Shimadzu AA-7000 Series Manual

C122- E05 8G

Atomic Absorption Spectrophotometers

AA-7000 Series

Atomic Absorption Spectrophotometers

AA-7000 Series

Reaching Even Greater Heights

Enhanced Flame Analysis

World-Class High-Sensitivity Furnace

Improved Dual Atomizer System

Advanced Safety Technology

4

The AA-7000 Series can be upgraded by adding units to allow the system to handle the analysis targets.

-

System Configuration can Evolve
with Your Needs

AA-7000 Series supports a wide range of
analysis applications.

Major Fields of Application

Analysis Sensitivities

Concentration limit of detection

(ppm) (ppb)

H

Li NeFONCB

ArClSPAl

Ca Sc Ti Cr Mn Fe Co Ni Cu Zn KrBrSeGa

YZrNbMo

Tc Ru Rh Pd Cd XeTe IIn

Cs Ba La

Fr Ra Ac

Hf Ta W Re Os Ir AuPt Hg RnAtPoBiPbTl

Ce Pr Nd Pm Sm Eu Gd Tb LuYbTmErHoDy

Th Pa U Np Pu Am Cm Bk LrNoMdFmEsCf

He

Ag

Sn Sb

Si

V

Be

Na

Rb Sr

Mg

K

Ge As

* May differ according to coexisting substances in the sample.

AA-7000G GFA-7000A

AA-7000G GFA-7000A Auto Sampler System

ASC

*2

Environment

Metals, Semiconductors, Ceramics

Petroleum, Chemicals, Polymers

Seawater, river water, effluent,
sludge, air-borne dust

Metals, minerals, glass,
ceramics, IC chips

Petroleum, oil, catalysts,
chemical products, biodiesel

Blood, animals, plants,
drugs, food products

Medical, Biology, Pharmaceuticals

Flame

Furnace

AA-7000F Manual Burner System

AA-7000F

AA-7000F/AAC

AA-7000F/AAC Auto Burner System

GFA

ASC

*1

ASC

*1

*2

*3

AAC

AAC

5

Flame and Measurement Procedures

Flame Selection

Air-C2H2N2O-C2H2HVG MVU

H

Be NeFONCB

Na Mg ArClSPAl

KCa Ti CrMnFeCoNiCuZn KrBrGa

Rb Sr Y Zr Nb Mo

Tc Ru Rh Pd Cd XeITeIn

Cs

Ba La

Fr Ra Ac

Hf Ta W Re Os Ir Pt Au RnAtPoBiPbTl

Ce Pr Nd Pm Sm Eu Gd Tb LuYbTmErHoDy

Th Pa U Np Pu Am Cm Bk LrNoMdFmEsCf

He

Ag

Ge

Si

V

Li

SeAs

Sb

Hg

Sc

Sn

AUTO

Graphite Furnace
Atomizer

GFA

AA-7000F/AAC Dual Atomizer System

Auto Atomizer
Changer

ASC

Autosampler

Dual Atomizer System
Automatic adjustment of atomizer
Automatic serach of burner height

AUTO

AAC

*1 Requires ASC stand kit.
*2 Requires ASK-7000.
*3 Automatic burner height search function can be used.
AA-7000F/AAC equips with AAC as standard.

AA-7000F Flame Model

AA-7000G Furnace Model (with options attached)

Detector

Hollow cathode lamp

Beam splitter

Monochromator

D2 lamp

Chopper mirror

Burner head (or graphite tube)

Reference beam

Sample beam

6

Enhanced Flame Analysis

The AA-7000 Series incorporates newly developed 3D double-beam optics.
The optical system has been designed to produce its maximum performance for each measurement method through
optimal adjustment of the light beam and light beam digital filter, and by using optical components that restrict light
losses.

Double-Beam Optics and Stable Hardware Achieve Superior Stability

7

Advantages of the Double-Beam System

Support for Developing Analytical Conditions

Optional Autosampler Reduces Analysis Workload

Long-term stability

The graph shows the results of
measurements on 2 ppm copper (Cu)
conducted over at least one hour.
(The plot shows mean values for 11
repeated measurements.) Over the
course of more than 600
measurements, the instrument
achieved a relative standard
deviation within 1%.

High sensitivity

The graph shows the direct
measurement results for 0.1
ppm lead (Pb).

Automatic gas flow rate optimization

Automatic searching for optimal fuel gas flow rate (Japanese Patent 2099886). It is important
to determine the optimal gas flow rate for the flame when using an organic solvent or after
changing the burner height. The AA-7000F Series automatically optimizes the gas flow rate
by measuring the changes in absorbance between a blank and a standard sample. The
difference between the two is displayed on the screen. The gas flow rate achieving the
highest sensitivity is detected and this value is automatically set as the gas flow rate value.

Automatic burner height optimization (AA-7000F/AAC)

The absorption sensitivity for flame analysis is also affected by the burner height. This results
from variations in the flame temperature due to the burner height. The flame temperature is
also affected by the matrix components. AA-7000F/AAC adjusts the burner height in 0.5 mm
steps to automatically search for the optimal conditions.
AA-7000F enables above function by AAC-7000 (option).

Low carryover

Great care must be taken to avoid carryover during flame analysis. The new ASC-7000
autosampler rinses the nozzle at the rinsing port on the overflow mechanism after each
sample measurement is complete. This ensures 10-4 max. carryover during the
measurements of multiple samples. The graph shows the results of consecutive analyses
of 10 ppm, 20 ppm, and 50 ppm sodium (Na) standard solutions in the EMISSION mode.
No carryover could be detected when measuring the 10 ppm standard sample
immediately after the measuring the 50 ppm Na standard sample.

Example of micro sampling analysis

Examples of the measured waveforms (overlaid) and calibration curve for micro
sampling analysis are shown to the right.
A 2-ppm Cu standard solution was prepared by auto-dilution using the autosampler.
The autosampler can also be used to conduct dilution measurements of the sample.
(Injection volume: 90 µL)

Trace Sample Analysis Using Micro Sampling

Micro sampling

At least 1 mL (1000 µL) volume of a liquid sample is required for the continuous intake of
sample during normal flame analysis. With micro sampling, however, approximately 50 to 90
µL of sample is injected in one shot into the flame and quantitation is based on the height
and area of the peak signal obtained. This method offers the advantages below.

Advantages

.

Permits analysis of small sample volumes

.

Multi-element analysis of small sample volumes

.

No blockage of burner slot with samples having a high salt concentration

.

Synchronized with the autosampler for auto-dilution measurements

* Synchronization with the autosampler requires the optional micro sampling kit.

Data Showing Long-Term Stability for
Flame Cu Measurements

0.1 ppm to 0.4 ppm Calibration Curve for Lead (Pb)

A
b

s

Conc(ppm)

Conventional method Overflow method

Discharge

Data showing low carryover

1. Sample injected into
micro sampling port.

2. Solenoid valve opens to inject sample
in one shot into the flame.

Sampling port

Solenoid
valve
(opened)

Solenoid
valve
(closed)

Sampling port

Absorbance

Measurement time

Pb 0.08ppb

Mn 0.02ppb

0.05ppb

0.01ppb

Enhanced Sensitivity due to Graphite Furnace

Advances in optics and a new graphite furnace design achieve improved
lower limits of detection for furnace analysis (comparison with previous
Shimadzu models).
This superb analysis performance is possible in all fields.

Achieves World-Class Lower Limits of Detection

Previous New

8

World-Class High-Sensitivity Furnace

High-Performance Autosampler

High-Sensitivity Application Data (Analysis of Selenium (Se))

Mix and inject up to four sample types (diluted solution, standard solution,
sample, matrix modifier, etc.). (Of course, unmixed samples can also be injected.)

Select a fluororesin tube or pipette tip as the injection nozzle.

Automatic dilution and re-analysis if the calibration curve concentration is exceeded.

Independent control of the gas flow through the graphite tube during
atomization achieves extremely high-sensitivity measurements.
(Japanese Patent 2067563)

Digital temperature control and electronic gas flow control enhance stability

Combination of a high-sensitivity optical sensor and unique digital temperature control
technology achieves highly accurate temperature control in all temperature regions from
drying to atomization. An electronic flow controller can precisely control the inner gas
flow rate in 0.01 L/min units. These control techniques significantly enhance both the
sensitivity and the data stability.

Example of Automatic Dilution and Re-Analysis

Analysis of cadmium (Cd): The maximum concentration of the calibration curve has been set to 1ppb. At 1.8ppb, the sample of [003] has exceeded the
maximum concentration. As a resultit has been automatically diluted by 4 times and re-measured.

* Depending on the state of the sample, some other combinations may be appropriate.

High-density graphite tube

(P/N 206-50587)

Pyro-coated graphite tube

(P/N 206-50588)

Platform tube

(P/N 206-50887-02)

Selecting the Graphite Tube

Effective for elements that readily form
carbides (Ni, Fe, Cu, Ca, Ti, Si, V, Mo, etc.).

Restricts chemical interference due to
coexisting substances. Effective for the
analysis of environmental samples and
biosamples, such as sea water and
industrial waste.

Can be used for all elements. Especially
effective for low-boiling point elements
(Cd, Pb, Na, K, Zn, Mg, etc.).

Measurement Example Showing High Sensitivity

Analysis of 0 to 5 ppb selenium (Se): Sensitivity is adequate for 1 ppb measurements.
(20 µL injected volume, Pd modifier, pyro-coated graphite tube)

Measurement Example Showing High Stability

Analysis of 0.5 ppb lead (Pb): Approx. 5% relative standard deviation after 5 repeated
measurements is adequate for quantitative analysis.

9

AA-7000F/AAC creates an integral burner and furnace that remains permanently installed in the combustion chamber.
It supports both flame analysis of high concentration samples and furnace analysis of trace samples, without changing
the atomizer unit. The integral construction with the atomizer saves space.
AA-7000F enables above function by AAC-7000 (option).

* The AAC-7000 cannot be attached to an AA-7000G instrument.

Single Unit Handles High Concentration to Trace Analysis Samples

10

Improved Dual Atomizer System

The new drive mechanism halves the switching time between flame and furnace measurements
(comparison with previous Shimadzu models).

Smallest footprint for a full system Easily attach an autosampler

Direct connection of the autosampler
to the AA instrument minimizes the
installation footprint and simplifies
maintenance.

Lamp house

Just slide the cover to the side for
easy replacement of the hollow
cathode lamps through the large
opening.

New Atomizer Design Permits Easy Switching Between Flame and Furnace Measurements

Slim, Easy-to-Use Design

The atomizer unit is switched automatically by software
operation. No troublesome replacement of the atomizer
unit is required. No need to disconnect pipes or wires.

In case of the flame measurement of high-concentration
sample, offsetting the burner head from the light axis,
instead of angle adjustment, allows to adjust the
sensitivity.

Flame measurement: Burner head
intersects the light axis (red line).

Furnace measurement: Furnace
intersects the light axis (red line).

Flame measurement Furnace measurement

A single autosampler can be used for both flame and
furnace measurements. Simply slide it left or right. No
need to purchase two autosamplers.

* Dimensions do not include ASC-7000. Height (H) does not include protrusions.

AA-7000F/AAC Dual Atomizer System

AA-6300

11

The system with a dual atomizer fits into a 960 mm width
(including power supply for the graphite furnace atomizer),
achieving the world's smallest installation footprint* for a full
system.

* Shimadzu in-house investigation. Current as of November 2008.

Safety is an extremely important consideration for flame atomic absorption spectrophotometers using acetylene gas.
The AA-7000 Series instruments are the first* ones in the world fitted with a vibration sensor as standard. They also
incorporate a comprehensive range of safety mechanisms, including gas leak detectors.

* Shimadzu in-house investigation. Current as of November 2008.

Comprehensive Safety Functions in Every System

12

Advanced Safety Technology

World first! –– flame extinguished automatically by vibration sensor

The flame is automatically extinguished when the new built-in sensor detects vibrations.
Instruments are completely safe during severe shaking caused by earthquakes.

Multimode automatic gas leak check

The fuel gas pipes inside the instrument gas controller are automatically
checked for gas leaks when the power is turned on and when the flame is
extinguished. Should a gas leak be detected, a warning buzzer sounds and a
warning is displayed on the screen.

Flame-retardant materials

UL 94V-0-rated flame-retardant materials
are used for the instrument external
covers and atomizer unit. This superior
design pays due consideration to safety.

Safe ignition switches

The switches perfectly fit finger contours and are positioned
near the window.
To prevent inadvertent operation, both switches must be
pressed simultaneously to start ignition.

Durable pipes and reliable couplings

All pipes are selected for durability and
used with highly reliable couplings.

Clear window

The large window permits observation of the flame, and the
burner can be easily accessed through the large opening.
The window closes when released to eliminate the chance
of it being left open.

Automatic flame ignition and extinguishing

Flame ignition and extinguishing operations are extremely simple. The
Air-C2H2 flame priority ignition mechanism prevents flashback.

Automatic Air-N2O switching system with acetylene flow-rate monitor

After the ignition of an Air-C2H2 flame, the flame automatically switches to
an N2O-C2H2 flame.
If the C2H2 flow rate does not increase due to solenoid valve trouble, for
example, switching to the support gas is disabled to prevent flashback.

Pressure monitor prevents flashback Automatic gas shut-off by flame monitor

Sudden power interruption detection and re-ignition safety measures

Drain tank level monitor

Mechanism to prevent misuse of the burner

Safety Functions for Flame-Specification Instruments

Safety Functions for Furnace-Specification Instruments

The connected options and operation of safety mechanisms are
checked during instrument initialization.

Cooling water flow rate monitor Argon gas pressure monitor Furnace cooling check

Overcurrent protection unit (double-checked by circuit protector and optical sensor)

Safety-Conscious Design

13

The optimal background correction methods are installed as standard:
high-speed self-reversal method (SR method) and deuterium lamp method (D

2

method).

Dual-Background Correction Functions

SR (high-speed self-reversal) method –– accurate background correction over a wide range

Samples with a complex matrix

(Containing a large quantity of a specific element as the main component)

Purified water, tap water, environmental water, etc.

Samples with a relatively simple matrix

Samples suitable for the SR method Samples suitable for the D2 method

These functions can correct for spectral interference in flame measurement.
Selecting the optimal background correction method for each sample ensures
accurate and reliable analysis results.

1. High-speed self-reversal (SR) correction is generally more accurate than deuterium lamp (D

2

) correction. As both atomic absorption and background
absorption can be measured using a single lamp, the correction errors due to light-axis misalignment are extremely small. This is ideal for the quantitation
of trace components in a matrix exhibiting complex background absorption, such as bio-samples and metals.

2. Permits background correction over the entire wavelength range from 185 nm to 900 nm.

3. This method can correct for spectral interference due to neighboring lines that can occur when a resonance line for another element exists near the
analytical line for the target element. (See table on next page.)

4. As no polarizer is used, measurements are possible with low light losses and a high S/N ratio.

5. The rapid lamp lighting permits accurate measurement unaffected by emission noise in the atomizer.

* Hollow cathode lamp L-2433 is required to use the SR method. Hollow cathode lamp L-2433 can also be used for the D

2

method.

Features

Principle

Background absorption

Background

Atomic absorption

Background

Atomic absorption

Time

Lamp current

IH spectrum

IH

IL

IL spectrum

(Lamp energy) (Sample measurement) (Energy component ratio)

Atomic
absorption

WavelengthWavelength

Atomic

absorption

Absorption
layer

A small current IL (approx. 10 mA) and a large current IH (approx. 500
mA) are alternately passed through the hollow cathode lamp. The
lamp emission spectrum when the large current flows has a depression
in the center (self-reverse), due to self-absorption of the large number
of sputtered atoms in the atom cloud, as shown in the diagram to the
left. No significant atomic absorption is apparent and background
absorption mainly occurs. Conversely, the lamp emission spectrum
when the small current flows comprises a single narrow peak resulting
from both atomic absorption and background absorption. By
determining the difference between the two types of absorption, it is
possible to accurately correct for the background absorption and
measure the true atomic absorption.

Examples suitable for SR method (where differences result between SR and D

2

methods)

Example: Measurement of trace levels of zinc in iron (analysis of Zn in Fe solution)

BGC-SR method

BGC-D

2

method

The identical 0.5 ppm Zn solution is accurately corrected to
the same absorbance at (2) and (6).

Due to inadequate correction, the absorbance is higher at
(6) than at (2) for the identical 0.5 ppm Zn solution.

Zn 0.25ppm

Zn 0.50ppm

Fe 0.1%

Fe 0.5%

Fe 0.5% Zn 0.25ppm

Fe 0.5% Zn 0.5ppm

Fe 0.75% Zn 0.3ppm

Atomic absorption signal
Background signal

14

Atomic absorption signal
Background signal

D2 (deuterium lamp) method –– highly sensitive background correction

1. Detection sensitivity is superior to the SR method. Therefore, this method is suitable for the analysis of samples with a simple matrix requiring high
sensitivity, such as the measurement of trace levels of impurities in ultrapure water or environmental analyses.

2. As the lighting frequency is higher than with the SR method, it can eliminate noise due to emission components of the flame or graphite tube to permit
accurate atomic absorption measurements.

3. The original hollow cathode lamp can be used.

Features

Principle

The deuterium lamp method involves lighting the hollow cathode lamp and the
deuterium lamp alternately at high speed. After separation by the monochromator,
the light from the deuterium lamp has a bandwidth from 0.1 to 5 nm. Therefore, an
atomic absorption with a line width of only about 1/1000 nm is almost unobservable
compared to the background absorption due to wide-bandwidth molecular
absorption. However, as the light from the hollow cathode lamp has approximately
the same bandwidth as the atomic absorption band, the total of the atomic
absorption and the background absorption can be observed. With the deuterium
lamp (D

2

) method, light from both sources passes through the atomizer. The

difference in absorbance is determined to conduct background correction.

The SR method is suitable for samples containing elements that cause
problems with spectral interference, as shown in the table to the left.

Measured ElementAlAnalytical Line (nm) Coexisting Element Absorption Line (nm)

309.28 Mg 309.30

As

193.76 Fe 193.73

Ca

422.67 Fe 422.64

Cd

228.80 Ni 228.84

Cu

324.75 Fe 324.73

Ga

294.36 Ni

285.18

Mg

285.21 Fe

Fe

Fe

Fe

Fe

Fe

294.39

Ni

232.00 232.04

Pb

217.00 216.95

Sb

217.58 217.55

Se

196.03 196.05

Si

251.61 251.69

FeZn 213.856 213.8589

Examples of elements and wavelengths causing spectral
interference problems due to neighboring lines

Atomic absorption + background absorptionHollow cathode lamp spectrum

Atomic absorption

D

2

lamp spectrum Background absorption

Examples suitable for D2 method (where no difference results between SR and D2 methods)

Example: Measurement of trace levels of lead in 2% NaCl solution by molecular absorption (analysis of Pb in 2% NaCl solution)

BGC-SR method

BGC-D

2

method

It can be seen that the sensitivity is higher with the BGC-D2 method.

Background signal

Atomic absorption signal

15

(deuterium lamp) method

––

hi

gh

ly

sensitive background correction

Spike 0ppb 2ppb 4ppb

Spike 0ppb 2ppb 4ppb

Features of the WizAArd Software

The WizAArd software used with the AA-7000 runs under Windows 7/ Vista/XP.

Wizard Functions Make Setting the Conditions So Simple That Even a Novice Can Do It.

Measurement Screen Layout Shows Measurement Status at a Glance

Just set the measurement conditions using WizAArd to
complete the general settings.

The initial settings can also be completed simply
by following the Wizard procedures.

Lamp History Function Assists with Lamp Management

The accumulated operation time for each lamp displayed on the lamp
registration screen assists with lamp service life management. Multiple
lamps for the same element are differentiated using lamp IDs.

Select element.

Start Wizard.

Set calibration curve and sample parameters.

Set monochromator parameters.

Connect to instrument.

16

The WizAArd software used with the AA-7000 runs under Windows 7

/

Vista/XP

.

Wizard Functions Make Setting the Conditions So Simple That Even a Novice Can Do It.

Wizard Functions Make Setting the Conditions So Simple Tha

easurement Screen Layout Shows Measurement Status at

Just set the measurement conditions usi

ng

WizAArd to

complete the general settings.

T

he initial settings can also be completed simpl

y

by following the Wizard procedures.

amp History Function Assists w

ith L

amp Managemen

t

T

he accumulated operation time for each lamp displa

y

ed on the lamp

egistration screen assists with lamp service life mana

g

ement. Multiple

amps for the same element are differentiated usin

g

lamp IDs.

element

.

rt Wizard.

et calibration curve and sample parameters.

et monochromator parameters.

nn

ect to

instrument.

p

1

6

Clear, Easy-to-Use Software

of

the WizAArd Software

Signal profile display

Measured element

Real-time signal monitor

MRT (Measured Results Table)
The worksheet shows sample names,
absorbance, concentrations,
and correction calibration results.

Calibration curve display

Software Provides Comprehensive Information Displays and Flexible Settings

Identical software operation for flame and furnace measurements

Combining a high-performance autosampler simplifies advanced settings

Even if the calibration curve is created after sample measurements,
concentration calculations can be conducted on past data. This
allows trial measurements to be directly used as actual
measurements.

Extrapolation of calibration curve range. If the sample concentration
exceeds the calibration curve range, additional measurements can be
performed on standard solutions to re-calculate the concentration.

Use existing calibration curves for measurements. Useful for sample
concentration order checks and for checking the instrument
sensitivity.

One-touch re-measurement operation. No need to repeat the
measurement from the beginning.

Create and save multiple calibration curves on a single worksheet.
Select the appropriate calibration curve for the sample concentration
and composition.

Real-time drying and ashing progress display for furnace
measurement

A higher temperature cleaning operation than the cleaning stage
can be added for each measurement. This reduces the graphite tube
memory effect. Tube deterioration is reduced by minimizing the
cleaning operations.

Add optional autosampler rinsing operations to ensure adequate
rinsing of the autosampler after completing the measurement of
high-concentration samples.

Set up sample dilution and spike-and-recovery tests on the same
screen.

Overlay function allows size and shape comparison of peak profiles.

Large-volume injection permits high-sensitivity measurements.

Precision control of drying and ashing temperatures reduces analysis
time.

17

ven if the ca

lib

ration curve is created after sample measurements,

concentration calculations can be conducted on past data. This

llows trial measurements to be directly used as actual

easurements.

xtrapolation of calibration curve range. If the sample concentration

exceeds the calibration curve range, additional measurements can be

erformed on standard solutions to re-calculate the concentration.

se existing calibration curves for measurements. Useful for sample

concentration order checks and for checking the instrument

s

ensitivity.

One-touch re-measurement operation. No need to repeat the

easurement from the beginning.

Create and save multiple calibration curves on a single worksheet.
Select the appropriate calibration curve for the sample concentration
and composition.

Real-time drying and ashing progress display for furnace

easuremen

t

A higher temperature cleaning operation than the cleaning stage
can be added for each measurement. This reduces the graphite tube

emory effect. Tube deterioration is reduced by minimizing the

cleaning operations.

Add optional autosampler rinsing operations to ensure adequate

insing of the autosampler after completing the measurement of

igh-concentration samples.

Set up sample dilution and spike-and-recovery tests on the same

s

creen.

Overlay function allows size and shape comparison of peak profiles.

Large-volume injection permits high-sensitivity measurements.

Precision control of drying and ashing temperatures reduces analysis

time

.

Provides Comprehensive Information Displays and Flexible Settings

g

p

FDA 21 CFR Part 11 Compliance

Supports System Management andAccuracy

21

CFR Part 11 Compliance

A combination of enhanced WizAArd software with Shimadzu's network-compatible CLASS-Agent data
management software supports FDA 21 CFR Part 11 Compliance.

WizAArd used alone provides comprehensive system policy setting, user management, log browser, audit trail,
and electronic signature system management functions.

Hardware validation software installed as standard.

Comprehensive Data Management Functions

User Management

User management restricts the users of
the system. It registers each user to
determine how each one uses the
software.

System Policy

The system policy settings allow advanced
password and lockout settings. The levels
can be set in stages from "unrestricted"
to "Part 11 compatible".

CLASS-Agent (Option)

Connection to CLASS-Agent permits
efficient, long-term database
management of large amounts of analysis
data.

Log Browser

The log browser easily displays a variety of logs to check the
system modification history and other log information.

18

Br

ows

er

r M

ana

gem

ent

to "P

art 11 compat

ible"

.

at

a

o

p

p

p

rehensive Data Mana

g

g

g

ement Function

s

Management

Accuracy Management (QA/QC) Functions Permit User Level Management, Audit Trail, and Electronic Signatures

QA/QC compatibility

The QA/QC functions permit accuracy
management.

Hardware validation software installed as standard

The hardware validation software makes it simple to evaluate the instrument
performance. When combined with the autosampler, it automatically determines
the wavelength accuracy, noise level, baseline drift, absorbance and repeatability,
and prints out the results of comparison with the pass criteria.

* Data from all Shimadzu analytical instruments can be centrally managed by CLASS-Agent.

19

A

ccurac

y

y

y

y

y

Mana

g

g

g

g

g

ement

(Q

(

A/

QC

)

Functions Permit User Level Managemen

t,

Standard Parts / PC / Software

20

* The PC, monitor, printer, hollow cathode lamps, high-temperature burner head, pressure regulator and compressor are not included in the standard configuration.

Part Name Quantity P/N

071-60821-08 (120 V), 071-60825-51 (230 V)1

206-52046-911

1 206-97176

Common to All AA-7000 Series Models

1 206-97225

1 228-30164

1 037-70238-01

1 221-40500

3 206-57770

206-777041

206-77551-121

206-84934-671

AA-7000G Standard Parts List

Part Name Quantity

1

1

2

1

2

1

1 (0.3 m)

1 (2.4 m)

1

1

1

206-50389-91

206-50389-92

037-61019

201-79229-01

204-05899-01

206-50772-91

200-31328-01

016-43201-02

206-77413-41

206-50442-91

206-77243-92

AA-7000F, AA-7000F/AAC Standard Parts List

1 206-84934-66/-68

1 206-77551-02/-22

* Windows is a registered trademark of Microsoft Corp., U.S.A.

Operating system

CPU

RAM

Monitor

Storage device

I/O port

Microsoft Windows 7 Professional (32 bit) Vista Business or XP Professional

Intel

®

Celeron 420 (1.60 GHz) or higher

1 GB or higher (Vista) or 512 MB or higher (XP)

XGA (1024 × 768 dots) or higher

One CD-ROM drive (for installing software) Requires 60 MB min. hard disk space for installation

One serial port (for AA control)

Personal Computer / Monitor

Cable set

Cards (set of 10)

Instruction manual

Safety inspection sheet (safety instruction)

Declaration of conformity, explanatory notes (ISO-9001)

Warranty label

Registration form

Serial number label

Hose ASSY (for air supply)

Hose ASSY (for C

2H2 gas supply)

Hose clamp (16 mm)

Cleaning wire

Sampling tube (PTFE)

Sampling tube (for organic solvent samples)

Polyethylene tubing, No. 3

Polyethylene tubing, 8 × 1 (drain tubing)

Drain ASSY

Grease (in cup)

Funnel

Declaration of conformity, English version (ISO-9001)

Inspection report

P/N

Part Name Quantity

P/N

Declaration of conformity, English version (ISO-9001)

Furnace mounting plate

Inspection report

* GFA-7000A is not included in the standard configuration.

21

High-density graphite tube

206-50587-11

Pyro-coated graphite tube

Platform tube

206-50588-11

Select one of the three types of graphite tubes according to the aim of the analysis.

206-50887-02

MAF-106S compressed gas regulator

040-72019-21

For Argon gas

I

Specifications

GFA-7000A graphite furnace atomizer

206-77777-XX

For Furnace Analysis

For cooling GFA, 100 VAC, 1100VA, 50/60 Hz

CA-1115A-1 cooling water circulation unit

044-01813-01

For connecting GFA and CA-1115A-1Cooler connection kit

Parts for cooling water connections

206-84373-41

Connecting tubes when using tap water to cool GFA Cooling water tube ASSY 206-51028-41

Decompression valve when using tap water to cool GFARegulator ASSY 206-86147-41

Heating control system: Drying: Digital current control
(with automatic temperature calibration function)
Ashing, atomization: Digital temperature control via
optical sensor
Heating temperature range: Ambient to 3000 °C
Inner gas type: Dual automatic switching type
Inner gas flow rate: 0 to 1.50 L/min, 0.01 L/min increments
Ar gas: 3.5 L/min max.
Cooling water: Cooling water circulation unit or tap for process water
Water temperature: 10 to 30 °C, flow rate: 0.6 to 1.5 L/min

* Separately order the parts below.

Part Name P/N Remarks

Flow meter kit

206-77617-41 Float-type flow meter for support gas

Dimensions: 250 W × 130 D × 170 H mm

206-77655-91 Vial mounting platform: 220 W × 95 D mm

Vial positions: 5-step switching

For Flame Analysis

Sample platform

208-91753-91

Air compressor

208-91750-36 100 VAC, 50/60 Hz, with mist separator

100 VAC, 50/60 Hz, with mist separator

Low-noise air compressor

206-52458-91 Required if using an air compressor other than above.

Mist separator kit

040-72020-01 For C2H2

For dinitrogen oxide gas

YR-71 compressed gas regulator

040-72019-11

MAF-85S compressed gas regulator

Required to use the flame micro sampling method. ASC-7000 and
ASK-7000 (or ASC stand kit) are also required.

206-77540-91

Micro sampling kit

Provides viewing inside the graphite tube.
Including Video View Software (CD-ROM)

206-52950-41

Graphite Furnace Camera GFA-TV

O-ring set for organic solvents206-77620-92

O-ring set

Made of pure titanium. Air-cooled. 5 cm slot for N2O-C2H2 flame

High-temperature burner head

Part Name P/N Remarks

206-77530-91

.

Extremely corrosion-resistant

.

Can also be used for Air-C2H2 flame.

For flame analysis For furnace analysis

ASC-7000 autosampler 206-77600-XX

Autosampler

Required to mount ASC-7000 to conduct flame analysis only. ASC stand kit 206-77650-41

Permits both flame and furnace analysis.

ASK-7000 extension unit for furnace analysis

Required to use ASC-7000 and HVG-1. Nozzle ASSY, HVG

I

Specifications

Part Name P/N Remarks

System: Flame / furnace
Function: Zero-point detection, auto rinse, auto diagnosis, random access
Maximum reagent / sample positions: Reagents: 8 positions, samples: 60 positions

* Separately order the parts below.

206-77550-41

206-67563

Optional Accessories

Optional Accessories / Related Products

For AA-7000G

For AA-7000F

206-52135-91

206-83755-91

Dimensions: 170 W × 110 D × 110 H mm
I.D.: ø25 × 170 mm
Heater: PYROMAX DS

Furnace

Controller

Operational temperature range: Ambient to 1100 °C
Temperature regulation range: ±2.5 °C
Load capacity: 1000 W max.
Power requirements: 100 VAC, 400 VA, 50/60 Hz

For Higher Sensitivity with the Hydride Generation Method

* Use a stepdown transformer in regions that do not have a 100 V power supply.

SARF-16C atomic muffle furnace
(Electronic Cell Heater)

208-97249

ComputerHVG-1 hydride vapor generator

Controller

Temperature sensor

Cell heater

Atomic absorption
spectrophotometer

Te

he

Mounting adaptor

For High-Sensitivity As, Se, Sb Analysis

HVG-1 hydride vapor generator 206-17143-XX

Environmental standards prescribe the hydride generation method as one
method of As, Se, and Sb analysis.

1. Used with the AA-7000 Series, HVG-1 permits the rapid and accurate
quantitation of elements such as As, Se, Sb and Hg at several-ppb levels.

2. Used with an ASC-7000 autosampler, it permits the automated serial
analysis of up to 60 samples.

* Nozzle ASSY, HVG (P/N: 206-67563) is required to use HVG-1 with an ASC-7000 Series

instrument. Order separately.

1. This dedicated furnace permits higher sensitivity measurements using the
hydride vapor generator than the flame heating method.

2. The temperature controller provides optimal control of the quartz cell
temperature.

3. Good temperature reproducibility. Extends cell life by preventing
damage due to overheating.

* The atomic muffler cannot be used when an AAC-7000 is installed on an AA-7000F/AAC
or AA-7000F.

Hydride vapor generator, absorption cell (P/N: 206-77607)
Reagent bottles (P/N: 206-58792-40/-42), gas hose, drain tube, etc.

Measurement method: continuous flow
Sample consumption: 0 to 7 mL/min, variable
Reagent consumption: 0 to 2.5 mL/min, variable
Atomizer: Heated absorption cell (heated by Air-C

2H2

flame in standard system)
Carrier gas: Ar pressure: 0.32 MPa, consumption: 70 mL/min
Power requirements: 100, 120, 220, 230, 240 VAC, 35 VA, 50/60 Hz
Dimensions: 340 W × 220 D × 200 H mm
Weight: Approx. 9 kg

I

Specifications

I

Standard Major Items

Required to add GFA-7000A to AA-7000F to conduct furnace analysis.
Permits automatic burner position setting for flame analysis with AA-7000F.

AAC-7000 auto atomizer changer 206-77701-41

Dual Atomizer System

For SR method

L-233 series

L-2433 series

200-38422-XX

200-38456-XX

Hollow Cathode Lamps

Used for analog output to a pen recorder, etc.
One cable required per channel (atomic absorption/energy signal, background signal).

Analog output cable 206-77707-91

Other Accessories

Part Name P/N Remarks

Part Name P/N Remarks

Part Name P/N Remarks

Part Name P/N Remarks

Part Name P/N Remarks

I

Specifications

22

For High-Sensitivity Hg Analysis

MVU-1A mercury vaporizer unit 206-58780-XX

This mercury vaporizer unit permits analysis using the reduction
vaporization –– atomic absorption method. It permits easy, high-sensitivity
water quality analysis.

Vaporization method: reduction vaporization with a reducing agent
Measurement method: recirculation
Flow cell: optical path length 100 mm (with quartz window)
Sample volume: 250 mL max.
Exhaust contamination prevention: adsorption trapping in mercury trap bottle
Dimensions: 310 W × 357 D × 288 H mm
Weight: Approx. 10 kg

I

Specifications

MVU-1A unit: 1
Reaction vial (P/N: 200-93018-01): 5
Reaction vial lid (P/N: 204-21989): 2
Stirrer tip (P/N: 046-00617-06): 10
Mercury trap bottle (P/N: 206-58777-42): 1

* Separately order the parts below.

s'ASFLOWCELL0.

s(OLDERFORGASFLOWCELL0.

s(GHOLLOWCATHODELAMP0. 

I

Standard Major Items

Part Name P/N Remarks

ICPE-9800 Series

ICP Emission Spectrometers

ICPE-9800 Series of simultaneous ICP atomic emission spectrometers offer
the superior accuracy necessary to simultaneously and quickly analyze
multiple elements regardless of their concentration levels. They also feature
user-friendly software that makes analysis easy. Various assistant functions
enable easy optimization of methods and a simpler, more efficient
analytical workflow.

Features
Eco mode, Mini-torch system, Vacuum spectrometer: reduce the argon gas
consumption
Vertical torch orientation: ensure stable low-maintenance analyses
1-inch CCD detector: capable of simultaneous recording of all wavelengths

Remarks

co mode, Mini-torch system, Vacuum spectrometer: reduce the argon

g

as

consumptio

n

V

ertical torch orientation: ensure stable low-maintenance analyses

-inch CCD detector:

cap

able of simultaneous recordi

f all wavele

ngth

s

23

Specifications

Basics

Main Unit

Flame

Furnace (GFA-7000A)

Wavelength range 185.0 to 900.0 nm

Aberration-corrected Czerny-Turner mounting, Number of grating grooves: 1800 lines / mm, Focal length: 300 mm

0.2, 0.7, 1.3, 2.0L nm (4-step automatic switching)

.

BGC-SR (high-speed self-reversal method) (185.0 to 900.0 nm)

.

BGC-D2 (D2 lamp method) (185.0 to 430.0 nm)

6-lamp turret, 2 lamps simultaneously lit (1 for measurement, 1 warming up for next measurement)

EMISSION, NON-BGC, BGC-D

2

, BGC-SR

Microsoft Windows 7 Professional / Vista Business / XP Professional

Wizard method

Flame continuous method, flame micro sampling method, furnace method, flame emission method

.

Calibration curve method (select primary, secondary, tertiary) .Standard addition method, simple standard addition method (primary expression)

Up to 20 repetitions. Mean value, standard deviation (SD) and coefficient of variation (RSD) display
Automatic exclusion of deviant values by setting SD and %RSD

Automatic correction of baseline drift by offset correction in peak height / peak area modes.

Automatic calibration curve correction function using sensitivity monitoring

Final concentration calculations based on sampled volume, dilution rate, fixed volume, and factor inputs

Template functions available

MRT (Measurement Results Table) worksheet

Summary report

Select whether to continue or discontinue measurements based on results of evaluation on coefficient of correlation,
%RSD, ICV.ICB, CCV.CCB, PB, LCS, SPK, PDS, and DUP.

Choose from 100, 120, 220, or 230 VAC, 50/60 Hz (Power is required separately for the personal computer.)

.

AA-7000F/AAC: 700 W × 588 D × 714 H mm, 76 kg .AA-7000F: 700 W × 588 D × 714 H mm, 73 kg

.

AA-7000G: 700 W × 580 D × 538 H mm, 66 kg

(Protruding parts and optional equipment are not included.)

10 to 35 °C, 20 to 80% (less than 70% when temperature is higher than 30 °C)

Monochromator

Bandwidth

Photomultiplier tube

Detector

Background correction method

Optical double-beam

Optics

Number of HC lamps

Lamp mode

Software requirements

Parameter setting

Measurement mode

Concentration computation mode

Repeat analysis

Baseline correction

Signal processing segments can be changed in peak height / peak area modes.

Signal processing segment setting

Sensitivity correction

2 channels (atomic absorption/energy signal, background signal)
Output range: 5.0, 2.5, 1.25, 0.625 Abs./V (each settable in 4 stages)
Fixed at 1 V F.S. in EMISSION mode.

Analog output

Tabular data processing

Recall of parameters

Procedure/result display

Report generation

QA/QC

Power requirements

Dimensions and weight

Ambient temperature / humidity

.

Select whether on not to conduct re-analysis.

.

Automatic dilution and re-analysis of unknown samples via autosampler (flame micro sampling method, furnace method)

Re-analysis

Digital recording

200, 220, 230, or 240 VAC ±5%, 7400 VA, 50/60 Hz

260 W × 560 D × 510 H mm, 47 kg

Power requirements

Dimensions and weight

Type

Burner head

Air-cooled pre-mix type

Titanium 10 cm slot (5 cm titanium slot for N

2

O-C2H2 flame available as an option)

.

Pt-lr capillary .PTFE orifice .ceramic impact bead (capable of handling hydrofluoric acid)

Engineering plastics

.

AA-7000F

.

Lateral/vertical manual adjustment

.

AA-7000F/AAC

.

Automatic flame/furnace switching by motor .Automatic search of optimum burner height

.

Automatic fuel gas flow rate setting (0.1 L/min step) .Automatic search of optimum gas flow rate

.

Automatic gas leak check

.

Automatic Air-N2O switching as C2H2 flow rate increases

.

Flame monitor

.

Prevention of wrong burner head use

.

Gas pressure monitor

.

Drain tank level monitor

.

Automatic flame extinction upon power outage or sudden power interruption

.

Automatic flame extinction via flame vibration sensor

.

Internal fan stop sensor

Nebulizer

Chamber

Positioning

Flow rate control

Safety measures

0 to 90° (Angle adjustment is not possible if the optional GFA-7000A is installed on the AA-7000F/AAC.)

Angle adjustment

Air-C

2H2

flame, N2O-C2H2 flame (Hydrogen flame is not applicable)

Type

Heating control system

Heating temperature range

.

Drying: Digital current control with automatic temperature calibration function

.

Ashing, Atomization: Digital temperature control via optical sensor

.

Ambient to 3,000 °C

.

Maximum 20 stages

.

Heating mode: RAMP/STEP

.

Inner gas type: Dual automatic switching type

.

High-sensitivity mode setting

.

Enrichment in furnace: Maximum 20 times

.

Optimum temperature program search support function

.

Inner gas flow rate: 0 to 1.50 L/min

.

Cooling water flow rate monitor

.

Gas pressure monitor

.

Overcurrent protection unit (double check by circuit protector and optical sensor)

.

Furnace block cooling check

.

AA-7000G

.

Lateral/vertical manual adjustment

.

AA-7000F/AAC

.

Automatic flame/furnace switching by motor

Setting heating conditions

Safety measures

Positioning

Optics

.

Management by login ID and password .Control user access authority by user level

.

Log record .Audit trail .Electronic signatures

Data
processing

Burner
unit

Gas
control

24

* Notes

.

The PC, monitor and printer are not included in the standard configuration. Prepare them separately.

.

The ASC-7000, ASK-7000 and GFA-7000A are optional accessories.

.

The separately available micro sampling kit is required for the flame micro sampling method.

.

Microsoft Windows 7 Professional / Vista Business and XP Professional are registered trademarks of Microsoft Corp., U.S.A.

.

The AA-7000 Series does not conform to IEC60601 –– Medical Electrical Equipment.

Flame Continuous Method

Required Software Operation Environment

Furnace Method / Flame Micro Sampling Method

Autosampler

Common Specifications

Functions Zero-point detection, auto diagnosis, auto rinse, random access

Sample volume Sample vials: 15 mL, reagent vials: 53 mL

Solvent rinse aspiration method

Sampler: 340 W × 280 D × 270 H mm, 8 kg
Controller (including stand): 260 W × 200 D × 320 H mm, 7 kg

Nozzle rinse

Dimensions and weight

Functions Zero-point detection, auto diagnosis, auto rinse, auto mixing, random access

Sample volume Sample vials: 2 mL, reagent vials: 20 mL

Solvent rinse discharge method

Sampler (including sliding parts): 340 W × 280 D × 400 H mm, 11 kg
Controller: 235 W × 110 D × 240 H mm (built into GFA-7000A), 6 kg

Nozzle rinse

Dilution function, reagent addition function

Sampling functions

250 μL

Syringe

2 to 90 μL

Injection volume

1%RSD (20 μL)

Repeatability

Rinse port: Less than 0.0001
Mixing port: Less than 0.00001

Carryover

Solvent rinse discharge method, solvent discharge and rinse with next sample

Mixing port rinse

Performed in mixing port. Maximum mixture volume: 0.6 mL

Mixing function

Up to 4 solutions
Number of solutions possible for mixing

.

Calibration curve method: 5 solutions max. (sample + 4 types of reagents)

.

Standard addition method: 6 solutions max. (sample + standard solution + 4 types of reagents)

Maximum number of
mixing reagents added

For measurement result on unknown samples:

.

If extrapolation of calibration curve is possible: automatic calculation of dilution rate and dilution to bring concentration within calibration curve range

.

If extrapolation of calibration curve is not possible: dilution rate fixed at 10x

Auto dilution / re-analysis

Dimensions and weight

Intel® Celeron 420 (1.60 GHz or higher)
To use GFA-TV, Intel

®

Pentium DualCore E2180 (2 GHz) or higher is required.

1 GB or higher (Vista) or 512 MB or higher (XP)
To use GFA-TV, 1 GB or higher (GFA-TV)

XGA (1024 × 768 dots) or higher

One CD-ROM drive (for installing a software)
Requires 60 MB min. hard disk space for AA installation.

One serial port (for AA control)
USB 2.0 port (for GFA-TV)

CPU

Microsoft Windows 7 Professional (32bit) / Vista Business / XP Professional

Operating system

RAM

Monitor

Storage device

I/O port

Monitor, keyboard, mouse, printerPeripheral device

Shimadzu recommends the PC and monitor in the PC Set for AA-7000 Series with WizAArd Software Pre-Installed.
Purchase a printer separately. The personal computer and monitor specifications are as follows.

RS-232C communication control from AA unitControl

Maximum reagent / sample positions

Rinse water bottle

Power requirements

Reagents: 8 positions Samples: 60 positions (random access available with reagents or samples)

2 L

Choose from 100, 120, 220, or 230 VAC, 50 VA, 50/60 Hz

25

26

Dimensions

Above dimensions do not include PC or printer.

Wall

870

588

465

280

200 max.

Table

Approx. 500 × 500

ø150 to ø200

714

1100 to 1200

390

960

700

Both for flame analysis and furnace analysis For furnace analysis

340

415

900 to 1000

960

415

ø150 to ø200

S=1: 2 0

Unit: mm

Damper

Damper

Exhaust fan

150 200

imensions

Above dimensions do not include PC or printer.

Wall

7

0

max.

Tabl

e

Appr

ox. 500 × 500

ø150 to ø200

1

00

to 1

200

960

700

Both for flame analysis and furnace analysi

s

or furnace analysis

340

41

5

to

1

000

960

4

ø150

to

ø200

S=10

nit: mm

amper

Dampe

r

xh

aust fan

200

Installation Conditions

27

Make sure all required equipment is available before starting instrument installation. See the installation guidelines for details.

*1 Atomic absorption spectrophotometer stand recommended
*2 Maintain a free maintenance space of 150 to 200 mm to the sides and rear of the instrument.
*3 Do not use pipes containing copper, silver, gold, mercury (or alloys containing these metals) as
pipes for acetylene.
*4 If tap-water equipment is used, ensure that it meets the specifications below.

Faucet 13 or 12 to 15 mm O.D. rimmed faucet

*5 If the supply pressure exceeds 0.17 MPa, use the optional Regulator ASSY.

10 to 30 °C

0.6 to 1.5 L/min

0.08 to 0.15 MPa

*5

7 mm min.

Example of recommended piping for the atomic absorption system

Stop cock

Stainless steel piping
(inner diameter greater than 7 mm)

Acetylene gas

Pressure regulator

Mist separator

Outdoor

Lab

80 mm max.

Argon gas

Dinitrogen
oxide gas

Pressure range 0.3 MPa
Setting pressure 0.09 MPa

Pressure range 1 MPa
Setting pressure 0.35 MPa

Pressure range 1 MPa
Setting pressure 0.35 MPa

Stop cock

Setting pressure 0.4 MPa

Setting pressure 0.4 MPa

Setting pressure 0.11 MPa

Air compressor

Setting pressure 0.4 MPa

Temperature range

Humidity range

Material

Dimensions

Acetylene

Air

Dinitrogen oxide

Argon

Material

Dimensions

Intake capacity

Gas tube

Cooling water (GFA-7000A)

Gas supply
pressure
(set secondary
pressure)

Testing bench

Operating
environment

10 to 35 °C

20 to 80% (less than 70% when temperature is higher than 30 °C)

1500 mm min. (W) × 700 mm min. (D)

Withstand load: 200 kg

*1, 2

Stainless

*3

7 mm min. I.D. × 80 mm min. (L)

Cylinder: 0.11 MPa

Lab: 0.09 MPa

Cylinder: 0.4 MPa

Lab: 0.35 MPa

Compressor: 0.4 MPa

Lab: 0.35 MPa

Cylinder: 0.4 MPa

Lab: 0.35 MPa

Stainless

For flame: Approx. 500 mm W × 500 mm D

For furnace: ø150 mm to ø200 mm

For flame: 600 to 1200 m

3

/hr

For furnace: 10 to 180 m

3

/hr

Cooling water circulation unit or tap-water equipment

*4

Compatible faucet

Water temperature

Water flow rate

Supply pressure

Supply port

Exhaust duct

Make sure all required equipment is available before starting instrument installation. See the installation guidelines for details.

*1 Atomic absorption spectrophotometer stand recommended
*2 Maintain a free maintenance space of 150 to 200 mm to the sides and rear of the instrument.
*3 Do not use pipes containing copper, silver, gold, mercury (or alloys containing these metals) a

s

pipes for acetylene.

*4 If tap-water equipment is used, ensure that it meets the specifications below.

F

aucet 13 o

r 12 to 15 mm O.D. rimmed f

aucet

*5 If the supply pressure exceeds 0.17 MPa, use the optional Regulator ASSY.

10

t

o 30 °C

0.6 to

1.5 L/m

in

0.08

to 0.15 MPa

*5

xample of recommended piping for the atomic absorption system

Stop cock

tainless steel piping

inner diameter greater than 7 mm)

A

cetylene ga

s

Pressure regulato

r

st separato

r

L

ab

80

mm max.

Argon gas

trog

en

oxide gas

g

Pressure range 0.3 MPa
Setting pressure 0.09 MPa

ressure range 1 MPa
etting pressure 0.35 MP

a

ressure range 1 MPa
etting pressure 0.35 MP

a

Stop cock

Setting pressure 0.4 MPa

Setting pressure 0.4 MPa

Setting pressure 0.11 MPa

Air compresso

r

etting pressure 0.4 MP

a

Temp

erature range

umidity range

ri

almensions

A

cetylene

initrogen oxide

Argon

ri

al

imensions

ntake capacit

y

tube

ooling water (GFA-7000A

)

Gas suppl

y

ressure

(set secondar

y

ressure)

Testing benc

h

Operating

e

nvironmen

t

0 to 35 °C

2

0 to 80% (less than 70% when temperature is higher than 30 °C)

1500 mm min. (W) × 700 mm min. (D

)

With

stand load: 200 kg

*1,

2

i

nles

s

*

3

7 mm min. I.D. × 80 mm min. (L

)

linder: 0.11 MPa

Lab: 0.09 MP

a

linder: 0.4 MPa

0.

3

5

MP

a

ompressor: 0.4 MPa

Lab: 0.35 MPa

linder: 0.4 MPa

Lab: 0.35 MPa

inl

ess

or flame: Approx. 500 mm W × 500 mm D

or furnace: ø150 mm to ø200 mm

or flame: 600 to 1200

m

3

/h

r

r furn

ace

: 10 to 180 m

3

/hr

Cooling water circulation unit or tap-water equipmen

t

*4

Compatible fauce

t

Water temperatur

e

W

ate

r flow r

ate

Supply pressure

Supply port

xhaust duct

AA- 7000 Series

Printed in Japan 3655-09416-30ANS

Company names, product/service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation or its
affiliates, whether or not they are used with trademark symbol “TM” or “®”.
Third-party trademarks and trade names may be used in this publication to refer to either the entities or their products/services. Shimadzu
disclaims any proprietary interest in trademarks and trade names other than its own.

For Research Use Only. Not for use in diagnostic procedures.
The contents of this publication are provided to you “as is” without warranty of any kind, and are subject to change without notice. Shimadzu
does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication.

© Shimadzu Corporation, 2014

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