
Line voltage variations
cause measurements to be
out of specifications
Reference voltage supply
drifts after 30-minute
warm-up, requiring frequent
adjusting of the range controls, R327, R334, R337 and
R339
Difficulty
is observed on all null
Probable cause Solution
Tube VlOOl, V1002 or V1003
is faulty
-6v power supply is drifting or oscillator circuit
is faulty
Faulty VClOl
Battery BlOl is faulty
Tube V3005 is defective
V3001, V3002, V3003 or
V3004 is defective
One of the divider resistors, R325 to R330, is
changing value rapidly during warm-up
Check tubes;
tY
Check power supply stability
PC104, and oscillator frequency (paragraph 5-7). If
faulty component cannot be
located, return instrument
to
factorv.
I
Replace VClOl
I
Replace BlOl
I
Check tube; replace if faulty
Check tubes; replace if faul,
I
w
Return the instrument for
factory check-out
replace if faul
Measurements out of tolerance on all ranges
Measurements are out of
specifications on one
range other than 500-
volt range
TABLE 4.
Zener diode, D302, is unstable
Light modulator, F,302,
is defective
Out of calibration
One of the divider resis- Return the instrument for
tars, R325 to R330, is
Resistor in the range divider network is faulty
(Sheet 1).
Model 630 Troubleshooting
Return the instrument for
factory check-out
I
Check light modulator by replacing.
Refer to paragraph 5-5 for
recalibration
factory check-out
Paragraph 3-2 d points out
the resistors used for each
range.
ranges within specifications
by calibrating with the potentiometers in the network.
See paragraph 5-5. If this
does not work, check individual resistors.
Try to bring the
18
MODEL 630 POTENTIOMETRIC ELECTROMETER
SERVICING
Difficultv
Measurements are Out of
specifications
ges other than 500-volt
Excessive ac interference
Non-symmetrical response
on polarity switching and
low sensitivity on most
sensitive ranges
Instrument does not respond
to a signal and offset on
all ranges
Greatly increased sensitivity on 10 and 100 null
ranges and 5, 50 and 500V
VTVM ranges
500V supply operates but
null detector is completely
inoperable
on all ran-
Probable cause
Resistor R333 is faulty
R131 out of adjustment
Oscillator frequency has
drifted
Relay K102B is defective
Relay KlOlB is defective
Fuse F201 is blown
Solution
Replace the faulty resistor
Adjust oer oaragraoh 4-8
Check frequency.
approximately 94 cps.
to paragraph 5-7).
Check operation of relay. 11
faulty replace with Keithley
relay or return t0 factory
Check operation of relay. If
faulty replace with new relay
from Keithlev
Check for possible short in
-6v supply (~~104).
Reset to
(Refel
or return to
Keasurements are Out of
specifications on any range
tihen the Reference Voltage
Dials are at anv settine
other than 4 9 9 9 10 -
TABLE 4.
Paragraph 6-2 describes how to remove the Model 630 :over.
b.
the troubleshooting, check the vacuum tubes.
difficulty.
ing a tube does not correct the trouble, continue the procedures.
not necessitate recalibration of the instrument.
c. Table 4 contains the mwze ccnnm~n troubles which might occur.
ted in the Table do not clear up the trouble,
a point-by-point check of the circuits. Refer to the circuit description in Section 3
to find the more crucial components and to determine their function in the circuit. The
complete circuit schematic, 18261E, is found in Section 7,
4-5. ADJUSTING GRID BIAS OF CATHODE FOLLOWER.
V1003 (Figure 15), should be -3 volts. Use the Keithley Model 610B to check this value
i5"/,.
If necessary, adjust the DC BAL potentiometer, R157 (Figure 16), to this value.
All tubes can be readily tested on a grid-modulated tube tester.
(Sheet ).
One of the Kelvin-Varley
divider resistors is
faulty
Model 630 Troubleshootir :.
Normally,
the difficulty will have to be found through
The grid bias of the cathode follower,
See paragraph 5-3
Before proceeding with
replacing tubes will clear up the
If replac-
Replacing tubes does
If the repairs indica-
0166R
19
SERVICING MODEL 630 POTENTIOMETRIC ELECT&OMETER
4-6.
ZEhXR DIODE REPLACEMENT.
resistors R325 to R330.
The values of resistors R329 and R330 (Figure 20) are determined
Zener diode, D302, is a reference for the voltage divider,
by the reference voltage across diode D302. When the zener is replaced, the value of
these two resistors may have to be changed.
4-7. METER ADJUSTMENT.
Potentiometer R155 (Figure 16) is the internal meter sensitivity adjustment. It
a.
sets the current through the mater to indicate a full-scale deflection for a full-scale
applied voltage.
Warm up the Model 630 for 30 minutes.
b.
Set the NULL Switch to the l-volt range and
set the Reference Voltage Dials to 1.0000. Adjust potentiometer R155 until the meter
reads full scale.
4-8. ADJUSTING QUADRATURE CONTROL.
Large quadrature components in the
a.
null detector can cause poor ac rejection,
sluggish response, and, in some cases, un-
symmetrical readings on the most sensitive
ranges. Use the QUAD ADJ potentiometer,
Rl31 (Figure 16),
ents when necessary.
to buck out these compon-
While a large component is troublesome, the quadrature need
not be completely eliminated.
To adjust the potentiometer, set the
b.
Reference Voltage Dials to zero and the
DETECTOR INPUT. Switch to ZERO CK. Attach
an oscilloscope to the junction of Cl16 and
R134 (from pin 6 of V1002, Figure 15). Adjust potentiometer, R131, for the correct
wave form (Figure 9).
FIGURE 9. Wave Form with Rl31 Adjusted.
A Type 503 Oscilloscope was used; horizon-
tal sweep was 5 mseclcm; vertical, 2 v/cm.
20
0166R
MODEL 630 POTh'NTIOMETRIC ELECTROMETER
SECTION 5. CALIBRATION
5-1. GENERAL.
CALIBRATION
The following procedures are recommended for calibrating the Model 630.
a.
equipment recommended in Table 5.
ibrating an fO.Ol% instrument
tact Keithley Instruments, Inc.,
The following procedures are covered:
b.
calibrate adjustment,
and oscillator adjustment.
If the Model 630 is not within specifications after the calibration, follow the
c.
troubleshooting procedures or contact Keithley Instruments, Inc., or its representative.
Instrument
Electra Scientific Industries Model SV194B
Voltage Calibrator, i-0.005% accuracy with
corrections on certificate
Electra Scientific Industries Model RV722
Decade Voltage Divider; terminal linearity
21 ppm; certificate corrected to kO.2 ppm
Electra Scientific Industries Model LC875B
Lead Compensator
voltage range calibration, reference voltage supply stability test
- are not available or if difficulty is encountered, con-
If proper facilities - especially important for cal-
or its representative to arrange for factory calibration.
Kelvin-Varley divider verification, divider
Use
Range voltage calibration
Voltage divider for range calibration
Range voltage calibration
Use the
Hewlett-Packard Model 200CD Oscillator
Keithley Instruments Model 15OB Microvolt
hmeter
Keithley Instruments Model 241 Regulated
High Voltage Supply
Keithley Instruments Model 662 Guarded dc
Differential Voltmeter
Keithley Instruments Model 370 Recorder
Tektronix Type 503 Oscilloscope
Weston Instruments Model 3 Type 7 Saturated
Standard cell
Weston Instruments Model 66 Oil Bath
TABLE 5.
equivalents.
Equipment Recommended for Model 630 Calibration.
Monitor oscillator frequency
Null detector for range calibration
ure picturing the location and the paragraph describing the adjustment.
5-2. CALIBRATION SCHEDULE.
a. Recalibrate the Model 630 yearly. This normally means performing the voltage range
calibration (paragraph 5-5). The other verifications need not be done.
b.
or if components in the divider have been replaced. Also make the voltage range calibra-
tion after verifying the divider accuracy.
Model 630 Internal Controls. The Table lists all internal controls, the fig-
Verify the Kelvin-Varley divider (paragraph 5-3) only if trouble is suspected in it,
Desig.
R104 15 5-4
R131 16 4-8
R155 16 4-7
R157 16 4-5
R210 18 5-7
Fig.
Ref. Paragraph
Refer to
Check the reference voltage supply stability (paragraph 5-6) only if trouble is
c.
suspected in the supply or if some of its components have been replaced.
5-3. KELVIN-VARLEY DIVIDER VERIFICATION.
There is no in-field calibration for the Kelvin-Varley divider; its accuracy can
a.
only be verified.
manufacture,
S304, is matched to *0.00125%. The resistors in the switches are checked as a set to an
accuracy of better than 0.0025%.
ching the string at Keithley Instruments.
b. Kelvin-Varley Divider Accuracy Verification Procedures.
1.
error to match the Model 630 under test.
the Model 630 to the HI terminal of the Model 662.
Be careful of high voltages when working within the Model 630. Up to 900 volts
dc is present at various points.
2.
iO.Ol%. This procedure, however, only indicates the Kelvin-Varley divider accuracy.
The errors of the two instruments may be additive, causing a false verification. The
most accurate way is to use standard procedures for checking a Kelvin-Varley divider
or to return the Model 630 to Keithley Instruments, Inc., for checking.
each resistor within the first two Reference Voltage switches, S303 and
Use the Model 662 Differential Voltmeter or equipment with better limit of
Set the dials to random settings on both instruments. Settings should match to
The divider accuracy depends upon matching resistors and switches. At
Individual resistors cannot be replaced without remat-
Connect the Low end of potentiometer R38L of
Connect both LO terminals.
NOTE
22
1265R
MODEL 630 POTENTIOMETRIC ELECTROMETER
If any resistor fails to test out,
3.
the entire divider string will have to he rc-
matched at the factory.
5-4.
INPUT DIVIDER CALIBRATION.
Above 1 volt the input is divided by a constant 5OO:L
ratio. R103 is pre-selected to approximate this ratio and R104 is adjusted to trim to
this ratio more closely.
'accuracy
on the l-volt and Lower ranges but appears in error for the higher ranges.
check the divider ratio,
put.
it does not,
5-5.
The Model 630 meter should have a full scale deflection on its 500-volt range.
trim R104 (Figure 15) until the meter indicates full scale.
RANGE CALIBRATION.
A misadjustment will show up if the Model 630 maintains spccificrl
'To
use the Model 241 to apply a 500-volt signal to the Hodel 630 in-
a. The reference voltage supply has a 500-volt output which can be attenuated to 50, 5
or 0.5 volts.
This voltage is then divided by the Kelvin-Varley divider to provide the
accurate buckout voltage. Each of the four voltage ranges is set by internally adjusting
potentiometers R327, R334, R337 and R339 (Figure 20).
The ranges are calibrated by applying an accurate voltage to the Model 630 for each
b.
setting of the RANGE Switch.
The Model 630 is set to furnish the equivalent buckout voltage, and the internal range potentiometer is adjusted until the voltmeter indicates a
null.
If
I
SUPPlY
d b
I
Mode, -~ --
i ‘C 8/,B
I
d I u-+-z Detector ]
o Compensator
9.9 lm
EXte"dGT
(5 and 0.5"
OlllY)
I
--+
_ Model
- sv 194B
Calibrator
p+Cd
I
Model R'J722
FIGURE 10.
Block Diagram to Establish System Accuracy for Model 630 Range Calibration.
Fully guard the entire system to prevent leakage errors.
to shunt the null detector.
See Table 5 for recoanended equipment.
Use a l-kilohm copper resistor
1067R
23
CALIBRATION
MODEL 630 POTENTIOMETRIC ELECTROMETER
NOTE
The accuracy of the Model 630 calibration will be no greater than the
accuracy of the voltage source used for calibrating.
Unless the user is
familiar with techniques for obtaining accuracy greater than 0.002%
(20
PPm) >
it is better to return the Model 630 to the factory for range
calibration.
The most critical part in range calibration is establishing a reference source
c.
whose accuracy exceeds 0.002%..
Use the Model SV194B Voltage Calibrator for the 500, 50,
5 and 0.5-volt outputs. Establish the accuracy of these outputs by determining the corrections for the calibrator's CALIBRATION and OUTPUT dials at these outputs.
accuracy can be determined to approximately 10 ppm. Added
to
the accuracy of the standard
The system's
cell, total accuracy should be approximately 12 ppm. Note that this depends upon proper-
ly executed procedures.
Procedures to Establish System Accuracy.
d.
Set up the system shown in Figure 10.
1.
Use the 9.9-megohm extender for only the
0.5 and 5-volt output.
Establish the corrections for the CALIBRATION dial setting for Model SV194B out-
2.
puts of 500, 50, 5 and 0.5 volts.
the Model RV722 Divider to a voltage equal to that of the standard cell.
Model SVl94B ratio dial until the null detector indicates a null.
Set the Model 241 Voltage Supply to 500 volts.
Adjust the
The difference between the settings of the Model RV722 Divider and the ratio dial is the Model SVl94B
correction factor at 500 volts.
With this correction, the 500 volts may be set to
within approximately 12 ppm.
Connect the null detector to the 50, 5 and 0.5-volt taps of the Model SVl94B Cal-
3.
ibrator in that order.
Set the Model RV722 Divider to corresponding voltages.
Use the
9.9-megohm extender for the 5 and 0.5-volt outputs. (See Figure 10). The difference
read on the null detector is the correction factor for each of the three voltages.
These voltages may also be set to within 12 ppm.
Use the four correction factors for calibrating the Model 630 range setting.
4.
f. Procedures for Range Calibration.
Set up the system shown in Figure 11.
1.
10 ppm.
Use the dial correction factors found for each output.
was properly determined,
the input voltage to the Model 630 should be correct to 20 ppm.
The standard cell should be certified to
If the system accuracy
set
500-volt Range Calibration: Set the Model 630 controls as follows:
2.
DETECTOR INPUT Switch 1010 OHMS
RANGE Switch
500
Reference Voltage Dials 4 9 9.9 9 10
NULL Switch VTVM
POLARITY Switch
Adjust the Voltage Calibrator to apply 500 volts to the Model 630.
+
Turn the Model 630
NULL Switch to 10 MV and adjust the 500 V CAL potentiometer, R327 (Figure ZO), for
null on the Potentiometric Electrometer.
24
0166R
MODEL 630 POTENTIOMETRIC FLECTROMETER
CALIBRATION
FIGURE 11. Block Diagram for Model 630 Range Calibration. Fully guard the entire system
to
prevent leakage errors. See Table 5 for recommended equipment.
50-volt Range Calibration: Set the Model 630 controls as follows:
3.
DETECTOR INPUT Switch 1010 OHMS
RANGE Switch 50
Reference Voltage Dials 4'9.9 9 9 10
NULL Switch 10 Mv
POLARITY Switch +
Adjust the Voltage Calibrator to apply 50 volts dc to the Model 630. Adjust the 50 V
CAL potentiometer, R334 (Figure ZO),
for an off-null reading on the Model 630 equal to
the correction factor at 50 volts.
5-volt Range Calibration:
4.
DETECTOR INPUT Switch
RANGE Switch
Reference Voltage
set the Model 630 controls as follows:
1010 OHMS
'5
Dials 4.9 9
9 9 10
NULL Switch 1Mv
POLARITY Switch +
Adjust the Voltage Calibrator to apply 5 volts dc to the Model 630. Adjust the 5 V CAL
potentiometer, R337 (Figure 2o), for an off-null reading on the Model 630 equal to the
correction factor at 5 volts.
0.5~volt Range Calibration:
5.
Set the Model 630 controls as follows:
1067~
DETECTOR INPUT Switch 1010 OHMS
RANGE Switch
Reference Voltage
NULL Switch
POLARITY Switch
Dials .4 9
0.5
9 9 9 10
0.1 MV
+
25
CALIBRATION
MODEL 630 PO'TENTIOMETRLC ELECTROMETER
Oil Bath;
I
I
t
- I
-
- I
- I
,-------
FIGURE 12. Circuit Diagram for Model 630 Reference Voltage Supply Stability Test.
voltage across the 530-ohm resistor is slightly higher than the standard cell.
Model 150B
H
Null
Recorder
The
Use the
lo-kilohm potentiometer to shunt the divider voltage down. All resistors are wirewound.
See Table 5 for recommended equipment.
Adjust the Voltage Calibrator to apply 0.5 volt dc to the Model 630. Adjust the 0.5 v
CAL potentiometer, R339 (Figure ZO), for an off-null reading on the Model 630 equal to
the correction factor at 0.5 volt.
5-6.
REFERENCE VOLTAGE SUPPLY STABILITY TEST.
The reference voltage supply,
a.
consisting of the power transformer and the main supply (printed circuit PC92), is factory calibrated for an output of 500 volts dc greater
than 0.002%. The 500-volt output is adjustable to meet specifications. If the stability
of the supply is not within specifications,
then troubleshoot for a faulty component.
Routine calibration of the Model 630 does not require a stability test of the ref-
b.
erence voltage supply. However, a stability test is recommended if one of the components
in the supply is replaced.
For the 24-hour test, the 500-volt output of the reference voltage supply is divided
c.
and compared to a 1.02-volt saturated standard cell using a sensitive null detector.
Var-
iations between the reference voltage supply and the standard cell are detected by the
Model 150A and are recorded on a recorder.
Refer to Figure 12 for the block diagram of
the test circuit.
In using the test circuit,
d.
Saturated standard cells,
1.
ture coefficient and require a controlled environment during use.
ton Oil Bath, which is maintained at ~350 M.OloC, is used for the test.
the following points are important.
though extremely stable with time, have a high tempera-
Therefore, the Wes-
Unsaturated
standard cells have a lower temperature coefficient, but they do not have the long term
stability required for this test.
The resistor divider network is constructed from wire of the same spool for an
2.
extremely close temperature coefficient match (4 ppm, typically).
26
Additional stability
1067R
MODEL 630 POTENTIOMETRIC ELECTROMETER
CALIBRATION
results when the resistors are immersed in an oil bath to hold the ambient temperature
variations
Procedures for the Reference Voltage Supply Stability Test.
e.
After the saturated standard cell and the resistor divider network are placed in
1.
to
+O.Ol%.
the oil bath, allow sufficient time for the cell to stabilize at ~35°C. (Consult Keith-
ley Instruments, Inc., or its representative for details.) Connect the standard cell
to the circuit after turning on the 500-volt supply. Set the Model 630 controls as
follows:
DETECTOR INPUT Switch
1010 OHMS
RANGE Switch 500
Reference Voltage Dials 4 9 9.9 9 10
NULL Switch 10 Mv
POLARITY Switch
OFF
Connect the resistor divider network across the Model 630's reference voltage supply,
the positive side of the divider input to the wiper arm of the last Reference Voltage
Switch, S306, and the negative side of the divider to the LO terminal on the Model 630
front panel.
Connect the Model 150B and the recorder as shown in Figure 12. Set the Model 1500
2.
to the 3-volt range.
Advance the Model 630 POLARITY Switch to -I- to put 500 volts across
the divider. If the Model 150B reads two volts, the standard cell and the divider voltages are improperly connected in series. If the circuit is correct, the Model l50B
will read zero. Increase the Model 15OB's sensitivity to the O.l-millivolt range. If
it reads more than 20 microvolts, adjust the 500 V CAL potentiometer, R327 (Figure 20),
shunting the divider.
NOTE
Any adjustment of potentiometer R327 requires all other ranges to be calibrated,
After l-hour warm-up,
3.
the drift of the entire system should not exceed i-25 micro-
volts in 24 hours.
5-7. OSCILLATOR ADJUSTMENT.
The oscillator circuit drives the light modulator, vibrating capacitor and bridge.
a.
demodulator. Before adjusting the oscillator, make sure the reference voltage supply
is operating correctly.
Connect the Type 503 Oscilloscope Vertical Input to the plate and low side of tube
b.
V1003 (Figure 15) and the Horizontal Input to the Model 200CD Oscillator. Adjust the
oscillator frequency to approximately 94 cps with potentiometer R210 (Figure 18). The
Model 630 oscillator is then adjusted for minimum meter noise - normally within a cycle
of 94 cps.
Disconnect the Oscilloscope before adjusting potentiometer R210. The
Oscilloscope will cause a small loading error.
1067R
27
CALIBRATION
MODEL 630 POTENTIOMETRIC ELECTROMETER
R30 1
0302
Q203
Cl22
(hid,
(Refer to Figures 15 and 16)
PC-103
FIGURE 13. Top view of Model 630 Chassis.
28
Null Detector Input
(Refsr to Figure 17)
Front panel faces to the right.
0166
MODEL 630 POTENTIOMETRIC ELECTROMETER
CALIBRATION
'IGURE 14. Bottom view of Model 630 Chassis.
13 shows the top view.
0166
Front panel faces to the right.
Figure
29
CALIBRATION
MODEL 630 POTENTIOMETRIC ELECTROMETER
Cl01
Cl15
Clll.-elj
Cl10 ----+
Cl19 -".q
A
OS101
Cl06
Cl07 Cl13
I
-cl08
+D104
~V1002
*cl16
Cl09
c12oa-+
c117nn"y
Dlb9
VCiOl Djoy166
I
;
Re-
Fl [GURE 15.
Capacitor,
D108
Tube and Diode Locations on Printed Circuit PC-103.
fer to Figure 16 for Resistor Locations. Hidden from view, in locations A and B
are, potentiometer Rl04, resistors R124 and R154, and capacitors Cl03 and C105.
30
0166
MODEL 630 POTENTIOMETRIC ELECTROMETER
R107-
CALIBRATION
Rl33 -mm..&
R130,
R158
29
R141
i,j
R109
thru
R118
0166
KeS1StOr
Diode and Tube Locati
on lx-L”J.
R15.1 R108
Keter
to Figure 13 tar Capacitor,
31
CALIBRATION
MODEL 630 POTENTIOMETRIC ELECTROMETER
I,
tector Input.
32
Locations
on Null De
'IGURE 18.
Component bzations on -6.3 vo
ower Supply, PClO4.
0166
MODEL 630 POTENTIOMETRIC ELECTROMETER
CALIBRATION
D301
I
v3003
I
c 5
P
,~_,,,., I‘....
008
C306
VW0 1
GURE 19.
,fer to Figure 20 for Resistor
Capacitor, Diode, Modulator and Tube Locations on Printed Circuit Board PC-92.
Locations.
CALIBRATION MODEL 630 POTENTIOMETRIC ELECTROMETER
R307
R33111
R30
9
R310
R308
4
“:“kc
R30 2
I
R312 R314
R303 R305 R315
I I I I I
,m
R313
R317
R316
-
R318
R319
R332
R328
-
?osition
R324
FIGURE 20.
.iii‘::*&
R339
Resistor Locations on Printed Circuit Board PC-92.
Capacitor, Diode, Modulator and Tube Locations.
R3.33
R325
Position
R326
Position
-R330
positiac
c
R334
R327
Refer to Figure 19 for
34
0166
MODEL 630 POTENTIOMETRIC ELECTROMETER
SECTION 6. ACCESSORIES
6-1. MODEL 6301 GUARDED PROBE. (Figure 21)
The Model 6301 is a guarded probe and shielded lead to make measurements with the
a.
Model 630 nvxe convenient.
furnished with 3 feet of low-noise cable,
plug connects directly into the Model 630 Input Receptacle.
It does not alter any Model 630 specification.
terminated by a special triaxial type plug.
ACCESSORIES
The lead is
The
b. Using the Model 6301 Probe allows point by point measurements.
Its operation witli
the Model 630 is explained in paragraph 2-4.
6-2. RACK MOUNTING.
The Model 630 is shipped for bench use with four feet and a tilt-bail
(See Figure 22)
The Model
4&% Rack Mounting Kit converts the instrument to rack mounting to the stan&nd EIA (RET@)
19-inch width.
To convert the Model 630, remove the four SC~BWS at the bottom of each side of the
b.
instrument case. Lift off the top cwer assembly with the handles; save the four screws.
To remcwe the feet aid tilt bail from the bottom cover assembly, turn the two screws near
the back. The two pawl-type fasteners will release the cwer and allow it to drop off.
Remove the feet and the tilt bail and replace the cwer (2).
c. Attach the pair of rack angles (3) to the cabinet with the four screws (4) previou
y removed.
Insert the top cwer assembly (1) in place and fasten to the chassis with t
S-
he
FIGURE 21.
probe tip,
Keithley Instruments Model 6301 Guarded Probe with the Model 630.
the Model 6301 can have banana plug, alligator clip, and bnc-type connections.
Unscrew tip to make the connection.
1265
m
Besides the
35
ACCESSORIES
MODEL 630 POTENTIOMETRIC ELECTROMETER
two pawl-type fasteners at the rear. Store the top cover with handles, feet and tilt-bail
for future use.
6-3.
PLACING IN RACK.
the rack.
It is recommended, however,
The Model 630, once converted for rack mounting, easily fits into
that a blower be used in the rack enclosure in
which the Model 630 is mounted. The instrument specifications state a 0.002% per "C tem-
perature coefficient. A temperature rise of 5 W (9 OF) will cause a 0.01% error.
Item
(See Fig. 22)
1 Cover Assembly
2
Cover Assembly, Bottom (Supplied with
Model 630)
3
Angle, Rack
4 SCYCeW)
(Supplied with Model 630)
5
Front Panel (Supplied with Model 630)
Description
Slot Head, lo-32 UNC-2 x l/4
Keithley
Part No. Quantity
14623B 1
14590B 1
14624B
---__--
2
4
1
I
Parts List for Model 4000 Rack Mounting Kit.
~@COVER ASSEMBLY
4
P
TABLE 7.
SCREW
OVER ASSEMBLY
FIGURE 22. Exploded
'Table 7 for parts.
View
for Rack Mounting with Model 4000 Kit.
Refer to
1265
MODEL 630 POTENTIOMETRIC ELECTROMETER
ACCESSORIES
FIGURE 23. Model 6013 pH Electrode Adapter Connected to pH Electrodes,
shown here with the Keithley Model 601 Electrometer,
6-5.
MODEL 370 RECORDER.
is used similarly with the Model630.
The Model 6013,
a. The Model 370 Recorder is uniquely compatible with the Model 630 as well as other
Keithley electrometers,
picoammeters and microvoltmeters.
The Recorder is a high quality
economical instrument that epitomizes the performance of the Model 630 and many other
Keithley instruments, even in the most critical applications.
with the Model 630 to
record
over the Model 630's entire range.
The Model 370 can be used
b. The Model 630 has the output necessary to drive the Recorder directly (1 volt, 1
milliampere), thus eliminating the need for a preamplifier.
The Model 370 floats f500
volts off ground, enabling the Model 630 to be used to its specified off-ground voltage.
The Recorder is specially shielded to avoid pickup of extraneous signals. The response
1067R
37
ACCESSORIES MODEL 630 POTENTIOMXTRIC ELECTROMETER
time of the Model 370 Recorder is 0.5 second; linearity is *l% of full scale. Ten chart
speeds - from 3/4 inch per hour to 12 inches per minute - are selectable with front panel
controls. The 6-inch chart has a rectilinear presentation. The Model 370 Recorder has a
self-priming inking system. Chart paper and ink refills are easy to install.
C. The Model 370 is ‘very easy to use with the Model 630.
Just connect the Model 630’s
OUTPUT Receptacle to the Model 370 with the furnished 3701 Input Cable and adjust an
easily accessible control for full-scale recorder deflection.
38
1067R
MODEL 630 POTENTIOMETER ELECTROMETER REPLACEABLE PARTS
SECTION 7. REPLACEABLE PARTS
7-l.
Model 630 and its accessories.
cription, a suggested manufacturer,
Number.
the manufacturers listed in the "Mfg.
REPLACEABLE PARTS LIST. The Replaceable Parts List describes the components of the
The List gives the circuit designation, the part des-
the manufacturer's part number and the Keithley Part
The last column indicates the figure picturing the part. The name and address of
Code" column are in Table 9.
7-2. HOW TO ORDER PARTS.
For parts orders,
a.
Part Number,
the circuit designation and a description of the part. All structual parts
include the instrument's model and serial number, the Keithley
and those parts coded for Keithley manufacture (80164) must be ordered through Keithley
Instruments, Inc. or its representative.
able Parts List,
Order parts through your nearest Keithley representative or the Sales Service Depart-
b.
completely describe the part, its function and its location.
In ordering a part not listed in the Replace-
ment, Keithley Instruments, Inc.
amp
Cb
CbF
CbVar
CerD
Comp
compv
DCb
Carbon
Carbon Film
Carbon Variable
Ceramic Disc
Composition
Composition Variable
Deposited Carbon
M
m
Mfg.
Mil. No.
MY
n
P
Poly
mega (106)
milli (10-3)
Manufacturer
Military Type Number
Mylar
ohm
pica (lo-12)
Polystyrene
EAL
EMC
ETB
ETT
f
Fig.
k
1065
Electrolytic, Aluminum
Electrolytic, Metal Cased
Electrolytic, tubular
Electrolytic, tantalum
farad
Figure
kilo (103)
Table 8.
Abbreviations and Symbols.
Ref.
u.
v
Ew
WWVar
Reference
micro (10-6)
volt
watt
Wirewound
Wirewound Variable
39
REPLACiUBLE PARTS
MODEL 630 POTEX'TIOMKTRIC ELECTROMETER
m 630 VBLE PARTS LIST
(Refer to Schematic Diagram 18261E for circuit designations)
CAPACITORS
Circuit Mfg. Mfg. Keithley Fig.
Desig.
Value Rating Type Code Part No.
Part No. Ref.
Cl01
Cl02
Cl03
Cl04
Cl05
Cl06
Cl07
Cl08
Cl09
Cl10
Cl11
Cl12
22
pf
56 &f 6v
47
pf
56
uf
47
if
2 Pf
0.1 I.Lf
1500 pf
2O/fXI/lOO
.a1 IJ.f
.a05
.005
Cl13 0.1 pf
Cl14
2
IJ.f
Cl15 0.1 pf
Cl16 .Ol uf
Cl17
Cl18
Cl19
Cl20
Cl21
Cl22
100 ,lf
0.5
Ilf
100 Kf 10 v ETT 05397
4
Pf
0.25
1 Pf
IJf
pf
yf
500
”
500 v
6v
500
v
50
v
400
v
600 v
pf
300/250/250 v
400 v
400
”
400
v
400
v
50
v
400
v
600
v
10 v
400
v
250
v
400
v
25
v
Poly 71590 CPR-225 Cl38-22P
ETT 01295 5MC566BP006A4 C70-56M
Poly 71590 CPR-47J Cl38-47P
ETT 01295 5MC566BP006A4 C70-56M
Poly 71590 CPR-475
100 kn lO%, l/2 w
820 ci lO%, l/2 w Comp
330 kn lO%, l/Z w Comp
4.7 MO
15 kn
1.5 kn
lO%, l/2 w Comp 01121 EB
lO%, 2 w
lO%, l/2 w
R147 10 kn l%, l/2 w
R148
10 R l%, l/2 w
R149 100 n l%, l/2 w
R150 1.11 kn
R151 200 n
R152
2.5 kn l%, l/2 w
R153 10 kn
R154
R155
R156
R157
R158
8.06 kQ
2&l
10 kn
1 kil
10 hl
l%, l/2 w
l%, l/2 w
l%, l/2 w
l%, l/S w MtF
20%, .2 w
lO%, l/2 w
20%, .2 w
lO%, l/2 w
Mfg. Mfg.
TYPO
Code Part No. Part NO. Ref.
camp 01121 EB
01121 EB
01121
EB
Keithley Fig.
Rl-100K 16
Rl-820 16
Rl-330K 16
Rl-4.7M
C?imp
01121
IIB
camp 01121 EB
DCb 00327 NllA
DCb
DCb
DCb
DCb
DCb
DCb
compv
00327 NllA RI?-10 17
00327
NllA
00327 NllA R12-l.llK 17
00327 NllA
00327 NllA Rl2-2.5K 17
00327 NllA Rl2-1OK 17
07716
CEA
71450 70 RP31-2K 16
R3-15K
Rl-1.5K 16
R12-101~
R12-100 17
Rl2-200
R88-8.06K
Comp 01121 EB Rl-10K
compv
camp
71450
01121
70
EB
RP31-1K 16
Rl-1OK 16
16
16
17
17
15
16
R201
R202
R203
R204
R205
R206
R207
R208
R209
R210
R211
R212
R213
R214
R301
R302
R303
R304
R305
R306
R307
1 kn
10 ko
4.7 kn
470 n
2.2 kn
5.6 kn
56 ko,
50 kn
27 ks2
20 kn
35 kn
47 12
680 11
39 kC2
108 n
220 0
820 kQ
150 Ia
50 kn
1 Mrl
1MQ
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
l%, l/2 w
lO%, l/2 w
lO%, 5 w
l%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
20%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
l%, 5 w
lO%, l/2 w
lO%, l/2 w
camp
01121
camp 01121
Camp
Comp
camp
01121
01121
01121 EB Rl-2.2K 18
EB
EB
EB Rl-4.7K
EB
Rl-1K 18
Rl-1OK 18
18
Rl-470
18
Comp 01121 EB Rl-5.6K 18
Comp
01121
EB
Rl-56K 18
DCb 00327 NllA RlZ-50K 18
Comp
01121
EB Rl-27K 18
wwvar 71450 AW RP34-20K 18
DCb
Comp
camp
Comp 01121
Comp
Comp 01121
Comp
Comp
m 91637
00327
01121
01121
75042
01121
01121
NllA R12-35K
EB Rl-47 18
EB
EB
Rl-680
Rl-39K 18
GBT R37-108
EB
EB
Rl-220
Rl-820K
EB Rl-150K
RS-5
R4A-50K
Comp 01121 EB Rl-1M
Comp
01121
EB Rl-1M
18
18
13
20
20
20
20
20
20
1067R
45
REPLACEABLE PARTS MODEL 630 POTENTIOMETRIC ELECTROMETER
RESISTORS (Cont'd)
Circuit
Desig.
R308
R309
R310
R311
R312
R313
R314
R315
R316
R317
R318
R319
R320
R321
R322
R323
R324
R325
Value
3.3 kiz
lM!z
470 n
470 m
2.7,
1Im
10 M!J.
680 k~
330 kil
270 kr2
2.2 l"G
5.6 kn
9<
K
1MCl
220 ksi
125 kn
Rating
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
lO%, l/2 w
O.l%, 50 w
0.25%, 1 w
lO%, l/2 w
lO%, l/2 w
O.l%, 2 w
Mfg. Mfg.
TYPO
camp
Comp
camp
camp
Comp
camp
Comp
camp
Comp
Comp
Comp
Comp
Comp
ww
Code
01121
01121 EB
01121
01121
01121
01121
01121
01121
01121
01121
01121
01121
01121
91637
ww 01686
Comp 01121
Comp '01121
ww 80164
Keithley
Part NO. Part No.
EB
Rl-3.3K
Rl-1M
EB
EB
EB
EB
EB
EB
EB
EB
EB
EB
EB
RH-50
T2
EB
EB
Rl-470
Rl-470K
Rl-1M
Rl-4.7K
Rl-1M
Rl-1OM
Rl-680K
Rl-330K
Rl-270K
Rl-2.2M
Rl-5.6K
R73-';
Rl30-9~
Rl-1M
Rl-220K
(1)
Fig.
Ref.
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
R326
R327
R328
R329
R330
R331
R332
R333
R334
R335
R336
R337
R338
R339
R340
68 kfi
68 k.Q
250 ka
1 kn
32.33 kn
180 kn
1 kn
2.563 Ici2
1 kn
250.9 n
O.l%, 2 w
lO%, 5 w
O.l%, l/4 w
0.25%, 50 w
0.25%, 50 w
lO%, l/2 w
lO%, l/2 w
O.l%, 2 w
lO%, 5 w
O.l%, l/2 w
lO%, l/2 w
lO%, 5 w
O.l%, l/2 w
lO%, 5 w
O.l%, ll2 w
ww 80164
wwvar
71450
ww 80164
ww
ww
Comp
80164
80164
01121
Comp 01121
ww 80164
WWVar 71450
ww 80164
Comp 01121
wwvar 71450
ww
80164
wwvar 71450
ww 80164
AW
EB
EB
AW
EB
AW
(1)
RP3-200
(1)
19102A
19102A
Rl-68K
ill-68K
(3)
RP3-1K
(3)
Rl-180K
RP3-1K
(3)
KP3-1K
(3)
R341
to R346
40 kn
O.OZ%, 1 w
ww 80164
(4)
f:Nominal value, factory set.
(1) R325, R326 and R328 comprise a matched set Keithley Part No. 15436A.
(2) See paragraph 4-6.
(3) R333, R335, R338 and R340 comprise a matched set, Keithley Part No. 154328.
(4) Part of Assembly with 5303, Keithley Part No. 18355B.