SKC 500-100 User Manual

Operating Instructions
Tel: 724-941-9701 Fax: 724-941-1369 e-mail: skctech@skcinc.com
863 Valley View Road, Eighty Four, PA 15330 USA
Passive Sampler for Formaldehyde
Cat. No. 500-100
Developed in collaboration with the National Institute of Working Life in Umea, Sweden and validated by OSHA, the SKC UME Formaldehyde Passive Sampler collects formalde­hyde in the 5 ppb to 5 ppm range.* The UME Passive Sampler contains a tape treated with 2,4-dinitrophenylhydrazine (DNPH). Each sampler incorporates a “blank/correction” section of tape in addition to the sample section of tape. Analysis is by high-performance liquid chromatography (HPLC) for identifi cation of formaldehyde that may be present in the sample. Designed for single use, the SKC
x
UME
100 Passive Sampler is packaged in an aluminized pouch for
easy sample transport to a laboratory.
x
100
x
100
* If sampling in an atmosphere containing formalin, see www.skcinc.com/instructions/1795.pdf for
eld study information.
Application Notes
Because of the UMEx 100 Sampler’s relatively high sampling rate and sensitive analysis, it can be used for 15-minute (STEL) sampling in the ppm range, personal monitoring up to 12 hours, and 24-hour to 7-day monitoring of contaminants found in indoor environments.
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Performance Profi le
Sampling Rate 28.6 ml/min with a relative standard deviation of 7.6% at a wind for Formaldehyde: velocity of 5 to 100 cm/sec for 15 minutes to 24 hours
20.4 ml/min wind velocities < 5 cm/sec for 1 to 7 days
Validation Range: 0.06 to 3.0 ppm
Detection Principle: Formation of stable DNPH-hydrazone in the presence of formaldehyde*
Analysis Method: Solvent extraction and analysis by HPLC (high-performance
liquid chromatography) with UV detection
Lower Detection Limits: 15 min: 200 ppb (.24 mg/m 8 hr: 5 ppb (.006 mg/m3) 24 hr: 2 ppb (.002 mg/m3) 7 days: 0.2 ppb (.0002 mg/m3)
Shelf-life: 12 mos from date of manufacture at freezer temperatures (39.2 F [4 C])
Storage: Before use: Freezer temperatures (39.2 F [4 C]) After use: Freezer temperatures (39.2 F [4 C]) and analyze within 3 weeks
Capacity: 29 μg/sample
Accuracy: ± 25%, exceeds OSHA requirements
Temperature Effects: No effect on sampling rate between 10 and 30 C
Humidity Effects: No effect from 10 to 80% relative humidity (RH).
Do not use sampler below 10% RH.
Wind Velocity Effects:
Interferences:* Highly speci c for formaldehyde. Large amounts of
carbonyl compounds may reduce the uptake of formaldehyde
• Use in ozone levels less than 0.5 ppm
Dimensions: 3.4 x 1.1 x .35 in (8.6 x 2.8 x .89 cm)
Weight: 0.38 oz (10.9 gm)
Slide Cover: Green
See the Passive Sampling Guide at www.skcinc.com for UMEx 100 sampling rates for other aldehydes.
3
)
No effect from 5 to 100 cm/sec
* If sampling in an atmosphere containing formalin, see www.skcinc.com/instructions/1795.pdf for
eld study information.
Sampling Instructions
Cautions: • Store at freezer temperatures ( 39.2 F [4 C]) before use.
• Do not store with food.
• SKC recommends using gloves when handling chemically
• Before sampling, check the expiration date on the pouch label.
UME
• Do not use Sharpie
treated media.
Do not use a er the last day of the month indicated.
x
samplers are designed for single use only. Do NOT reuse
x
UME
samplers.
®
markers or equivalent to mark label or
pouch as these can off -gas VOCs.
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