SKC Preloaded Disposable Parallel Particle Impactor Operating Instructions Manual

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Operating Instructions
863 Valley View Road, Eighty Four, PA 15330 USA
Tel: 724-941-9701 • www.skcinc.com
SKC Preloaded Disposable
Parallel Particle Impactors (PPI)
The patented† impaction-based SKC Disposable Parallel Particle Impactor (PPI®) Samplers are designed to match precisely the collection efficiency curves for respirable and thoracic dust specifi ed by ISO 7708/CEN and adopted by ACGIH, CEN, and other occupational hygiene organizations. The performance of the respirable PPI samplers also meets the ISO 7708/CEN criteria included in the OSHA nal silica rule. The thoracic model meets the requirements of NIOSH Method 5524 for metalworking fl uids and compounds with ACGIH PPI Samplers off er the convenience of single use to eliminate sampler assembly and cleaning; small size for worker comfort, even under helmets or other PPE; and a choice of fl ow rates for maximum fl exibility in pump options, sample duration, and contaminant concentration. These instructions are for PPI models pre-assembled
with fi lter, support, and impaction substrates.
®
thoracic TLV®s. Disposable
Preloaded fi lters in some models are available preweighed by SKC for gravimetric analysis. See the table below.
Respirable PPIs Preloaded Filter
225-3841 225-3851 225-3871 225-3841-PW 225-3851-PW 225-3871-PW
Thoracic PPIs Preloaded Filter
225-3861 0.8-μm MCE fi lter, not preweighed 225-3862 Quartz fi lter, not preweighed
† U.S. Patent No. 7,073,402
5.0-μm PVC lter for chemical analysis, not preweighed. For gravimetric analysis, contact your laboratory to pre and postweigh fi lter.
5.0-μm PVC fi lter preweighed by SKC for gravimetric analysis Preweighed at 70 F ± 3 F and 50% ± 5% relative humidity
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Performance Profi le
Sampling Rate: 2 L/min respirable or thoracic, 4 or 8 L/min respirable
Sample Pump: • Universal XR or AirChek
• Leland Legacy for 8 L/min
Sample Time: Dependent on method used.
mass of up to 6.8 mg on the four impaction substrates would not aff ect PPI performance. This amount is equivalent to sampling for 6 hours at 4 L/min in environments where respirable mass concentration is 4.76 mg/m and equals 50% of total dust. However, labs have reported to SKC that they prefer no more than 2 mg on the fi lter for analytical reasons. Therefore, SKC recommends that you work with your lab to determine optimum sample times for your unique sampling conditions.
Sample Media: Respirable models: 37-mm, 5.0-μm PVC fi lter and cellulose
support pad
Thoracic model: 37-mm, 0.8-μm MCE fi lter and cellulose
support pad or 37-mm Quarfi lter and cellulose support pad
Impaction Four 3/8-in diameter pre-oiled porous plastic discs Substrate: (Assembled in all Disposable PPIs)
Analysis: Chemical or gravimetric
Body Material: Conductive ABS plastic
Dimensions: Height: 4.25 in (10.8 cm) - clip to exhaust Diameter: 1.8 in (4.6 cm) Depth: 1.2 in (3 cm)
Weight: 1.1 oz (31.2 gm)
Shelf-life: 18 mos from date of manufacture
®
Series for 2 and 4 L/min
Note: SKC tests indicate that a particulate
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Principle of Operation
SKC Disposable PPI Samplers are impaction-based fi lter samplers that perform precise size-selection for either thoracic or respirable dust, depending on the model. PPI Samplers contain four small impactors in the inlet section of the device. Each impactor features a unique 50% cut-point to target a specifi c one-quarter segment of the ISO/CEN curve resulting in a precise fi t along the entire curve. A sample pump operating at 2, 4, or 8 L/min (2 L/min only for thoracic) pulls air through the inlet nozzle of each impactor in the inlet plate. Particles larger than each impactor’s 50% cut-point are scrubbed and retained by impaction onto the porous oiled impaction substrate contained in each impactor. Smaller particles continue to the standard 37-mm collection fi lter for analysis.
Dust enters here
Inlet plate (contains 4 impac­tors with unique cut-points preloaded with 4 impaction substrates and sonically welded) Standard 37-mm collection lter (assembled)
Protective end cap
Exhaust to pump
Base plate
PPI Performance
Collection effi ciency of the 2, 4, and 8 L/min
respirable PPI Samplers compared to the
ISO respirable curve
37-mm support pad (assembled)
Collar clip
Collection effi ciency of the 2 L/min
thoracic PPI Sampler compared to the
ISO thoracic convention
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Sampler Preparation
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SKC Preloaded Disposable PPIs are supplied assembled and ready to use.
For gravimetric analysis: PPIs 225-3841-PW, 225-3871-PW, and 225-3851-PW are preloaded with a preweighed 5.0-μm PVC fi lter. If using PPIs preloaded with a 5.0-μm PVC lter that has not been preweighed (Cat. Nos. 225-3841, 225-3871, and 225-3851), contact your laboratory to pre and postweigh fi lter.
1. Remove shrink wrap.
2. Write sample ID on sampling label. Adhere sampling label to bo om of
base plate.
3. Remove protective end cap from exhaust.
Calibration and Sampling
As the particle load on the fi lter increases during sampling, the pressure drop will also increase. Therefore, use a compensating sample pump such as the AirChek Series or Leland Legacy depending on fl ow rate requirements.
Calibration
Calibrate the pump fl ow rate with a representative Preloaded Disposable PPI sampler. See pump and calibrator operating instructions.
1. Ensure the pump has run for 5 minutes before calibrating.
2. Ensure representative impactor is loaded with a support and collection fi lter and that it is fully assembled. See Sampler Preparation above.
3. Align the bo om of the calibration adapter with the inlet plate of an assembled, loaded representative Disposable PPI and press down firmly until the calibration adapter’s O-ring is engaged and creates an even seal.
4. Use fl exible tubing to connect the exhaust of the Disposable PPI to the inlet of a sample pump.
5. Use fl exible tubing to connect the inlet of the calibration adapter to the suction port (outlet) of a calibrator.
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6. Calibrate to 2 L/min for the 2 L/min respirable and thoracic model PPIs, 4 L/min for the 4 L/min respirable model, or 8 L/min for the 8 L/min respirable model. Follow the calibration instructions in the pump and calibrator operating instructions.
7. When calibration is completed, disconnect the tubing from the calibrator and calibration adapter.
8. Grasp the Disposable PPI with one hand and the calibration adapter with the other hand. Firmly pull/twist to remove the calibration adapter from the Disposable PPI inlet plate.
9. Replace the representative Disposable PPI used to set the fl ow with a new, unused preloaded Disposable PPI for sample collection.
Using excessive pressure to seal the calibration adapter to the Disposable PPI may make the calibration adapter diffi cult to remove.
Flexible
tubing
Calibration
adapter
Sample
pump
Flexible
tubing
Disposable PPI
Calibrator
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Sampling
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SKC tests indicate that a particulate mass of up to 6.8 mg on the four impaction substrates would not affect PPI performance. This amount is equivalent to sampling for 6 hours at 4 L/min in environments where respirable mass concentration is
4.76 mg/m3 and equals 50% of total dust. However, labs have reported to SKC that they prefer no more than 2 mg on the fi lter for analytical reasons. Therefore, SKC recommends that you work with your lab to determine optimum sample times for your unique sampling conditions.
1. As per good industrial hygiene practice, replace representative sampler used for calibration with a new, unused preloaded sampler.
2. Record sample start time on label.
3. Clip Disposable PPI onto a worker’s collar or lapel in the breathing zone or in the area to be sampled.
4. Clip sample pump at the worker’s waist or close to the Disposable PPI.
5. Use fl exible tubing to a ach the Disposable PPI exhaust to the inlet of the sample pump.
6. Turn on pump and record pertinent sample data.
7. After the desired sample time has elapsed, turn off the pump and unclip sampler from sampling location.
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8. Apply Post-use label to inlet plate to seal the sampler.
9. Record sample stop time on label on the bo om of sampler.
10. Disconnect sampler from pump and reinstall protective end cap on the exhaust.
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11. Reinstate calibration train with representative Disposable PPI and verify fl ow rate. See Calibration.
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Sample Transport and Analysis
Package and transport samples and blanks to an accredited laboratory for gravimetric or chemical analysis.
References
Trakumas, S., Hall, P., Personal Respirable Sampler Containing Four Impactors Arranged in Parallel, Abstracts of 23rd Annual AAAR Conference, Atlanta, GA, 2004, p. 78
Trakumas, S., Salter, E., “Parallel Particle Impactor - Novel Size-selective Particle Sampler for Accurate Fractioning of Inhalable Particles,” Journal of Physics: Conference Series 151 (2009), 16 pp., 012060, www.skcinc.com/instructions/Parallel Particle Impactor Paper.pdf
Reference 2 is an author-created, non-copyrighted version of an article accepted for publication in the Journal of Physics; Conference Series 151. IOP Publishing Ltd. is not responsible for any errors or omissions in this version of the manuscript or any version derived from it. The defi nitive publisher authenticated version is available online. Go to h p://dx.doi.org, enter doi: 10.1088/1742-6596/151/1/012060.
Trakumas, S., “High-fl ow Personal Respirator Dust Sampler for Increased Sensitivity,” Poster 261, AIHce 2010, Denver, CO
Trakumas, S., “High-fl ow Personal Sampler to Monitor Exposure to Respirable Crystalline Silica at New Lower TLV,” IOHA 2010 8th Conference Book of Abstracts, Rome, p. 59
Trakumas, S., Salter, E., “High-Flow Personal Sampler to Monitor Exposure to Respirable Crystalline Silica at New Lower TLV” PowerPoint Presentation
OSHA Final Rule on Respirable Crystalline Silica, www.osha.gov/silica/
ISO 7708:1995 (2008), Air Quality — Particle Size Fraction Defi nitions for Health-related Sampling, www.iso.org, search on 7708
Stacey, P., Thorpe, A., and Echt, A., “Performance of High Flow Rate Personal Respirable Samplers When Challenged with Mineral Aerosols of Diff erent Particle Size Distributions,” Ann. Occup. Hyg., 60, 2016, pp. 479-492, h p://annhyg.oxfordjournals.org/content/60/4/479.full.pdf
Görner, P., Simon, X., Boivin, A., Bau, S., “Sampling Effi ciency and Performance of Selected Thoracic Aerosol Samplers,” Annals of Work Exposure and Health, 2017, Vol. 61, No. 7, 784-796
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Ordering Information
Preloaded Disposable Plastic PPI Samplers, select the PPI for the desired convention. Designed for one-time use Cat. No.
Preloaded Disposable PPI Samplers contain four porous plastic
disc impaction substrates, one 37-mm collection fi lter, and one 37-mm cellulose support
Respirable PPI (red), 8 L/min, plastic, 5.0-μm PVC lter
225-3841
Respirable PPI (red), 8 L/min, plastic, 5.0-μm PVC lter
preweighed to 5 decimals
Respirable PPI (orange), 4 L/min, plastic, 5.0-μm PVC lter
Respirable PPI (orange), 4 L/min, plastic, 5.0-μm PVC lter
preweighed to 5 decimals
Respirable PPI (gold), 2 L/min, plastic, 5.0-μm PVC lter
Respirable PPI (gold), 2 L/min, plastic, 5.0-μm PVC lter
preweighed to 5 decimals
Thoracic PPI (blue), 2 L/min, plastic, 0.8-μm MCE lter 225-3861
Thoracic PPI (blue), 2 L/min, plastic, Quartz lter 225-3862 Accessory Calibration Adapter for Disposable PPI 225-389
225-3841-PW
225-3871
225-3871-PW
225-3851
225-3851-PW
SKC Limited Warranty and Return Policy
SKC products are subject to the SKC Limited Warranty and Return Policy, which provides SKC’s sole liability and the buyer’s exclusive remedy. To view the complete SKC Limited Warranty and Return Policy, go to h p://www.skcinc.com/warranty.
www.skcinc.com
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Form 38056 Rev 1811
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