Spectrasensors SS1000 Operator's Manual

SS1000
Gas Analyzers
Operator’s Manual
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
SS1000 Operator’s Manual
vi 49000-02079 rev. A 4-29-10
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
Products of
11027 Arrow Route
Rancho Cucamonga, CA 91730
Tel: 800.619.2861
Fax: 909.948.4100
www.spectrasensors.com
Copyright © 2010 SpectraSensors, Inc. No part of this manual may be reproduced in whole or in part without the express written permission of SpectraSensors, Inc. SpectraSensors reserves the right to change product design and specifications at any time without prior notice.
SS1000
Gas Analyzers
Operator’s Manual
This manual applies to firmware version:
v2.41
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
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SS1000 Operator’s Manual i
TABLE OF CONTENTS
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . i
List of Figures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .v
List of Tables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . vii
1: Introduction
Who Should Read This Manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1
How to Use This Manual. . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1
Special Symbols Used in This Manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2
General Warnings and Cautions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2
SpectraSensors Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4
About the Gas Analyzers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . 1-4
Ho
w the Analyzer Works . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4
2: Installation
What Should be Included in the Shipping Box . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
Inspecting the Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
Hardware and Tools for Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
Hardware . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . .
. . 2-1
Tools . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Setting up the Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Connecting the Gas Lines. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
To connect the sample supply line . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-3
To connect the sample return . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . .
. 2-4
Conditioning the SCS Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-4
Connecting Electrical Power to the Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-5
Connecting the Output Signals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-5
3: Operating the Analyzer
Powering Up the Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1
To power up the analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . 3-1
Powering Down the Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2
To power down the analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2
Operating the Analyzer from the Keypad . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2
Modes Defined . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-3
Mode 1: (Normal Mode) . . . . . . . . . . . . . . . . . . . .
. . . . . . . .
. . . . . . . . . . 3-4
Mode 2: (Set Parameter Mode) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-4
Mode 3: (Not Used) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-4
Mode 4: (System Diagnostic Parameters) . . . . . . . . . . . . . . . . . . . . . . . . . . 3-4
Mode 5: (Not Used) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-5
Mode 6: (Diagnostic Data Downl
oad) . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . 3-5
Mode TEST: (System Test) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-6
Changing Measurement and Control Parameters. . . . . . . . . . . . . . . . . . . . . . . . 3-6
To change parameters in Mode 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-6
Measurement and Control Parameters Defined . . . . . . . . . . . . . . . . . . . . . . . . . 3-8
S Factor . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . 3-8
S
Factor Offset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-8
# Spectrum Average . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-8
Logger Rate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-9
Peak Tracking . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-9
Temperature Unit . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-9
Pressure Unit. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10
Concentration Unit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10
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Pipeline Pressure (if applicable) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10
Modbus Address . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11
Modbus Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11
User Analyzer ID . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11
User Sample ID . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-12
User Component ID . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . 3-12
Adj
usting Analyzer Reading to Match Specific Standard(s) . . . . . . . . . . . . . . . . 3-12
To adjust the analyzer reading . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-13
Changing Measurement Range (for dual-range moisture systems only) . . . . . . . 3-13
To change measurement range . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-13
Faults . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . 3-15
Va
lidating the Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-15
To validate the analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-15
Calibrating the Analyzer. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-16
4: Serial Port Communications
Receiving Serial Data (RS-232 Output) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1
To launch HyperTerminal . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . 4-1
To capture and save data from the serial port . . . . . . . . . . . . . . . . . . . . . . . 4-4
To read diagnostic data with HyperTerminal . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Viewing Diagnostic Data with Microsoft Excel . . . . . . . . . . . . . . . . . . . . . . . . . . 4-5
To import the data file into Excel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-5
Modbus Communications Protocol . . . . . . . . . .
. . . . . . . . . .
. . . . . . . . . . . . . 4-10
Framing/Protocol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-12
Functions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-12
Addressing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-12
Reading/Writing in Daniel Modbus Mode . . . . . . . . . . . . . . . . . . . . . . . . . . 4-12
Reading/Writing in Gould Modb
us Mode . .
. . . . . . . . . . . . . . . . . . . . . . . . 4-13
To enable Modbus communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-13
Modbus Accessible Parameter Definitions. . . . . . . . . . . . . . . . . . . . . . . 4-16
Appendix A: Troubleshooting
Gas Leaks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1
Membrane Separator Filter. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1
To replace the membrane . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . A-1
C
ontamination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-2
To keep the sampling lines clean . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-2
Cleaning the Mirrors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-3
Tools and Supplies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-3
To clean the mirrors. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-4
Excessive Sampli
ng Gas Temperatures and Pressures . . . . . . . . . . . . . . . . . . . . A-5
Electrical Noise . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-5
Peak Tracking Reset Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-5
To check the PkDf and PkD1 values . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-6
To reset the Peak Tracking Function. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-6
Instrument Problems. . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-7
Re
moving the Cover . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-7
Checking the Fuses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-8
Service Contact . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-8
Disclaimers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . A-8
War
ranty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-8
Appendix B: Specifications
Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-5
Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Index-1
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Table of Contents
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SS1000 Operator’s Manual v
LIST OF FIGURES
Figure 1–1: Schematic of a typical laser diode absorption spectrometer. 1-5 Figure 1–2: Typical raw signal from a laser diode absorption spectrometer with and
without mirror contamination. 1-6
Figure 1–3: Typical normalized absorption signal from a laser diode absorption
spectrometer. 1-6
Figure 1–4: Typical normalized 2
f signal where the species concentration is propor-
tional to the peak height. 1-7 Figure 3–1: SS1000 keypad. 3-3 Figure 4–1: Connection Description window. 4-2 Figure 4–2: Connect To windo
w. 4-2
Fi
gure 4–3: COM Properties window. 4-3 Figure 4–4: Hyperterminal window with streaming data. 4-3 Figure 4–5: Sample diagnostic data output. 4-6 Figure 4–6: Sample diagnostic data output (continued). 4-7 Figure 4–7: a) Opening a data file in Excel. b) Setting data type in Text Import
Wizard. 4-8
Figure 4–8: a) Setting Tab and Space as delimiters. b) Highlighting imported data
for plotting in Excel. 4-9 Figure 4–9: Chart Wizard - Step 1 window. 4-10 Figure 4–10: a) Data file plot in Excel. b) Format Data Series window. 4-11 Figure B–1: SS500/SS2000
analyzer externa
l features. B-3
Figure B–2: Fuse location on DC to DC converter. B-4
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SS1000 Operator’s Manual vii
LIST OF TABLES
Table 3–1: Measurement and control parameters. 3-7 Table 4–1: Modbus register map . 4-15 Table A–1: Fuse specifications (refer to Figure B–1 or Figure B–2). A-8 Table A–2: Potential instrument problems and solutions . A-10 Table B–1: SS1000 moisture in natural gas analyzer specifications. B-1 Table B–2: SS1000 carbon dioxide in natural gas analyzer specifications. B-2 Table B–3: Replacement parts for SS1000 SS1000 Operator’s Manual
analyzers. B-5
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SS1000 Operator’s Manual
01-92-4 A .ver 97020-00094iiiv
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SS1000 Operator’s Manual 11
1 - INTRODUCTION
SpectraSensors SS1000 products are high-speed, diode-laser based extractive analyzers designed for extremely reliable monitoring of very low (trace) to standard concentrations of H
2
O or CO2 in Natural Gas. In order to ensure that the analyzer performs as specified, it is important to pay close attention to the details of the installation and operation. This manual contains a comprehensive overview of the SS1000 analyzer and step-by-step instructions on:
Inspecting the Analyzer
Setting up the Analyzer
Powering Up the Analyzer
Operating the Analyzer
Serial Port Communications
Powering Down the Analyzer
Troubleshooting
Who Should Read This Manual
This manual should be read and referenced by anyone installing, operating, or having contact with the analyzer.
How to Use This Manual
Take a moment to familiarize yourself with this Operator’s Manual by reading the Table of Contents.
There are a number of options and accessories available for the SS1000 analyzers. This manual has been written to address the most common options and accessories. Read each section in the
manual carefully so you can quickly
and easily install and operate the analyzer. The manual includes images, tables, and charts that provide a visual
understanding of the analyzer and its functions. Special symbols are also used to make you aware of potential hazards, important information, and valuable tips. Pay close attention to this information.
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Special Symbols Used in This Manual
This manual uses the following symbols to represent potential hazards, caution alerts, and important information associated with the analyzer. Every symbol has significant meaning that should be heeded.
General Warnings and Cautions
Following are general warnings and cautions to observe when servicing the analyzer.
This icon denotes a warning statement. Warning statements indicate a potentially hazardous situation which, if not avoided, may result in serious injur
y or death.
Failure to follow all directions may result in fire.
Failure to follow all directions or substitution of components may result in explosion.
Class IIIb radiation product. When open, avoid exposure to beam.
Failure to follow all directions may result in damage or malfunction of the analyzer.
Important information concerning the installation and operation of the analyzer.
Process samples may contain hazardous material in potentially flammable
and/or toxic
concentrations. Personnel should have a thorough knowledge and understanding of the physical properties of the sampler and prescribed safety precautions before operating the Sample Conditioning System.
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Introduction
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Explosion hazard. Substitution of components may impair suitability for Class I, Div. 2.
Explosion hazard. Do not connect or disconnect equipment unless power has been switched off or the area is known to be non­hazardous.
Always disconnect the main power to the instrument before attempting any repair.
Read and understand all instructions before attempting to operate the instrument. Observe all caution notes and warning labels.
Class IIIb invisible laser radiation. When open, avoid expo
sure to
beam.
Conforms to provisions of US 21 CFR1040 10. Class I laser product. Refer servicing to the manufacturer’s qualified personnel.
Use a damp cloth to clean display and keypad to avoid static electric discharge.
Do not exceed 10 psig (0.7 barg) in sample cell. Damage to cell may result.
Do not hold or carry the analyzer by the measurement heads or sample cells. Doing so may result in optical misalignment affecting the performance of the sensor.
When selecting an
analyzer, the
total system design must be considered to ensure safe, trouble-free performance. Function, sizing, proper installation, operation, and maintenance are beyond the control of SpectraSensors and are the responsibilities of the system designer and user.
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SpectraSensors Overview
SpectraSensors, Inc. (SSI) is a leading manufacturer of state-of-the-art electro-optic gas analyzers for the industrial process, gas distribution and environmental monitoring markets. Headquartered in Houston, Texas, SSI was incorporated in 1999 as a spin-off of the NASA/Caltech Jet Propulsion Laboratory (JPL) with the purpose of commercializing space-proven measurement technologies initially developed at JPL.
About the Gas Analyzers
The SS1000 is a tunable diode laser (TDL) absorption spectrometers operating in the near- (IR-A, 0.75
1.4 µm) to short-wavelength infrared (IR-B, 1.43
µm). Each compact sensor consists of a TDL light source, sample cell and detector specifically configured to enable high sensitivity measurement of a particular component in the presences of other gas phase constituents in the stream. The sensor is controlled by microprocessor-based electronics with embedded software that incorporates advanced operational and data processing algorithms.
An appropriate
sample conditionin
g system may also be included with the system that has been specifically designed to deliver an optimum sample stream that is representative of the process stream at the time of sampling. Most SS1000 analyzer systems are configured for use at extractive natural gas sampling stations.
How the Analyzer Works
The SS1000 analyzer employs tunable diode laser absorption spectroscopy (TDLAS) to detect the presence of trace substances in process gases. Absorption spectroscopy is a widely used technique for sensitive trace species detect
ion. Because the measurement is made in the volume of the gas, the response is much faster, more accurate and significantly more reliable than traditional surface-based sensors that are subject to surface contamination.
In its simplest form, a diode laser absorption spectrometer typically consists of a sample cell with a mirror at one end and a mirror or window at the other through which the laser beam can pass, as shown in Figure 1–1. The laser beam enters the cell and reflects off the mirror(s) making one or more trips through the sample ga
s and eventu
ally exiting the cell where the remaining beam intensity is measured by a detector. With the SS1000 analyzers, sample gas flows continuously through the sample cell ensuring that the sample is always representative of the flow in the main pipe.
If equipment is used in a manner not specified by the manufacturer, the protection provided by the manufacturer may be impaired.
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Due to their inherent structure, the molecules in the sample gas each have characteristic natural frequencies (or resonances). When the output of the laser is tuned to one of those natural frequencies, the molecules with that particular resonance will absorb energy from the incident beam. That is, as the beam of incident intensity, I
0
(λ), passes through the sample, attenuation occurs via absorption by the trace gas with absorption cross section σ(λ). According to the Beer-Lambert absorption law, the intensity
remaining, I(λ), as measured by the detector at the end of the beam path of length l (cell length × number of passes), is given by
)1(,
where N represents the species concentration. Thus, the ratio of the absorption measured when the laser is tuned on-resonance versus off-resonance is directly proportional to the number of molecules of that particular species in the beam path, or
)2(.
Figure 1–2 shows typical raw data from a laser absorption spectrometer scan including the incident laser intensit
y, I
0
(λ), and the transmitted intensity, I(λ), for a clean system and one with contaminated mirrors (shown to illustrate the systems relative insensitivity to mirror contamination). The positive slope of the raw data results from ramping the current to tune the laser, which not only increases the wavelength with current, but also causes the corresponding output power to increase. By normalizing the signal by the incident intensity, any laser output fluctuations are cancelled, and a typical, yet more pro
nounced, abs
orption profile results, as shown in Figure 1–3. Note that contamination of the mirrors results solely in lower overall signal. However, by tuning the laser off-resonance as well as on-resonance and normalizing the
L
D
DETECTOR
LASER
RORRIMRORRIM
I
0
(λ)
I(λ)
TRACE GAS ABSORPTION
α(λ)
GAS IN
GAS OUT
Figure 1–1 Schematic of a typical laser diode absorption spectrometer.
I λ( ) I0λ( )exp σ λ( )lN[ ]=
N
1
σ λ( )l
--------------
I λ( )
I0λ( )
-------------
ln=
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Figure 1–2 Typical raw signal from a laser diode absorption spectrometer with and without mirror contamination.
Figure 1–3 Typical normalized absorption signal from a laser diode absorption spectrometer.
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data, the technique self calibrates every scan resulting in measurements that are unaffected by mirror contamination.
SpectraSensors takes the fundamental absorption spectroscopy concept a step further by using a sophisticated signal detection technique called wavelength modulation spectroscopy (WMS). When employing WMS, the laser drive current is modulated with a kHz sine wave as the laser is rapidly tuned. A lock­in amplifier is then used to detect the harmonic component of the signal that is
at twice th
e modulation frequency (2f), as shown in Figure 1–4. This phase­sensitive detection enables the filtering of low-frequency noise caused by turbulence in the sample gas, temperature and/or pressure fluctuations, low­frequency noise in the laser beam or thermal noise in the detector.
With the resulting low-noise signal and use of fast post-processing algorithms combined with careful calibration to correct for secondary effects caused by temperature and pressure variations and occasional spectral o
verlap with
ba
ckground species, reliable parts per million (ppm) or even parts per billion (ppb) detection levels are possible (depending on target and background species) at real-time response rates (on the order of 1 second).
All SpectraSensors TDL gas analyzers employ the same design and hardware platform. Measuring different trace gases such as H
2
O, HCl, H2S, NH3, CO2, CO
and O
2
in various mixed hydrocarbon background streams, including natural gas (alkanes), ethylene, propylene, refinery fuel gas, hydrogen reformer gas, sy
ngas and others, is accomplished by simply choosing a different optimum diode laser wavelength between 700 nm and 3000 nm which provides the least amount of sensitivity to background stream variations. Use of ultra-high
Figure 1–4 Typical normalized 2f signal where the species concentration is proportional to the peak height.
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reliability optical telecommunications diode lasers (manufactured to stringent Telcordia GR 468 specifications), 316L stainless steel, coated optical reflectors, absence of any moving parts, tolerance to condensation of process liquids and accumulation of particulates from gas streams eliminates requirements for field calibration and frequent maintenance making SpectraSensors TDL analyzers the most reliable gas analyzer platform with the lowest total cost of ownership.
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SS1000 Operator’s Manual 21
2 - INSTALLATION
Installing the analyzer is relatively easy requiring only a few steps that, when carefully followed, will ensure proper mounting and connection. Once the analyzer arrives, you should take a few minutes to examine the contents before installing the unit.
What Should be Included in the Shipping Box
The contents of the box should include:
The SpectraSensors SS1000
This Operator’s Manual with instructions on setting up and operating
the analyzer
Carrying case
Membrane separator filter (installed)
100250 VAC, 50/60 Hz battery charger
Quick-connect fittings for inlet and outlet tubes
One external serial cable to connect the analyzer to a computer
Additional accessories or options as ordered.
If any of these contents are missing, contact your sales representative.
Inspecting the Analyzer
Unpack and place the unit on a flat surface. Carefully inspect all enclosures for dents, dings, or general damage. Inspect the inlet and outlet connections for damage, such as bent tubing. Report any damage to the carrier.
Hardware and Tools for Installation
Depending on the particular model, the configuration of accessories and options ordered, you may need the following hardware and tools to complete the installation process.
Hardware:
Heated pressure regulator (if inlet pressure is >10 psig or no probe
regulator exists)
Avoid jolting the instrument by dropping it or banging it against a hard surface. Do not attempt to pick up the instrument using the sample cell. Either action may disturb the optical alignment.
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Stainless steel tubing or flexible stainless steel tubing
(SpectraSensors recommends using 1/4" O.D. x 0.035" wall thickness, seamless stainless steel tubing).
Tools:
7/16" open-end wrench
9/16" open-end wrench.
Setting up the Analyzer
The SS1000 analyzer is manufactured for temporary installation at a sampling point. Place the analyzer at a location relatively free of vibration and close to the sampling point. Choose a shaded area or use an optional analyzer hood (or equivalent) to minimize sun exposure. Refer to the
layout di
agrams in
Appendix B for detailed dimensions.
Connecting the Gas Lines
Once the analyzer has been suitably place, you are ready to connect the sample supply and sample return lines. All work must be performed by technicians qualified in pneumatic tubing.
When setting up the analyzer, be sure not to position the instrument so that it is difficult to operate adjacent devices. Allow 3 feet of room in front of the analyzer and any switches.
It is critical to set up the analyzer so that the
inlet and outlet li
nes reach the inlet and outlet connections on the chassis while still maintaining flexibility so that the sample lines are not under excessive stress.
In order to capture a representative sample of gas, the sample must be captured from the pipeline using a probe equipped with a standard or heated field-pressure reducing regulator. For more information, refer to the American Petroleum Institute's “Manual of Petroleum Measurement Standards,” Chapter 14, Se
ction 1 -
N
atural Gas Samples for Custody Transfer.
The sample supply port on the analyzer is equipped with a membrane separator filter to prevent liquid from entering the sample cell and accumulating on the internal optics.
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To connect the sample supply line:
1. The analyzer comes with a 1/8" quick-connect fitting for the sample supply and a 1/4" quick-connect fitting for the sample return. Attach these fittings to the analyzer.
2. Confirm that the sample probe is correctly installed at the supply tap and that the sample probe isolation valve is closed.
3. Also, confirm that the field-pressure reducing station is installed properly at the sample probe and that the pressure regulator at the field-pressure reducing station is closed (adjustment knob turned fully co
unter-clockwise).
4. Check that the relief valve vent line is properly installed from the field-pressure reducing station to the low-pressure flare (or atmospheric vent connection).
5. Determine appropriate tubing route from the field-pressure reducing station to the analyzer.
6. Run stainless steel tubing from the field-pressure reducing station (set for the specified inlet pressure) to the sample supply port of the analyzer. Bend tubing using industrial grade benders, check tubing fit to ensure proper seating
between the
tubing and fittings. Fully
ream all tubing ends. Blow out the lines for 10
15 seconds with
clean, dry nitrogen or air prior to making the connection.
7. Connect the inlet tube to the analyzer using the 1/8" stainless steel compression-type quick connect fitting provided.
8. Tighten all new compression fittings 1 1/4 turns with a wrench from finger tight. For connections with previously swaged ferrules, thread the nut to the previously pulled up position, then tighten slightly with a wrench. Secure tubing to appropriate structural supports as requir
ed.
9. Chec
k all connections for gas leaks. SpectraSensors recommends
using a liquid leak detector.
The sample at the sample tap may be at a high pressure. Use extreme caution when operating the sample probe isolation valve and field-pressure reducing regulator.
All valves, regulators, switches, etc. should be operated in accordance with site lock-out/tag-out procedures.
Do not exceed 10 psig (0.7 barg) in sample cell. Damage to cell may result.
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10. While gas is flowing, briefly open the bypass valve on the membrane separator filter to clear out any liquids that may have accumulated during startup.
To connect the sample return:
1. Confirm that the low-pressure flare or atmospheric vent header shut-off valve is closed.
2. Determine appropriate tubing route from the analyzer to the low­pressure flare or atmospheric vent header.
3. Run stainless steel tubing from the sample return port to the low­pressure flare or atmospheric vent header connection. Bend tubing using industrial
grade benders, check tubing fit to ensure proper seating between the tubing and fittings. Fully ream all tubing ends. Blow out the lines for 10–15 seconds with clean, dry nitrogen or air prior to making the connection.
4. Connect the sample return tube to the analyzer using the 1/4" stainless steel compression-type quick connect fitting provided.
5. Tighten all new fittings 1 1/4 turns with a wrench from finger tight. For connections with previously swaged ferrules, thread the nut to the previously pulled up position, then tighten slightly wi
th a wrench.
Secure
tubing to appropriate structural supports as required.
6. Check all connections for gas leaks. SpectraSensors recommends using a liquid leak detector.
Conditioning the SCS Tubing
Newly installed systems invariably have some trace contaminants and/or are intended for measuring trace amounts of gas constituents that tend to cling to system walls resulting in erroneous readings if the constituents are not in equilibrium with the system walls. Therefore, once the analyzer is completely connec
ted, the ent
ire system (i.e., from the sample source valve to the vent or return) should be conditioned by flowing sample gas through the system for up to 12 hours (or until reading stabilizes) after the system is powered up and before actual readings are taken. Progress of the system conditioning can be monitored via the gas concentration readings. Once the gas constituents have reached equilibrium with the system walls, the readings should stabilize.
All valves, regulators, switches, etc. should be operated in accordance with site
lock-out/tag-out procedures.
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Connecting Electrical Power to the Analyzer
The analyzer comes equipped with a fully charged internal battery. Battery life is approximately 12 hours under normal operating conditions. A 100
250 VAC,
50/60 Hz battery charger is supplied with the analyzer. To recharge the battery, plug the charger cable into the jack on the back of the analyzer under the serial port.
Connecting the Output Signals
The serial output is supplied from the serial port located on the back of the analyzer below the on/off switch. The analyzer can be connected to a serial port on a computer with the factory-s
upplied external serial cable. If the receiving computer has only a USB port available, a USB-to-serial adapter can be used. SpectraSensors recommends RadioShack
®
P/N 26-183.
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SS1000 Operator’s Manual 31
3 - OPERATING THE ANALYZER
Powering Up the Analyzer
After setting up the analyzer and connecting the gas lines, you are ready to power up the analyzer.
To power up the analyzer:
1. Power up the analyzer by turning on the power switch on the back of the analyzer.
2. The analyzer goes through an initialization period counting down from 15 while showing the firmware version, release date and measurement type [Dual Peak (DP) or Direct Measurement (DM)] on the bottom line.
The laser housing labels on the flanges of the sample cell warn about exposure to laser radia
tion inside. Never open the sample cell unless directed to do so by a service representative and the analyzer power is turned off.
The optical head has a seal and “WARNING” sticker to prevent inadvertent tampering with the device. Do not attempt to compromise the seal of the optical head assembly. Doing so will result in loss of device sensitivity and inaccurate measurement data. Repairs can then only be performed by the factory and
are
not
covered under warranty.
See Figure B–1 or Figure B–2 for locating fuses. If you need to replace a fuse, use only the same type and rating of fuse as the original, as listed in Table A–1.
Initializing...
15
v2.41 08-12-09 DM
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3. After initialization, the LCD displays the Normal Mode screen with four lines (the third of which is blank for single-channel units).
4. Enable Peak Tracking following the procedure outlined in “To change parameters in Mode 2” on page 3-6.
5. Continuous updates of the measurement parameters displaying on
the LCD indicate that the analyzer is operating normally.
6. Allow approximately three additional minutes for the analyzer to stabilize before recording measurements.
Powering Down the Analyzer
It may be necessary to power down the analyzer for problem solving or maintenance reasons.
To power down the analyzer:
1. Power down the analyzer by turning off the power switch on the back of the analyzer.
2. If the analyzer is going to be shut down for a long period of time, turn off sample flow to the analyzer by closing the sample probe shut-off valve at the sample supply tap.
3. Allow pressure in the field-pressure reducing regulator to dissipate until only a low residual pressure is indicated on the pressure gauge at the field station.
4. C
lose the field-pressure reducing regulator (adjustment knob turned
fully counterclockwise).
Operating the Analyzer from the Keypad
The keypads enable the operator to modify measurement units, adjust operational parameters, and perform diagnostics. During normal operation, the LCDs continuously display the measured components’ concentrations, sample cell temperatures, and sample cell pressures.
<NORMAL MODE>
H2O: 1.0256lb/mmscf
P: 954.4mb T: 76.1F
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The SpectraSensors keypad is shown in Figure 3–1. To activate any functions on the keypad, press the mode key # followed by a number on the keypad to specify a mode.
When you press the # key, the word MODE displays on the LCD. At this point, the analyzer waits for you to press a second key.
The * key functions as the “enter” key. The analyzer saves the displayed parameter value when you press this key. Always press * after entering a value on the keypad (unless the entr
y was made in erro
r).
If you do make an error, press the # key followed by the 1 key to return to Mode 1 without saving.
Modes Defined
Use the keypad to access the following modes by pressing the key # key first followed by a number (1, 2, 4 or 6) to activate a mode. The following section explains each mode and the corresponding information that displays on the LCD.
You must press the # key before pressing a number or function key to trigger a response from the keypad.
LCD Panel
Reserved for Service Diagnostics
System Diagnostics
Diagnostic Data Export to Serial Port
Functions as
“ENTER” Key
Activates Keypad
Functions
Normal Display
Change Parameters
System Diagnostic
Parameters
#
MODE
E
TEST
ENTER
1
4
7
_
2
5
8
0
3
6
9
.
*
NORM
DIAG
PARAM
DIAG
PARAM
DATA
CH.A
CH.B
CH.A
CH.B
TRANS
Figure 3–1 SS1000 keypad.
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Mode 1: (Normal Mode)
Continuously displays updated measurements. Press the # key followed by the 1 key.
The measurements displayed are:
H2O — Concentration in units selected in Mode 2.
P — Pressure in the sample cell in units selected in Mode 2.
T — Temperature in the sample cell in units selected in Mode 2.
Mode 2: (Set Parameter Mode)
Enables user to view and change measurement parameters. Follow the procedure under “To change parameters in Mode 2” on page 3-6 for viewing and changing any of the parameters.
Mode 3: (Not Used) Mode 4: (System Di
agnostic Parameters)
Displays system diagnostic data for Channel A. These values may be useful when troubleshooting the system. Press the # key followed by the 4 key.
The diagnostic parameters in Mode 4 displayed are:
PP2F: Shows the value of the concentration signal in A/D counts. A
normal range is 0 to 8190 depending on the concentration.
+
# 1
<NORMAL MODE>
H2O: 1.0256lb/mmscf
P: 954.4mb T: 76.1F
+
# 4
PP2F:8190 PkDf:34.00 Powr:2538 PkD1:34.00 Indx: 301 Zero: -24
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Powr: Shows the laser power detected at the absorption peak in A/D
counts. Acceptable values are between 1000 and 2000. A number below 1000 may indicate that either the optics need to be cleaned or there is an alignment problem. A value below 200 will cause a Power Fail.
Indx: Shows the position of the absorption peak within the
wavelength scan. It should normally be at 290 with the peak tracking turned on. Typically, values outside of the range of 241 to 339 indicate a Spectrum Fail condition.
Zero: Shows the detector signal value when the laser is turned off.
It should be in the range of -50 to +50. Outside of this range, a Null Fail displays.
PkDf: The factory laser current set point in mA that matches the
target absorption line.
PkD1: The laser current set point after adjustment by the peak-
tracking software. It should be within a few mA of the PkDf value. If the analyzer is experiencing problems, one of the first troubleshooting steps should be to check the peak tracking. Tracking Fail may be displayed if PkD1 differs by more than 4 mA from
PkDf. For more information on troubleshooting these issues,
see “Peak Tracking Reset Procedure” on page A-5.
Mode 5: (Not Used) Mode 6: (Diagnostic Data Download)
Used to transfer diagnostic data to the serial port and read the individual data points of both the DC and 2f spectra that the instrument analyzes to calculate the gas concentration. Viewing these data can be helpful in diagnosing problems with the analyzer. Press # key followed by the 6 key.
The data points, along with int
ermediate calculation results, are output to the
serial port(s) whenever Mode 6 is selected.
+
#
6
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Mode TEST: (System Test)
Provides basic diagnostic test results indicating that the laser power, pressure/temperature sensors, and the infrared spectrum that the system records for analysis are all nominal. Press the # key followed by the TEST key.
The LCD displays the system test data.
Changing Measurement and Control Parameters
In Mode 2, all of the pertinent measurement and control parameters can be viewed and changed. Refer to Table 3–1 for a list of parameters and value ranges.
To change parameters in Mode 2:
1. Press the # key followed by the 2 key. The LCD prompts for a
numeric password.
2. Enter the user password (3142) on the keypad, then press the * key to enter the number.
3. Starting with the first parameter, enter a new value and/or press the * key to store the value and cycle to the next parameter.
+
#
TEST
<SYSTEM TEST> Laser Power: OK PT Sen: OK Trak: OK Spectr: OK Null: OK
<SET PARAMETER MODE>
Enter password
v2.41 08-12-09 DM
<SET PARAMETER MODE>
S Factor
1.00000 Enter a value
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4. When finished changing or viewing the measurement and control parameters, press the # key followed by the 1 key to return to Mode 1 and normal operation.
Table 3–1 Measurement and control parameters.
Parameter Setting Function
teS resUrotcaF S
-99 – 99 Default = 1
Analyzer response adjustment to match calibration standard in the field.
S Factor Offset User Set
-999999 – 999999 Default = 0
Analyzer offset adjustment to match calibration standard in the field.
# Spectrum Average 1 – 240
Default = 4
Sets the number of scans aver­aged for each measurement
sgnidaer 003 – 1etaR reggoL
Default = 4
Sets the number of measure­ments to include in a running average
ot ytilibapac gnikcart kaep steS2 ,1 ,0gnikcarT kaeP
off, on, or reset
DO
Alarm Setup Not applicable for SS1000 Alarm Setpoint Not applicable for SS1000 4-20 mA Alarm Action Not applicable for SS1000 4-20 mA % Test Not applicable for SS1000 4 mA Span Not applicable for SS1000 20 mA Span Not applicable for SS1000
-met rof tinu yalpsid eht steS1 ro 0tinU erutarepmeT
perature
-serp rof tinu yalpsid eht steS3 ro ,2 ,1 ,0tinU erusserP
sure
-noc rof tinu yalpsid eht steS1 ro 0tinU noitartnecnoC
centration
ot desu erusse
rp enilepip steS999999 – 0erusserP enilepiP
calcula
te dew point
Modbus Address User Set
0 – 250
Sets Modbus address for the analyzer
teS resUedoM subdoM
0, 1, or 2
Sets type of Modbus protocol
teS resUDI rezylanA
0 – 2147483647
Customer definable value for analyzer ID
teS resUDI elpmaS
0 – 2147483647
Customer definable value for sample ID
teS resUDI tnenopmoC
0 – 2147483647
Customer definable value for component (analyte) ID
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Measurement and Control Parameters Defined
S Factor
The S Factor parameter is a user definable value that enables adjustment (without affecting the factory calibration) of the analyzer response (or slope) in the field [see “Adjusting Analyzer Reading to Match Specific Standard(s)” on page 3-12].
S Factor Offset
The S Factor Offset parameter is a user definable value that enables adjustment (without affecting the factory calibration) of the analyzer offset in the field [see “Adjusting Analyzer Reading t
o Match Specific
Standard(s)” on page 3-12].
# Spectrum Average
The # Spectrum Average parameter sets the number of scans that the analyzer averages for when determining the concentration. Averaging over multiple scans lowers noise in the measurement but inherently increases the response time. Each scan adds about 0.25 seconds to the response time. For example, if #Spectrum Average is set to “4,” an updated concentration value will be calculated about once every second.
<SET PARAMETER MODE>
S Factor
1.00000 Enter a value
<SET PARAMETER MODE>
S Factor Oset
0.00000 Enter a value (%)
<SET PARAMETER MODE> # Spectrum Average 16 Enter a value
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Logger Rate
For applications where an external data logger is employed, use the logging rate to set the number of measurements to include in the running average. The display and the current loop output will each have a value representing the running average of the concentration over a number of measurements equal to Logger Rate.
Peak Tracking
The peak tracking function is a software utility that continuously adjusts the laser current to keep the absorption peak of the measured component at the center of the scan. There are thre
e choices: 0 for no peak tracking, 1 for peak tracking (default), or 2 to reset the peak tracking function. In most cases, the peak tracking should be left on (i.e. Peak Tracking set to 1).
Temperature Unit
The Temperature Unit parameter designates the display units for the measured cell temperature. There are two choices: 0 for degrees Celsius and 1 for Fahrenheit. The default value is the standard unit of measurement in the region the analyzer is being used.
<SET PARAMETER MODE> Logger Rate 4 Enter a value
<SET PARAMETER MODE> Peak Tracking 1 0:O 1:Track 2:Reset
<SET PARAMETER MODE> Temperature Unit 0 0:C 1:F
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Pressure Unit
The Pressure Unit parameter designates the display units for the measured absolute pressure in the cell. There are four choices: 0 for millibar, 1 for Torr, 2 for kPa, and 3 for psia.
Concentration Unit
The Concentration Unit parameter designates the display units for the measured concentration. There are three choices: 0 for ppmv, 1 for lb/MMscf, and 2 for dew point (calculated at the Pipeline Pressure set below and displayed in the Temperature Unit set above). For percentage level analyzers
, the choices are: 0
for ppmv and 1 for %.
Pipeline Pressure (if applicable)
On moisture systems, the Pipeline Pressure parameter sets the pressure for the calculation of dew point. The value entered here will have the units designated by the Pressure Unit parameter, which will be reflected by the term in parentheses in the display.
<SET PARAMETER MODE>
Pressure Unit
0:mb1:Torr2:kPa3:psi
<SET PARAMETER MODE>
Concentration Unit 0 0:ppmv 1:lb 2:DP
<SET PARAMETER MODE>
Pipeline Pressure
0.00000 Enter a value (mb)
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Modbus Address
The Modbus Address parameter sets the analyzer address for when the analyzer is used as a Modbus device. Addresses from 1 to 250 can be used.
Modbus Mode
The Modbus Mode parameter sets the communications protocol for the RS232 port. There are three choices: 0 for turning the Modbus capabilities off and
defaulting to generic serial output as described in “Receiving Serial Data (RS-232 Output)” on page 4-1; 1 for enabling the analyzer to respond to Gould Modbus RTU function codes 3, 6 and 16; and 2 for enabling the analyzer to respond
to Daniel Modbus R
TU function codes 3, 6 and 16.
User Analyzer ID
The User Analyzer ID parameter assigns a numeric identification to the data enabling SCADA or DCS systems to associate data with a particular analyzer.
<SET PARAMETER MODE> Modbus Address 1 Enter a value(1-250)
<SET PARAMETER MODE> Modbus Mode 0 0:O 1:GMR 2:DMR
<SET PARAMETER MODE> User Analyzer ID 0 Enter a value
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User Sample ID
The User Sample ID parameter assigns a numeric identification to the data enabling SCADA or DCS systems to associate the data with a particular sample point.
User Component ID
The User Component ID parameter assigns a numeric identification to the data enabling SCADA or DCS systems to associate the data with a particular analyte.
Adjusting Analyzer Reading to Match Specific Standard(s)
In some instances, the user may wish to adjust the analyzer reading to match the concentration (or concentrations) of a spec
ific standard (or standards). The S Factor and S Factor Offset parameters are used to adjust the analyzer output in the field without affecting the factory calibration. Both parameters are used when samples from two different concentration standards are available, whereas only the S Factor Offset parameter is used when a sample from only one concentration standard is available.
The value of the S Factor parameter,
S, is determined by
,
where
C
1
is the certified concentration of standard No. 1, C2 is the certified
concentration of standard No. 2,
A
1
is the measured concentration (analyzer
reading) of standard No. 1, and
A
2
is the measured concentration (analyzer
reading) of standard No. 2. The S Factor Offset parameter,
O, is determined by
,
<SET PARAMETER MODE> User Sample ID 0 Enter a value
<SET PARAMETER MODE> User Component ID 0 Enter a value
S
C2C1–
A
2A1
--------------------
=
O C1S A1( )=
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where when a sample from only one concentration standard is available.
To adjust the analyzer reading:
1. Validate the analyzer using one or two concentration standards [see “Validating the Analyzer” on page 3-15].
2. Calculate the S Factor and/or S Factor Offset parameter(s) using
the equations above.
3. Follow the procedure under “To change parameters in Mode 2” on page 3-6 to enter the new values.
Confirm the new values by re-measuring the bottle(s) of test gas.
Changing Measurement Range (for dual-range moisture systems onl
y)
The measurement range on moisture systems that have been specifically calibrated for dual-range operation can be switched by changing a few key parameters. Refer to the parameter specifications that come with the analyzer calibration documents.
To change measurement range:
1. Follow the procedure under “To change parameters in Mode 2” on page 3-6 to enter new parameter values.
2. Scroll through the parameters by pressing the * key until arriving at the Peak Tracking parameter.
SpectraSensors recommends validating the analyzer using only H
2
O & CO2 in CH4. Bottles of test gas with certified concentrations of approximately 20% and 80% of full scale are recommended for two point validation. For single point validation, a bottle with a certified concentration of approximately 50% of full scale should be used.
When procuring a gas standard, make sure the background gas is that specified (H
2
O & CO2 in CH
4
) or a mix that closely resembles
the contents of the process stream and have the gas stan
dard certified to better than the specified precision of the analyzer, if possible.
S 1=
<SET PARAMETER MODE> Peak Tracking 1 0:O 1:Track 2:Reset
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3. Press the 0 key followed by the * key to turn peak tracking off. Press the # key followed by the 1 key to return to Mode 1.
4. Press the # key followed by the 2 key. The LCD prompts for a
numeric password.
5. Enter the user password (7758) on the keypad, then press the * key to enter the number. This puts you into the factory mode.
6. Enter the Phase value (as provided with the calibration documents) for the desired range followed by the * key.
7. Enter the Midpoint value (as provided with the calibration document
s) for the desired range followed by the * key.
8. Repeat for Ramp Amplitude, Imod, RCalb, Zero Offset, Span, PA1, PA2, PA3 and PA4.
9. Press the # key followed by the 1 key to return to Mode 1.
10. Follow the procedure under “To change parameters in Mode 2”
on page 3-6 to enter new parameter values.
When changing parameters in factory mode, be careful not to change any parameters other than those specified for range change or the calibration and/or operation of the analyzer may be adver
sely affected.
<SET PARAMETER MODE>
Enter password
v2.40 08-12-08 DM
<SET PARAMETER MODE> Phase 320 Enter a value
<SET PARAMETER MODE> Midpoint
59.70000 Enter a value
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11. Scroll through the parameters by pressing the * key until arriving at the Peak Tracking parameter.
12. Press the 1 key followed by the * key to turn peak tracking on. Press the # key followed by the 1 key to return to Mode 1.
The analyzer should stabilize at the new settings within a few minutes.
Faults
Fault messages appear on the front panel LCD. System faults include one or more of the following:
Power Fail: this fault occurs when the DC signal becomes too weak
for a reliable measurement typically as a result of mirr
or
contamination.
Null Fail: this fault occurs if the detector signal value is out of the
range of -50 to +50 when the laser is turned off.
Spectrum Fail: this fault occurs when the system is unable to
adequately fit a curve to the measured signal typically as a result of DC signal saturation in the absence of absorbing gas in the measurement cell, too much noise in the signal or an unexpected gas mixture in the measurement cell.
P/T Fail: this fault occurs when the pressure and/or temperature in
the measurement cell exceeds the specified maximum operating levels.
Track Fail: this fault occurs when the peak tracking function is out
of range [PkDf (factory set midpoint) and PkD1 (peak track midpoint) differ by more than 4 counts].
See Appendix A for recommendations and solutions to common problems resulting in a system fault.
Validating the Analyzer
Validation of the analyzer can be achieved by measuring an appropriate gas standard.
To validate the analyzer:
1. Connect a bottle of validation gas to the sample supply port (at the specified supply pressure).
<SET PARAMETER MODE> Peak Tracking 1 0:O 1:Track 2:Reset
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2. Turn on the validation gas and adjust the flow to the specified value.
3. Check the factory calibration report for S Factor and/or S Factor Offset parameter values to be used when measuring validation gas.
4. If applicable, set the appropriate S Factor and/or S Factor Offset
parameter values (see “To change parameters in Mode 2” on page 3-6).
5. Make a measurement after the gas flows for approximately five minutes or when the value on the LCD settles.
6. After validation, switch the analyzer back to process ga
s adjust the
flow to the specified value to return to normal operation.
7. If applicable, reset the S Factor and/or S Factor Offset parameter values to those used for normal operation (typically 1 and 0, respectively).
SpectraSensors recommends validating the analyzer using only
H2O & CO2 in
CH
4
. A bottle of test gas with a certified concentration representing 50% of full
scale should be used.
Calibrating the Analyzer
Calibrating the analyzer is typically not required under normal circumstances. SpectraSensors calibrates each analyzer to a National Institute of Standards and Technology (NIST) traceable standard before shipping the unit to the end user. Because SpectraSensors analyzers use a non-contact form of measurement, they are relatively insensitive to contamination, are quite rugged and virtually maintenance free ensuring years of reliable service.
The adjustment setpoints of the analyzer flowmeters and pressure regulators will be interactive and may require readjustment multiple
times until the final setpoints are obtained.
The analyzer system has been designed for the sample flow rate specified. A lower than specified sample flow rate may adversely affect analyzer performance. If you are unable to attain the specified sample flow rate, contact your factory sales representative.
When procuring a gas standard, make sure the background gas is that specified (CO
2
in CH4) or a mix that closely resembles the
contents of the process stream and have the
gas standard certified to better than the specified precision of the analyzer, if possible.
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SS1000 Operator’s Manual 41
4 - SERIAL PORT COMMUNICATIONS
Receiving Serial Data (RS-232 Output)
When the Modbus Mode parameter is set to 0, the analyzer is configured to transfer a string of data from the analyzer to a serial device via the RS-232 output. The receiving device is typically a computer terminal running HyperTerminal, which is a program included with Microsoft
®
Windows® 95, 98, & XP that enables serial communication and the viewing, capturing and storage of serial port data and messages.
To launch HyperTerminal:
1. On your Windows desktop, click Start followed by Run (usually located in the lower right side of the Start Menu).
2. Type Hypertrm.exe and hit Return to launch HyperTerminal.
3. Once HyperTerminal is activated, the Connection Description
window appears, as shown in Figure 4–1. Type in a Filename (where the terminal session settings will be stored for future recall) and click on any icon. Click OK.
4. The Connect To window appears prompting for a connection, as
shown in Figure 4–2. Click the Menu Arrow under Connect Using to view the choices.
5. Click on the appropr
iate port to which your analyzer is connected
(COM1, COM2, COM3, etc.) as established under “Connecting the
Output Signals” on page 2-5. Click OK.
6. Once the port is chosen, the COM Properties window appears.
Make sure the COM properties for the port selected reflect those shown in Figure 4–3 (9600 baud, 8 data bits, 1 stop bit, no parity, and no flow control).
7. Click OK to establish the connection.
Once connected, the data will start streaming through the Hyperterminal Window as shown in Figure 4–4.
For quicker access to HyperTerminal, save a HyperTerminal shortcut to the desktop.
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Figure 4–1 Connection Description window.
Figure 4–2 Connect To window.
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Figure 4–3 COM Properties window.
Figure 4–4 Hyperterminal window with streaming
data.
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The data string is comma and space delimited with a carriage return and includes:
Concentration - analyte concentration (user selected units)
Pressure - cell pressure (user selected units)
Temperature - cell temperature (user selected units)
PP2F - magnitude of concentration signal (counts)
Powr - DC signal at absorption peak (counts)
Indx - position of absorption peak in scan
Reference Peak PP2F (only for DP systems)
Reference Peak Powr (only for DP systems)
Reference Peak Indx (only for DP systems)
Zero - detected signal with laser turned off (counts)
PkD1 - present midpoint value (mA)
To capture and save data from the serial port:
1. To save the data from the serial port, use the Transfer/Capture
Text function and enter the Filename to where you would like to
store the captured data.
2. To stop the capture of the serial data, click on Transfer/Capture
Text/Stop.
To read diagnostic data with HyperTerminal:
1. Before entering Mode 6, make sure the serial port on the computer
used for serial communication is connected to the analyzer
and the
output stream is showing on the screen as described in “To launch
HyperTerminal” on page 4-1.
2. To save the data from the serial port, use the Transfer/Capture
Text function and enter the Filename to where you would like to
store the captured data.
The number of seconds between each line of data output should be the # Spectrum Average number set in Mode 2 or Mode 3 divided by 4.
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3. Once capturing is in place, enter Mode 6 by pressing # key followed
by the 6 key.
The index shown on the LCD display counts by 50’s from 0 to 511 in a few seconds and the screen displays:
4. Press the # key followed by the 1 key to return to Mode 1.
5. Once normal operation resumes, wait approximately three minutes
then stop the capture of the serial data. To stop the capture of the serial data, click on Transfer/Capture Text/Stop. The resulting data files contain the downloaded data as shown in Figure 4–5.
You c
an import th
e stored data file into a spreadsheet program such as
Microsoft Excel
®
to plot the data (see "Viewing Diagnostic Data with
Microsoft Excel" for more information.
Viewing Diagnostic Data with Microsoft Excel
A spreadsheet program such as Microsoft Excel can import the data collected in the Mode 6 data dump for viewing and plotting.
To import the data file into Excel:
1. In Excel, click Open and choose the name of the spectrum file saved
while in Mode 6. Be sure to select All Files (*.*) under Files of
type: while searching, as shown in Figure 4–7a.
2. T
he Text Import Wizard should open. Choose the Delimited
option and click Next, as shown in Figure 4–7b.
3. Under Delimiters, choose the Tab and Space options, check the
Treat Consecutive Delimiters as One box, as shown in Figure
4–8a, and then click Finish to display the spreadsheet. The first few
+
# 6
Dump Stats Mode...
Index: 0
Mode
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Figure 4–5 Sample diagnostic data output.
SpectraSensors HardHat: v2.31 Single 08-08-08 DM Idx DC AC
0 3181 3830 1 2699 3727 2 2007 3493 3 1359 3207
<<Information Deleted>> 509 3150 4095
510 3153 4095 511 3157 4095
Computational Statistics v2.31 Single 08-08-08 DM Ambient counts after averaging
Voltage: -1368 Temperature: -1532 Pressure: -206 ac counts after averaging
Peak Index: 240 Raw Count: 4095 Left Dip Index: 240 Raw Count: 4095 Right Dip Index: 278 Raw Count: -4095 pp2f (peak minus average of dips): 8190
dc counts after averaging raw at peak index: 2025 computed at peak index: 1714 raw at [peak index - 140]: 736 index: 100 raw at [peak index + 140]: 2692 index: 380 laser off, zero level: -10 dc level (computer power at peak - zero level): 1724 Lf_response (rcalb * dc level): 6616712
Calculated values Supply Voltage: 4.588 volts Concentration: 10.9129 ppmv Temperature: 27.1 C Pf_MidShift: 0.0000 Pressure: 1076.9 mb
Settings Phase: 90 Midpoint: 60.0000 Ramp amplitude: 35 Imod: 8 Rcalb: 3.838000E+03 Zero Offset (ppmv): 0.000000E+00 SpanFct(x1000): 1000 Span (ppmv):422.00 PA 1: 1.000E+00 PA 2: 0.000E+00 PA 3: 0.000E+00 PA 4: 0.000E+00 c0 Coeff: 0.00000E+00 c1 Coeff: 1.00000E+00 c2 Coeff: 0.00000E+00 c3 Coeff: 0.00000E+00 Peak Index Location: 290 Xleftvmr: 240 Xrightvmr: 340 Left Dip Range: 100 Right Dip Range: 100 DC Left Range: 140 DC Right Range: 140 Null Fail Range Min: -50 Null Fail Range Max: 50 mA Index Scale: 0.03030303 Peak Track Range Min: 3 Peak Track Range Max: 70 Peak Track Num Avgs: 3600 Peak Track Con Span: 10 Peak Track Con Span: 95 Peak Track Temp Min: -5
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Figure 4–6 Sample diagnostic data output (continued).
Peak Track Temp Max: 60 PT Matrix: 1 fc0 Background Coeff: 1.00000E+00 fc1 Background Coeff: 0.00000E+00 fc2 Background Coeff: 0.00000E+00 fc3 Background Coeff: 0.00000E+00 fp0 Background Corr: 1.00000E+00 fp1 Background Corr: 0.00000E+00 fp2 Background Corr: 0.00000E+00 fp3 Background Corr: 0.00000E+00 pp2f Direction: 1 Ref Peak Range Min: -180 Ref Peak Range Max: -80 Ref PeakTo Dip Range: -100 Serial Number: 100000000 S Factor: 1.00000 S Factor Offset: 0.00000 # Spectrum Average: 4 Logger Rate: 4 Peak Tracking: 0 DO Alarm Setup: 0 Alarm Setpoint(ppmv): 430.0 4-20mA Alarm Action: 0 4-20mA % Test: 101 4 mA span (ppmv): 0.000 20 mA span (ppmv): 422.000 Temperature Unit: 0 Pressure Unit: 0 Concentration Unit: 0 Pipeline Pressure: 0.00 Modbus Address: 0 Modbus Mode: 0 User Analyzer ID: 0 User Sample ID: 0 User Component ID: 0
Constants Kf_spanfactorFactor: 0.001000 Null Point: 6
Diagnostics ppmv: 10.9129 PP2F: 8190 Power: 1714 PkDf: 60.0000 PkDl: 60.0000 Index: 240 Zero: -10
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Figure 4–7 a) Opening a data file in Excel. b) Setting data type in Text Import Wizard.
b)
a)
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Figure 4–8 a) Setting Tab and Space as delimiters. b) Highlighting imported data for plotting in Excel.
a)
b)
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lines look like the normal serial output data received before the Mode 6 command was entered. Look for the three columns of numbers at the bottom of the file.
4. Click on the upper right cell of the three columns, as shown in Figure 4–8b. Hold the Shift key down while pressing the End key followed by the Down Arrow key to highlight the third column. Keep holding down the Shift key and press the End key followed by the Left
Arrow key to select the three columns by 512 rows.
5. Click the Chart Wizard button on the Task Bar.
The Chart
Wizard
should open, as shown in Figure 4–9.
6. Choose the X-Y (Scatter) chart type and the Smoothed Lines Without Markers sub-type. Click Finish to display a graph of the
spectrum, as shown in Figure 4–10a. If the 2f curve appears flat, double click on it to get to the Format Data Series Window. Select the Axis tab, and select Plot Series on Secondary Axis, as shown in Figure 4–10b. Click OK to rescale the plot.
Modbus Communications Protocol
Modbus is a serial communications protocol published by Modicon in 1979 for use with its programmable logic controllers (PLCs). It has become a de facto
Figure 4–9 Chart Wizard - Step 1 window.
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-500
0
500
1000
1500
2000
2500
3000
0 200 400 600
-150
-100
-50
0
50
100
150
200
250
Series1
Series2
Figure 4–10 a) Data file plot in Excel. b) Format Data Series window.
a)
b)
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standard communications protocol in industry, and is now the most commonly available means of connecting industrial electronic devices. Modbus is used
extensively in leu of other communications protocols because it is openly published and royalty-free, relatively easy to deploy, and capable of moving raw bits or words without placing many restrictions on vendors.
Modbus enables communication between many devices connected to the same network, for example, a supervisory computer with a remote terminal unit (RTU) in supervisory control and data acqui
sition (SCADA) systems.
The S
pectraSensors analyzer acts as a slave in a master/slave(s) network of devices. It can receive queries from a master and send responses back using either Gould Modbus RTU protocol or Daniel Extended Modbus RTU protocol.
Framing/Protocol
The transmission mode used to communicate is either Gould Modbus RTU or
Daniel Modbus RTU with port parameters 9600 (baud rate), 8 (data bits), 1 (stop bit), no (parity), and none (flow control/handshake).
The transmission mode is set by the user via the Modbus Mod
e parameter. See “To change parameters in Mode 2” on page 3-6. Note that the generic serial output (HyperTerminal) is disabled if either Gould or Daniel Modbus is selected.
Functions
Available functions are 0x03 (read holding registers), 0x06 (write to a single
register), 0x16 (write to multiple registers), and 0x43 (read device identification).
Addressing
The analyzer's Modbus slave node address can be in the range of 0-250 with
the default being 1. All analyzers will respond to an address of 0, so this address can be used to interrogate a single
unit when its address is unknown
or to determine its address. See Table 4–1 on page 4–15 for register definitions for both Gould and Daniel
Modbus modes. Be aware that for Gould Modbus the table follows the convention of identifying the register with an offset of 40001. For example, the actual value transmitted in the starting register field of the command is the listed register value minus 40001, e.g. register 47001 is addressed as 7000.
Reading/Writing in Daniel Modbus Mode
Daniel Modbus supports three types of registers: short integer, long integer and
floating point. Each “short integer” register is two bytes in length and will contain an integer value. Each “long integer” register is four bytes in length and will contain an integer value and each “floating point” register is four bytes in length and will contain a floating point value.
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Reading/Writing in Gould Modbus Mode
Gould Modbus supports three types of variable data, short integer, long integer and floating point, but all registers are addressed as word (two byte) registers. A “short integer” value is contained in one register whereas a “long integer” or “floating point” value requires two contiguous registers. The registers are defined as Read or Read/Write.
An appropriate password must be downloaded to the password register prior to writing to most registers. The User Level 1 (L1)
user password 314
2 will allow access to those registers which have been pre-defined as user configurable. Other writable registers can only be downloaded or changed by SpectraSensors support personnel using a User Level 2 (L2) password.
To enable Modbus communications:
1. Confirm that the serial cable has been properly connected. See “Connecting the Output Signals” on page 2-5.
2. Power up the analyzer (see “Powering Up the Analyzer” on page
3-1).
3. Press the # key followed by the 2 key (Channel A) or the # key followe
d by the 3 key (Channel B). The LCD prompts for a numeric
password. Enter the user password (3142) on the keypad, then press the * key to enter the number to enter Mode 2 (Set Parameter
Mode - Channel A) or Mode 3 (Set Parameter Mode - Channel B).
Use caution when writing to registers as changing the value of a writable register may affect the calibration of the analyzer.
<SET PARAMETER MODE>
Enter password
v2.41 08-12-08 DM
<SET PARAMETER MODE>
S Factor
1.00000 Enter a value
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4. Press the * key repeatedly until the Modbus Address parameter is displayed.
5. Enter the desired Modbus Address and press the * key to store the value and cycle to the Modbus Mode parameter.
6. Enter the desired Modbus Mode and press the * key to store the value.
7. Press the # key followed by the 1 key to return to Mode 1.The analyzer is now ready to receive Modbus queries.
<SET PARAMETER MODE> Modbus Address 1 Enter a value(1-250)
<SET PARAMETER MODE> Modbus Mode 0 0:O 1:GMR 2:DMR
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Table 4–1 Modbus register map .
Parameter
Daniel
Reg.
Gould
Reg.
Data Type
Action Min Max
Concentration 7001 47001 Float Read 0 0 Temperature 7002 47003 Float Read 0 0
00daeRtaolF500743007erusserP 00daeRtaolF9007450071DkP
Firmware Version 7057 47113 Float Read 0 0
taolF102741017rotcaF S
R/W L1
a
0 9
S Factor Offset 7102 47203 Float
R/W L1
a
-9 9
Pipeline Pressure 7104 47207 Float
R/W L1
a
0 9999.9 4 mA span Not applicable for SS1000 20 mA span Not applicable for SS1000 Zero Offset 7151 47301 Float
R/W L2
b
-100000 100000
Span Not applicable for SS1000
taolF5037435171AP
R/W L2
b
-299 299
taolF7037445172AP
R/W L
2
b
-299 299
taolF9037455173AP
R/W L2
b
-299 299
taolF1137465174AP
R/W L2
b
-299 299
taolF313747517ffeoC 0C
R/W L2
b
-999999 999999
taolF513748517ffeoC 1C
R/W L2
b
-999999 999999
taolF713749517ffeoC 2C
R/W L2
b
-999999 999999
taolF913740617ffeoC 3C
R/W L2
b
-999999 999999
taolF323742617fDkP
R/W L2
b
1 249
taolF523743617blaCR
R/W L2
b
10 100000 Alarm Flags 5001 45001 Long Read 0 0 Analyzer ID 5101 45201 Long
R/W L1
a
0 2.0E9
Sample ID 5102 45203 Long
R/W L1
a
0 2.0E9
Component ID 5103
45205 Long
R/W L1
a
0 2.0E9
Serial Number 5152 45303 Long
R/W L2
b
0 4.2949E9
00daeRtrohS100341003F2PP 00daeRtrohS200342003rwoP 00daeRtrohS300343003xdnI 00daeRtrohS400344003oreZ
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Modbus Accessible Parameter Definitions
Concentration – current live concentration in selected engineering
units.
Temperature – current live temperature of the gas sample in
selected engineering units.
Pressure – current live pressure reading of the gas sample in
selected engineering units atmospheric.
PkD1 – midpoint current (mA) of laser scan being used in the
analyzer when peak tracking is turned on.
Firmware Version – firmware version running in the analyzer.
S Factor – slope adjustment enabling the analyzer to be tuned to
match a specific calibration standard without affecting the factory calibration.
# Spectrum Average 3201 43201 Short
R/W L1
a
1 240
Logger Rate 3202 43202 Short
R/W L1
a
1 299
Peak Tracking 3203 43203 Short
R/W L1
a
0 2 Alarm Action Not applicable for SS1000 Temperature Unit 3205 43205 Short
R/W L1
a
0 1 Pressure Unit 3206 43206 Short
R/W L1
a
0 3 Concentration Unit 3207 43207 Short
R/W L1
a
0 2 Modbus Device Address 3208 43208 Short
R/W L1
a
0 250 Modbus Mode 3209 43209 Short
R/W L1
a
0 2 DO Alarm Setup 3210
43210 Short
R/W L1
a
0 107 4-20mA % Test Not applicable for SS1000
trohS103341033esahP
R/W L2
b
1 358 Ramp Amplitude 3303 43303 Short
R/W L2
b
1 249
trohS403344033domI
R/W L2
b
0 99 Password 4999 44999 Short R/W 0 9999
a. Write privilege requires User Level 1 (L1) password to be downloaded to the Pass-
word register.
b. Write privilege requires User Level 2 (L2) password to be downloaded to the Pass-
word register
Table 4–1 Modbus register map (Continued).
Parameter
Daniel
Reg.
Gould
Reg.
Data Type
Action Min Max
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S Factor Offset – offset adjustment enabling the analyzer to be
tuned to match a specific calibration standard without affecting the factory calibration.
Pipeline Pressure – sets the pressure used in calculating dew point.
The pressure unit is mb when setting this parameter via Modbus communications and as set by the Pressure Unit parameter when setting via the front panel.
Zero Offset – factory set offset applied to the concentration
calculation before compensation coefficients. A negative value adds and a positive value subtra
cts.
PA1, PA2, PA3, PA4 – factory set coefficients in the pressure
compensation equation. Should not be changed in field.
C0, C1, C2, C3 – factory set non-linearity coefficients for extended
range equipment. Should not be changed in field.
PkDf – midpoint current (mA) of laser scan.
Rcalb – factory set gain adjustment for the concentration reading.
Alarm Flags – long integer register identifying the status of each
individual alarm in the analyzer as follows:
Bit 0 = 1, general fault condition exists Bi
t 1 = 1, Null Fail alarm cond
ition exists Bit 2 = 1, Spectrum Fail condition exists Bit 3 = 1, P/T Fail condition exists Bit 4 = 1, Power Fail condition exists Bit 5 = 1, Track Fail condition exists
User Analyzer ID – user defined numeric analyzer ID.
User Sample ID – user defined numeric sample ID.
User Component ID – user defined numeric component ID.
Serial Number – factory assigned hardware serial number for the
analyzer.
PP2F – (counts) concentration signal.
Powr – (counts) laser power detected at the absorption peak.
Indx – position of the absorption peak along scan.
Zero – (counts) detected signal level with laser off.
# Spectrum Average – number of scans averaged for each
measurement.
Logger Rate – running average of the concentration reading.
Peak Tracking – turns peak tracking on and off.
Temperature Unit – sets the temperature units.
Pressure Unit – sets the pressure units.
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Concentration Unit – sets the concentration units.
Modbus Address – user assigned numeric address identifying
analyzer to Modbus host system.
Modbus Mode – sets the Modbus communication protocol type.
DO Alarm Setup – sets function of the secondary digital output.
Phase – factory set phase relationship between the modulating
current and lock-in detection circuit.
Ramp Amplitude – factory set laser current scan range about the
midpoint.
Imod – factory set laser current modulation amplitude.
Password – password required to change register settings. In the
above table those registers denoted as R/W L1 can be modified if the User Level 1 password is downloaded to this register. Likewise, those registers denoted as R/W L2 can only be modified if the level 2 password is downloaded to this register. Level 2 registers are reserved for SpectraSensors personnel use only.
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SS1000 Operator’s Manual A1
Appendix A: Troubleshooting
This section presents recommendations and solutions to common problems, such as gas leaks, contamination, excessive sampling gas temperatures and pressures, and electrical noise. If your analyzer does not appear to be hampered by one of these related problems, contact your sales representative for service.
Gas Leaks
Probably the most common cause of erroneous measurements is outside air leaking into the sample supply line. It is recommended the supply lines be
periodically leak-tested, especially if the
analyzer has been relocated or has been replaced or returned to the factory for service and the sample lines have been reconnected.
Membrane Separator Filter
The analyzer comes equipped with a membrane separator filter that separates out entrained liquids from the sample gas. If moisture accumulation is suspected, briefly open the bypass valve on the membrane separator filter to clear out any liquids.
If measured moisture concentration levels are higher than actual or an excess amount of wet ga
s has pass
ed through the filter, the membrane may need to
be replaced.
To replace the membrane:
1. Detach the 1/8" inlet tubing and the 1/4" compression fitting from the sample supply port on the analyzer.
2. Unscrew the two 10-32 socket head cap screws that attach the filter to the analyzer.
Do not use plastic tubing of any kind for sample lines. Plastic tubing is permeable to moisture and other substances which can contaminate the sample stream. SpectraSensors recommends using 1/4" O.D x0.035" wall thic
kness, seamless
stainless steel
tubing.
Process samples may contain hazardous material in potentially flammable and/or toxic concentrations. Personnel should have a thorough knowledge and understanding of the physical properties and safety precautions for the sample contents before operating the SCS.
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01-92-4 A .ver 97020-000942
3. Once detached, remove the four socket head cap screws in the filter body.
4. Open the filter body and replace the membrane.
5. Reassemble the filter body and attach the filter to the analyzer.
6. Connect the 1/8" inlet tubing and the 1/4" compression fitting to the
sample supply port on the analyzer.
7. Tighten all new compression fittings 1-1/4 turns with a wrench from finger tight. For connections with previously swaged ferrules, thread the nut to the previously pulled up position, then tighten slightly with a wrench. Secure tubi
ng to appropriate structural supports as
required.
8. Check all connections for gas leaks. SpectraSensors recommends using a liquid leak detector.
Contamination
Contamination and long exposure to high humidity are valid reasons for periodically cleaning the gas sampling lines. Contamination in the gas sampling lines can potentially find its way to the sample cell and deposit on the optics or interfere with the measurement in some other way. Although the analyzer is designed to withstand some contaminat
ion, it is recomme
nded to always keep
the sampling lines as contamination free as possible.
To keep the sampling lines clean:
1. Make sure that a membrane separator filter (included with most systems) is installed ahead of the analyzer and operating normally. Replace the membrane if necessary. If liquid enters the cell and accumulates on the internal optics, a Power Fail will result.
2. If mirror contamination is suspected, see “Cleaning the Mirrors” on page A-3.
3. Turn off the sample valve at the tap in accordance with site loc
k-out,
tag-out rules.
4. Disconnect the gas sampling line from the supply port of the analyzer.
5. Wash the sampling line with alcohol or acetone and blow dry with mild pressure from a dry air or nitrogen source.
6. Once the sampling line is completely free of solvent, reconnect the gas sampling line to the supply port of the analyzer.
Do not exceed 10 psig (0.7 barg) in sample cell. Damage to cell may result.
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7. Tighten all new compression fittings 1-1/4 turns with a wrench from finger tight. For connections with previously swaged ferrules, thread the nut to the previously pulled up position, then tighten slightly with a wrench. Secure tubing to appropriate structural supports as required.
8. Check all connections for gas leaks. SpectraSensors recommends using a liquid leak detector.
Cleaning the Mirrors
If contamination makes its way into the cell and accumulates on the internal optics, a Power Fail will result. If mirror contamination is sus
pected, please consult with your factory sales representative before attempting to clean the mirrors. If advised to do so, use the following procedure.
Tools and Supplies:
Lens cleaning cloth (Cole Parmer
®
EW-33677-00 TEXWIPE
®
Alphawipe® Low-Particulate Clean Room Wipes or equivalent)
Reagent-grade isopropanol (ColeParmer
®
EW-88361-80 or
equivalent)
Small drop dispenser bottle (Nalgene
®
2414 FEP Drop Dispenser
Bottle or equivalent)
Acetone-impenetrable gloves (North NOR CE412W Nitrile Chemsoft™
CE Cleanroom Glo
ves or equivalent)
Hemostat (Fisherbrand™ 13-812-24 Rochester-Pean Serrated
Forceps)
Bulb blower or dry compressed air/nitrogen
Torque wrench
Do not attempt to clean the cell mirror until you have consulted with your factory service representative and have been advised to do so.
The sample cell assembly contains a low-power, 10 mW MAX, CW Class IIIb invisible laser with a wavelength between 700­3000 nm. Never open the sample cell flanges or the optical assembly unless
the power is turned off.
Alway
s handle the optical assembly by the edge of the mount.
Never touch the coated surfaces of the mirror.
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SS1000 Operator’s Manual
A 01-92-4 A .ver 97020-000944
Marker
Flashlight
To clean the mirrors:
1. Power down the analyzer following the procedure outlined in “To power down the analyzer” on page 3-2.
2. Close the pressure regulator at the field-pressure reducing station
(adjustment knob turned fully counter-clockwise).
3. Close the sample probe isolation valve.
4. Close the low-pressure flare or atmospheric vent header shut-off
valve.
5. Disconnect the analyzer from the sample supply and return lines.
6. If possible, purge the system with nitrogen for 10 minutes.
7. Carefu
lly mark the orientat
ion of the mirror assembly on the cell
body.
8. Gently remove the mirror assembly from the cell by removing the 6 socket-head cap screws and set on a clean, stable and flat surface.
9. Look inside the sample cell at the top mirror using a flashlight to ensure that there is no contamination on the top mirror.
10. Remove dust and other large particles of debris using a bulb blower or dry compressed air/nitrogen. Pressurized gas duster products are not recommended as the propellent may deposit liquid droplets onto the optic
surface.
11. Put on clean acetone-impenetrable gloves.
12. Double fold a clean sheet of lens cleaning cloth and clamp near and
along the fold with the hemostats or fingers to form a “brush.”
13. Place a few drops of isopropanol onto the mirror and rotate the mirror to spread the liquid evenly across the mirror surface.
Careful marking of the mirror orientation is critical to restoring system performance upon reassembly after cleaning.
Due to its proximity to the optical head, SpectraSensors does not reco
mmend cleaning the top mirror. If the top mirror is visibly
contaminated, contact your factory service representative.
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14. With gentle, uniform pressure, wipe the mirror from one edge to the other with the cleaning cloth only once and only in one direction to remove the contamination. Discard the cloth.
15. Repeat with a clean sheet of lens cleaning cloth to remove the streak left by the first wipe. Repeat, if necessary, until there is no visible contamination on the mirror.
16. Carefully replace the mirror assembly onto the cell in the same orientation as previously marked making sure the o-ring is properly seated.
17. Tighten the 6 socket-head cap screws evenly with a
torque wrench
to 13 in-lbs.
Excessive Sampling Gas Temperatures and Pressures
The embedded software is designed to produce accurate measurements only within the allowable cell operating range (see Table B–1 on page B–1 or Table B–2 on page B–2). Pressures and temperatures outside these ranges will trigger a P/T Fail fault.
Electrical Noise
High levels of electrical noise can interfere with laser operation and cause it to become unstable. Always connect the analyzer to a properly grounded po
wer
source.
Peak Tracking Reset Procedure
The analyzer’s software is equipped with a peak tracking function that keeps the laser scan centered on the absorption peak. Under some circumstances, the peak tracking function can get lost and lock onto the wrong peak. If the difference between PkDf and PkD1 is more than 4, or Track Fail is displayed, the peak tracking function should be reset.
Never rub an optical surface, especially with dry tissues, as this can mar or scratch the coated surface.
If the press
ure, temperature, or any other readings on the LCD appear suspect, they should be checked against the specifications (see Table B–1 on page B–1 or Table B–2 on page B–2).
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To check the PkDf and PkD1 values:
For Channel A, press the # key followed by the 4 key to enter Mode 4 (System Diagnostic Parameters - Channel A) or press the # key followed by the 5 key
to enter Mode 5 (System Diagnostic Parameters - Channel B). A brief wait screen will appear as the diagnostic data for Channel B is polled.
18. Compare the values for PkDf and PkD1. If the difference is more than 4, reset the peak tracking function.
To reset the Peak Tracking Function:
1. Press the # key followed by the 2 key (Channel A) or the # key followed by the 3 key (Channel B). The LCD prompts for a numeric
password. Enter the user password (3142) on the keypad, then
PP2F:8190 PkDf:34.00 Powr:2538 PkD1:34.00 Indx: 301 Zero: -24
<Diagnostic for CHB>
Please wait...
PP2F:8190 PkDf:47.00 Powr:2028 PkD1:47.00 Indx: 253 T: 50.7 Zero: -16 P: 955.7
<SET PARAMETER MODE>
Enter password
v2.40 08-12-08 DM
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Troubleshooting
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press the * key to enter the number to enter Mode 2 (Set Parameter
Mode - Channel A) or Mode 3 (Set Parameter Mode - Channel B).
2. Press the * key to cycle through the screens until the Peak Tracking parameter appears.
3. Press 2 (RESET) followed by the * key. The peak tracking function
will cycle off then on and reset.
4. Press the mode key # followed by 1 to return to Mode 1 (Normal Mode).
Instrument Problems
If the instrument does not appear to be hampered by gas leaks, contamination, excessive sampling gas temperatures an
d pressures, or electrical noise, refer
to Table A–2 before contacting your sales representative for service.
Removing the Cover
If necessary, the analyzer cover can be removed by first unscrewing the ten
cover screws, as shown in Figure B–1, and gently lifting the cover off the system taking care not to damage the display and keypad cables. Disconnect
the display and keypad cables if necessary to gain access to the internal components.
The display and keypad cables are attached to the electronics inside the housing. Care must be taken when removing the cover to avoid damaging the cables or connectors. If disconnecting the cables is necessary, be sure to reconnect each one with the proper orientation. When reattaching the cover make sure the cables are not pinched between the body and the cover.
<SET PARAMETER MODE>
S Factor
1.00000 Enter a value
<SET PARAMETER MODE> Peak Tracking 1 0:O 1:Track 2:Reset
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Checking the Fuses
The main fuse is located on the back panel of the analyzer, as shown in Figure
B–1. An additional fuse is located on the DC to DC converter board inside the housing, as shown in Figure B–2. If you need to replace a fuse, use only the
same type and rating of fuse as the original as listed in Table A–1.
Service Contact
If the troubleshooting solutions do not resolve the problem, contact your sales representative. If returning the unit is required, obtain a Return Materials
Authorizatio
n (RMA) Number from your sales representative before
returning the analyzer to the factory. Your sales representative can determine whether the analyzer can be serviced on-site or should be returned to the factory.
Disclaimers
SpectraSensors accepts no responsibility for consequential damages arising from the use of this equipment. Liability is limited to replacement and/or repair of defective components.
This manual contains information protected by copyright. No part of this guide may be photocopied or reproduced
in any form without prior written consent
from SpectraSensors.
Warranty
The manufacturer warrants the items delivered shall be free from defects (latent and patent) in material and workmanship for a period of one year after delivery to the Buyer. The Buyer’s sole and exclusive remedy under this warranty shall be limited to repair or replacement. Defective goods must be
returned to the manufacturer and/or its distributor for valid warranty claims. This warranty shall become inapplicable in instances where the items ha
ve
been misus
ed or otherwise subjected to negligence by the Buyer.
Notwithstanding any other provision of this contract, no other warranties, whether statutory or arising by operation of law, expressed or implied, including but not limited to those of merchantability or fitness for particular
Table A–1 Fuse specifications (refer to Figure B–1 or Figure B–2).
DWG Ref. Description Rating
F1 Miniature Fuse, 5 x 20 mm, Time Delay 250VAC/3.00A F2 Miniature Fuse, 5 x 20 mm, Time Delay 250VAC/3.15A
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Troubleshooting
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purpose, shall apply to the goods or services hereunder, other than the repair and replacement warranty above. Seller shall in no event be liable to Buyer or any third party for any damage, injury or loss, including loss of use or any direct or indirect incidental or consequential damages of any kind.
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Table A–2 Potential instrument problems and solutions .
Symptom Response
Non-Operation (at start up) Is the power switch on?
Is the battery dead? If so, connect the charger.
Non-Operation (after start up) Is the battery dead? If so, connect the
charger. Check fuse(s). If bad, replace with
equivalent amperage, slow-blow fuse. Contact a factory sales representative
for service information.
Power Fail
Turn off the power switch, remove the cover and check the optical head cables for a loose connection. Do not discon-
ne
ct or reconnect any optical head
cable
s with the power turned on.
Verify power failure by pressing the # key followed by the 4 key and checking the DC value. If it is greater than 200, then the Power Fail fault is spurious. Return to Mode 1 by pressing the # key followed by the 1 key and see if the fault has changed.
Check the inlet and outlet tubes to see if they are under any stress. Remove the connections to the inlet and outlet tubes and see if the power goes up. Perhaps th
e existing tubing ne
eds to be replaced with stainless steel flexible tubing.
Capture diagnostic data and send the file to SpectraSensors (see “To read
diagnostic data with HyperTermi­nal” on page 4-4).
Possible alignment problem. Contact a factory sales representative for service information.
Possible mirror contamination issue. Contact a factory sales representative for service information. If advised to do so, clean the mirrors by following the instructions under
“To clean the mir-
rors
on page A-4.
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Troubleshooting
A01-92-4 A .ver 97020-00094
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Null Fail Verify Null Fail fault by pressing the #
key followed by the 4 key and checking the zero reading is outside the range of
-50 to 50. If not, the Null Fail fault is spurious. Return to Mode 1 by press­ing the # key followed by the 1 key
and see if the fault has changed. Capture diagnostic data and send the
file to SpectraSensors (see “To read
diagnostic data with HyperTermi­nal” on page 4-4).
Table A–2 Potential instrument problems and solutions (Continued).
Symptom Response
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01-92-4 A .ver 97020-0009421
Spectrum Fail Turn off the power switch, remove the
cover and check the optical head cables for a loose connection. Do not discon-
nect or reconnect any optical head cables with the power connected.
Turn the analyzer off for 30 seconds and then turn it on again.
Reset the peak tracking (see “Peak Tracking Reset Procedure” on page A-5).
Capture diagnostic data and send the file to SpectraSensors (see “To read
diagnostic data with HyperTermi­nal” on page 4-4).
P/T Fa
il Chec
k that the actual pressure in the measurement cell is within specification (see Table B–1 on page B–1 or Table B–2 on page B–2).
If the pressure reading is incorrect, Turn off the power switch, remove the cover and check that the pressure/tem­perature cable is tight. Check the con­nector on the pressure transducer. Check the pressure connector on the driver board.
Check that the actual temperature in the measurement cell is within specifi­cation (
see Table B
–1 on page B–1 or
Table B–2 on page B–2). If the temperature reading is incorrect,
Turn off the power switch, remove the cover and check that the pressure/tem­perature cable is tight. Check the con­nector on the cell temperature sensor. Check the temperature connector on the driver board. (Note: A temperature reading greater than 150 °C indicates a short circuit on the temperature sensor leads; a reading of less than –40 °C indicates an open ci
rcuit).
Table
A–2 Potential instrument problems and solutions (Continued).
Symptom Response
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Troubleshooting
A01-92-4 A .ver 97020-00094
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Track Fail Press the # key followed by the 4 key
and see if PkDf and PkD1 differ by more than 4, otherwise erroneous fault.
Reset the peak tracking (see “Peak
Tracking Reset Procedure” on page A-5).
Front panel display is not lit and no char­acters appear
Turn off the power switch, remove the cover and check connections of the dis­play cable.
Strange characters appear on front panel display
Turn off the power switch, remove the cover and check conn
ections of t
he dis-
play cable.
Pressing keys on front panel do not have specified effect
Turn off the power switch, remove the cover and check connections on keypad
cable.
Reading seems to always be high by a fixed amount
See “Adjusting Analyzer Reading to Match Specific Standard(s)” on page 3-12.
Capture diagnostic data and send the file to SpectraSensors (see “To read
diagnostic data with HyperTermi­nal” on page 4-4).
Reading seems to always
be high by a
f
ixed percentage
See “Adjusting Analyzer Reading to Match Specific Standard(s)” on page 3-12.
Capture diagnostic data and send the file to SpectraSensors (see “To read
diagnostic data with HyperTermi­nal” on page 4-4).
Reading seems to always be low by a fixed amount
See “Adjusting Analyzer Reading to Match Specific Standard(s)” on page 3-12.
Capture diagnostic data and send the
file to SpectraSensors (see “To read
diagnostic data with H
yperTermi-
na
l” on page 4-4).
Reading seems to always be low by a fixed percentage
See “Adjusting Analyzer Reading to Match Specific Standard(s)” on page 3-12.
Table A–2 Potential instrument problems and solutions (Continued).
Symptom Response
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01-92-4 A .ver 97020-0009441
Reading is erratic or seems incorrect Check for contamination in the sample
system, especially if the readings are much higher than expected.
Capture diagnostic data and send the
file to SpectraSensors (see “To read
diagnostic data with HyperTermi-
nal” on page 4-4).
Reading goes to full scale
Gas concentration is greater than or
equal to full scale value.
Serial Output is displaying garbled data
Make sure the computer COM port is
set for 9600 baud, 8 data bits, 1 stop
bit, no par
ity, and no flow c
ontrol.
Be sure no other programs are using the COM port selected.
Make sure the connections are good.
Verify the correct pin connections with
an ohmmeter.
Make sure to select the correct COM
port that the cable is plugged into.
LCD does not update. Unit is locked up.
Switch off power, wait 30 seconds, and
then switch power back on.
eht naht ssel si noitartnecnoc saG0“ ot seog gnidaeR
lower detection limit.
Serial output is prov
iding no
data Make sure the computer COM port is
set for 19200 baud, 8 data bits, 1 stop bit, no parity, and no flow control.
Be sure no other programs are using
the COM port selected.
Make sure the connections are good.
Verify the correct pin connections with
an ohmmeter.
Make sure to select the correct COM
port into which the cable is plugged.
Table A–2 Potential instrument problems and solutions (Continued).
Symptom Response
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SS1000 Operator’s Manual B1
Appendix B: Specifications
Table B–1 SS1000 moisture in natural gas analyzer specifications.
Performance
Concentration (H20)
a
a. Consult factory for alternative ranges.
0.5–20 lbs/MMSCF (10–422 ppmv) )vmpp4±( FCSMM/bl2.0± ytilibataepeR
Response time
b
b. Software adjustable.
Display updates every second
Application Data
Environmental Temperature Range -4 to 122 °F (-20 to 50 °C) Standard
14 to 140 °F (-10 to 60 °C) Optional
Environmental Relative Humidity 80% for temperatures up to 31°C MAX
m
0004 ot pUedutitlA
)grab1.27.1( gisp0352erusserP telnI elpmaS
)grab7.0 ot 3.0–( gisp01 ot 5.4erusserP gnitarepO lleC
)MPL 0.15.0( HFC 21etaR wolF elpmaS
,senima ,lonahtem ,locylg esahp sag rof enoNytivitisneS tnanimatnoC
hydrogen sulfides or mercaptans.
Electrical & Communications
Input Voltages
c
c. Supply voltage not to exceed ±10% of nominal. Transient over-voltages according to
category II.
100–240 VAC, 50/60 Hz
9–16 VDC or
18–32 VDC
CAV042@A5.0 ,CAV021@A1tnerruC
1.6 A @ 24 VDC, 3.2 A @ 12 VDC subdoM leinaD/dluoG ro 232SR cireneGstuptuO
4–20mA Loop (concentration only)
erutarepmet llec ,erusserp llec ,noitartnecnoCyalpsiD DCL
Physical Specifications
Dmm041xWmm604xHmm754eziS
(18"Hx 16" W x 5.5" D)
)gK5.11( sbl52 .xorppAthgieW
leetS sselniatS dehsiloP seireS L613noitcurtsnoC lleC elpmaS
Area Classification
D & C spuorG ,2 noisiviD ,I ssalC ASCnoitacifitreC
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SS1000 Operator’s Manual
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01-92-4 A .ver 97020-000942
Table B–2 SS1000 carbon dioxide in natural gas analyzer specifications.
Performance
Concentration (CO2)
a
a. Consult factory for alternative ranges.
0–10%
%2.0± ytilibataepeR
Response time
b
b. Software adjustable.
Display updates every second
Application Data
Environmental Temperature Range -4 to 122 °F (-20 to 50 °C) Standard
14 to 140 °F (-10 to 60 °C) Optional
Environmental Relative Humidity 80% for temperatures up to 31°C MAX
m0004 ot pUedutitlA
)grab1.2
7.1( gisp0352erusserP telnI elpmaS
)grab7.0 ot 3.0–( gisp01 ot 5.4erusserP gnitarepO lleC
)MPL 0.15.0( HFC 21etaR wolF elpmaS
,senima ,lonahtem ,locylg esahp sag rof enoNytivitisneS tnanimatnoC
hydrog
en sulfides or mercaptans.
Electrical & Communications
Input Voltages
c
c. Supply voltage not to exceed ±10% of nominal. Transient over-voltages according to
category II.
100–240 VAC, 50/60 Hz
9–16 VDC or 18–32 VDC
CAV042@A5.0 ,CAV021@A1tnerruC
1.6 A @ 24 VDC, 3.2 A @ 12 VDC subdoM leinaD/dluoG ro 232SR cireneGstuptuO
4–20mA Loop (co
ncentration only)
erutarepmet llec ,erusserp llec ,noitartnecnoCyalpsiD DCL
Physical Specifications
Dmm041xWmm604xHmm754eziS
(18"Hx 16" W x 5.5" D)
)gK5.11( sbl52 .xorppAthgieW
leetS sselniatS dehsiloP seireS L613noitcurtsnoC lleC elpmaS
Area Classification
D & C spuorG ,2 noisiviD ,I ssalC ASCnoitacifitreC
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Specifications
B01-92-4 A .ver 97020-00094
3
PO WE R S WI TC H
RS232 PORT
FU S E (F1)
BATT ER Y CH ARG E R
INP UT
SA MP LE
R E TURN
LIQUI D DRA I N
SA MP LE S U PP LY
(10 PS IG M AX.)
MEM BRAN E
S E PARATOR
HAND LE ( S HO WN I N
FO L DE D POS ITI ON)
L CD
DISP L AY
KEY PAD
6.68
[170 ]
16. 60
[422 ]
18.1 9
[462 ]
8.66
[220 ]
6.68
[170 ]
CO VE R
SCR EW (X1 0)
Figure B–1 SS500/SS2000 analyzer external features.
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SS1000 Operator’s Manual
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01-92-4 A .ver 97020-000944
Figure B–2 Fuse location on DC to DC converter.
FU S E (F 2)
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Specifications
B01-92-4 A .ver 97020-00094
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Spare Parts
Below is a list of spare parts for the SS1000 Operator’s Manual analyzer with recommended quantities for 2 years of operation. Due to a policy of continuous improvement, parts and part numbers may change without notice. Not all parts listed are included on every analyzer. When ordering, please specify the system serial number to ensure that the correct parts are identified.
Table B–3 Replacement parts for SS1000 SS1000 Operator’s Manual analyzers.
Part
Number
Description
2 YR
QTY
-elbaC laireS lanretxE60171-20910
-draoB lortnoC erutarepmeT00031-20910
-ylbmessA dapyeK11003-20910
-ylbmessA yalpsiD00013-20910
-CD/CA ,esuF ,tiK11000-99120
-ylbmessA recudsnarT erusserP20171-20910
-ssaP 2 ,notiV ,)swercs ,sgnir-o( serapS , tiK50000-99120
-lleC lacitpO ,slooT gninaelC ,tiK70000-99120
2 rotarapeS enarbmeM ,gniR-O & enarbmeM39120-00016
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SS1000 Operator’s Manual
B
01-92-4 A .ver 97020-000946
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
xednIlaunaM s’rotarepO 0001SS 1
INDEX
Absorption 1–4, 1–5 Absorption coefficient 1–5 Absorption profile 1–5 Absorption spectrometer 1–4 Absorption spectroscopy 1–4 Accessories. See Options. Acetone A–2 Acetone-impenetrable gloves A–3, A–4 Alarm flags 4–17 Attenuation 1–5 Background gas 3–13, 3–16 Beam path 1–5 Beer-Lambert absorption law 1–5 Cautions 1–2 Cleaning
Gas sampling lines A–2
Mirrors A–3 COM port A–14 COM properties 4–1, 4–3 Concentration 3–2, 3–5, 3–8, 3–9 Contamination 1–5, 3–16, A–1, A–2 Current loop 3–9 Current tuning 1–5 Data 1–5
Dia
gnostic 3–4, 3–5
, 4–6, 4–7 Normalized 2f 1–7 Normalized absorption 1–6 Raw 1–5
Data string 4–4 Detection levels 1–7 Detector 1–4, 1–5 Diode laser absorption spectrometer 1–4 Electrical noise A–1, A–5 Erroneous readings 2–4 Excessive sampling gas pressure A–1,
A–5, A–7
Excessive sampling gas temperature
A–1, A–5, A–7
External data logger 3–9 Faults
Null Fail 3–5, 3–15, A–11 P/T Fail 3–15, A–5, A–12 Power Fail 3–5, 3–15, A–2, A–3,
A–10
Spectrum Fail 3–5, 3–15, A–12 Track Fail 3–5, 3–15, A–5, A–13
Field-pressure reducin
g station 3–
2 Firmware version 4–16 Flowmeter 3–16 Gas leaks 2–3, 2–4, A–1, A–2, A–3
Gas sampling line A–2 Gas standard 3–15 Hardware 2–1 HyperTerminal 4–1 Import stored data into spreadsheet 4–5 Incident intensity 1–5 Initialization period 3–1 Installation 2–1 Intermediate calculation 3–5 Isopropanol A–3, A–4 Keypad 3–2, 3–3 Laser absorption spectrometer 1–5 Laser beam 1–4 Laser output fluctuations 1–5 LCD display 3–2 Leak detector 2–3, 2–4, A–2, A–3 Leaks A–1 Lens cleaning cloth A–4, A–5 Lens tissue A–3 Lock-in amplifier 1–7 Measurement
parameter
s 3–2 Measurement units 3–2 Membrane separator A–2 Microsoft Excel 4–5 Mirror contamination 1–5, 1–7, A–2, A–3 Modes
Mode 1 (Normal Mode) 3–3, 3–4,
3–7, 3–14, 3–15, 4–5, 4–14, A–7
Mode 2 (Set Parameter Mode) 3–4,
3–6, 4–4, 4–13, A–7
Mode 3 (Not Used) 3–4 Mode 3 (Set Parameter Mode -
Channel B) 4–4, 4–13, A–7
Mode 4 (System Diagnostic
Parameters - Channel A) A–6
Mode 4 (System Diagnostic
Parameters) 3–4
Mode 5 (Not Used) 3–5 Mode 5 (System Diagnostic
Parameters - Channel B) A–6
Mode 6 (Diagnostic
Data Downl
oad)
3–5, 4–4, 4–5, 4–10
Mode TEST (System Test) 3–6
National Institute of Standards and
Technology 3–16 Natural frequencies 1–5 Noise in the measurement 3–8 Optional analyzer hood 2–2 Options 1–1 Outline schematic B–4
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
SS1000 Operator’s Manual
Index
01-92-4 A .ver 97020-000942
Output Signal
Serial output 2–5
Parameters
Calibration
C0 4–17 C1 4–17 C2 4–17 C3 4–17 Imod 3–14, 4–18 Midpoint 3–14 PA1 3–14, 4–17 PA2 3–14, 4–17 PA3 3–14, 4–17 PA4 3–14, 4–17 Phase 3–14, 4–18 PkDf 4–17 Ramp Amplitude 3–14, 4–18 RCalb 3–14, 4–17 Span 3–14 Zero Offset 3–14, 4–17
Diagnostic
Indx 3–5, 4–4, 4–17 PkD1 3–5, 3–15, 4–4, 4–16, A–6,
A–13
PkDf 3–5, 3–15, A–6, A–13 Powr 3–5, 4–17 PP2F 3–4, 4–4, 4–17 Reference Peak Index 4–4 Reference Peak Power 4–4 Reference Peak PP2F 4–4 Zero 3–5, 4–4, 4–17
Measurement and control 3–6
# Spectrum Average 3–8, 4–4,
4–17
Channel B
S Factor 3–16 S Factor Offset 3–16
Concentration Unit 3–10, 4–18 DO
Alarm Setup
4–18
Logger Rate 3–9, 4–17 Modbus Address 3–11, 4–14,
4–18
Modbus Mode 3–11, 4–1, 4–12,
4–14, 4–18
Peak Tracking 3–2, 3–9, 3–13,
3–15, 4–17, A–7
Pipeline Pressure 3–10, 4–17 Powr 4–4 Pressure Unit 3–10, 4–17 S Factor 3–8, 3–12, 3–13, 4–16 S Factor Offset 3–8, 3–12, 3–13,
4–17
Temperature Unit 3–9, 3–10,
4–17
User Analyzer ID 3–11, 4–17 User Component ID 3–12, 4–17 User Sample ID 3–12, 4–17
Password 3–6, 3–14, 4–13, 4–16, 4–18,
A–6 Peak tracking function 3–9 Port
Sample inlet 2–3
Sample return 2–4 Potential hazards 1–2 Pressure regulator 3–16 Recommendations and
solutions to
common
problems 3–15, A–1 Resonances. See Natural Frequencies Response time 3–8 Return materials authorization (RMA)
number A–8 RS-232 Output 4–1 Sample 1–4 Sample cell 1–4, A–2 Sample cell pressure 3–2 Sample cell temperature 3–2 Sample conditioning system (SCS) 1–4 Sample gas 1–4, 1–5 Serial number 4–17 Serial port 4–4 Service contact A–8 Species concentration 1–5 Spectra
2
f 3–5, 4–10
DC 3–5 Spectral overlap 1–7 Stainless steel tubing 2–3, A–1 Symbols 1–2 System conditioning 2–4 Tools 2–1, 2–2 Tools and suppli
es A–3
Tr
ace species detection 1–4 Tunable diode laser 1–4 Units 3–9
Concentration 3–10 Pressure 3–10
Temperature 3–9 Validation 3–15 Valve
Shut-off 3–2 Variations 1–7
Pressure 1–7
Temperature 1–7 Warnings 1–2 Wavelength modulation spectroscopy
1–7
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
UK Distibution by IMA Ltd Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
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