Sartorius MC 410 S, MC 210 S, MC 210 P, MC 21S, MC 5 Installation And Operating Instructions Manual

...
98648-004-81
Sartorius Micro
Analytical, Semi-micro- and Microbalances Installation and Operating Instructions
0–0
Contents
General Views of the Balances: MC 210 S, MC 210 P and MC 410 S (-0CE) 1– 0 General Views of the Balances MC 5 (-0CE) and SC 2 (-0CE) 1– 2 Warranty 1– 4
Storage and Shipping Conditions 1– 4
Transporting the Balance 1– 5 Equipment Supplied 1– 7 Installation Instructions 1– 8 Using Verified Balances
Approved as Legal Measuring Instruments in the EU 1– 9
Getting Started 1–10 General Instructions for
“Analytical Weighing” 1–16
Weighing Electrostatically Charged Samples and Containers 1–16 Weighing Magnetic or Magnetizable Samples 1–17 General Instructions for Handling Samples and Containers 1–18
Operating the Balance 1–19 Balance Display 1–19 Turning the Display On and Off 1–20 Self-Test 1–20 Opening and Closing the Draft Shield 1–21 Simple Weighing 1–26 Taring 1–26 Weighing Range Structure 1–27 Weighing in the IQ-Mode 1–28
Mass Unit Conversion by Toggling
1–29 Displaying the Balance Model and the Serial Number 1–29
Calibration/Adjustment and Linearization Functions 1–30
Data Interface 1–36 Below-Balance Weighing 1–37 Fastening an Antitheft
Locking Device 1–37 Troubleshooting Guide 1–38 Care and Maintenance 1–40
Servicing 1–40
Cleaning the Balance Housing 1–40 Cleaning the Weighing Chamber 1–40
Safety Precautions 1–41
Balance Operating Menu 2– 1 Weighing in Three Ranges on Standard Balances 2– 7 Weighing in Two Ranges on Verified Balances Approved for Use as Legal Measuring Instruments 2–10 Display Modes for Standard Balances 2–11 Display Modes for Verified Balances Approved for Use As Legal Measuring Instruments 2–13 Calibration Functions on Standard Balances 2–14 Calibration Functions on Verified Balances Approved for Use as Legal Measuring Instruments 2–16 Utilities for Printouts or Data Transfer 2–18 Additional Functions 2–21
ISO/GLP-compliant Printout or Record 2–25
Setting the ID No./Date/Time 2–30
0–1
Application Programs 3– 1 Functions Common to
All Programs 3– 3
c Key 3– 3 Information and Printouts or Data Transfer 3– 4 Data ID Code K* or NUM 3– 4
“EUREKA” Air Buoyancy Correction Program 3– 5
Differential Weighing and Backweighing 3–14
Weighing Sequence 3–15 Selecting the Memories 3–17 Key Functions 3–18 Clearing the Memory 3–31
Density 3–34 Diameter Determination 3–42 Tare Memory 3–44 Weighing in Percent 3–47 Over/Under Checkweighing 3–51 Counting 3–55 Error Codes 3–59
Interface Description 4– 1
Pin Assignment Chart 4–19 Cabling Diagrams 4–20
Specifications 5– 1 English Translation of the EC Type-Approval Certificate for MC 5-0CE 5– 6
Accessories (Options) 5– 7
Declarations of Conformity 6– 1
Index 7– 1
Supplement:
Brief Operating Instructions
General View of the Balances: MC 210 S, MC 210 P and MC 410 S (-0CE)
1–0
1–1
1 Large draft shield cover
2 Small draft shield cover
3 Exterior draft shield element,
semicylindrical (can be moved by hand)
4 Interior draft shield door,
semicylindrical (can be moved by motor control or by hand)
5 Interior weighing chamber
draft shield only on MC 210 S, MC 210 P (-0CE)
6 Protective ring
7 Weighing pan
8 Protective disk
9 Leveling foot
10 Level indicator
11 Display unit
12 AC jack/power socket
13 Menu access switch
14 Data interface port
15 Terminal for connecting an
equipotential bonding conductor
16 Lug for attaching an antitheft
locking device
17 Metrological ID label for verified
balances approved for use as legal measuring instruments
18 Manufacturer’s label
19 Application display
20 Numeric keys
21 f function key
22 F function key
23 r and l draft shield
function keys
24 p Print key (data transfer)
25 Function display for the
f and F keys
26 t Tare key
27 Application program display
28 Weight display
29 w toggle key
30 Info key
31 ON/OFF key e
32 c key
33 Bar graph (range indicator)
34 Verification ID label with
metrological data for verified balances approved for use as legal measuring instruments
General View of the Balances: MC 5 (-0CE) and SC 2 (-0CE)
1–2
34
35 36 10
7 9
8
37
1–3
7 Weighing pan
8 Protective disk
9 Leveling foot
10 Level indicator
11 Display and control unit
12 AC jack
13 Menu access switch
14 Data interface port
15 Terminal for connecting an
equipotential bonding conductor
16 Lug for attaching an antitheft
locking device
17 Metrological ID label for verified
balances approved for use as legal measuring instruments
18 Manufacturer’s label
(on bottom of balance)
19 Application display
20 Numeric keys
21 f function key
22 F function key
23 r and l draft shield function keys
(for opening and closing)
24 p Print key (data transfer)
25 Function display for
the f and F keys
26 t Tare key
27 Application program display
28 Weight display
29 w toggle key
30 Info key
31 ON/OFF key e
32 c key
33 Bar graph (range indicator)
34 Draft shield
35 Weighing cell
36 Inner draft shield
37 Below-balance weighing port
38 Male connector on weighing cell
39 Male connector on computing
device
40 Electronic computing device
Please read these installation and operating instructions carefully before you begin to operate your new balance.
Warranty
Do not miss out on the benefits of our full warranty. Please contact your local Sartorius office or dealer for further information. If available, complete the warranty registration card, indicating the date of installation, and return the card to your Sartorius office or dealer.
Storage and Shipping Conditions
Allowable storage temperature: +5°C ... +40°C
+41°F to +104°F
The complete packaging has been designed to ensure that the balance will not be damaged even if it is dropped from a height of 80 cm (about 31 inches).
After unpacking the balance, please check it immediately for any visible damage as a result of rough handling during shipment. If this is the case, proceed as directed in the section entitled “Safety Inspection.”
Save all parts of the packaging and the box for your balance to avoid damage during transportation. Ship your balance only in the complete original standard packaging supplied.
The packaging consists of the following: – 2 boxes – 3 polystyrene inserts – 2 polypropylene pads
The inner packaging is not suitable for shipping because it provides the balance little protection from blows. Before packing your balance for shipment, unplug all connected cables to prevent damage.
Do not expose the balance unnecessarily to extreme temperatures, moisture, shocks, blows or vibrations.
1–4
Transporting the Balance
To transport the balance, lift it by the housing base using both hands. Never lift your balance by grasping the display unit or the draft shield!
Transport Arrestment
Before unplugging the balance from the power supply or unplugging the connecting cable, turn off the balance using the e key (31). For MC5 (-0CE) and SC 2 (-0CE): After approximately 10 seconds, the balance will be arrested, or locked, for transportation. While the balance is raising the weights after you have turned it off, the symbol “Mot” from a calibration or linearization procedure is displayed.
Warmup Time
Condition your balance for 12 hours to the temperature of a new location. After initially connecting the balance to AC power (or after a relatively long power outage), allow it to warm up for at least 2 hours.
Each time you move your balance to another location, you must condition it for at least 12 hours to the new location. After initially connecting the balance to AC power (or after a relatively long power outage), allow the balance to warm up for at least 2 hours.
1–5
Note to Users of Verified Balances Approved for Use as Legal Measuring Instruments:
Linearization after Transport
After transport, the linearity and calibration of your balance may be out of the permissible tolerances (see the “Specifications”). Always carry out internal
linearization of the balance after transport.
Repeating this procedure – several times, if necessary – enhances the linearization. This procedure is described on page 1–35.
Preparing a Verified Balance for Use as a Legal Measuring Instrument: After initially connecting the balance to AC power (or after a relatively long power outage), allow it to warm up for at least 24 hours.
1–6
Equipment Supplied
The equipment supplied includes the components listed below:
MC 210 S, MC 210 P and MC 410 S (-0CE)
– Weighing cell – AC adapter – Weighing pan – Protective disk – Protective ring – Interior weighing chamber draft shield – 2 draft shield covers – Dust cover for the draft shield and the
balance housing
– Dust cover for the display unit
MC 5 (-0CE) and SC 2 (-0CE)
– Weighing cell – Draft shield – Electronic computing device – Connecting cable – Power supply – Kit of standard accessories – Inner draft shield (models SC 2 and SC 2-0CE only)
The kit of standard accessories contains the following: – Weighing pan – Protective disk – Brush – Forceps – Lint-free cloth
MC 21 S
– Weighing cell – Electronic computing device – Connecting cable – Power supply – Protective disk – Protective ring – Weighing pan
1–7
Installation Instructions
Ambient Conditions
Before you set up your balance, choose a suitable place which meets the following requirements:
– level, low-vibration weighing table
or a wall console;
– no direct exposure to sunlight, heaters, or similar
sources of heat. This can considerably increase the temperature inside the draft shield (greenhouse effect), resulting in incorrect readouts due to convection currents, turbulence and buoyancy effects;
– no drafts from open windows or doors;
– avoid brief fluctuations in room temperature.
The balance is not allowed to be used in hazardous areas/locations where there is danger of explosion.
Do not expose the balance to extreme moisture over long periods. Moisture in the air can condense on the surfaces of a cold balance whenever it is brought to a substantially warmer place. If you transfer the balance to a warmer area, make sure to condition it for about 2 hours at room temperature, leaving it unplugged.
1–8
Using Verified Balances Approved as Legal Measuring Instruments in Europe (only applies to MC5-0CE)
Using Verified Balances as Legal Measuring Instruments You must calibrate the balance at the place of installation before using it as a legal measuring instrument (see the section entitled “Calibration/
Adjustment” starting on page 1–31).
This balance is not allowed to be used for weighing goods intended for direct sale to the public. The type-approval certificate for verification applies only to non-automatic weighing instruments; for automatic operation with or without auxiliary measuring devices, you must comply with the regulations of your country applicable to the place of installation of your balance. A suitable thermometer and barometer are recommended for monitoring ambient conditions.
For balances of accuracy class k, a thermometer and barometer are recommended for monitoring ambient conditions. The temperature range indicated on the verification ID label must not be exceeded during operation.
The balance must warm up for at least 24 hours
after initial connection to AC power or after a relatively long power outage.
The legal background for using Sartorius balances in legal metrology is the EC Council Directive No. 90/384/EEC for non-automatic weighing instruments, which has been in effect since January 1,1993, within the Internal European Market, as well as the accreditation of the Quality Management System of Sartorius AG by Lower Saxony’s Regional Administrative Department of Legal Metrology (Niedersächsische Landesverwaltungsamt – Eichwesen) from February 15, 1993.
1–9
Getting Started
MC 210 S, MC 210 P and MC 410 S (-0CE):
Place the components listed below inside the
weighing
chamber one at a time in the order given: – Shield disk (8) – Weighing pan (7) – Protective ring (6) – Interior weighing chamber draft shield (5)
(only on MC 210 S, MC 210 P (-0CE))
– Place the small draft shield cover (2) on top of the
semicylindrical interior draft shield door (4).
Then place the large draft shield cover (1) on top of the semicylindrical exterior draft shield element (3). Secure the draft shield cover in place using the fastener (see arrow).
Important Note Concerning Verified Balances Approved for Use as Legal Measuring Instruments:
Provided that an official lead seal is required for the verified balance, a control seal is affixed to the balance. Unauthorized attempts to remove this seal will irreversibly damage it. If you break the seal, the validity of the verification will become void, and you must have your balance subsequently verified.
1–10
Adjusting the Exterior Draft Shield Element
Turn the exterior draft shield element (3) by the riffled part on the bottom to the position you desire. Depending on your application, you can define the menu code so that the interior draft shield door (4) is operated by motor or by hand (see section starting on page 1–21).
Adjusting the Swivel-Mounted Display Unit
Move the swivel-mounted display unit (11) around the base of the draft shield to adjust it to the position you desire (+/– 85°).
MC 21S:
Installing the Components
§ Place the following components on the balance in the order given below:
– Shield plate
– Weighing pan
Note: To position the weighing pan, rotate it back and forth while pressing down gently.
– Protective ring
– Glass plate
1–11
MC 5 (-0CE) and SC 2 (-0CE):
Assembling the Components
§ Place the components listed below on the
weighing cell (35) one at a time in the order given: – Protective disk (8) – Weighing pan (7)
Important Note: After placing the weighing pan on the weighing cell, press down on it gently while turning it slightly to the left and right.
– Inner draft shield (36) (models SC 2 and
SC 2-0CE only)
Installing and Adjusting the Draft Shield
– Place the small draft shield (34) on the weighing cell
and adjust it so that the gap fits over the projection on the weighing cell (see arrows).
Connecting the Weighing Cell to the Computing Device
Connect these two units so that the two points where the connecting cable is attached to the female connectors face each other (see arrows). Tighten the screws on the female connectors by hand.
1–12
Connecting the Balance to AC Power
The balance is energized by a power supply/AC adapter. Make sure that the voltage rating printed on this unit is identical to your local line voltage.
If the voltage specified on the label or the plug design of the power supply/AC adapter does not match the rating or standard you use, please contact your Sartorius office or dealer.
Important Note:
Use only original Sartorius power supplies/AC adapters. Use of power supplies/AC adapters from other manufacturers, even if these units have an approval identification marking from a national testing laboratory, requires the consent of an authorized Sartorius service technician.
Detailed information on additional options for powering the balance is available in our service information bulletin, no.15/88 (for example, using local extra-low voltage).
Plug the cord of the AC adapter/power supply into the DC jack on the rear panel of the balance/computing device. Then insert the plug
of
the power supply or the AC adapter into a wall outlet.
1–13
Voltage Selection
You can select the voltage if you use our portable power supply (6971172) that has a European-type plug (rounded prongs).
Safety Precautions
The power supply/AC adapter rated to Class 2 can be plugged into a wall outlet without taking any additional safety precautions. The pole of the output voltage is connected to the balance housing, which can be grounded for operation.
The data interface (see also “Interfacing Devices” on page 1–36) is also electrically connected to the balance housing (ground).
Information on Radio Frequency Interference Warning!
This equipment generates, uses and can radiate radio frequency energy and,if not installed and used in accordance with the instruction manual, may cause interference to radio communications. It has been tested and found to comply with the limits for a Class A computing device pursuant to Subpart J of Part 15 of FCC rules, which are designed to provide reasonable protection against such interference, when operated in a commercial environment. Operation of this equipment in a residential area is likely to cause interference, in which case the user at his own expense will be required to take whatever measures may be required to correct the interference.
Connecting Electronic Devices (Peripherals)
Make sure to unplug the balance from the power supply/AC adapter before you connect or disconnect a peripheral device (printer or PC) to or from the interface port.
1–14
230 V~ 115 V~
Leveling the Weighing Cell Using the Level Indicator
At the point of use, level the weighing cell using the leveling feet (9) so that the air bubble is centered within the circle of the level indicator (10).
To level the weighing cell using the level indicator as a guide: Extend the leveling feet (turn clockwise) to lift the weighing cell. Retract the feet (turn counterclockwise) to lower the weighing cell.
1–15
General Instructions for “Analytical Weighing”
Weighing Electrostatically Charged Samples and Containers
Major measuring errors can occur when electrostatically charged samples and containers are weighed. This problem particularly involves samples that have an extremely poor electrical conductivity (glass, plastic, filters) since they can discharge electrostatic – i.e., friction-induced – charges only over a relatively long period of time. The result is an interaction of forces among the charges adhering to the sample and the stationary components of the balance (base plate of the weighing chamber, draft shield construction, balance housing). This is noticeable when the weight readout drifts. At a high humidity, this effect is not so pronounced or does not even occur at all due to the thin layer of water that condenses on the sample and, through conductive discharge, counteracts interfering static electricity.
In addition to taking purely mechanical counteractive measures (protecting the sample using a special antistatic weighing pan – see the “Accessories”), you can neutralize the surface charges by “bombarding” them with ions of the opposite polarity. This is an extremely effective method of eliminating static electricity on surfaces (antistatic ionizing blower, order no. YIB01).
The balance’s environment, including the operator, can considerably interfere with weighing on account of static electricity. The balances of the MC Series have been designed to counteract this phenomenon: the glass surfaces of the draft shield have a special metallic coating.
The rear panel of the balance/weighing cell has a terminal (15) for connecting an equipotential grounding conductor. It is used for additionally grounding a peripheral device (for example, a vibrating spatula). This terminal is designed for single grounding wires up to .25” standard gauge or 6 mm2and for .18” standard gauge or 4 mm
2
stranded wires.
1–16
Weighing Magnetic or Magnetizable Samples
It is technically impossible to avoid the use of magnetizable materials in the manufacture of balances. Ultimately, the operating principle of high-resolution balances is based on electromagnetic force compensation of the load placed on the weighing pan.
When magnetic or magnetizable samples or containers (e.g., beaker with a stirrer) are weighed, interactions among the above-mentioned components of the balance may occur, distorting weight readouts. Unlike deviations caused by electrostatic charges, magnetic interference is usually constant over time. However, it is sensitive to and depends on the position of the sample or container on the weighing pan and is also characterized by poor reproducibility.
To reduce the effect described above, we recommend increasing the distance between the sample and the weighing pan by using a non-magnetizable material (the reduction in force is proportional to the quadrate of the distance). In special cases, soft-magnetic plates should be used to shield against interfering magnetic effects.
In the presence of extremely strong magnetic fields – for instance, when measuring the susceptibility of a sample in an electromagnet – you should use the below-balance weighing port which comes standard on your balance.
1–17
1–18
General Instructions for Handling Samples and Containers
As a general rule, the sample to be weighed should be conditioned to the temperature of the balance. This is the only way to avoid air buoyancy errors and deviations caused by convection currents at the surface of the sample. Since these effects increase proportionally to the volume and surface of the sample, make sure that the size of the tare vessel selected is in the appropriate proportion to the size of the sample to be weighed.
Never use your bare hands to touch samples to be weighed. In addition to the effect on the temperature, the extremely hygroscopic behavior of fingerprints left on the sample will cause considerable interference during weight measurement. Use forceps or other suitable utensils to place your sample carefully on the pan.
Working with your balance requires a steady hand and a smooth, uninterrupted technique.
Perform a few trial weighing operations before you begin with the actual weighing of your sample because the temperature in the weighing chamber
may differ from that of the balance’s surrounding environment, if the weighing chamber has not been opened for a relatively long period.
When you open the weighing chamber, a change in temperature will inevitably occur, due to the laws of physics, and may show up as a change in the weight readout. In this case, we recommend that before you begin
the actual weighing series you
open and close the
weighing chamber at the same
rate as you will be doing during weighing.
After the weighing chamber has been closed, the weight readout will usually stabilize after about 10 seconds. The accuracy of the weight readout will increase as you perform successive weighing procedures with greater consistency.
Operating the Balance
Balance Display
The display shows the following special codes for your information:
OFF
The balance was disconnected from AC power
(power failure or outage; the balance was reconnected
to AC power).
O (standby)
The display has been turned off by the e key (31). The balance is now in the ready-to-operate mode.
b (busy)
Once you have turned on the balance, the b symbol will be displayed until you press a key. During operation, this symbol indicates that the balance processor is still busy processing a function and will not accept commands to perform any other functions at this time.
CAL I
The balance has internal calibration weights and can be calibrated using the f key.
R1 W or R2 W The number in the R code identifies the particular weighing range you have selected.
W
Symbol for the application selected (in this case, the weighing mode and toggling among the weighing ranges).
Important Note: If the W symbol flashes, this means that the balance
wants to self-calibrate (see pp.1–30).
1–19
Turning the Display On and Off (Standby Mode) Press the e key (31) to turn the display on or off.
Self-Test
After the balance has been turned on, an automatic self-test of the balance’s electronic circuitry is performed, and the draft shield closes automatically. When a zero readout is displayed, the balance is ready for operation.
Automatic Warmup of the Balance Electronics in MC 210 S, MC 210 P and MC 410 S (-0CE), MC 21 S
Once you have connected the balance to AC power and turned on the power, the balance’s electronics automatically begin to warmup. The timer for warmup is set to 4 minutes. The remaining warmup time in minutes and seconds is displayed in a countdown mode.
When the remaining time displayed is less than one minute, you can interrupt this warmup procedure by pressing the e key to turn the balance off and back on again. Following the self-test and display of a zero readout, the balance is ready to operate again.
After 4 minutes have elapsed, the balance displays a zero readout and is then ready to operate.
* = including the Signatories of the Agreement on
the European Economic Area
Important Note Concerning Verified Balances Approved for Use as Legal Measuring Instruments in the E.U.*
For verified balances that have a verification scale interval “e” which is greater than the scale
interval “d,” and a scale interval “d” 0.1 mg,
the last digit on the display is bordered.
1–20
Opening and Closing the Draft Shield
MC 210 S, MC 210 P or MC 410 S (-0CE):
To load small objects, open the draft shield only as far as is absolutely necessary for your application. This reduces the amount of draft so your balance will stabilize faster than it normally does when the draft shield is wide open. You have several options for operating the interior draft shield door (4):
– Semi-automatically using the l or r key (23)
(max. aperature angle: 170°)
– Using an external foot or hand switch
(see part 5, “Accessories”)
– By a command from an on-line computer
(see part 4, “Interface Description”)
– Fully automatically, e.g., for the functions tare,
calibration, print, etc. (see part 2, “Balance Operating Menu”)
– With a special display mode while the draft shield
is open (see part 2, “Balance Operating Menu”)
– Manually
Semi-automatic Mode with an Aperture Angle of 10° to 140°
By a “self-teaching” function, the draft shield door can “learn” to open automatically to a user-defined aperture angle between 10° and 140°:
To define this angle, manually move the interior draft shield door (4) to the desired position.
1–21
Press either l or r to close the draft shield automatically by motor. While closing, the interior draft shield door moves slowly. The previously adjusted aperture angle is stored.
If you press either l or r once again, the draft shield door will open at a faster speed to the position you have selected. Press l or r for approx. 2 seconds to open the draft shield door
automatically
as far as it will go (170°).
You can always change the aperture angle by manually adjusting the position of the draft shield door.
Important Note
The aperture angle remains stored even after you have turned off the display by pressing e. A stored aperture setting will not be erased until you unplug the balance from AC power.
Manual Mode
Of course, you can also open and close the draft shield door by hand.
1–22
MC 5, SC 2 (-0CE):
You can operate the motorized draft shield (34) in one of the following ways:
– Semiautomatically using the l or r key (23)
(aperature angle approx.100°)
– Using an external foot or hand switch
(see part 5, “Accessories”)
– By a command from an on-line computer
(see part 4, “Interface Description”)
– Fully automatically, e.g., for the functions tare,
calibration, print, etc. (see part 2, “Balance Operating Menu”)
– With a special display mode while the draft shield
is open (see part 2, “Balance Operating Menu”)
– Manually
1–23
Semi-automatic Mode with the Aperture Angle of Your Choice
To define the aperture angle and the direction in which the draft shield opens, move the draft shield to the desired position manually (aperture angle 45° to 315°).
Press either the l or r key (23) to have the draft shield closed by motor. The previously adjusted aperture angle and the direction are stored in the
process. You can always change the aperture angle by manually adjusting the position of the draft shield.
You can clear the aperture angle by either – entering an aperture < 45° using the numeric keys
(e.g., “0”) and confirming this entry by pressing
the l or r key or – by closing the draft shield manually
Important Note:
The aperture angle and the direction in which the draft shield opens remain stored even after you have turned off the display using the e key. This information will not be erased until you unplug the balance from AC power.
1–24
Numeric Entry of an Aperture Angle
The numeric entry of an aperture angle corresponds to a fixed position. The aperture is measured counter­clockwise starting from the closed draft shield position:
– Enter an aperture angle between 45° and 315°
using the numeric keys (20); e.g., 210
– Confirm this entry by pressing either the
l or r key (23), depending on the direction you wish the draft shield to open
– The aperture angle and the direction are now
stored for further operation
You can clear the aperture angle by either – entering an aperture < 45° using the numeric
keys (e.g., “0”) and storing this entry by pressing
the l or r key or – by closing the draft shield manually
Important Note:
The aperture angle and the direction in which the draft shield opens remain stored even after you have turned off the display using the e key. This information will not be erased until you unplug the balance from AC power.
Opening and Closing the Draft Shield Manually
Of course, you can also open and close the draft shield by hand.
Important Note:
An open draft shield will always close automatically if you have not operated the balance for 1 minute.
!
Exception: – It will not close automatically if you have set menu
code 8 8 1 “Automatic draft shield function off”
(see part 2, “Balance Operating Menu”)
1–25
Simple Weighing
Place your sample on the weighing pan (7), and close the draft shield door. Read off the weight indicated on the display (28) only after the weight unit (“g”, or a different
unit selected – see part 2, “Balance
Operating Menu”)
appears as the stability symbol.
Taring
If you wish to use a container or if the weight display does not indicate 0.000 mg (depending on the display mode or weight unit selected), zero the display before you weigh.
To do so, press t key (26).
During taring, you can have the fully automatic draft shield function either on or off.
For more information on turning this fully automatic draft shield function on or off by menu code, refer to part 2, “Balance Operating Menu.”
Important Note for Verified Balances Approved for Use as Legal Measuring Instruments:
The small circle in the weight display (on the left) shows that the balance is exactly tared to “0” (± 0.25 of a scale interval).
Important Note Concerning Verified Balances of Accuracy Class k
To avoid measuring errors, the respective air density must be allowed for. The following formula is used to calculate the mass of the sample:
1– ρL/8000 kg m
–3
m = n
w
1– ρL/ρ
m = mass of the sample nw= weight readout
ρ
L
= air density during weighing
ρ = density of the sample
1–26
Weighing Range Structure SuperRange “Single Wide-Range”
(identified by S in the model name MC.....S)
SuperRange models have an extraordinarily high resolution; i.e., the weighing range has a resolution ranging from100,000 to a few million digits. There is one level of fine readability for the entire weighing range (for example: 0.01 mg).
PolyRange “Multi-Interval”
(identified by P in the model name MC.....P)
Wide weighing range with multiple levels of accuracy that change as the load increases or decreases
The PolyRange function divides the weighing range into as many as 4 ranges, each with a different readability. In the various ranges, the readability will adjust so that the last numeral of a weight readout is displayed with a resolution of 1, 2 or 5 digits. After you have pressed the tare key (26), you will obtain the highest possible resolution, even when the balance is loaded.
1–27
210 g 0.05 mg
110 g 0.02 mg
60 g 0.01 mg
- 0.00 mg -
210 g 0.01mg
Weighing in the IQ-Mode*
(Load-Dependent Readability)
In the IQ-mode, weighing is done with a load­dependent readability of, e.g., 0.01% (for different settings, see part 2, “Balance Operating Menu”) throughout the entire weighing range of the balance.
Oftentimes, a display accuracy of 10 mg is sufficient for a load of approx. 110 g. In this case, it makes sense to select weighing range R 1 with an accuracy of 0.01% by pressing the w key (29). While you are filling up to a target weight, it is certainly easier to work with a target of 110.20 g than with an absolutely accurate readout of 110.19885 g.
* = not with verified models; other settings in
the balance operating menu are necessary on model MC 5
1–28
Mass Unit Conversion by Toggling
You can have the weight displayed in milligrams or grams.
To select the weight units one after the other, press the w key (29) each time.
In addition to milligrams and grams, the standard balances give you a wide variety of other menu­definable international weight unit options. For more information, refer to part 2, “Balance Operating Menu.”
Displaying the Balance Model and Serial Number on the Weight Display
– Turn off the balance display – Turn it back on – While all segments are displayed, briefly press
the p key (24)
– The balance model is displayed
(example: model “MC 5”)
– Press the c key (32) to have the serial
number displayed
– Press c to quit this function
1–29
Calibration/Adjustment and Linearization Functions
During calibration, the span* of your balance is adjusted to changes in ambient conditions.
Relinearize your balance each time you set it up in a different area or recalibrate (re-adjust) it when the ambient conditions change (for example, temperature or barometric pressure). Even if these conditions are constant, the balance should be calibrated once a day. To meet the highest requirements for accurate weighing, we recommend that you calibrate the balance before each weighing series or set the isoCAL self-calibrating function to “ON.”
W : Self-calibrating Function “isoCAL”
The criteria for fully automatic calibration are as follows: – Two hours have passed since the balance was
turned on (“cold start”)
– The difference between the current temperature and
the temperature during the last calibration procedure is greater than ± 1° Kelvin
– (Up to) four hours have passed since the last
automatic calibration
Flashing W Symbol
If the W symbol flashes, the balance wants to self­calibrate. You do not need to interrupt your weighing series; the balance will wait until you have unloaded the weighing pan and have not used the balance for one minute before performing internal self-calibration. During this procedure, the draft shield must be closed to ensure that calibration is done correctly. The symbol flashes until the balance begins self-calibration or until you activate one of the calibration functions manually (see next page).
To turn off the self-calibrating function by menu code, refer to part 2, “Balance Operating Menu.”
* = The difference between the indication of a weight
at maximum capacity and the indication at zero
1–30
The balance offers you various calibration and linearization functions.
You can interrupt any calibration or linearization procedure by pressing the c key (32).
In the fully automatic mode, the draft shield closes after the f or the t key has been pressed.
Important Note:
! During calibration or linearization, you must observe
the following:
– Unload the weighing pan – Do not disconnect the balance from AC power – Do not unplug the connecting cable
Important Note to Users of Verified Balances Approved for Use as Legal Measuring Instruments:
Internal Calibration CAL Function Using the f Key:
Unload the pan and tare (if necessary, close the draft shield). When the balance shows a zero readout, press the
f key (21). “C” will now be displayed. The built-in calibration
weights are internally applied by servomotor and removed at the end of calibration.
If external interference affects the calibration procedure, you may obtain a brief display of the error message “Err 02. In this case, tare and then press the f key again when a zero readout appears.
An acoustic signal indicates the end of calibration.
Before using your balance as a legal measuring instrument, you must carry out the internal calibration function at the place of installation (see below).
1–31
Internal Calibration Using the Tare Key:
Calibrate the balance using the tare key if an application program (such as the tare memory) is assigned to the f key by menu code in the balance operating menu (see parts 2 and 3).
Press the tare key (26) for at least 2 seconds until “C.I.” and “CAL” are displayed (next to the f key). Unload the pan and tare (if necessary, close the draft shield).
When the balance displays a zero readout, press the f key (21). “C” will now be displayed. The built-in calibration weights are internally applied by servomotor and removed at the end of calibration. If external interference affects the calibration procedure, you may obtain a brief display of the error message “Err 02. In this case, tare and then press the f key again when a zero readout appears.
An acoustic signal indicates the end of calibration.
External Calibration (with Numeric Entry of the Weight 5 g/200 g ±2%)
Use only calibration weights that have tolerances equal to or better than those of accuracy class E2.
How to unlock the access switch on verified balances approved for use as legal measuring instruments:
Remove the protective cap from the rear panel of the computing device and move the menu access switch (13) in the direction of the arrow.
Press the t key (26) for at least 2 seconds, until “C.I.” and “CAL” are displayed (next to the f key).
1–32
For “external calibration,” press the F key (22) until “C.E.” is displayed.
C.E.stands for “external calibration.”
Unload the weighing pan (7) and tare (close the draft shield).
Press the f key (21) when a zero readout is displayed. Afterwards, the calibration weight readout will be in grams.
If external interference affects the calibration procedure, you may obtain a brief display of the error message “Err 02. In this case, tare and then press the f key again when a zero readout appears.
Numeric Entry of a Value Listed on a Weight Certificate (5 g/200 g ±2%)
If you are using a certified calibration weight, enter the exact weight value specified using the numeric keys (20). Then press the f key identified on the
display by “STO” to store this
value (only possible
within the given limits).
Center the calibration weight on the weighing pan (7) and close the draft shield.
An acoustic signal indicates the end of calibration.
1–33
Calibration Test
The calibration test is carried out with internal weights as follows:
– MC 210 S and MC 210 P (-0CE)
with approx. 170 g – MC 410 S (-0CE) with approx. 300 g – MC 5 (-0CE) with approx. 5 g – SC 2 (-0CE) with approx. 2 g
Press the tare key (26) for at least 2 seconds until “C.I.” and “CAL” are displayed (next to the f key).
Select the calibration test by pressing the F key (22) twice until “C.t.” is displayed.
Unload the balance and tare (close the draft shield). C.t.stands for “calibration test. When the balance displayes a zero readout, press
the f key (21). The built-in calibration weights are now internally applied by servomotor. Afterwards, the deviation of the momentary weight readout from the target weight (displayed in grams only) is indicated.
If external interference affects the calibration test procedure, you may obtain a brief display of the error message “Err 02.” In this case, tare and then press the f key again when a zero readout is displayed.
The balance should be adjusted (calibrated) if the devi­ation in the weight measurement no longer meets the accuracy requirements of your particular application.
f key: The balance is automatically calibrated
(see also page 1–31)
or
F key: Quits the calibration test
An acoustic signal indicates the end of the sensitivity test.
Important Note:
For the setting “CAL calibration test using the f key” see part 2, “Balance Operating Menu.”
1–34
Internal Linearization Press the t key (26) for at least 2 seconds until
“C.I.” and “CAL” are displayed (next to the f key).
Select “internal linearization” by pressing the
F key (22) several times until “L.I.” is displayed.
Unload the balance and tare (close the draft shield). L.1.stands for “internal linearization.
When a zero readout is displayed, press the f key (21). “C” will now be indicated. The built-in weights are internally applied one after the other by servomotor, and the balance is automatically linearized.
If external interference affects the linearization procedure, you may obtain a brief display of the error message “Err 02.” in this case, tare and then press the f key again when a zero readout appears.
An acoustic signal indicates the end of linearization.
Important Note: The balance automatically self-calibrates after each
internal linearization procedure.
1–35
Data Interface
If you wish to record weight data using a Sartorius Data Printer, plug the printer connector into the interface port (14) of the balance. You do not need to adjust any settings.
Important Note for Verified Balances Approved for Use as Legal Measuring Instruments:
Make sure to unplug the balance from the power supply (12) before you connect or disconnect
a peripheral
device (printer or PC) to or from the
interface port (14).
To print data on hard copy or output them on the screen of an on-line computer, press the p key (24).
For information about special data output parameters, see
part 2, “Utilities” of the Balance Operating Menu.
For details on the data interface, see part 4, “Interface Description.”
Interfacing Devices with the Balance
Please note that the interface port is electrically connected to the protective grounding conductor of the balance housing. The interface cables supplied as standard equipment are shielded, and both ends of each cable are electrically connected to the connector cases. This connection may result in interference caused by ground loops or by transient currents if you have grounded the housing or connected the protective grounding conductor for AC power. If necessary, connect an equipotential bonding conductor to the balance.
When using the balance as a legal measuring instrument, you may connect to it only auxiliary devices that are legally permitted.
1–36
001: + 1608,628 mg 002: + 608,715 mg 003: + 722,744 mg 004: + 1722,655 mg
Below-Balance Weighing
A port with a below-balance weighing hanger is available on the bottom of the balance.
To hook a sample on the hanger, open the below-balance port by removing the two screws from the bottom of the balance and detaching the cover plate and gasket.
Now you can attach a sample using a suspension wire, for example. You also have to install a shield to protect against drafts.
Fastening an Antitheft Locking Device
Use the lug (16) located on the rear panel of the weighing cell to secure the weighing cell with a chain or a lock at the place of installation.
Important Note for Verified Balances Approved for Use as Legal Measuring Instruments:
The below-balance weighing port may not be opened when an approved balance is being operated as a legal measuring instrument.
1–37
Troubleshooting Guide
Problem... Causes... Solution
No segments appear – No AC power available
Check the AC power supply
on the weight
The power supply/AC adapter
– Plug in the power
display (28) is not plugged in supply/AC adapter
The weight display – The connecting cable is – Plug in the female shows “Err 235” not plugged in correctly connectors correctly and
secure them by tightening the screws
– The computing device or the – Connect the units that
weighing cell was switched belong together with a unit from another balance
The weight display – The weighing pan (7) is not – Position the pan and then shows “Err 54” in place press down on it gently or “L” while turning it slightly to
the left and right
The weight display – The load exceeds the – Unload the balance shows “H” capacity of the balance
The weight display – The value that should appear
Set the appropriate code in
shows “Err 01” cannot be displayed
the balance operating menu
The weight display – The display did not show – Press the t key first, briefly shows a zero readout when
then press the f key again
“Err 02” the f key (21) was pressed
to calibrate
– The balance is loaded – Unload the balance
The weight display – The balance is in the warmup – After plugging the briefly shows phase balance into AC power, “Err 03”or “Err 04” condition it for 12 hours
– The weighing system – Set up the balance in
is affected by drafts another area or vibrations
The weight display – The function activated is not – Unlock the menu shows “Err 07” allowed on a verified access switch
balance used as a legal measuring instrument
1–38
Problem... Causes... Solution
The special code “C” – The balance is not ready to – After plugging the does not go out on calibrate or is in the balance into AC power, the weight display (28)
warmup phase allow for at least
2 hours’ warmup
– The weighing system – Access the menu to select
is affected by drafts the correct code for the or vibrations weighing environment
– The draft shield is not closed – Check draft shield
function and close
– The port for the below- – Fasten the cover plate to
balance weighing close the port for below­hanger is open balance weighing
The special – None of the keys has been – Press a key code b” does not pressed since the balance go out on the weight was turned on display
The weight readout – Unstable ambient conditions – Set up the balance changes constantly in another area
– Too much vibration or the
Access the menu (see part 2)
balance is exposed to a draft
to select the correct code for
the weighing environment
– The draft shield is not – Close the draft shield
completely closed
– A foreign object is caught – Remove the foreign
below the pan object
– The port for the below- – Fasten the cover plate to
balance weighing hanger close the port for below­is open balance weighing
– The sample does not have a
stable weight (absorbs moisture or evaporates)
The weight readout – The balance is not calibrated
Calibrate (see pp.1–30 f.)
is obviously wrong – The balance was not tared – Tare before weighing
before weighing
– The air bubble in the level – Level the weighing cell
indicator (10) is not within (see page 1–15) the circle
1–39
Care and Maintenance
Servicing
Regular servicing by a Sartorius service technician will extend the service life of your balance. Sartorius can offer you service contracts with your choice of regular maintenance intervals ranging from 1month to 2 years.
Cleaning the Balance Housing and the Draft Shield
Before cleaning the balance, unplug the power supply from the wall outlet.
Please do not use any aggressive cleaning agents (solvents or similar agents). Instead, use a piece of lint­free cloth which has been wet with a mild detergent. Make sure that no liquid enters the balance housing. After cleaning, wipe down the balance with a soft, dry piece of cloth. To clean the draft shield, remove it from the weighing cell. Clean the draft shield with a commercially available glass cleaning agent or in a dishwasher.
Cleaning the Weighing Chamber
Carefully remove spilled powder from underneath the protective disk (8) by using a small car vacuum cleaner with a mini-hose attached.
Do not clean the weighing chamber by blowing off powder from the balance components!
To remove liquid spills, use blotting paper.
Do not insert a pair of forceps or any other object behind the draft shield closing plate.
Important Note:
The weighing system is hermetically sealed from the draft shield closing plate area so that dirt cannot enter.
1–40
Safety Precautions
If there is any indication that safe operation of the balance with the power supply/AC adapter is no longer warranted, turn off the power and unplug the equipment from AC power immediately. Lock the equipment in a secure place to ensure that it cannot be used for the time being.
Safe operation of the balance with the power supply/AC adapter is no longer ensured when – there is visible damage to the power supply – the power supply no longer functions properly – the power supply has been stored for a relatively
long period under unfavorable conditions
In this case, notify your nearest Sartorius Service Center or the International Service Support Unit based in Goettingen, Germany. Only service technicians who have access to the required maintenance manuals are allowed to perform maintenance and repairwork on the equipment.
We recommend that the balance together with the power supply be inspected by a qualified Sartorius service technician according to the following checklist: – Insulation resistance > 7 megohms measured
with a constant voltage of at least 500 V at a 500 kohm load
– Equivalent leakage current < 0.05 mA measured
by a properly calibrated multimeter
The duration and number of measurements should be determined by a qualified Sartorius service technician according to the particular ambient and operational conditions for the power supply. Such inspection should be done at least once a year.
1–41
Balance Operating Menu
The Sartorius MC 1 Balance can be adjusted to meet your special requirements; e.g., to weigh in various units of measure, adapt to unfavorable conditions and process weight data for a variety of applications.
In the operating menu, you can define how your balance will adapt to ambient conditions, and also how it will work to meet your needs.
The factory-set menu codes are identified by an “*.” You can select the functions not identified by an “*” by setting the respective menu code.
Important Note Concerning Verified Balances Approved for Use as Legal Measuring Instruments:
The balance operating menu can also be changed when the balance is being used as a legal measuring instrument. Codes that are not permitted for operation of the balance as a legal measuring instrument are blocked or not displayed as a rule. After verification, the balance operating menu cannot be locked with the menu access switch (-L- not displayed).
2–1
Changing a Menu Code Setting
To select specific functions, you will need to set the respective menu code.
There are three steps to changing a code:
– Accessing the menu – Setting a code – Confirming and storing this code
For setting menu codes, the keys have special functions. To set a code, use the four keys which are defined on the display as arrow points to indicate the direction:
< w and > p = Move to the left or right ^
f and v F = Increase or decrease a number
by one with each press
t = Confirm a code setting c = Store a code setting and exit
the menu
Now try changing the weight unit in the second weighing range from grams to carats “ct,” code 314.
Accessing the Menu (Example Code 3 1 4)
– Turn the balance off – Turn it back on again
– While all segments are displayed, briefly press the
t key (10).
– If -L- is displayed, unlock the menu as follows:
Remove the protective cap located on the
left-hand side of the balance’s/electronic computing
device’s rear panel to expose the menu
access switch – Move the switch in the direction of the arrow
2–2
– Press the f key to change the left-hand number
to “3”
– Press p to move to the middle number
– Now press the p key to move to the right-hand
number (When you move to the right-hand number, the previously set numeric code will be indicated).
– Press the f key to change the right-hand number
to “4”
Confirm the Code Setting
– You must press the t key in order to confirm
the code you have just set. This is indicated by the “o” after the code.
– Press c to store the new menu code setting
The current menu code setting in the balance operating menu is identified by a small “o” after the last number. When you access the operating menu, the previously set numeric code will be displayed after you have selected the left-hand and middle numbers, which means the entire menu code setting will be displayed. This makes it easy for you to check the previously set menu codes.
If you would like to change several menu code settings, you do not have to press c after each change to exit the balance operating menu.
2–3
Please do not forget to relock the balance operating menu. The “-L-” indicates that it is currently locked:
To use the locking function, make sure code 812 is set in the balance operating menu. If code 811is set, the menu access switch will not lock. In this case, “-C-“ will be displayed whenever you access the menu:
Undoing All Menu Code Changes – Reset Function
The reset function lets you undo all menu code changes, which means that you will obtain the original factory-set menu codes indicated by an “*” so that your balance will operate according to them.
To use this function, you will need to select code 9 – – 1o. See the previous pages for information on confirming and storing a menu code setting.
The charts on the next pages give just a small sampling of the code options available for the balance operating menu. These options include standard balance operating parameters, utilities for printouts or data transfer and additional functions.
2–4
Balance Operating Parameters
Adapting the Balance to Ambient Conditions
To adapt your balance to ambient conditions, you may need to change the response time (see the “Specifications”).
Code Very stable conditions 1 1 1 Stable conditions 1 1 2* Unstable conditions 1 1 3 Very unstable conditions 1 1 4
Standard Weighing Mode – Manual Filling Mode
You can optimally adapt your balance to meet either of these requirements. In the manual filling mode, the display compensates for fluctuations of the load on the balance so that you obtain a steadier readout.
Code Standard weighing mode 1 2 1* Manual filling mode 1 2 2
Stability Range
When the stability symbol is displayed, the weight readout is stable within the defined range.
Readout is stable within +/– Code
0.25 digit 1 3 1
0.5 digit 1 3 2 1 digit 1 3 3* 2 digits 1 3 4* 4 digits 1 3 5 8 digits1)136
* = factory setting; depends on the balance model in some cases
1
) = not applicable to verified balances approved for use as legal
measuring instruments
2–5
Stability Symbol Delay
This setting allows your balance to compensate for individual interfering factors which slowly subside, such as turbulent air currents generated within the weighing chamber.
Code No delay 1 4 1 Short delay 1 4 2* Long delay 1 4 3 Extremely long delay 1 4 4
Tare Parameter
You can define when the balance will perform the taring operation:
Code** At any time 1 5 1 Not until the readout is stable 1 5 2*
Auto Zero Function
When this zero tracking function is activated, any changes off the zero readout
that are equal to a defined fraction of digits per second are automatically tared. In other words, it ensures a stable zero.
Code Auto Zero on 1 6 1* Auto Zero off 1 6 2
* = factory setting ** = setting does not apply to verified balances approved for use as legal
measuring instruments
2–6
Weighing in Three Ranges on Standard Balances
The toggle key w, lets you switch back and forth between two weighing ranges, R1 and R2.
If the menu code is set for three ranges, press the “w “ key each time to toggle to a different range.
Selecting the Number of Ranges
Code Block the w key/one weighing range 2 1 1 Two weighing ranges 2 1 2* Three weighing ranges 2 1 3*
ID symbol displayed
1st range 2nd range 3rd range Two weighing ranges W ** R1 W Three weighing ranges W ** R1 W R2 W
Weight Units
The “initial weight unit” is the unit in which your balance will weigh the moment you turn it on. This unit is defined in the 1st range. You can select a different unit for each weighing range by setting the appropriate menu code.
** = factory setting; depends on the balance model in some cases ** = The standard weighing range automatically displayed when you turn
on the scale is identified only by the scale symbol in the display.
2–7
Overview of the Weight Units
Symbol Code
1st range 2nd range 3rd range Grams o 171 311 331 Grams g 172* 312* 332 Kilograms o 1 7 3 3 1 3 3 3 3 Carats ct 1 7 4 3 1 4 3 3 4 Pounds lb 1 7 5 3 1 5 3 3 5 Ounces oz 1 7 6 3 1 6 3 3 6 Troy ounces ozt 1 7 7 3 1 7 3 3 7 Hong Kong taels tl 1 7 8 3 1 8 3 3 8 Singapore taels tl 1 7 9 3 1 9 3 3 9 Taiwanese taels tl 1 7 10 3 1 10 3 3 10 Grains gr 1 7 11 3 1 11 3 3 11 Pennyweights dwt 1 7 12 3 1 12 3 3 12 Milligrams mg 1 7 13* 3 1 13 3 3 13* Parts/pound o 1 7 14 3 1 14 3 3 14 Chinese taels tl 1 7 15 3 1 15 3 3 15 Mommes m 1 7 16 3 1 16 3 3 16 Austrian carats o 1 7 17 3 1 17 3 3 17 Tola t 1 718 3 118 3 318 Baht b 1 7 19 3 1 19 3 3 19 Mesghal m 1 7 20 3 1 20 3 3 20
Codes 1 7 1, 3 1 1 and 3 3 1 are reserved for programming special units to meet the needs of customized applications. The standard, factory-set unit is grams. In the display, you will see “o” as the stability symbol for a stable readout, just as for kilograms.
* = factory setting; depends on the balance model in some cases
2–8
Some unit symbols printed on hard copy or output on a computer screen will differ from the way they are shown on the balance display:
This applies to code numbers ending with 3 = kg
8 = tlh
9 = tls 10 = tlt 11 = GN 14 = /lb 15 = tlc 16 = mom 17 = K 18 = tol 19 = bat 20 = MS
2–9
Weighing in Two Ranges on Verified Balances Approved for Use as Legal Measuring Instruments
The toggle key, w, lets you switch back and forth between two weighing ranges, provided you are using the factory-set menu code.
Selecting the Number of Ranges
Code Block the w key 2 1 1 Two weighing ranges 2 1 2*
Weight Units
Overview of the Weight Units
Symbol Code
1st range 2nd range Grams g 172* 312* Milligrams mg 1 7 13 3 1 13
* = factory setting
2–10
Display Modes for Standard Balances
You can select the display mode that best meets your individual requirements.
Last Numeral Blanked When the Load Changes
As the load on your balance changes, the display resolution is reduced by a factor of 10 so that you will obtain a faster and more stable readout. Once the load has stabilized, the readout is shown again with the full display accuracy, which means the last numeral is displayed.
Display Accuracy
You can define the level of accuracy by changing the display increments, also called “scale intervals” (of the last numeral). The display increments possible are as follows: 1, 2, 5, 10, 20, 50, etc. Starting with the basic increments of a weight unit, the display accuracy can be reduced by as many as three levels so that you will obtain a faster readout. This accuracy is reduced in relation to the selected basic increment of the weight unit. Example: weight unit “ct” for carats (5 increments) with code setting 1 8 3 10 increments. To make this concept easier to understand, the three levels are designated as “rounding factors” in the tables summarizing the various menu code settings.
IQ-Mode
(Load-Dependent Readability)
In the IQ-mode, weighing is done with a menu-definable, load-dependent readability throughout the entire weighing range of your balance. In the process, the display resolution of the last digit of the weight readout changes in increments of 1, 2, 5, 10, 20, etc., in proportion to the weight of the sample.
This mode for adapting the display accuracy enables you to weigh with a constant relative accuracy between 1% and 0.01% over the entire weighing range of your balance. Select the load-dependent display accuracy independently for each of the three weighing ranges. The accuracy selected is shown in the top right-hand corner of the application display field.
2–11
PolyRange Function (application for single-range balances)
The PolyRange function divides a single weighing range into as many as 4 ranges, each with a different readability. In the various ranges, the readability will adjust so that the last numeral of a weight readout is displayed with a resolution of 1, 2, 5 or 10 digits (10 digits = only the next to the last numeral of the readout will change; the last numeral is blanked). The PolyRange function makes filling easier because the readability becomes slightly coarser as the load increases and you will not immediately lose an entire place of readability. Press the tare key at any range level to restore the full resolution of the first range, even when the balance is loaded.
Code
Display mode 1st range 2nd range 3rd range Highest possible accuracy 1 8 1* 3 2 1* 3 4 1* Last numeral blanked when
load changes 1 8 2* 3 2 2 3 4 2* Rounding factor 2 1 8 3 3 2 3 3 4 3 Rounding factor 5 1 8 4 3 2 4 3 4 4 Rounding factor 10 1 8 5 3 2 5 3 4 5
1.0% accuracy 1 8 6 3 2 6 3 4 6
0.5% accuracy 1 8 7 3 2 7 3 4 7
0.2% accuracy 1 8 8 3 2 8 3 4 8
0.1% accuracy 1 8 9 3 2 9 3 4 9
0.05% accuracy 1 8 10 3 2 10 3 4 10
0.02% accuracy 1 8 11 3 2 11 3 4 11
0.01% accuracy 1 8 12 3 2 12* 3 4 12 PolyRange function 1 8 13 3 2 13 3 4 13
* = factory setting, depends on the balance model in some cases
2–12
Display Modes for Verified Balances Approved for Use as Legal Measuring Instruments
You can select the display mode that best meets your individual requirements.
Last Numeral Blanked When the Load Changes
As the load on your balance changes, the display resolution is reduced by a factor of 10 so that you will obtain a faster and more stable readout. In the process, the last numeral is blanked until the load stabilizes. Once the load has stabilized, the readout is shown again with the full display accuracy, which means the last numeral is displayed.
Code
Display mode 1st range 2nd range 3rd range Highest possible accuracy 1 8 1* 3 2 1* – Last numeral blanked
when load changes 1 8 2 3 2 2 – Rounding factor 10 3 4 5*
IQ-Mode
(Load-Dependent Readability)
The IQ-mode does not apply to EC type-approved balances verified for use as legal measuring instruments.
* = factory setting
2–13
Calibration Functions on Standard Balances
Select the appropriate menu code to define the access status for each of the calibration functions, which are activated by holding down the t key for a few seconds.
If the menu access switch is unlocked (“accessible” status indicated by -C- after you have accessed the balance operating menu), the “external calibration” function will be accessible even though you have set the menu code 1 9 2 for “access denied.”
External calibration Code Accessible 1 9 1* Access denied 1 9 2
Internal calibration Code Accessible 1 10 1* Access denied 1 10 2
Calibration test Code Accessible 1 11 1* Access denied 1 11 2
External Linearization
The linearization weights to be loaded are displayed on the balance one after the other in increasing order. The balance must be re-calibrated after external linearization.
Important Note:
If you use linearization weights that differ from the values displayed, this will cause errors.
External linearization Code Accessible 1 12 1 Access denied 1 12 2*
Internal linearization Code Accessible 1 13 1* Access denied 1 13 2
* = factory setting
2–14
Multiple Calibration Mode
The calibration value is calculated from the average of the individual calibration procedures. You can use the “multiple calibration mode” for both internal and external calibration. The number of calibration procedures is indicated in the 3rd place of the application display field (e.g., “C.I.3”).
Important Note:
If “Err 04” is briefly displayed, the calibration values deviate too much from one another. This means the calibration value measured is not stored, and the calibration procedure will be repeated.
Multiple calibration mode Code Off 1 14 1* On 1 14 2
Self-Calibration “isoCAL”and Linearization
Code Off 1 15 1 Calibration status displayed only 1) 1 15 2 Self-calibration “isoCAL” on 1 15 3* Self-calibration “isoCAL” and linearization on 1 15 4
1
) = The symbol “W” flashes in the display until you press the appropriate key
to activate one of the calibration functions
CAL Using f
You can activate the “internal calibration” function anytime at the touch of the f key (factory setting).
Function of the f key Code Acces denied 2 2 1 Internal calibration “CAL I” 2 2 5* Calibration function “CAL T” 2 2 6
* = factory setting
2–15
Calibration Functions on Verified Balances Approved for Use as Legal Measuring Instruments
Select the appropriate menu code to define the access status for each of the following calibration functions, which are activated by holding down the t key for a few seconds:
– External calibration C.E. – Internal calibration C.I. – Calibration C.t. – Internal linearization L.I. – Air density determination A.d. (see part 3, “Application Programs”)
However, if the menu access switch is unlocked (“accessible” status indicated by
-C-
after you have accessed the balance operating menu), the “external calibration” function will be accessible even though you have set the menu code 1 9 2 for “access denied.”
External calibration Code** Accessible 1 9 1 Access denied 1 9 2*
Internal calibration Code Accessible 1 10 1* Access denied 1 10 2
Multiple Calibration Mode
The calibration value is calculated from the average of the individual calibration procedures. You can use the “multiple calibration mode” for both internal and external calibration. The number of calibration procedures is indicated in the 3rd place of the application display field (e.g., “C.I.3”).
Important Note:
If “Err 04” is briefly displayed, the calibration values deviate too much from one another. This means the calibration value measured is not stored, and the calibration procedure will be repeated.
Multiple calibration mode Code Off 1 14 1* On 1 14 2
** = factory setting ** = setting does not apply to verified balances approved for use as legal
measuring instruments
2–16
Self-Calibration “isoCAL” and Linearization
Code Off (restricted temperature range) 1 15 11) Self-calibration “isoCAL” on 1 15 3* Self-calibration “isoCAL” and linearization on 1 15 4
1
) = With the appropriate modifications, your local Sartorius authorized service
technician can make code 1 15 1 accessible. Afterwards, you may use the balance only in the legally restricted temperature range from +15 °C to +25 °C.
CAL Using f
You can activate the “internal calibration” function anytime at the touch of the f key (factory setting).
Function of the f key Code Access denied 2 2 1 Internal calibration 2 2 5* Calibration 2 2 6
* = factory setting
2–17
Utilities for Printouts or Data Transfer
The balance operating menu lets you define the various parameters for data output. For information on the data formats and for interfacing a computer or a different peripheral device, see part 4, “Interface Description.”
Data Output Parameter
This parameter is coupled with the stability parameter; stability = stable readout or no motion is detected
Print on request = data is output only when the print key, p, is pressed
or a software command is received
Auto print = continuous, automatic data output
Code Print on request regardless of stability 6 1 1 Print on request after stability, with storage of the function 6 1 2* Print on request at stability, without storage of the function 6 1 3 Auto print regardless of stability 6 1 4 Auto print at stability 6 1 5
Automatic Data Output
You can stop and start automatic data output by pressing the print key, p.
Code Start/stop auto print using the p key 6 2 1 Auto print not stoppable 6 2 2*
* = factory setting
2–18
Data Output at Defined Intervals
You can reduce the volume of data in the “auto print” mode by defining the interval at which data will be output automatically. This auto print interval is based on the number of times the display is updated.
Auto print interval Code 1 display update 6 3 1* 2 display updates 6 3 2 5 display updates 6 3 3** 10 display updates 6 3 4** 20 display updates 6 3 5** 50 display updates 6 3 6** 100 display updates 6 3 7**
Automatic Taring after Data Output
This convenient setting lets you checkweigh a series of samples or products without having to unload the balance after each weighing operation.
This means less work for you:
– the sample remains on the pan after the weight readout has been printed
or transferred to an on-line computer
– the balance is tared automatically after the weight readout has been printed
or transferred to an on-line computer
– you simply load the next sample or part
Automatic taring after data output Code Data output without automatic taring 6 4 1* Data output with automatic taring 6 4 2
** = factory setting ** = not applicable for MC 210 S-0CE, MC 210 P-0CE, MC 410 S-0CE
2–19
Data ID Codes
To help you identify weights, piece counts, percentages, etc., a code letter is printed or displayed in front of these values. For example, an “N” printed or displayed before a weight value identifies it as a net weight. If you set the code for “without data ID code,” only net weights, results in percent, and counting results will be output. The ID code increases the data output format from 16 to 22 characters for each weight readout. You will find the data ID codes of a particular application program listed in the corresponding description.
ID code for data output Code Without 7 2 1* With 7 2 2
* = factory setting
2–20
Additional Functions
Menu Access Function
You can define the function of the menu access switch by setting the code for the balance operating menu to “accessible.” In this setting, “-C-” will be displayed on your balance whenever you access the menu.
Access to the balance operating menu Code Accessible 8 1 1 Depends on setting of menu access switch 8 1 2*
Beep Tone (Acoustic Signal)
Acoustic signal Code On 8 2 1* Off 8 2 2
Blocking the Function Keys
You can block all function keys on the balance (except for e).
Key functions Code Accessible 8 3 1* Blocked 8 3 2
* = factory setting
2–21
Blocking the Numeric Keys
You can block the numeric keys by setting the appropriate menu code.
Numeric keys Code Blocked 2 5 1* Accessible 2 5 2
Important Note:
A control command can be input via the balance interface to block the function and numeric keys (except for e). For more information, see part 4.
Power-On Mode
Depending on the operating mode – line current, battery operation or continuous operation – you can change the power-on mode of your balance. The factory setting is: (power) off —> on <—> standby.
In the setting “toggle between on and standby,” the balance power will turn back on automatically after a power failure has occurred, or after you have disconnected your balance temporarily from line current.
In the setting “automatic power-on,” the balance will turn back on automatically after a power failure has occurred or after the balance has been disconnected, then reconnected to line current. In this setting, the balance can no longer be turned off by the e key.
Power-on mode Code (Power) off —> on <—> standby 8 5 1* On <—> standby 8 5 3 Automatic power-on 8 5 4
Display Backlighting
Display backlighting Code On 8 6 1* Off 8 6 2
* = factory setting
2–22
Fully Automatic Draft Shield Function
You can define the fully automatic draft shield function to meet the most diverse requirements. After you have pressed a function key (or after a control command has been received – see part 4, “Interface Description”), the draft shield will close automatically and the balance will then perform the particular function activated by the key. If code 8 8 2 or 8 8 3 is set, the draft shield will open once the function selected has been performed. In addition, when codes 8 8 2 through 8 8 5 are set, the draft shield closes automatically if the balance has not been used for more than one minute.
To be on the safe side for automatic operation of the balance with a robot, you should turn off the fully automatic draft shield function (code 8 8 1).
The draft shield status should always be polled for operation with a robot (see part 4, “Interface Description”).
The draft shield operates automatically for the following functions:
– powering on the balance (e key)
– taring once the balance has stabilized (t key)
– printing on request after stability (p key)
– starting all calibration functions (f key)
– using the tare memory once the balance has stabilized (f key) –
see also part 3, “Application Programs”
– storing weights during differential weighing and backweighing, weighing in
percent and counting (F key) – see also part 3, “Application Programs”
– storing weights during over/under checkweighing (f key) –
see also part 3, “Application Programs”
2–23
Automatic draft shield function Code Off 8 8 1 Close draft shield – perform function – open draft shield 8 8 2 Close draft shield – perform function with stability symbol delay –
open draft shield 8 8 3 Close draft shield – perform function 8 8 4* Close draft shield – perform function with stability symbol delay 8 8 5
Display Accuracy with the Draft Shield Automatically Opened or Manually Adjusted
You can define the display accuracy for the automatically opened or manually adjusted draft shield by changing the increments, also called “scale intervals” (of the last numeral). The display increments possible are as follows: 1, 2, 5,10, 20, 50, etc. To make this concept easier to understand, the six levels are designated as “rounding factors” in the table summarizing the various menu code settings.
Display accuracy Code Highest possible accuracy 8 9 1* Rounding factor 2 8 9 2 Rounding factor 5 8 9 3 Rounding factor 10 8 9 4* Rounding factor 20 8 9 5 Rounding factor 50 8 9 6 Rounding factor 100 8 9 7**
** = factory setting ** = does not apply to verified balances approved for use as legal
measuring instruments
2–24
ISO/GLP-compliant Printout or Record
Application:
Use of the balance in quality assurance systems and in areas subject to compliance with ISO, GLP, GMP and EN, etc.
The balance can record all completed calibration/adjustment operations and output data in compliance with the requirements of Good Laboratory Practice (GLP) and ISO. The balance, interfaced with a data printer or a computer, creates a document that records the date, time, serial number and model number, making it possible to clearly trace data to the balance that generated it and the time at which it was generated.
Select the ISO/GLP printout/record mode by setting the respective code in the balance operating menu.
ISO/GLP-compliant printout/record mode Code Off 8 10 1* Only for calibration and linearization functions 8 10 2 Always on for calibration and weighing functions 8 10 3
The following menu code must be set in order to obtain an ISO/GLP-compliant printout/record:
With data ID code 7 2 2
!
Important Note:
ISO/GLP-compliant printouts/records will not be output if the factory setting 7 2 1 “without data ID code” is selected. When the “auto print” data output parameter (menu code 6 1 4 or 6 1 5) is set, only calibration and linearization functions are printed/recorded.
* = factory setting
2–25
Printout/Record for Calibration and Linearization Functions (menu code 8 10 2)
A printout or record is generated only at the end of the following functions:
– all calibration operations – all linearization operations – air density determination (see part 3, “Application Programs”)
The printout of the record can have the following lines:
-------------------­MC1 - Sartorius : Balance family and manufacturer Model MC5 : Balance model S/N 030800046 : Serial no. of the balance Id 4-32-1 : ID no.(e.g., for identifying
a workstation/operator)
-------------------­Date : 30-Jul-95 : Current date Start: 10:05:30 : Time at which the application started Cal. : Test :
Calibration mode (in this case, “calibration”)
Diff.:- 0.000013 g : Data generated during the calibration test Cal. : Intern : Calibration mode (in this case,
“internal calibration”)
Stat.: Complete : Status comment for calibration or
linearization functions
End : 10:05:45 : End of application Name : : Field for signature of the operator responsible
-------------------­Set. : 5.000000 g : Calibration weight (only for “external
calibration”)
Set. : 1.175 kg/ : Air density Cal. : Air
2–26
Data Printout/Record (menu code 8 10 3)
To have a data record printed out, perform the following:
– Press p to output the printout heading and the first value (after you have turned
on the balance or cleared a function by pressing c)
– Press p to output additional data
– To end printout generation and recording of data, press the c key
(generation of an ISO/GLP-compliant printout or record is also ended when a calibration or linearization operation is started)
During data printout, the print symbol p appears on the display of the balance.
The printout of the record can have the following lines:
------------------­MC1 - Sartorius : Balance family and manufacturer Model MC5 : Balance model S/N 030800046 : Serial no. of the balance Id 4-32-1 : ID no.(e.g., for identifying
a workstation/operator)
------------------­Date : 30-Jul-95 : Current date Start: 10:05:30 : Time at which the application started Ser. : : Field for entering the project number N + 4.490 mg: Measured values/weights N + 14.486 mg N + 53.350 mg End : 10:05:45 : End of application Name : : Field for signature of the operator responsible
-------------------
2–27
Data Printout/Record for Application Programs (menu code 8 10 3)
For application programs, the reference data (parameters) can be included in the printout/record.
Automatic output of the reference data (parameters) Code Off 7 1 1* Reference %/qty. and reference weight 7 1 2 Reference weight only 7 1 3
You can also add the reference data to the printout/record later by pressing i (information function), p and then either the f or F key.
To have data printed out, perform the following:
– Press the f or F key to output the printout heading and reference data
(the reference data will be stored at the same time)
or
– Press the p key to output the printout heading and the first value
If you input and store new references while an ISO/GLP-compliant record is being printed out, the new reference data will be output. If you enter different data before generation of an ISO/GLP-compliant record is started, the printout heading and the reference data will automatically be printed once you press p. Then the measured value will be output.
– Press p to output weighing data
– Press the c key to end printout generation (generation of an ISO/GLP-compliant
printout also ends once a calibration or linearization operation has been started)
– Then press the c key to clear the reference data for the application programs
During data printout, the print symbol P appears on the display of the balance.
* = factory setting
2–28
The printout of the data record can have the following lines:
--------------------­MC1 - Sartorius : Balance family and manufacturer Model MC5 : Balance model S/N 030800046 : Serial no.of the balance Id 4-32-1 : ID no. (e.g., for identifying
a workstation/operator)
--------------------­Date : 30-Jul-95 : Current date Start: 10:05:30 : Time at which the application started Ser. : : Field for entering the project number Lim + 1.0 % : Reference data (in this case, “tolerance
and target weight”– see also part 3,
Setp + 42.903 mg : “Application Programs”) pRef + 100 % Wxx% + 42.903 mg Prc + 100.6 % : Value measured (in this case,
“calculated percentage”)
End : 10:05:45 : End of application Name : : Field for signature of the operator responsible
---------------------
2–29
Setting the ID No./Date/Time
– Turn the balance off – Turn it back on
– Briefly press w when all segments are displayed
– Toggle among the identification number “1d,”
the date “
dAt
” and the time “
t1N
” using the f key
identified in the display by “^”
“ID No.for the ISO/GLP-compliant Printout or Record”
Enter the ID number with 8 places maximum using digits 0 through 9 and the “–” symbol. Zeros in front of the decimal point will not be output. The decimal points are output as “–” via the data interface.
– Enter ID number, e.g., 4.32.1
– Press F identified in the display by “STO”
to confirm the setting
2–30
“Date”
– Separate the day, month and year by pressing
the “.” key, e.g., 10.09.93
– Press F identified in the display by “STO”
to confirm the setting
“Time”
– Separate the hours, minutes and seconds by
pressing the “.” key, e.g., 19.05.30
– Use F identified by “STO” to set the hours, minutes
and seconds entered according to your local time
– Press f identified by “^” to select the “12-hr”
display mode, and store this setting by pressing F identified by “STO” (in this display mode, an “A” (morning) or a “P” (afternoon) is displayed for the “hours”)
or
– Press F identified by “STO” to directly store the
“24-hr” display mode
End this function by pressing c
2–31
Application Programs
In addition to the functions implemented strictly for weighing, Sartorius MC Balances offer you a variety of application programs.
In this description, you’ll find a few simple examples for the following applications:
“EUREKA” air buoyancy correction program
Differential weighing and backweighing program
Density1)
Diameter determination 2)
Tare memory
Weighing in percent
Over/under checkweighing
Counting
1
) only on models MC 210 S (-0CE), MC 210 P (-0CE), MC 410 S (-0CE)
2
) only on models MC 5 (-0CE) or SC 2 (-0CE), MC 21S
3–1
You can also use these programs in combination. How? You’ll discover the ins and outs in the examples described on the next pages.
To select an application program or a specific function, set the appropriate code in the menu. Part 2 describes in detail how to set menu codes.
Additional settings for running the particular program and displaying or printing the data on hard copy are listed in a table of codes. For your convenience, we’ve indicated all factory-set codes with an “*.”
Important Note for Verified Balances Approved for Use as Legal Measuring Instruments:
* including the Signatories of the Agreement on the European Economic Area
Use of Balances Approved for Use as Legal Measuring Instruments in the EU*
All application programs can be selected on balances used as legal measuring instruments. Non-metric values are indicated as follows: Percent = % Piece count (counting) = pcs Computed value = o
The display symbol “R2” flashes to identify non-verified weights (not legal for trade).
3–2
Functions Common to All Programs
The f, F and w keys are assigned different functions by the individual programs. The functions assigned to the f and F keys are always identified on the display next to each key.
c Key
c clears the function of a program you are using and resets the program.
Clear function Code Global – clears functions of all keys 2 4 1* Selective clearing in the order of f F 242 Selective for f or F 243
Use the selective code if you intend to run two different programs at the same time. Select code 2 4 2 if you would like to clear the program assigned to the f key
before you clear the program assigned to the F key. If you would like to clear a function in any order, choose code 2 4 3. When you
press the c key, this clear function is indicated on the application display. Now you can activate it by pressing f or F to clear the particular program function. To clear “CF” indicated on the display, press c again.
* = factory setting
3–3
Information and Printouts or Data Transfer
The info key i has two functions:
– one brief press: displays information and prints/transfers stored data; – one long press: selects the reference percentage or reference sample
quantity for weighing in percent, diameter determination or counting; clears the memory in the backweighing mode (for more information, see the descriptions of these programs)
Briefly press the i key to select the information function: an “i” will appear on the display.
If you press f or F now, the data stored in the memory will be retrieved and displayed. What is displayed depends on the program selected.
Example: counting Readout: reference sample quantity (pcs)
These data will also be output via the
nRef + xxxxxxxx pcs interface (printed or transferred) if you wRef + xxxxxxxx g press the print key after the info key.
In this case, the print symbol P will be displayed
Data output only for next to the “i” until you press code 7 2 2 a function key.
Data ID Code K* or NUM
Just by pressing a key on the balance, you can have numeric entries with ID codes transmitted to an on-line device via the interface.
Function: Keys: Output data ID code “K*” numeric entry + i Output data ID code “NUM” numeric entry + p
Info + print + function key displays and prints data stored
Info + function key displays data stored in the memory
3–4
“EUREKA” Air Buoyancy Correction Program
“EUREKA” Air Buoyancy Correction Program Code 2 1 8
Symbol displayed: +/–
Key identified by: – STO - F when the air density is 1.2 kg/m
3
– STO●- F when the air density is different from 1.2 kg/m3*
Because of air buoyancy, samples or objects with the same mass but different
densities have different weights. To obtain the true mass of the sample, the weight is multiplied by the following factor:
ρ
L
1 – –––
ρ
ST
K = ————————
ρ
L
1 – ———-
ρ
W
where:
ρ
L
= air density in kg/m
3
ρ
ST
= density of steel 8000 kg/m3(calibration weight)
ρ
W
= density of the object/sample to be weighed in kg/m
3
** = for directions on air density determination, see page 3–9
** = including the Signatories of the Agreement on the European Economic Area
Important Note for Verified Balances Approved for Use as Legal Measuring Instruments in the EU:*
You may not use weights corrected for the effects of air buoyancy when the balance is being used as a legal measuring instrument. The display symbol “R2” flashes to identify non-verified weights (not legal for trade).
3–5
The following diagram shows the required corrections of mass values m for a few selected density values ρW. The incorrect values result from the effects of air buoyancy. The corrections depend on the weights displayed on the balance.
Example: aluminum: conventional mass of 2 g (density 2.7)
Readout
Without air buoyancy correction+ 2000.000 mg
With air buoyancy correction + 2000.589 mg
3–6
Add the mass error to the weight
displayed on the balance
Weight displayed on the balance (grams)
Correction of the mass ∆m
(milligrams)
Subtract the mass error from
the weight displayed on the balance
g
ρ
w
= 0.8 —–
cm
3
g
ρ
w
= 1.0 —–
cm
3
g
ρ
w
= 1.4 —–
cm
3
g
ρ
w
= 2.0 —–
cm
3
g
ρ
w
= 4.0 —–
cm
3
g
ρ
w
= 22.5 —–
cm
3
g
ρ
w
= 8.0 —–
cm
3
g
ρ
w
= 0.0012 —– (air)
cm
3
Density of the object
to be weighed
Changing the Density of a Sample
Enter the density of a sample using the numeric keys and then confirm this value
by pressing the F key identified by “STO.” Afterwards, the density that you
entered will be shown in the application display. This density is used to calculate
the absolute mass of the sample on the balance.
The density must be entered in grams per cubic centimeter (g/cm3). A density
may not be greater than 22.5 g/cm3or less than 0.1 g/cm3. The density that you
enter will be stored in the non-volatile memory.
Recalling a Stored Density
You can recall the density that you last used by pressing the F key identified
in the display by “STO.”
Press the w key at any time to toggle between weight and mass.
Air Buoyancy Correction after an Air Density Determination
A special function makes it possible to determine and store the air density (for more
information see p.3–9). The density can be between 1.0 kg/m3and 1.4 kg/m3.
If the air density determined deviates from the standard value of 1.2 kg/m3,
the F key normally identified by STO is shown as STO●.
Use in Combination with Other Programs
The air buoyancy correction program can be used in combination with
other application programs. This means you will have all functions of the
combined program available in addition.
Program Code
Over/under checkweighing (net weight) 2 2 3
Over/under checkweighing (difference in weight) 2 2 4
3–7
Practical Example: Air Buoyancy Correction in the Manufacture of an Alloy
Menu codes used in the example:
Function Code Air buoyancy correction 2 1 8
Automatic output of the air density and density of the sample 7 1 2 With data ID code 7 2 2
Application: Manufacture of alloys according to stoichiometric proportions; for
example, superconductor “Nb3Ge” (molecular weight: niobium 41, germanium 64)
Step/Key ID/Key Readout Data Output
Place container on pan
+ 122.650 mg
Zero the balance using
t
0.000 mg
Enter density for first sample (germanium):
5.32 and confirm: STO-F 5.32 RhoL + 1.200 kg/
RhoG + 5.32 g /
Add germanium and press
p
+ 500.000 mg
m + 500.000 mg
t
0.000 mg
Enter density for 2nd sample (
niobium):
8.4
and confirm using
8.4 RhoL + 1.200 kg/
STO-
F RhoG + 8.4 g /
Add niobium and press p
+ 1921.875 mg
m + 1921.875 mg
The data ID codes mean:
RhoL + 1.200 kg/ air density RhoG + 8.4 g / density of the sample m + 1921.875 mg weight which has been corrected for air buoyancy
* = factory setting
As an alternative, you can select this code:
Data output – manual mode 7 1 1*
3–8
Air Density Determination
For highly precise analyses, the balance offers you a function with which
fluctuations in the air density can be determined.
!
The air density at the place you set up your balance can be determined
within the range of 1.0 kg/m3and 1.4 kg/m
3
.
For determining the air density, use the special weight set which is available as an accessory (see also part 5, “Accessories”). This weight set consists of one steel and one aluminum weight. Their exact mass values are specified on a certificate, which is included with the set. By a differential weighing method, the air density is determined using the two weights.
To access this function, set the appropriate code in the balance operating menu:
Air density determination Code
Accessible 1 16 1
Access denied 1 16 2*
Use the c key at any time to stop air density determination.
* = factory setting
3–9
The air density is calculated according to the following formulas:
Formula 1:
ρ
L
= Air density in kg/m
3
m
a
*
W
S
m
S
*
W
a
ρ
S
= Density of steel in kg/m
3
ρ
L
= ––––––––––––––––––– mS= Mass of steel
m
a
*
W
S
m
S
*
W
a
WS= Measured value of steel
–––––––– –––––––––
ρ
A
= Density of aluminum in kg/m
3
ρ
a
ρ
s
mA= Mass of aluminum
WA= Measured value of aluminum
Formula 2:
1
– ––––––
8000
1.2
ρ
S
= Density of steel in kg/m
3
mS=M
S
*
––––––––––
1.2
MS= Conventional mass of steel
1– ––––
ρ
S
mS= Mass of steel
Formula 3:
1
– ––––––
8000
1.2
ρ
A
= Density of aluminum in kg/m
3
mA=M
A
*
––––––––––
1.2
MA= Conventional mass of aluminum
1– ––––
ρ
A
mA= Mass of aluminum
3–10
Activating the Air Density Determination Function
Hold down the tare key for more than 2 seconds until “C.I.” and “CAL” are displayed next to the f key.
To activate the air density determination function, press F, identified by “v,” several times until “A.d.” is displayed.
A.d.” stands for “air density.”
Unload the weighing pan and tare the balance.
Starting Air Density Determination
To start air density determination, press the f key when the display shows a zero readout. Afterwards, a weight for steel “St” is displayed.
”Err 02”: The effects of an external disturbance
can cause the error code “Err 02” to be displayed briefly. If this occurs, tare the balance and then press the f key again when the display shows a zero readout.
Interrupt procedure: You can stop an air density
determination procedure at any time: – By pressing the c key so that
a previously stored air density is not changed or
– By pressing F identified in the
display by “RES” to set the standard air density 1.2 kg/m
3
3–11
Using the Weight Set for Air Density Determination
– Steel Weight –
Use the numeric keys to enter the exact mass value specified for the certified steel weight (e.g. 4.999990) and store this value by pressing the f key identified in the display by “STO.”
If you press f, identified by “STO,” without making a numeric entry, the display changes to the density readout. Now you can change it for a special steel weight. Enter the mass value and press f to define this density.
Center the steel weight on the weighing pan and close the draft shield. After the steel weight has been confirmed, the display will show a zero readout. Now, remove the steel weight from the weighing pan and close the draft shield. Afterwards, if the value for the aluminum weight “Al” is displayed, you can continue with the procedure.
”Err 03”: The effects of an external disturbance
can cause the error code “Err 03” to be displayed briefly. If this occurs, restart the air density determination procedure.
3–12
– Aluminium Weight –
Use the numeric keys to enter the exact mass value specified for the certified aluminum weight (e.g., 5.018072), and store this value by pressing the f key identified in the display by “STO.”
If you press f, identified by “STO,” without making a numeric entry, the display changes to the density readout. Now you can change it for a special aluminum weight. Enter the mass value and press f to define this density.
Center the aluminum weight on the weighing pan and close the draft shield.
After the aluminum weight has been confirmed, the calculated air density between 1.1 kg/m3and
1.3 kg/m3will be displayed.
If the air density determination result is a value which is not between 1.0 kg/m3and
1.4 kg/m3, the determination procedure is interrupted with two beeps and the previous air density remains stored. If this occurs, restart the air density determination procedure after the two beeps.
Storing the Air Density and Ending the Procedure
– Store the air density displayed by pressing the
F key identified by “STO” or
– Reset the display to the standard value 1.2 kg/m
3
with the c key and store this value by pressing the F key identified by “STO”
An acoustic signal indicates the end of the air density determination procedure.
3–13
Differential Weighing and Backweighing
Differential Weighing and Backweighing Code 2 1 6
Symbol displayed: % S
The purpose of this application is to weigh a certain sample in original condition and then after treatment, such as drying, to determine the difference between the two weights and the remaining sample quantity. This is done either in percent or in a weight unit.
For each sample, the net weights are compared with each other, since the tare weights are stored first and later subtracted. Tare weighing can be de-activated, if a container will not be used in the treatment process. There are memory locations for a maximum of 50 samples. Backweighing, which means weighing a sample after a chemical or thermal reaction, can be done in any sequence (known as “random” backweighing). It is also possible to perform several backweighing operations. In this case, each backweighing operation is done in reference to the original sample weight (= 100%).
Therefore, the usual sequence of the weighing operations is as follows: tare weighing - weighing-in - backweighing. This sequence can be performed according to the individual or combined weighing mode.
!
Charging the Battery for Data Storage
It goes without saying that the data are stored in a battery-backed memory. When the balance is unplugged from AC power, the data generated will remain stored for approximately three months. In the standby mode, the data are retained by the internal power supply. The rechargeable battery can also become discharged after relatively long periods of storage. In this case, or for initial startup, leave the balance connected to AC power for about 12 hours to charge the battery.
3–14
Weighing Sequence
Individual or Combined Weighing Mode
Individual Weighing Mode
In the individual weighing mode, the weights are stored in the following sequence:
– Tare weighing – weighing-in – backweighing
– If necessary, selection of an available memory location
– Tare weighing – weighing-in – backweighing...
The data of a sample in a memory location are overwritten until a new memory
location is selected.
In the consecutive individual weighing mode, the weights are stored in this sequence:
– Tare weighing – weighing-in – backweighing
– Automatic selection of the next memory location
– Tare weighing – weighing-in – backweighing...
Beginning at a specific memory location, the memory locations that follow
are selected automatically using the F key. It is also possible to switch to a new
memory location using the numeric keys and the F key.
Combined Weighing Mode
In the combined weighing mode, the values are stored in the following sequence: – Tare weighing – weighing-in – tare weighing – weighing-in... Backweighing is done only after all of these operations have been completed.
2
1
1
2
3–15
After each weighing-in operation has been completed, the next memory location is automatically selected. To proceed from weighing-in to backweighing, you must select the corresponding memory location ID by entering the appropriate number and pressing the F key.
Configure your weighing sequence according to your particular requirements:
Weighing sequence Code
For MC 210 S, For MC 5 (-0CE), MC 210 P, SC 2 (-0CE) MC 410 S (-0CE) and MC 21S
Individual weighing 3 7 1 3 6 1 Consecutive individual weighing 3 7 2* 3 6 2* Combined weighing 3 7 3 3 6 3
* = factory setting
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Selecting the Memories
Use the numeric keys to enter any memory location ID number up to “50.” Press the F key to have your entry accepted and shown in the application display (in the upper, right-hand corner). At the same time, the weight readout will reappear.
Number of Sample Data Stored in a Memory Location
One memory location can store the following data for a sample: – Tare value identified by tAr – Net initial sample weight identified by NEt – Net sample residue (backweighed qty.)
identified by rE5
– Date on which the last value(s) were stored dAt
(Tar, Net, Res)
– Time when the last value(s) were stored t1N
(Tar, Net, Res)
Each time the balance is turned on, the memory location ID that was active before the unit was turned off is selected. The program automatically resumes at the place where you left off.
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Key Functions Function: Key(s):
Select memory location ID Numeric entry + F
Store tare value
- F
Store initial sample weight STO - F
Store residue (backweighed sample) RE S - F
Toggle between backweighing/standard w weighing modes in the individual weighing mode
Toggling after backweighing between two w calculated values and the “weighing mode”
Proceed from weighing-in to back- Numeric entry (memory weighing in the combined weighing mode location ID no.) + F
Output of all values up to p current operation
Cancel previous operation c
Delete stored data from the memory Press c >2 sec. location displayed
Delete entire memory Press i >2 sec. and
then press STO - F
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Procedures for the Individual Weighing Mode
Tare Weighing
Symbol displayed: Net
Key identified by: ●- F
Press the F key identified on the display by “●” to accept and store a weight
as the tare value. The tare weight will be stored only if the balance has stabilized.
At this point, the balance display is zeroed. After tare weighing, the net weight
of a sample is determined. The ID code of F in the display changes from “●”
to “STO.” Afterwards, weighing can be done starting from “zero.”
The tare weighing mode can be turned off by setting the appropriate menu code:
Weighing sequence Code
For MC 210 S, For MC 5 (-0CE), MC 210 P, SC 2 (-0CE) MC 410 S (-0CE) and MC 21S
Off 381* 371
On 3 8 2 3 7 2*
Weighing-in
Key identified by: STO - F
The stable net weight displayed is stored when you press F identified
on the display by “STO.”
Backweighing
Key identified by: RE S - F
Key identification when a value is stored: RE S v - F
The stable backweighed sample, the residue, is stored when you press F
identified on the display by “RE S.”
By setting the appropriate codes in the balance operating menu, you can select
the display modes for two calculated values. Use the w key to toggle
between these two values. The first difference calculated between the net initial
sample weight and the residue is automatically displayed
. In the display
modes “residue in the specified weight unit” and “residue in percent,
” the “Net” symbol indicates that the tare value was subtracted. At the same time, the identification code shown on the display for the F key changes
to “RES v” to indicate that a value has been stored in the particular memory.
* = factory setting
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The calculated value is locked into the display once the sample residue has been stored. To “unlock” this readout, press RE S v - F or select a different memory location using the numeric keys and F. Afterwards, you can proceed with the next tare weighing.
A stored value of a backweighed sample can be overwritten with a current value anytime after the corresponding memory location has been selected. To do this, pressc. A backweighing operation is done in reference to the original sample weight (=100%).
Once you have completed processing or treatment of a series of samples, you can select another memory location using the numeric keys. Therefore, you can perform backweighing in any sequence (known as “random backweighing”). In the consecutive individual weighing mode, the next memory location is automatically selected using the RE S v - F key after backweighing (code 3 6 2).
* including the Signatories of the Agreement on the European Economic Area
Important Note for Verified Balances Approved for Use as Legal Measuring Instruments in the EU:*
You may not use the calculated value when the balance is being used as a legal measuring instrument. The display symbol “R2” flashes to identify non­verified weights (not legal for trade).
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Practical Example: Residue Determination of Samples in Containers
Menu code settings used in the example:
Function Code
For MC 210 S,
For
MC 210 P,
MC 5 (-0CE),
MC 410 S (-0CE)
SC 2 (-0CE) and MC 21S
Differential weighing and backweighing 2 1 6 2 1 6 Consec. indiv. weighing 3 7 2* 3 6 2* Automatic data output 7 1 2 7 1 2 With data ID code 7 2 2 7 2 2 2 decimal places for the results in percent 3 6 3* 3 5 3 With tare weighing 3 8 2 3 7 2* 1st calculated value: residue in wt. unit 3 9 1* 3 8 1* 2nd calculated value: residue in percent 310 2 3 9 2 Record/printout with net initial sample weight 7 5 3* 7 5 3* Record/printout with residue in wt. unit and percent 7 6 4 7 6 4
Application: Brief sample treatment, such as ashing (incineration).
A value is recorded/printed out automatically after backweighing.
As alternatives, you can select these codes:
Different number of decimals 3 6 x 3 5 x Without tare weighing 3 8 1 3 7 1 Different calculated value 3 9 x 3 8 x Different calculated value 3 10 x 3 9 x Other record printout/output 7 5 x 7 5 x Other record printout/output 7 6 x 7 6 x
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Step/Key ID/Key Readout Data Output
Enter memory location/ container ID; e.g., 7
,
7
and press F to confirm
Zero the balance using
t
0.000 mg
Place container on pan;
+
376.307 mg
store weight using ●-
F
0.000 mg
Net
Add prepared sample to +
1095.335 mg
Net
container; store weight using STO - F +
1435.642 mg
Treat sample (e.g., incinerate)
Place container with treated sample on pan +
991.571 mg
Backweigh using RE S - F +
615.264 mg
Net
Num 7 Date 19-Jul-95 Time 10:34:54 Net + 1059.355 mg Res + 615.264 mg Res + 58.08 %
Toggle to readout of 2nd
+
58.08 %g
Net
calculated value:
w
Repeat procedure for the next 8 memory location: RE S v- F, or to delete data stored in the memory location for this sample, press c > 2 sec.
The data ID codes mean:
Num 7 memory location ID number Date 9-Jul-95 date of backweighing Time 10:34:54 time of backweighing Net + 1059.355 mg net initial sample weight Res + 615.264 mg net residue (backweighed sample) in wt. unit Res + 58.08 % residue in percent
* = factory setting
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