Sigma 4-15 User manual

———————————————
Centrifuge
4-15C
Dear customer,
Congratulations for purchasing a SIGMA laboratory centrifuge. You have selected a device which combines many advantages.
A wide spectrum of programming options and an electronic operation control allow a trouble­free use of the centrifuge. With its 3-phase drive, maintenance-free, quiet operation without any carbon dust pollution is guaranteed.
Your device is equipped with user-friendly options which make the operation and standard settings easier for you. Built-in error-detecting functions keep the user from entering incorrect values and check the complete operation.
A special advantage is the storage capacity the centrifuge offers. The instrument has a program memory which can store up to 50 data sets and is capable of keeping the last run program in its memory for an unlimited amount of time allowing the program to be restarted at any time - even if the centrifuge was turned off in between. All important operation parameters can be seen at a glance.
The settings are executed via the knob in the control panel which has a coated surface protecting the device against moisture and dust. In addition, the interior of the centrifuge is also easy to clean. We are able to offer you a device that combines functional variety with practical applications.
We thank you for your confidence and wish you a successful application of the centrifuge.
SIGMA Laborzentrifugen GmbH P.O. Box 1713 - 37507 Osterode/Germany Phone 05522/5007-0 - Fax 05522/500712 Internet: www.sigma-zentrifugen.de eMail: info@sigma-zentrifugen.de SIGMA Service-Tel. 05522/5007-25
Operating Manual SIGMA 4-15C, page 3 of 95
03/06
Konformitä tserklä rung
(73/23/EWG; 89/336/EWG; 98/37/EWG)
Statement of Conformity
(73/23/CEE; 89/336/CEE; 98/37/CEE)
Déclaration de conformité
(73/23/CEE; 89/336/CEE; 98/37/CEE)
Die nachfolgend bezeichnete Maschine wurde in Ü bereinstimmung mit den Richtlinien 73/23/EWG; 89/336/EWG und 98/37/EWG hergestellt und geprüft. The following machine is manufactured and tested in compliance with directions 73/23/CEE; 89/336/CEE and 98/37/CEE. La machine désignée ci-dessous est produit et examiné conforme aux directives 73/23/CEE; 89/336/CEE et 98/37/CEE
Bezeichnung der Maschine: Laborzentrifuge Machine: Laboratory Centrifuge Désignation de la machine: Centrifugeuse de laboratoire
Maschinentyp : 4 - 15 Type: Type de la machine:
Bestell Nr. : 10750, 10751, 10752, 10753, 10730, 10731, 10732 Part No.: 10733 Réf. usine:
Normen: EN 61010-2-020 Standards: EN 61000-3-2 ; EN 61000-3-3 Normes : EN 61326
Sigma Laborzentrifugen
An der Unteren Sö se 50 D-37520 Osterode
01.02.2002 Geschä ftsführer Managing Director Directeur Gérant
........................................................................
Fabr. Nr. Serial No. Numé ro de fabrique
Konformitätserklärung dreisprachig 4-15 20020201.DOC
Operating Manual SIGMA 4-15C, page 5 of 95
03/06
General Information
1.1 Technical data
1.2 Suitable accessories
1.3 Scope of supply
1.4 Standards and regulations
1.5 Safety instructions
1.6 Symbol table
Description of the Centrifuge
2.1 General outlay
2.2 Construction and constructive safety measures
2.3 Drive
2.4 Operation and display
2.5 Electronic control
2.6 Safety devices
2.6.1 Lid lock, cover closing device
2.6.2 Imbalance monitoring system
2.6.3 Rotor monitoring
2.6.4 Standstill monitoring
2.6.5 System check
2.6.6 Ground wire check
Installation and Start-up
3.1 Unpacking of the centrifuge
3.1.1 Transport safety device
3.2 Installation
3.2.1 Site
3.2.2 Connection/Fuse
3.2.3 Fuses / emergency circuit breaker on site
3.3 Installation of rotors and accessories
3.3.1 Fastening of angle rotors with hermetically sealed lid
3.4 Initial start-up
3.4.1 Switching on of the centrifuge
3.4.2 Opening lid
3.4.3 Installation of a rotor
Operating Manual SIGMA 4-15C, page 7 of 95
03/06
Operating Elements
4.1 Operating panel
4.1.1 Start-key
4.1.2 Stop-key
4.1.3 Lid-key
4.1.4 Knob
4.2 Display
4.2.1 Set
4.2.2 Speed
4.2.3 Relative Centrifugal Force (RCF)
4.2.4 Time
4.2.5 Program
4.2.6 Rotor
4.2.7 Parameters
4.2.7.1 Acceleration
4.2.7.2 Deceleration
4.2.7.3 Radius
4.2.7.4 Density
4.2.7.5 Start delay
4.2.7.6 Automatic lid opening after end of run
4.2.8 Configuration
Operation
5.1 Selection, display and alteration of program parameters
5.1.1 Selection and alteration of the parameters and activation of the start delay and the automatic lid opening after end of run
5.1.2 Selection and alteration of the rotor part number
5.1.3 Alteration of the parameter values during the centrifuge run
5.1.4 Alteration of the configuration
5.1.4.1 Curves
5.1.4.2 Creation of curves for variable accelerations and decelerations
5.1.4.3 Alteration of existing curves
5.1.5 Alteration of the contrast
5.1.6 Imbalance monitoring
5.1.7 Shortrun and faststop
Programming
6.1 Load, save and delete programs
6.1.1 Load a program
6.1.2 Save a program
6.1.3 Delete a program
Operating Manual SIGMA 4-15C, page 8 of 95
03/06
Notes for Centrifugation
7.1 Practical notes for centrifugation
7.2 Forbidden centrifuging operations
Care and Maintenance
8.1 Care and cleaning of centrifuge
8.2 Care and cleaning of accessories
8.3 Rotor pins
8.4 Glass breakage
8.5 not applicable
8.6 Sterilization and disinfection of rotor chamber and accessories
8.6.1 Autoclaving
8.7 Checks by operator
Appendix
9.1 Slope of the specified curves, linear curves
9.2 Quadratic curves
9.3 Entry limitations
9.4 Mathematical relations
9.4.1 Relative Centrifugal Force (RCF)
9.4.2 Density
9.5 Error correction
9.5.1 Centrifuge cannot be started
9.5.2 Centrifuge decelerates during operation
9.5.3 Lid cannot be opened/closed
9.5.4 Emergency lid release
9.5.5 Problems with the centrifuge?
9.6 Error codes
9.7 Speed-RCF-diagram
9.8 Declaration of decontamination/Return declaration
9.9 Form program data
9.10 Leaflet
Operating Manual SIGMA 4-15C, page 9 of 95
03/06
1.1 Technical Data
Manufactuer: S I G M A
Laborzentrifugen GmbH D-37520 Osterode
Germany Type: 4-15C Electr. connection: Protection class: Power consumption (kVA): Rated power (kW): Max. current (A):
Power data: Max. speed (rpm): Max. capacity (l): Max. gravitational field (x g): Max. kin. energy (Nm): Further parameters Time range: Programs: Acceleration curves:
Deceleration curves:
Radius: Rotor part no.: Dimensions: Depth (mm): Width (mm): Height (mm): Weight (kg): EMC (acc. to EN 55011): Noise level (dBA):
Notes of user: Serial number:
Supply date: Inventory number: Location: Responsibility:
The figures are valid for an ambient temperature of 23 °C +/- 2 °C and nominal voltage +/- 5 %. (Allowable ambient temperature +4 °C - +40 ° C; max. humidity 80 %.) Subject to technical alterations.
see nameplate
I
1,5
1,2
6,5 (230 V/50 Hz) respectively
13,0 (120 V/60 Hz)
13 500
2
20 376
50 487
9 h, 59 min/continuous operation
50 No. 1 - 50
10 linear No. 0 - 9
10 quadratic No. 10 - 19
10 freely programmable
No. 20 - 29
9 linear No. 1 - 9
1 brakeless No. 0
10 quadratic No. 10 - 19
10 freely programmable
No. 20 – 29
max./min. s. 1.2
s. chapter 1.2
685
490
405
82 kg
Class B
75 (at max. speed)
.....................................................
.....................................................
.....................................................
.....................................................
.....................................................
Operating Manual SIGMA 4-15C, page 11 of 95
03/06
1.2 Accessories Suitable for SIGMA 4-15C
Part No.
11150 Swing-out rotor for 4 buckets 13215, 13220,
13220 Bucket , aluminium, for microtitre plates,
13221 Bucket , aluminium, for microtitre plates,
13231 Bucket, aluminium, for 1 pointed bottom
13175 Adapter for pointed bottom bottle 15175,
13233 Bucket, aluminium, for 50 RIA-tubes Ø 12.5
13234 Bucket, aluminium, for 4 tubes 100 ml,
13235 Bucket, aluminium, for 7 culture tubes
Description
13221, 13231, 13234, 13235, 13236, 13350
max. allowed data with rotor 11150: radius edge 16.6 cm, radius max. 16.0 cm, radius min. 11.3 cm, max. plate height 54 mm
max. allowed data with rotor 11150: radius edge 16.6 cm, radius max. 16.0 cm, radius min. 10.0 cm, max. plate height 56 mm, incl. plate holder 17979
bottle 150 or 200 ml e.g. 15175, approx. Ø 61.5 x 140 mm, incl. adapter 13175, suitable for 11150, max. radius 19.0 cm, min. radius 8.7 cm,
suitable for 13231, 17347
x 70 - 90 mm, e.g. 15060, suitable for 11150
Ø 45 x 100 mm, e.g. 15100, 15102, 15103, 15106, incl. rubber cushion 16051, suitable for 11150, max. radius 17.8 cm, min. radius
7.8 cm
50 ml 15151, suitable for 11150, max. radius
19.0 cm, min. radius 9.3 cm
Max. speed (rpm)
4 100
4 500
4 500
4 300
4 500
Max. gravitational field (x g)
3 120 3 007 2 124
3 758 3 622 2 264
4 302
3 680
4 302
Operating Manual SIGMA 4-15C, page 13 of 95
03/06
Part No.
13236 Bucket, aluminium, for 12 culture tubes
13350 Round bucket, aluminium, with thread, incl.
17134 Aluminium sealing cap for 13350 17135 Polysulfone sealing cap, clear, for 13350 17350 Round carrier for 24 reaction vials 0.5-
17351 Round carrier for 12 Monovettes, max.
17352 Round carrier for 25 RIA-tubes 5 ml, max.
17353 Round carrier for 16 reaction vials 1.5-
17354 Round carrier for 16 glass tubes 7 ml, max.
17355 Round carrier for 12 tubes with screw cap
17356 Round carrier for 16 Vacutainer/hemolyse/
Description
15 ml 15115, suitable for 11150, max. radius
18.8 cm, min. radius 9.6 cm
O-ring 482840, for the 500 ml bottles 15500, 15501 and for the round carriers 85 mm 17350 up to 17402, sealable with caps 17134, 17135, suitable for 11150, max. radius 19.0 cm, min. radius 8.7 cm
0.75 ml, 7.9/10 x 28/31 mm, e.g. 15005, polypropylene
15.5/18 x 50 - 75 mm, polypropylene
12.5 x 65 - 80 mm, e.g. 15060,
polypropylene
2.2 ml, max. 11 mm, e.g. 15008, 15040, polypropylene
12.5 x 85 - 115 mm, e.g. 15007, 15027, polypropylene
10-12 ml, max. 16.2/19 x 65 x 90 mm, e.g. 13026 plus 17126, 15000, 15010, 15039, polypropylene
RIA-tubes 5-6 ml, max. 13.5/17.5 x 70 - 90 mm, polypropylene
Max. speed (rpm)
4 500
4 500
Max. gravitational field (x g)
4 246
4 302
Operating Manual SIGMA 4-15C, page 14 of 95
03/06
Part No.
17358 Round carrier for 12 tubes 10-15 ml, max.
17359 Round carrier for 9 culture tubes 15 ml,
17360 Round carrier for 10 culture tubes 15 ml,
17362 Round carrier for 5 sterilin tubes 30 ml,
17370 Round carrier for 5 tubes 25-30 ml, max.
17375 Round carrier for 3 tubes 50 ml, max.
17376 Round carrier for 4 tubes with screw cap
17377 Round carrier for 4 culture tubes 50 ml
17378 Round carrier for 4 culture tubes 50 ml with
17385 Round carrier for 1 tube with screw cap
Description
17.2/19.5 x 90 - 115 mm, e.g. 15015, 15020, 15022, 15023, 15024 and Monovettes 9 ml and 10 ml, polypropylene
max. cap 23 mm, e.g. 15115, Greiner or Corning tubes, polypropylene
max. cap 22 mm, e.g. 15115, Greiner or Corning tubes, polypropylene
graduated up to 20 ml, with skirt, incl. cap, max. 25/31 x 65 - 95 mm, polypropylene, see www.bibby-sterilin.co.uk, no. 03008
25.4/29 x 85 - 115 mm, e.g. 15025, 15026, 15029, 15030, 15032, 15033, polypropylene
35/38 x 90 - 110 mm, e.g. 15049, 15050, 15056, polypropylene
40-50 ml, max. 29/34 x 85 - 110 mm, e.g. 13055 plus 17054, 15051, 15052, 15054, polypropylene
15151, polypropylene
skirt, polypropylene
78-85 ml, max. 38/40 x 85 - 115 mm, e.g. 13085 plus 17185, 15074, 15075, 15076, 15080, polypropylene
Max. speed (rpm)
Max. gravitational field (x g)
Operating Manual SIGMA 4-15C, page 15 of 95
03/06
Part No.
17390 Round carrier incl. rubber cushion 16051
17395 Round carrier for 1 bottle with screw cap
17400 Round carrier for 1 bottle with screw cap
17401 Round carrier incl. rubber cushion 16250
17402 Round carrier for 1 tube with pointed
17347 Round carrier for 1 bottle with screw cap
13215 Rectangular bucket, aluminium, sealable
11156 Swing-out rotor for 6 buckets for the
11140 Swing-out rotor for 4 buckets for the
Description
for 1 tube 100 ml, max. 45/50 x 85 - 110 mm, e.g. 15100, 15102, 15103, 15106, polypropylene
125 ml, max. 51 x 90 - 115 mm, e.g. 15125, polypropylene
200 ml, max. 57 x 90 - 115 mm, e.g. 15202, 15203, polypropylene
for 1 round bottom tube 175-250 ml, max. 57.5 x 90 - 137 mm, e.g. 15201, 15206, 15250, 15251, 15254, polypropylene
bottom 150-250 ml, max. Ø 60 x 120 - 140 mm, polypropylene
250 ml, max. Ø 61.5 x 90 - 125 mm, e.g. 13255, 15247, 15248, 15249 and for 15175 with adapter 13175 (suitable for bucket 13350 without screw cap 17135), polypropylene
with cap 17112, for the system of rectangular carriers, max. tube length 115 mm, suitable for rotor 11150, max. radius 18.2 cm, min. radius 8.8 cm
following accessories, data with 13115: max. radius 18.2 cm, min. radius 9.5 cm data with 13127: max. radius 19.1 cm, min. radius 9.7 cm
following accessories
Max. speed (rpm)
4 500
4 500 4 500
5 000
Max. gravitational field (x g)
4 120
4 120 4 324
4 668/4 416
Operating Manual SIGMA 4-15C, page 16 of 95
03/06
Part No.
13115 Rectangular bucket, aluminium, suitable for
13127 Rectangular bucket, aluminium, incl.
18000 Rectangular carrier, undrilled, for tubes 85 -
18002 Rectangular carrier for 20 reaction vials
18003 Upper part for 18002 for 20 reaction vials
18005 Rectangular carrier for 20 RIA-tubes 5 ml,
18007 Rectangular carrier for 20 glass tubes 7 ml,
18009 Rectangular carrier for 20 hemolyse tubes,
18010 Rectangular carrier for 12 tubes with screw
18012 Rectangular carrier for 12 Vacutainer-tubes
18015 Rectangular carrier for 12 tubes 10-15 ml,
Description
the system of rectangular carriers, max. tube length 110 mm
polysulfone sealing cap 17112, suitable for the system of rectangular carriers, max. tube length 115 mm
110 mm, polyallomer
1.5-2.2 ml, max. 11 mm, e.g. 15008, 15040, polypropylene
1.5-2.2 ml, max. 11 mm, e.g. 15008, 15040 (can be used together with 18002), polypropylene
max. 12.2 x 60 - 75 mm, flat and round bottom, e.g. 15060, polyallomer
max. 12.3 x 80 - 105 mm, flat and round bottom, e.g. 15007, 15027, polyallomer
max. 12.8 x 70 - 90 mm, polypropylene
cap 10-12 ml, max. 16.8/17.5 x 60 - 85 mm, e.g. 13026 plus 17126, 15000, 15010, 15039, polyallomer
13.5/18 x 65 - 90 mm, polypropylene
max. 17 x 90 - 105 mm, e.g. 15015, 15020, 15022, 15023, 15024, polyallomer
Max. speed (rpm)
5 000
5 000
Max. gravitational field (x g)
4 416
4 668
Operating Manual SIGMA 4-15C, page 17 of 95
03/06
Part No.
18016 Rectangular carrier for 4 culture tubes
18017 Rectangular carrier for 10 tubes 15 ml and
18025 Rectangular carrier for 5 glass tubes 25 ml,
18022 Rectangular carrier for 4 sterilin tubes
18030 Rectangular carrier for 5 tubes with screw
18050 Rectangular carrier for 2 tubes 50 ml, max.
18051 Rectangular carrier for 2 tubes with screw
18052 Rectangular carrier for 2 culture tubes
18053 Rectangular carrier for 2 culture tubes
18085 Rectangular carrier for 1 tube with screw
Description
15 ml 15115, polypropylene
tubes with cap, max. 17.2/18 x 80 - 112 mm, e.g. Monovettes 9 ml and 10 ml, polypropylene
max. 24 x 85 - 105 mm, e.g. 15025, 15026, polyallomer
30 ml, graduated up to 20 ml, with skirt, incl. cap, max. 25/31 x 65 - 95 mm, polypropylene, see www.bibby-sterilin.co.uk, no. 03008
cap 27-30 ml, max. 25.4/27.5 x 80 - 110 mm, e.g. 15029, 15030, 15032, polypropylene
35/38 x 85 - 110 mm, e.g. 15049, 15050, 15056, polyallomer
cap 40-50 ml, max. 29/35 x 80 - 110 mm, e.g. 13055 plus 17054, 15051, 15052, 15054, polypropylene
50 ml 15151, polypropylene
50 ml with skirt, max. 29.5/38 x 85 - 118 mm, polypropylene
cap 78-85 ml, max. 38/40 x 85 - 112 mm, e.g. 13085 plus 17185, 15074, 15075, 15076, 15080, polyallomer
Max. speed (rpm)
Max. gravitational field (x g)
Operating Manual SIGMA 4-15C, page 18 of 95
03/06
Part No.
18100 Rectangular carrier for 1 tube 100 ml, max.
18105 Rectangular carrier for 20 RIA-tubes 5 ml,
18107 Rectangular carrier for 20 glass tubes 7 ml,
18115 Rectangular carrier for 12 tubes 10-15 ml,
18125 Rectangular carrier for 1 bottle with screw
18200 Rectangular carrier for 1 bottle with screw
13201 Round bucket for 1 glass tube 200 ml
11141 Swing-out rotor 48 x 15 ml complete,
11157 Swing-out rotor 72 x 15 ml complete,
Description
45.5/48 x 85 - 110 mm, e.g. 15100, 15102, 15103, 15106, polyallomer
max. 12.2 x 60 - 75 mm, flat and round bottom, e.g. 15060, decantable, polyallomer
max. 12.3 x 80 - 105 mm, flat and round bottom, e.g. 15007, 15027, decantable, polyallomer
max. 17 x 90 - 105 mm, e.g. 15015, 15020, 15022, 15023, 15024, decantable, polyallomer
cap 125 ml, max. 51 x 90 - 115 mm, e.g. 15125, polypropylene
cap 200 ml, max. 57 x 90 - 115 mm, e.g. 15202, 15203, polypropylene
15201, 15206, incl. rubber cushion 16250, sealable with aluminium cap 17121
consisting of rotor 11140, 4 rectangular buckets 13115, 4 carriers 18015 and 48 polystyrene tubes 15020, max. radius
15.7 cm, min. radius 6.1 cm
consisting of rotor 11156, 6 rectangular buckets 13115, 6 carriers 18015 and 72 polystyrene tubes 15020, max. radius
18.2 cm, min. radius 9.5 cm
Max. speed (rpm)
5 000
4 500
Max. gravitational field (x g)
4 416
4 120
Operating Manual SIGMA 4-15C, page 19 of 95
03/06
Part No.
11144 Swing-out rotor for microtiter plates, incl.
11118 Swing-out rotor for microtiter plates, incl.
17108 Rectangular sealing cap, polysulfone, clear,
17978 Plate holder for bucket 13218 12165 Angle rotor 6 x 78-85 ml for sealed tubes,
12166 Angle rotor 8 x 40-50 ml for sealed tubes,
12172 Angle rotor 12 x 27-30 ml for sealed tubes,
12168 Angle rotor 20 x 10-12 ml for sealed tubes,
12130 Angle rotor 30 x 1.5-2.2 ml for reaction
Description
2 buckets 13145 and plate holder 17977, radius edge 12.85 cm, radius max. 10.7 cm radius min. 6.3 cm, max. plate height 64 mm
2 buckets 13218 and plate holder 17978, radius edge 15.15 cm, radius max. 13.8 cm radius min. 5.8 cm, max. plate height 80 mm, buckets sealable with cap 17108
incl. 4 clips 17118, for bucket 13218
e.g. 13085 plus 17185, 15074, 15075, 15076, 15080, incl. hermetic aluminium lid, max. radius 9.8 cm, min. radius 2.7 cm, angle 25°
e.g. 13055 plus 17054, 15051, 15052, 15054, incl. hermetic aluminium lid, max. radius
9.6 cm, min. radius 3.3 cm, angle 25°
e.g. 15029, 15030, 15032, incl. hermetic aluminium lid, max. radius 11.0 cm, min. radius 5.1 cm, angle 30°
e.g. 13026 plus 17126, 15000, 15010, 15039, incl. hermetic aluminium lid, max. radius
9.8 cm, min. radius 5.8 cm, angle 25°
vials, e.g. 15008, 15040, incl. hermetic aluminium lid, max. radius 10.0 cm, min. radius 6.7 cm, angle 45°
Max. speed (rpm)
5 000
5 500
12 500
12 500
12 500
12 500
13 500
Max. gravitational field (x g)
3 592 2 991 1 761
5 124 4 667 1 961
17 119
16 770
19 216
17 119
20 376
Operating Manual SIGMA 4-15C, page 20 of 95
03/06
Part No.
11148 Swing-out rotor 32 x 1.5-2.2 ml, incl. 8
12200 Angle rotor 100 x 1.5-2.2 ml for reaction
12169 Angle rotor for 8 culture tubes 50 ml, e.g.
13060 Adapter for 1 culture tube 15 ml 15115,
12170 Angle rotor for 12 culture tubes 15 ml, e.g.
12256 Angle rotor for 6 bottles 250 ml, e.g. 13255,
Adapters, tubes and steel tubes
13000 Adapter , POM, for reaction vials 0.25-
13002 Adapter, POM, for reaction vials 0.5-0.75 ml,
13021 Adapter for PCR-tube 0.2 ml, Ø 5.85/6.95 x
Description
buckets, for reaction vials, e.g. 15008, 15040, incl. hermetic aluminium lid, max. radius 8.4 cm, min. radius 4.4 cm
vials, e.g. 15008, 15040, incl. aluminium lid 17824, 2 lines, max. radius 16.3/15.18 cm, min. radius 13.11/11.9 cm
15151, incl. hermetic aluminium lid, max. radius 10.4 cm, min. radius 4.3 cm, angle 25°
suitable for 12169, polypropylene
15115, incl. hermetic aluminium lid, max. radius 10.0 cm, min. radius 4.6 cm, angle 25°
15247, 15249, incl. aluminium lid 17801, max. radius 14.5 cm, min. radius 3.9 cm, angle 30°
0.4 ml 15014, suitable for 11148, 12130, 12200, 17353, 18002, 18003
15005, 7.9/10 x 28/31 mm suitable for 11148, 12130, 12200, 17353, 18002, 18003
20/23.4 mm, suitable for 11148, 12130, 12200, 17353, 18002, 18003
Max. speed (rpm)
12 000
9 000
12 500
12 500
8 000
Max. gravitational field (x g)
13 523
14 761/13 747
18 168
17 469
10 375
Operating Manual SIGMA 4-15C, page 21 of 95
03/06
Part No.
13079 Bottom adapter for 1 tube 40-42 ml 15051,
13080 Adapter for 1 culture tube 50 ml 15151,
13081 Adapter for 1 culture tube 15 ml 15115,
13082
13083
13084
15005
15008 Reaction vials 1.5 ml, 1 pack contains
15040 Reaction vials 2.2 ml, 1 pack contains
15014 Reaction vials 0.4 ml (Beckman system),
15060
13026
Description
15052, 15054, suitable for 12169, polypropylene
suitable for 12165, polypropylene
suitable for 12165, polypropylene Adapter for 1 tube 40-50 ml, max. 28.8 x
105 - 110 mm, e.g. 13055, 15051, 15052, 15054, suitable for 12165, polypropylene
Adapter for 1 tube 27-30 ml, max. 25.5 x 90 - 110 mm, e.g. 15029, 15030, 15032, suitable for 12165, polypropylene
Adapter for 2 tubes 10-12 ml, max. 16/17.5 x 75 x 90 mm, e.g. 15000, 15010, 15039, suitable for 12165, polypropylene
Reaction vials 0.5 ml, 7.9/10 x 28/31 mm, 1 pack contains 100 pcs., suitable for 13002, 17350
100 pcs., suitable for 11148, 12130, 12200, 17353, 18002, 18003
100 pcs., suitable for 11148, 12130, 12200, 17353, 18002, 18003
polypropylene, 1 pack contains 100 pcs., suitable for 13000
Polystyrene tube 5 ml (RIA-tube), 12 x 75 mm, suitable for 13233, 17352, 17356, 18005, 18009, 18105
Stainless steel tube 10 ml, 15.7 x 76 mm, closeable with cap 17126, suitable for 12168, 17355, 18010
Operating Manual SIGMA 4-15C, page 22 of 95
03/06
Part No.
17126 Stainless steel sealing cap for 13026 15000
15010 ditto, polycarbonate 15039 ditto, polypropylene 15020
15021 Polypropylene stopper for 15020, 15023 15023
15115 Falcon tube with screw cap 15 ml, pointed
15029
15030 Polycarbonate tube with screw cap 30 ml,
15032 Polypropylene tube with screw cap 27 ml,
15049
13055 Stainless steel tube 50 ml, sealable with
17054 Stainless steel sealing cap for 13055
Description
Teflon tube with screw cap 12 ml, 16.1 x
81.1 mm, suitable for 12168, 13084, 17355, 18010
Polystyrene tube 15 ml, 17 x 100 mm, suitable for 17358, 18015, 18115
Polypropylene tube 15 ml, 17 x 100 mm, suitable for 17358, 18015, 18115
bottom, polypropylene, suitable for 12170, 13060, 13081, 13236, 17359, 17360, 18016
Teflon tube with screw cap 28 ml, 25.3 x 96 mm, suitable for 12172, 13083, 17370, 18030
25.3 x 98 mm, suitable for 12172, 13083, 17370, 18030
25.3 x 97 mm, suitable for 12172, 13083, 17370, 18030
Polycarbonate tube 50 ml, 34 x 100 mm, graduated 0 - 50 ml in steps of 1 ml, suitable for 17375, 18050
cap 17054, 29 x 101.5 mm, suitable for 12166, 13082, 17376, 18051
Operating Manual SIGMA 4-15C, page 23 of 95
03/06
Part No.
15051
15052 Polypropylene tube with screw cap 42 ml,
15054 Polycarbonate tube with screw cap 40 ml,
15151 Culture tube with screw cap 50 ml, pointed
13085 Stainless steel tube 85 ml, sealable with
17185 Stainless steel sealing cap for 13085 15074 Polycarbonate tube with special screw cap
15075 Polycarbonate tube with screw cap 82 ml,
15076 Polypropylene tube with screw cap 78 ml,
15080
15102
15103 ditto, polycarbonate, graduated 2 - 100 ml
15125 Polypropylene bottle with screw cap 125
Description
Teflon tube with screw cap 42 ml, 28.5 x 107 mm, suitable for 12166, 13082, 17376, 18051
28.8 x 107 mm, suitable for 12166, 13082, 17376, 18051
28.8 x 107 mm, suitable for 12166, 13082, 17376, 18051
bottom, polypropylene, suitable for 12169, 13080, 13235, 17377, 18052
cap 17185, 38/40 x 100/107 mm, suitable for 12165, 17385, 18085
made of aluminium with seal for high speeds 72 ml, 38 x 109 mm, suitable for 12165, 17385, 18085
38 x 112 mm, suitable for 12165, 17385, 18085
38 x 112 mm, suitable for 12165, 17385, 18085
Polyflor tube with screw cap 81 ml, 38 x 112 mm, suitable for 12165, 17385, 18085
Polypropylene tube 100 ml, 45 x 100 mm, suitable for 13234. 17390, 18100
in steps of 2 ml
ml, 51 x 99 mm, suitable for 17395, 18125
Operating Manual SIGMA 4-15C, page 24 of 95
03/06
Part No.
15175 Polypropylene bottle with pointed bottom
15202 Polypropylene bottle with screw cap
15203 Polycarbonate bottle with screw cap
13255 Stainless steel bottle 250 ml, sealable with
17256 Stainless steel sealing cap for 13255 15247 Teflon bottle with screw cap 250 ml, Ø 61.4
15248 Polycarbonate bottle with screw cap 250
15249 ditto, polypropylene 15500 Polycarbonate bottle 500 ml, incl. screw
15501 ditto, polypropylene
Glass tubes
15007
15027 ditto, graduated 0 - 5.5 ml in steps of 0.1 ml 15015
15024 ditto, graduated 0 - 10 ml in steps of 0.1 ml
Description
200 ml, Ø 61.5 x 139 mm, graduated up to 175 ml (N-3143-0175), suitable for 13231 with 13175, 17347 with 13175
190 ml, 56 x 112 mm, suitable for 17400, 18200
200 ml, 56 x 113 mm, suitable for 17400, 18200
cap 17256, Ø 61.4 x 125 mm, suitable for 12256, 17347
x 122 mm, suitable for 12256, 17347
ml, Ø 61.4 x 125 mm, suitable for 12256, 17347
cap, Ø 85 x 135 mm, suitable for 13350
Glass tube 7 ml, 12 x 100 mm, suitable for 17354, 18007, 18107
Glass tube 10 - 12 ml, 16 x 100 mm, suitable for 17358, 18015, 18115
Operating Manual SIGMA 4-15C, page 25 of 95
03/06
Part No.
15022
15025
15026 ditto, graduated 5 - 25 ml in steps of 1 ml 15033
15050
15056 ditto, graduated 4 - 50 ml in steps of 1 ml 15100
15106 ditto, graduated 1 - 100 ml in steps of 1 ml 15201 Glass tube 200 ml, Ø 56 x 112 mm, suitable
15206 ditto, graduated 15 - 175 ml in steps of 5 ml 15250 Glass tube 230 ml, Ø 56 x 135 mm, suitable
15254 ditto, graduated 15 - 200 ml in steps of 5 ml
Further accessories
16018 Rubber adapter for 15 ml glass tube 15022,
16019 Rubber adapter for 15 ml glass tube 15022,
16030 Rubber adapter for 30 ml glass tube 15033,
Description
Special glass tube 15 ml, 17 x 110 mm, suitable for 12166 with 16018 and for 12165, with 16019, max. permitted speed 7 000 rpm
Glass tube 25 ml, 24 x 100 mm, suitable for 17365, 18025
Special glass tube 30 ml, 24 x 105 mm, suitable for 12166 with 16030 and for 12165 with 16031, max. permitted speed 7 000 rpm
Glass tube 50 ml, 34 x 100 ml, suitable for 17375, 18050
Glass tube 100 ml, 44 x 100 mm, suitable for 17390, 18100
for 13201, 17401
for 17401
suitable for 12166
suitable for 12165
suitable for 12166
Operating Manual SIGMA 4-15C, page 26 of 95
03/06
Part No.
16031 Rubber adapter for 30 ml glass tube 15033,
16906 Rubber plate for 18025 16907 ditto, only for 18050 16908 16909 Rubber plate for rectangular carriers 16250 Rubber cushion for 13201 17112 Rectangular polysulfone sealing cap, clear,
17118 Sealing clip for caps 17108, 17112 17801 Lid for rotor 12256 17919 Table for centrifuge made of varnished
17913 Fasteners for table 17919 Further accessories are available on request.
Description
suitable for 12165
ditto, only for 18100
incl. 2 clips 17118, for 13215 and spare for 13127
sheet steel with 2 doors and space for accessories, movable on lock-type castors, dimensions: w 490, d 635, h 490 mm
Maximum speed for tubes
Some tubes, e.g. centrifuges glass tubes, microtubes, culture tubes, Teflon tubes and especially high volume tubes can be used in our rotors, buckets and adapters at higher speeds than their breaking limit. We recommend to always fill up the tubes and to follow the recommendations of the manufacturer.
Operating Manual SIGMA 4-15C, page 27 of 95
03/06
Operating Manual SIGMA 4-15C, page 28 of 95
03/06
1.3 Scope of Supply
The following belongs to the centrifuge: 1 Rotor wrench SW 13 Part No. 930 102
1 Square wrench Emergency lid release Part No. 80 054 1 Tube grease for rotor trunnion pins Part No. 70 284 20 ml slushing oil Part No. 70 104
Documentation: 1 Short operating instructions
1 Operating Manual 1 "Rotor and Accessories, Operation and Use" 1 EU-Statement of Conformity 1 Equipment Decontamination Certificate
Accessories according to your order, our order confirmation and our delivery note.
Rotor Part No. Rotor No.
....................... .....................
....................... .....................
....................... .....................
....................... .....................
....................... .....................
....................... .....................
....................... .....................
1.4 Standards and Regulations
Please refer to the enclosed EU-Statement of Conformity.
Operating Manual SIGMA 4-15C, page 29 of 95
03/06
Loading...
+ 66 hidden pages