Sartorius LMA110S, Mark 3 LTE, LMA100P, Mark 3 Operating Instructions Manual

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Operating Instructions
Sartorius LMA110S Moisture Analyzer
Model Mark 3 LTE Electronic Moisture Analyzer
98040-699-09 Rev. D
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Contents
Warning and Safety Information 4 Sample Pans 6 Safety Precautions 7
Getting Started 8 Storage and Shipping Conditions 8 Unpacking the Moisture Analyzer 8 Instructions for Recycling the Packaging 9 Equipment Supplied General Views of the Moisture Analyzer 10 Assembly 12 Choosing a Suitable Location 13 Connecting the Moisture Analyzer to AC Power 13 Leveling the Moisture Analyzer 14
Operating Design 15 Keypad 15 Display Modes 17 Menu Structure 19
Data Output 20 LED Status Lights 20
Operating the Moisture Analyzer 21 Standby Screen 21 Standby Temperature with a New Program 22 Default Drying Program 23 Recalling a Program 24 Testing a Sample 25
Setup Menu 28 Setting the Device Parameters in Program Manage Menu 28 Edit Current Program 29 Table: Program Settings 30 Units 31 Factors 32 Temperature 1 and 2 33 Time 1 and 2 34 Slope 34 Target Limits 39 Test Mode 40 Program Name 41 Create a New Program 42 Delete Program 42
Sort Programs 42 Configuring the Printout 43 Print Current Program 43 Print Program List 43 Print All Programs 43 Data Log 44 Device Information 45 Modify Operators 46 Graphing 47 Results Printout Format 48 Setting the Time and Date 51 Communication Ports 52 Pin Assignment Chart 52 Serial Command List 53 Conserve Mode 60 Security 61 Activate and Deactivate Security 61 Setup Security Access 62 Clear Data Log 63 Clear Operators 63 Restore Factory Defaults 64 Manage Program Storage 64 Transfer Programs 66
Audio, Video and Language 67 Audio Adjustments 67 Video Contrast Adjustment 68 Video Color Scheme 68
Service 69 System 69
Calibration | Adjustment Functions 70 Calibrate Balance 70 Heater Adjustment 73 Adjust Temperature 73 Verify Temperature 73
Concentration Mode 77 Multi-module Mode 78 Cleaning 80 Dispoal 81 Specifications 82 Accessories (Options) 83 Regulatory Compliance 84
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Introduction
Thank you for choosing the Sartorius Mark 3 LTE moisture analyzer, the inter­national version of the field-proven Mark 3 from Sartorius. This analyzer is a modu­lar analytical instrument that can be con­figured to meet various performance requirements. Each analyzer consists of two parts, a control module and a heater module. The control module is comprised of a keypad, a display and a printer (optional) with the appropriate electron­ics. The heater module consists of the electronic balance and heating cavity. Up to two heater modules may be interfaced with a single control module. On initial power-up, the control module will auto­matically detect how many heater mod­ules have been connected and are pow­ered on. If more than one heater module is detected, the analyzer will run in the Multi-module mode.
The Mark 3 LTE moisture analyzer is used as a quick and reliable means of deter­mining the moisture content in various samples by the principle of loss on drying.
Key features of the Mark 3 LTE include:
§ Sample heating with infrared quartz tubes
§ Precision electronic balance for accurate
weighing and continuous weight moni­toring during analysis
§ Quarter VGA screen for easy viewing
§ Large storage of methods for easy recall
of frequently used drying procedures
§ Modular system for add-on capability of multiple heater modules
Please take the time to read these Operating Instructions to learn the safe operation of this analyzer. The Mark 3 LTE has many features that will be described and can be of benefit to your moisture testing program.
The Operating Instructions contain guidance in the form of descriptions, charts, software flow charts, and pictorial diagrams:
§ Key names are presented in bold:
Start|Stop
§ Safety symbols indicate notes or caution of risks as detailed below.
Descriptions and Symbols
Important safety related instructions are highlighted visually throughout the Operating Instructions with a descrip­tion:
Danger
Warning of a possible danger that may lead to a serious injury.
Caution
Warning of a possible danger that may result in minor injury or damage.
Note
Important guideline on how to use the moisture analyzer correctly.
Instrument labels
Caution:
!
Read manual before operating
Danger: Electrical hazard
Caution: Hot surface
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Warning and Safety Information
This moisture analyzer complies with the European Council Direc­tives as well as international regu­lations and standards for electrical equipment, electromagnetic com­patibility, and the stipulated safety requirements. Improper use or handling, however, can result in damage and/or injury.
Read these operating instructions thoroughly before using your mois­ture analyzer to prevent damage to the equipment. Keep these instruc­tions in a safe place.
Follow the instructions below to ensure safe and trouble-free opera­tion of your moisture analyzer:
!
Use the moisture analyzer only for performing moisture analysis of samples. Any improper use of the analyzer can endanger persons and may result in damage to the ana­lyzer or other material assets.
!
Samples or containers (e.g., beakers or graduated flasks) that are too large or bulky to permit complete closure of the sample chamber hood must not be placed in the analyzer.
!
Do not use this moisture analyzer in a hazardous area/location; oper­ate it only under the ambient con­ditions specified in these instruc­tions.
The moisture analyzer may be
operated only by qualified persons who are familiar with the properties of the sample to be analyzed.
!
Class A Warning
Warning: This is a class A product. In a domestic environment this product may cause radio interfer­ence in which case the user may be required to take adequate measures.
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!
Make sure before getting started that the voltage rating printed on the manufacturer‘s label is identical to your local line voltage (see the section on “Connecting the Mois­ture Analyzer to AC Power” in the chapter entitled “Getting Started”)
The analyzer comes with a power
supply that has a grounding con­ductor
The only way to switch the power
off completely is to unplug the power cord.
Position the power cable so that it
cannot touch any hot areas of the moisture analyzer.
Use only extension cords that meet
the applicable standards and have a protective grounding conductor.
Disconnecting the ground conduc-
tor is prohibited.
Connect only Sartorius accessories
and options, as these are optimally designed for use with your mois­ture analyzer.
Protect the moisture analyzer from
contact with liquid.
If there is visible damage to the
moisture analyzer or power cord: unplug the equipment and lock it in a secure place to ensure that it cannot be used for the time being.
!
Clean your moisture analyzer according to the cleaning instruc­tions only (see “Cleaning”).
Do not open the analyzer housing. If the seal is broken, this will result in forfeiture of all claims under the manu­facturer’s warranty.
In case you have any problems with your moisture analyzer:
$ contact your local Sartorius office,
dealer or service center
Warning: Severe Burns!
– When setting up the moisture analyzer,
leave enough space to prevent heat from building up and to keep your analyzer from overheating: – leave 20 cm (about 8 inches) around
the moisture analyzer
– 1 m (3 ft.) above the device
– Do not put any flammable substances
on, under or near the moisture analyzer, because the area around the heating unit will heat up.
– Be careful when removing the sample
from the chamber: the sample itself, the heater module and the sample pan used can still be extremely hot.
– Do not remove the heater module unit
during operation: the heating element and its protective glass panels can get extremely hot!
– Prevent excess heat build-up around the
analyzer.
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Hazards for persons or equipment posed by using specific samples:
Fire Explosion
– Flammable or explosive substances
– Substances that contain solvents
– Substances that release flammable or
explosive gases or vapors during the drying process
In some cases, it is possible to operate the moisture analyzer in an enclosed nitrogen atmosphere to prevent the vapor released during drying from coming in contact with oxygen in the surrounding atmosphere. Check on a case-to-case basis whether this method can be used, because installation of the analyzer in too small an enclosed space can affect its functions (for instance through excessive heat build-up within the analyzer). When in doubt, perform a risk analysis.
The user shall be liable and responsible for any damage that arises in connec­tion with this moisture analyzer.
Poisoning Caustic burns
– Substances containing toxic or caustic
or corrosive substances: These may be dried only under a fume hood. The value for the “lower toxic limit” in a work area must not be exceeded.
Corrosion:
– Substances that release aggressive
vapors during the heating process (such as acids): In this case we recom­mend that you work with small sample quantities. Otherwise, vapors can con­dense on cold housing parts and cause corrosion.
The user shall be liable and responsible for any damage that arises in connec­tion with this moisture analyzer.
– Sample Pans (Delivered with the
Analyzer): The reusable metal pans are not made of stainless steel. For this reason, they are not resistant to corrosion. These pans can be used only for powder and granules (e.g. plastics) with very low moisture content. If the moisture content is higher, the disposable aluminium pans (90 mm diameter) must be used (see chapter “Accessories”).
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Caution
Do not touch the metal surfaces inside the drying chamber while removing or placing a sample in the analyzer since the surfaces are very hot.
Do not touch the heater hood ventila­tion area at any time because this area can be hot during and after a test.
§ Do not test flammable or toxic materials.
§ Use the analyzer in a fume hood if the samples emit fumes which could be harmful.
§ Know where the fire extinguisher is located. Use only an extinguisher rated for use with electrical fires.
§ Keep the analyzer clean. Always unplug the analyzer and cool it thoroughly before cleaning or performing service.
§ Do not block the ventilation areas of the heating chamber.
§ If necessary, press the Start|Stop key during a test to stop the test.
§ Locate the analyzer away from flammable materials.
§ If liquid is spilled into the analyzer, unplug the Heating Module from the electrical supply immediately.
§ Analyzer is suitable for continuous operation
Safety Precautions
Danger
Use of this product in a manner not specified by the manufacturer may impair any safety protection provided by the equipment!
Every attempt has been made to make this analyzer safe and easy to use. However, like any laboratory instrument respect must be given to the operation of the analyzer due to environmental conditions, the nature of the samples being tested and of the chemicals which might be near the analyzer. To avoid personal injury or damage to the analyzer, please observe the following precautions: Read all instructions in the Operat­ing Instructions prior to operating your analyzer.
Warning
Control module contains 3V Lithium Battery. Please dispose of in accor­dance with local regulations and conventions.
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Getting Started
Thank you for choosing the Sartorius LMA110S moisture analyzer. The LMA110S is a modular analytical instru­ment designed to be configured to meet various performance requirements. Each analyzer consists of two parts, a control module and a heater module. The con­trol module contains the keypad, dis­play and a printer (optional) with the appropriate electronics. The heater module consists of an electronic bal­ance and heating cavity. Up to two heater modules may be interfaced with a single control module. On initial power-up, the control module will automatically detect how many heater modules have been connected and are powered on. If more than one heater module is detected, the analyzer will run in the multi-module mode.
Storage and Shipping Conditions
Allowable storage temperature: –10 to +50°C –14°F to +122°F
Allowable shipping temperature: –40 to +70°C –40°F...+158°F
Unpacking the Moisture Analyzer
The moisture analyzer is delivered in a set of two custom-made boxes specif­ically designed for this precision instru­ment to provide optimum protection during transportation.
Note
Retain the original packaging in order to ship the analyzer if it needs to be transported or stored at some future time.
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Follow the instructions carefully when unpacking the analyzer:
§ Unpack the analyzer carefully and gently.
§ Remove all the contents of the carton. Check carefully to make sure you have removed all accessory items.
§ The LMA110S consists of two modules, a control module and a heater module. Up to two heater modules may be connected to a single control module.
§ Inspect each module for physical dam­age and report any damage immediately to Sartorius or the distributor that you purchased the analyzer from.
§ Verify that you have received the following accessories:
Instructions for Recycling the Packaging
To ensure adequate protection for safe shipment, your moisture analyzer has been packaged to the extent necessary using environmentally friendly materi­als. After successful installation of the moisture analyzer, you should return this packaging for recycling because it is a valuable source of secondary raw material. For information on recycling options, including recycling of old weighing equipment, contact your municipal waste disposal center or local recycling depot.
Equipment Supplied
– Inter-module cable
– Power module cable
– Pan support
– Pan shield
– Power cord
– Tweezers
– Sample pans
– Operating instructions manual
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General Views of the Moisture Analyzer
No. Designation
Heater Module
1 Pan shield 2 Pan support 3 Cylindrical quartz heating tubes 4 RTD temperature sensor 5 Heater adjustment tool connector 6 LED status lights 7 Service panel, heaters & RTD
temperature sensor 8 Level vial 9 Adjustable leveling feet
10 Inter-module cable receptacle 11 Main power switch 12 Main cord receptacle 13 Fuse 1 (250 V~5A T) 14 Fuse 2 (250 V~5A T) 15 Module power cable receptacle
No. Designation
Control Module
16 Storage Bin 17 VGA display 18 Soft keys and display overlay 19 Keypad 20 Inter-module cable receptacle 21 Module power cable receptacle 22 Ethernet socket: only for Sartorius
Service
23 USB socket: only for Sartorius
Service
Cables and Power cord
24 Serial connector 25 Inter-module cable 27 Main power cord
10
16
17
18
19
4
3
8 7 5
1 2
6
9
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Control Module Connector Panel
Heater Module Connector Panel
Cables Connected to Control and Heater Modules
11
23
20
21
11
15
12
21 20
25 26
27
24
22
10
13
14
15
10
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Assembly
The analyzer does not come fully assembled. The control and heater modules are placed next to each other and may be placed on either side of each other. Assemble the modules and individual components in the following order:
1. Open the heater hood using the handle and install the pan shield so that the center hole fits over the center ring of the cavity base plate.
2. Next, place the stem of the pan support through the center ring of the base plate and into the hole of pan receiver.
3. Remove the foam from the heater chamber.
4. Connect the power module cable between the control module and the heater module, observing the pin orien­tation.
5. Connect the inter-module cable between the control module (MOD COMM 1 connector) and the heater module, observing the connector orien­tation.
6. If multiple heater modules are used, install the additional inter-module cables from each heater module to the control module inter-module cable receptacle (MOD COMM 1-2). Refer to the chapter in this manual on multi­mode operation for instructions specific to operating multiple heater modules.
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Choosing a Suitable Location
In order to ensure that the analyzer functions properly, select a location that meets the following requirements:
§ Permissible ambient environment – Temperature:
+15 to +40°C (59°F to 104°F)
– Relative humidity:
10 – 85%, non-condensing
– Altitude:
0 to 2,000 meters (0 to ~6562 ft)
§ The analyzer is intended for indoor use.
§ Place the analyzer on a rigid, horizontal
surface, preferably free of vibration.
§ Avoid drafts and excessive temperature fluctuation.
§ Locate the analyzer away from flammable materials.
Connecting the Moisture Analyzer to AC Power
This Class I Equipment (grounded type) analyzer contains a universal self-adjusting power supply rated to 100-120/200-250V~5/2.5A 50/60 Hz. Check that this voltage matches your local line voltage. If your voltage is not within this rating, do not connect the power cord to the power supply.
Danger
! The analyzer may only be operated
using the original power cord supplied. Please do not use it with an extension cord. The wall socket must be grounded. The AC Power mains supply fluctuations are not to exceed +/–10% of the nomi­nal supply voltage. The (Over Voltage) Category II for transient over voltages is EN 61010-1. The pollution Degree 2 is supplied EN 61010-1. The analyzer is rated to Normal Protection (not protected against harmful ingress of moisture).
§ Insert the power cord that with the analyzer into the power input receptacle on the back of the heater module.
§ Then plug the power cord into a wall socket.
§ Turn the analyzer on by moving the power switch on the back of the analyzer to the On position. The analyzer will briefly proceed through a self-diagnostic routine and then display the standby screen. It will automatically enter a warm-up period as noted on the screen. Should the analyzer display any warn­ings, consult the troubleshooting sec­tion of this manual, or call Sartorius.
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Leveling the Moisture Analyzer
In order to function properly, the heater module should be horizontal. The heater module has a level vial. You can tell when the analyzer is level by checking whether the bubble is centered in the vial.
§ Check that all four feet are in the fully inserted position.
§ Observing the level vial, rotate one foot at a time to level.
Adjust control module so that it does not rock.
Note
The heater module must be re-leveled each time the analyzer is moved.
LMA110S Keypad
Warm-up
To enable the analyzer to function optimally, plug it in and leave it pow­ered on for a minimum of 15 minutes. The analyzer is preprogrammed to alert the operator that the device is in the warm-up period. It is best to allow the analyzer to complete this warm-up period before testing samples; however, this may be overridden by pressing the Enter key.
14
Numeric keys
Soft keys
Navigational keys
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Operating Design
The Mark 3 LTE analyzer is operated through the keypad in conjunction with the quarter VGA screen. The Mark 3 LTE is preprogrammed with operational and setup software that enables the analyzer to be custom configured to meet the particular needs of the application, environ­ment or user ability.
Keypad
The analyzer has two membrane type keypads: the main keypad and a second that also serves to sealed the display. The keypad consists of three dedicated keys, numeric keys, navigational keys and soft keys. The following is a description of each of the key functions:
Dedicated keys:
Each key has a particular function. Pressing the key once will initiate the desired action.
Initiates the testing of a sample
Stops a test in progress
u Press to finalize the entry of
a numeric value
– Selects the highlighted menu
selection in a list
– From the Standby screen will print
the last result
Start|Stop
Numeric and Decimal Point Keys
Numbers from 0 to 9 and the deci­mal point are pressed either to enter a specific numeric value or to make a selection from a list of menu choices preceded by a number.
Navigational Keys
Four keys are intended to move the highlighted cursor on the screen in a particular direction.
Moves the cursor to the right
Moves the cursor to the left
Moves the cursor up
Moves the cursor down
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Soft keys:
The functionality of these keys will change depending on what is on the display. A label on the display just above the key will describe the key function at the moment. Some examples of the soft keys are as follows:
Prints various items corresponding to the menu selection
Toggles a highlighted selection between on and off
Used to select a drying program from the Program menu
Access to all setup parameters from the Setup menu.
Setup
Recall
On/off
Print
Used to select an operator. Name will be printed on the results printout.
Display will return to the previous menu.
Display will return to the Standby menu.
Deletes the single highlighted character when entering alphanu­meric program names and operators.
Sets analyzer to the weighing mode.
Weigh
Delete
Users
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Display Modes
The large quarter VGA display is designed to make operation and setting up the analyzer easy through of detailed information in clear descriptions, choices or menus. The analyzer will display information in several different formats as described below:
Warm-up:
This mode is entered whenever the analyzer is pow­ered on. The warm-up period ensures that the ana­lyzer is properly conditioned before testing is begun. During warm-up the screen will be mostly blank.
Standby (or Test Done):
In this mode the analyzer is in an ideal status. This is the period between testing samples. The temperature of the chamber is controlled to a particular level based on the Standby temperature set for the last test performed. The screen will display the program name, date and time, temperature and the last result, if a test has been run.
Test:
This mode is entered when the Start|Stop key is pressed to initiate a test. The screen is similar in design to the Standby mode but also includes prompts to guide the operator through the steps of adding a sample, entering an ID, if desired, and displaying the result when the test is completed.
Default
05/01/2011 02:14 PM
WARMIN G UP
Ver. 1.00.00
Mark 3 LTE Moisture Analyzer
Recall
Setup
Weigh
Users
Press ENTER to override warm up
Default
05/01/2011 02:14 PM
WARMIN G UP
Ver. 1.00.00
Mark 3 LTE Moisture Analyzer
Recall
Setup
Weigh
Users
Press ENTER to override warm up
Add sample to pan
DRY MILK POWDER
05/01/2011 02:14 PM
Module 1
0.000
g
Zero
{ }
0%
Standby
Current
60 57
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Graph:
The graph mode can be entered during or after a test to show a graph of the weight versus time, temperature versus time, or result versus time.
Data Log:
The data log mode is used for reviewing past samples that have been tested. The log of samples can be sorted, or samples can be manually selected to perform statistical calculations.
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Temperature / time
DRY MILK POWD ER
05/01/2011 02:14 PM
Print Result
210
30
0.5 1.0 1.5 2.0 2.5 3.0
3.5 4.0 4.5 5.0 min
25.67 %
View Data Log
Down Up
Top
Dry milk power 05/01/2011 02:10
3.45%M 6.7min 672001 Dry milk power 05/01/2011 02:02
3.50%M 6.8min 672002 Dry milk power 05/01/2011 01:53
3.47%M 7.0min 672003
05/01/2011
02:18 PM
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Menu Structure
The Mark 3 LTE set up software is structured according to a series of menus. The Setup menu lists several topics of instrument setup. By drilling down into these topics, sub-menus will allow specific choices to be selected. See the Setup section for details.
How to navigate in the menu structure:
§ To select a menu and to drill down to more specific information: – Press the preceding number key of this listing or – Use the navigational arrow keys to highlight the
desired listing first, then press the Enter key
§ To return to a preceding menu level, press the arrow soft key. Subsequent presses will return you to the Standby screen.
§ To return to the Standby screen, press the bent arrow if one is available from that screen. To choose
a specific selection option or to enter a value:
A selection can be made by: – Pressing the preceding number key of this listing, or – Using the navigational arrow keys to highlight the
desired listing first, then press the Enter key.
§ How to make a numeric input: – Use the numeric keypad to enter a value fist, then
press the Enter key.
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1)Program manage
2)Data log
3)Modify operators
4)Results printout format
5)Time and date
6)Communication ports
7)Conserve mode
8)Security
9)Audio & video
0)Module port scan
. ) Service
Setup Menu
05/01/2011 02:18 PM
Page 20
Data Output
LED Status Lights
The Mark 3 LTE heater module has two LED lights on the front left corner that visually indicate the status of the ana­lyzer. The left LED shows the status of the balance. The right LED indicates the status of the heating function.
Each LED may have three colors: red, green or amber. Red is generally associated with a warning state and shows that corrective action must be taken. Green is generally associated with a positive condition, indicating you can proceed. Yellow generally indicates a transitional period or that the test is in progress.
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Warmup
Balance LED
Heater LED
Warming up
Rapidly ashing RED Rapidly ashing RED
Ready to test
Steady GREEN Steady GREEN
Heater in conserve mode
Steady GREEN Steady YELLOW
Standby
Balance LED Heater LED
Sample in chamber heating cavity (chamber)
Flashing YELLOW Flashing GREEN
Test mode Balance LED
Heater LED
Test in progress Steady YELLOW
Steady YELLOW
Test done
Flashing YELLOW Flashing GREEN
Sample loading
Below target
Flashing GREEN
Steady GREEN
Within target Flashing YELLOW
Steady GREEN
Above target Flashing RED
Steady GREEN
Diagnostics Balance LED
Heater LED
Failed diagnostics
Flashing RED
Flashing RED
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The Mark 3 LTE Moisture Analyzer is designed to test moisture content in a large variety of materials including powders, pastes and liquids. The perform­ance of the analyzer is dependent upon selecting optimum drying analysis conditions for your specific sample type. Sartorius will support you in finding the set of testing parameters (referred to as a pro­gram) you need for your specific tests. On request, we will provide a chart of the parameters and test results we have compiled by testing samples in our laboratory and comparing the results to those obtained by reference methods.
If our chart of applications shows a drying program that is not already programmed into your analyzer, you may do this yourself by following the instruc­tions under Setup in this manual.
Standby Screen
During warm-up, your analyzer will enter the Stand­by mode and the Standby screen will be displayed. It is from the Standby (or Test Done) screen that all functions of operating the analyzer, including test­ing samples and setting parameters, take place.
The standby screen shows the following information:
§ Program name
§ Time and date
§ Standby temperature and actual temperature
§ Various soft keys for options that are available
depending on the security setup options engaged
§ Warnings that will need to be addressed before testing
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Operating the Moisture Analyzer
DRY MILK POWDER
Standby
Recall Setup
Weigh Users
Press START key to begin test
Standby
Current
60 59
05/01/2011 02:18 PM
Ver. 1.00.00
Mark 3 LTE Moisture Analyzer
Page 22
Functions available from the Standby screen:
§ Press Start|Stop key to initiate a test
§ Press Recall soft key to change the program to
be used for testing a sample
§ Press User soft key to select an operator name
(feature must be turned on in Setup)
§ Press Setup soft key to enter the Setup menu in
order to make all parameter changes
§ Press Graph soft key to display a graph
§ Press Weigh soft key to use as a balance
Standby-Temperature
!
with a New Program
When creating a new program, the standby temperature setting from the previous drying program is used automatically by the analyzer.
Example: You have created a new program for drying a temperature-sensitive sample at low tempera­ture. The analyzer uses the standby tempera­ture, e.g. 165°C, from the previous program. You must call up the standby temperature parameter and change the temperature value. If you forget performing this setting, your ana­lyzer is always too hot before starting the test.
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Default Drying Program
Your analyzer is delivered with a default drying pro­gram. The drying program contains all the specific parameters to test a sample including temperature, endpoint, unit of measure, standby temperature, etc. You will notice if you are in the default program or a specific material program by the program name at the top left of the display.
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Program name: Default Temp1=105C Time1=Off Temp2=Off, Time2=Off Slope=0.050%/1 minute, Actual Start delay=0 second Standby temp=60C, ­Ideal weight=5g, Lock=Off Target limits=Off Mode=Standard
Page 24
Recalling a Program
Drying programs are stored for easy access at a later time. This eliminates the need to change parameters for frequently tested samples. Up to 60 drying pro­grams can be stored. Creating and storing a program is described under Developing a Drying Program.
To recall a stored program, perform the following steps:
1. From the Standby screen, press the RECALL soft key. The screen will change to the first page of stored programs as show below.
2. To display programs on the next pages, press the Down soft key.
3. Press the number(s) key followed by the Enter key for the number that precedes the program name. As an alternative, use the arrow keys to highlight the desired program name, then press Enter. The display will change to the Standby screen with the new program in the top left corner. This program will be used for the next test. If a blank program is entered, the analyzer will use the last valid program that was entered.
Note
As a shortcut, it is not necessary to have the desired program listed on the display to recall it. Simply enter the desired number from your memory on the first page and press the Enter key.
24
11)
2) Whey Protein 12) )3
1 )3
)4
1
)
4
)5
1
)
5
)6
1
)6
)71 )7
)8
1
)
8
)91
)9
)0
2
)01
Programs
Program #:
Down
1)
Dry Milk Powder
Up
_
Top
05/01/2011 02:18 PM
Page 25
Testing a Sample
A test can only be initiated from the Standby or Test Done screen. The program that will be used is shown in the upper left corner.
To test a sample, perform the following:
1) Open the hood of the heater module using the handle on the front of the analyzer.
Caution
The heater hood will be hot during testing and the standby mode. Only touch the heater hood by the handle.
2) Place one pan onto the pan support and close the heater hood.
3) From the Standby screen, press the Start|Stop key. The display will change to the test mode as shown on the left. The balance will automatically tare and show zero weight on the screen.
Note
If you forgot to place the pan onto the balance ahead of time, you may open the heater hood now, add the pan, close the heater hood and manually tare by pressing the Zero soft key.
25
DRY MILK POWDER
Standby
Recall Setup
Weigh Users
Press START key to begin test
Standby
Current
60 59
05/01/2011 02:18 PM
Ver. 1.00.00
Mark 3 LTE Moisture Analyzer
Sampling
DRY MILK POWDER
Module 1
0.000
g
Zero
{ }
0%
Standby
Current
60 57
05/01/2011 02:19 PM
Page 26
4. At the “Add sample to pan” prompt, open the heater hood and begin adding sample to the pan. A bar graph on the display will guide the operator to place the correct amount of sample as set by the ideal weight parameter of the drying program. Continue adding sample until the beeper sounds, indicating that the sample amount is within 10% of the ideal weight. The exact weight is also displayed on the screen.
5. At the “Close heater hood” prompt, close the heater hood. The balance will capture the initial weight of the sample “Sampling” and then show that the test is in progress. The display will change to show cur­rent information including the elapsed time and the current percentage weight loss in the units as speci­fied in the drying program.
Note
To stop the test in progress, press the Start|Stop key.
The optional printer will begin to print as the test begins. Printout information can be selected in Setup menu under Printer.
At the end of the test the display will show “Test Done.” The result will stay on the screen as well as be printed. The analyzer will enter the Standby mode until the next test is initiated.
26
Dry Milk Powder
Test in Progress
0.01
% Moisture
Elapsed time: 00.10
Graph
Press STOP key to stop test
Temp 1
Current
105
71
05/01/2011 02:18 PM
Press START key to begin test
Dry Milk Powder
Test Done
3.47 % Moisture
Result time: 7.0 min
ID: 126399.1
Target: Pass
Recall Setup
Graph User
Warning: Sample on pan
Standby
Current
105 105
05/01/2011 02:18 PM
Page 27
The display will prompt you, the operator to remove the sample before the next sample can be test­ed. Open the hood and carefully remove this sample using tweezers, and while the hood is open, add the sample pan for the next sample to be tested.
Caution
!
The sample is hot during and after the test. Remove the sample with care by using the tweezers provided with the analyzer. Do not touch any internal part of the heating chamber or pan shield as they will be very hot.
Press the Start|Stop key to begin the next test using the same program.
Note
The analyzer balance must be calibrated before putting the unit into routine service. See the section on Calibrate Balance in this manual.
27
Page 28
Setup Menu
All settings for to the Mark 3 LTE, including chang­ing of instrument options and program parameters, are selected in the Setup menu. Each subject is listed on the Setup menu screen.
To enter the Setup menu:
§ From the Standby screen, press the Setup soft key to display the Setup Menu screen.
Note
Pressing the arrow soft key from the Setup menu or any submenu will always take you back one level.
Setting the Device Parameters in the Program Manage Menu
The Program Manage Menu provides access to all setup functions associated with creating, editing, or managing sample drying programs.
To enter the Program Manage Menu:
§ From the Setup menu screen, press the 1 key or highlight “Program manage”, using the naviga­tion keys and press Enter.
28
1)Program manage
2)Data log
3)Modify operators
4)Results printout format
5)Time and date
6)Communication ports
7)Conserve mode
8)Security
9) Audio & video
0) Module port scan
.
) Service
Setup Menu
05/01/2011 02:31 PM
Page 29
Edit Current Program
All parameters associated with a currently stored drying program can be edited and re-stored or changed without re-storing. The program to be edited will be in the top left corner of the display. If this is not the program you wish to edit, then it must first be recalled.
To edit a current program:
§ From the Program manage menu, press the 1 key to display the Program Menu screen.
All the parameters of the drying program are displayed on this screen for the program named in the top left corner. To make a change to any of the parameters, enter the submenu for that topic. A complete list of all variables for each parameter is shown on the next page.
To edit a current program without storing:
§ Make the change, then press the arrow key to return one level.
§ Alternatively make the change, then press the bent arrow key to return to the Standby screen. On the
Standby screen, the warning will show that the changes have not been saved.
To save an edited program:
§ Make changes, then press the Save soft key to return to the Standby screen.
29
Default
Program Manage Menu
1)Edit current program
2)Create new program
3)Delete program
4)Sort programs (alphabetize)
5)Sort programs (fill in blanks)
6)Print current program
7)Print program list
8)Print all programs
05/01/2011
02:18 PM
1) Unit Moisture (0.00%)
2) Temp 1 105C, std, Time 1 O
3) Temp 2 O, Time 2 O
4) Slope 0.05%/1min, actual
5) Start delay 0 sec
6) Standby temp 60C, Equilibrate O
7) Ideal weight 5g, lock O
8) Target limits O
9) Mode Standard
0) Program name Default
Press Save soft key to save changes.
Program Menu
Default
05/01/2011 02:18 PM
Print
Save
Page 30
Table: Program Settings
Screen Parameter Variables Explanation
Units Units Moisture Initial wt. – final wt. / Initial wt. + 100
Solids Final wt. / Initial wt. + 100 Volatiles Initial wt. – final wt. / Initial wt. + 100 Moisture/dry Initial wt. – final wt. / Final wt. + 100 mg/l Final wt. + 1000 / volume in mL
Weight Initial wt. – final wt. Result display Decimal place 0.01% or 0.001% Factors Scale factor Factored result = (result + scale factor) + offset
Offset Factored result = (result + scale factor) + offset
Temperature 1 Temperature Maximum 210°C Set temperature or Off
Time 10.0 – 99.9 minutes Set time or Off
Temperature 2 Temperature Maximum 210°C Set temperature or Off
Time 20.0 – 99.9 minutes Set time or Off
Slope % Initial weight 0.01 – 9.99 Weight variable of endpoint criteria
Window of time 0.1 – 99.9 minutes Time variable of endpoint criteria Calculation Actual slope Slope criteria met for endpoint
Calc 1 Calculated endpoint
Calc 2 Calculated endpoint
Calc 3 Calculated endpoint
Start delay Start delay 0 - 9 seconds Delay before starting test
Mode Mark 2 Simulates Mark 2 start delay
LMA110S LMA110S start delay
Standby temp. Standby temp. Maximum 165°C Set temperature between tests Ideal weight Ideal weight 0.1 – 99.0 g Set ideal sample weight for test
Percent 1 – 10% Set tolerance of ideal weight Ideal weight Lock On or Off Set ideal weight lock strict (On) or Off
Target limit Target limit Upper limit Set upper limit of result tolerance
Lower limit Set lower limit of result tolerance Turn limits Off Turns target limit feature Off
Mode Mode Standard Standard test mode
Concentration Corrects a result for sample volume
30
Page 31
Units
The analyzer will calculate the test result in a variety of units of measure, depending on your specific application. This menu also provides access to the advanced options associated with units: displayed readability and correlation factors.
To change the unit of measure:
§ Press the 1 key from the Program Menu to display the Units menu. The current unit will be shown.
§ Press a number key for the new unit of choice.
§ Note that there is an advanced option indicated by
Factor on the soft key. To change this feature, see “Factors.”
§ When all the parameters for units have been changed, then press the arrow soft key to accept the changes. The display will return to the Program Menu.
31
Current units: Moisture
1)Moisture
2)Solids
3)Volatiles
4)Moisture/dry
5) Weight
Units
Default
Factors: active
05/01/2011 02:24 PM
Factor
Page 32
Factors
The analyzer has a feature for entering a scale or offset factor to adjust the result to a more accurate value. Only under special circumstances will either of the factors ever be used.
To set or change factors:
§ Press the 1 key for Units to display the Units screen.
§ Press the Factor soft key. The display will change to
the Factors screen.
§ Press the 1 or 2 key to display either the scale factor or offset screen.
§ Enter the desired value and press the Enter key to return to the Factors screen.
§ Press the Arrow soft key to return to the Units screen.
(result) · (scale) + offset
32
Current units: Moisture
1)Moisture
2)Solids
3)Volatiles
4)Moisture/dry
5) Weight
Units
Default
Factors: active
05/01/2011 02:24 PM
Factor
Factors
Default
1) Set scale factor: 1.000
2) Set offset: 0.000
Enter the scale and offset to apply to the result calculation:
(Result)*(Factor) + Offset
05/01/2011 02:21 PM
Page 33
Temperature 1 and 2
The analyzer will dry the sample at one or two temperatures set in one degree of Celsius incre­ments. A second temperature is optional and is nor­mally set to Off. See the Applications section for a description of when to use a second temperature for two-step drying.
To set or change Temperature 1 or Temperature 2:
§ Press the 2 or 3 key for Temp 1 or Temp 2, respectively. The display will change to the Temp 1 or Temp 2 screen. The current temperature will be shown.
§ Using the numeric keys, type in the desired tempera­ture and press Enter.
§ Note that there are some advanced options indicated by Ramp and Time 1 (or 2) on the soft keys. To change these features see, “Time 1 and 2.”
§ When all the parameters for Temperature 1 or 2 have been changed, press the Enter again or the Arrow key to accept the changes. The display will return to the Program Menu.
33
Temperature: 105 C
Max. Temperature: 210 C
Time: 99.9 minutes
Temperature 1
Default
| C
Clear
Time
05/01/2011 02:21 PM
Page 34
34
Time 1 and 2
Each the Temperature 1 and 2 setting can have a set period of time. Time 1 or 2 is the time during which the sample will be dried at each temperature before advancing to the next temperature. Once the time for the last temperature has elapsed, the test will terminate unless a slope endpoint has been turned On. If Temperature 2 is set, then at the end of Time 1, the analyzer will ramp to Temperature 2.
To set or change Time 1 or 2:
§ Press the Time 1 or Time 2 soft key to display the Time 1 or Time 2 screen.
§ Use the numeric keys type in the desired temperature, then press the Enter key. The display will return to the Tempera­ture 1 or 2 screen.
Slope
The slope function provides an auto­matic endpoint for the test. The slope function consists of two variables: window of time and percent of initial weight (%IW) change. During the test, the weight change of the sample is con­tinuously monitored within a moving window of time. When the loss of weight within the window is less than the initial weight percentage set, the slope criteria has been met. The final weight is taken and calculation is performed to end the test. This slope is referred to as “actual slope” because the endpoint is actually achieved.
Tim
e
W
e i g h t
% of I.W.
W
indow of time
End of test (Endpoint)
W
Page 35
To set or change slope:
§ Press the 4 key from the Program Menu to display the Slope screen. The current initial weight percent­age is shown.
§ Use the numeric keys type in the desired %IW, then press the Enter key.
§ Note that there are some advanced options indicat­ed by Time and Calc on the soft keys. To change these features, see “Windows of Time” or “Calcula­tion Endpoint.”
§ When all the parameters for Slope have been changed, press the Enter again or the Arrow key to return to the Program menu.
Window of Time
To set or change window of time:
§ Press the Time soft key to display the Window of time screen.
§ Use the numeric keys to type in the desired window of time, then press the Enter key. The display will return to the Slope screen.
Endpoint Calculation
There are three additional advanced slope settings called Calc 1, Calc 2 and Calc 3, which are algo­rithms that calculate the endpoint prior to achieving the actual slope. These will provide more rapid results on some samples; however, the success of the Calc mode varies from case to case.
To set or change Calc endpoint:
§ Press the Calc soft key to display the Calc menu.
§ Press a number key to select the desired calculation
setting. The display will return to the Slope screen.
§ If developing a method, check the correlation of each Calc mode starting with Calc 1 to the actual endpoint result.
35
Enter percent of initial weight: 0.05
Range: 0.00 to 9.99%
Enter 0.00 to turn off slope
Time: 1.0 Minute
Calculation: Actual
Slope
Default
| %
Time
New
Calc
05/01/2011 02:24 PM
Page 36
Start Delay
The start delay is a time in seconds that can be set to ensure that a good initial weight is taken at the beginning of the test.
To set or change start delay:
§ Press the 5 key from the Program Menu to display the Start delay screen. The current start delay is shown.
§ Use the numeric keys to type in the desired %IW, then press the Enter key.
§ Note the mode: Mark 2 or LMA110S. If in the Mark 2 mode, start delay will simulate the previous Mark 2 analyzer. Press the Mode soft key to toggle between Mark 2 and LMA110S.
§ Press the Enter key again or the Arrow soft key to return to the Program Menu.
Standby Temperature
The standby temperature is the temperature that the analyzer chamber will be controlled to at the end of a test or prior to a test when a new program is recalled.
To set or change standby temperature:
§ Press the 6 key from the Program Menu to display the standby temperature screen. The current standby temperature is shown.
§ Use the numeric keys to type in the desired standby temperature, press the Enter key.
§ When all the parameters for slope have been changed, press the Enter key again or Arrow key to return to the Program Menu.
36
Enter standby temp: 60 C
Maximum temperature 165 C
Standby Temperature
Default
| C
Clear
05/01/2011 02:31 PM
Page 37
Ideal Weight
The ideal weight is the amount of sample in grams that should be used for the test as prompted with a bar graph and beeper in the Test mode.
To set or change the ideal weight:
§ Press the 7 key from the Program Menu to display the Ideal Weight screen. The current ideal weight is shown.
§ Use the numeric keys to type in the desired ideal weight then press the Enter key.
§ Note that there are some advanced options indicat­ed by Lock and % on the soft keys. To change these features, see “Ideal Weight Percent Limit” and “Ideal Weight Lock.”
§ When all the parameters for slope have been changed, press the Enter key again or the Arrow key to return to the Program Menu.
37
Enter ideal weight: 5.0 g
Range: 0.1 –39.0 g
Ideal weight percent: 10%
Lock: Off
Ideal weight
Default
| g
Lock
Clear
%
05/01/2011 02:24 PM
Page 38
38
Ideal Weight Percent Limit
The ideal weight limit is a tolerance range for the ideal weight in percent that the sample weight must be in. Example: If the ideal weight is 10 grams, and the target limit is 10%, then an acceptable sample weight is between 9 and 11 grams.
To set or change the Ideal weight per­cent limit:
§ Press the % soft key to display the Ideal weight percent screen.
§ Use the numeric keys to type in the desired time, press the Enter key. The display will return to the Ideal Weight screen.
Ideal Weight Lock
When activated, the ideal weight lock prevents the use of any other sample weight other than the one that is within the target limits. If the lock is not acti­vated, when in the test mode, the target weight guide is still shown but any sample weight can be used for the test.
To set or change ideal weight lock:
§ Press the Lock soft key to toggle On or Off on the Ideal Weight screen.
Page 39
Target Limits
The Target limit Menu provides a statistical process control (SPC) feature that can be set to identify when a tested sample is within or outside the desir­able limits selected. If this feature is activated, a Pass or Fail will be displayed after each test, indicating the sample is within or outside the set limits; this will also appear on the printout.
To turn the Target Limits feature on and to enter limits:
§ Press the 8 key from the Program Menu to display the Target Limits screen. The current target limits are shown.
§ Press the On|Off soft key to toggle target limits: On
§ Press the 1 key to set the upper limit.
§ Press the 2 key to set the lower limit.
When all the parameters for target limits have been changed, press the Arrow key to accept the changes. The display will return to the Program Menu.
39
1. Upper Limit 100.00% Moisture
2. Lower Limit 0.00% Moisture
Target Limits Menu
Default
On/off
05/01/2011 02:24 PM
Page 40
40
Test Mode
This feature provides a few special test modes for specific applications:
§ Standard: normal test mode where a sample is placed directly onto the pan or pan with sample pads to take a direct weight of the initial weight.
§ Concentrate: used for determining total suspended solids in low solid samples. The sample solids are first concentrated onto a filter pad placed in a vacuum apparatus. During the test mode, the operator will then be prompted to enter the number of milliliters of sample that was filtered. Results are displayed in mg/l. See details in the chapter on Concentration Mode in this manual.
To change the test mode:
§ Press the 9 key from the Program Menu to display the Mode screen.
§ Press the number key for the mode of choice. The display will return to the Program Menu.
Page 41
Program Name
Each program is stored by a unique program name. Your analyzer may be preprogrammed with a default set of programs or a set customized for your company. Program names can be alphanumeric and have some characters.
To change or set the program name:
§ Press the 0 key from the Program Menu to display the Program Name screen.
§ Use the navigational arrow keys, up and down, to enter letters, symbols or a space at the cursor. Pressing the up arrow key first shows a space, then scrolls through the alphabet starting with “A” forward, followed by symbols. Pressing the down arrow scrolls through the symbols followed by letters in backwards order. To change to lower case letters, press the Lower soft key.
§ After selecting the first character, press the naviga­tional arrow right key to move to the cursor to the next character space and repeat the process.
§ The navigational arrow left key moves the cursor left.
§ When finished entering the program name, press the Enter key to return to the Program Manage menu Menu.
41
Program name: Default
Enter numbers with keypad
Program Name
Default
Lower
Clear
Delete
05/01/2011 02:24 PM
Page 42
42
Create a New Program
The analyzer will store 60 drying pro­grams. New programs can be created and stored for routine usage. All drying program parameters are set as described in “Edit Current Program” on page 30. When creating a new program, the parameters will be used of the last pro­gram to be recalled.
Note
When creating a new program, you will edit the last program to be recalled and shown on the Program Menu screen. However, you will need to give it a new program name for storing. Therefore, first choose a program that is most sim­ilar to your new program to minimize the amount of changes to make.
To create a new program:
§ From the Program Manage menu press the 2 key for “Create new program” to display the Program Menu screen.
§ The program name will be labeled “New.” Change program to your desired name.
§ Finish making changes to all program parameters as desired.
§ Press the Save key to store the new program in the first available blank program slot.
Note
Programs will be saved when down­loading a new software version.
Delete Program
At times you may want to delete a drying program that you will no longer need.
To delete a program:
§ From the Program Manage menu, press the 3 key to go to the Delete screen showing the list of programs.
§ Type in the number of the program you want to delete or move the highlight with the navigation arrow keys and press the Enter key. The screen will return to the Program Manage menu.
Sort Programs
Programs can be sorted in two ways to make them easier to view when recalling programs:
§ Alphabetical: sorts by alphabetical order starting with characters, numbers and then letters.
§ Fill in the blank: removes all the blank program positions and places programs in the storage positions starting at 1 in the same order as before the sort.
To sort programs:
§ From the Program Manage menu, press the 4 or 5 key. The display will change, indicating that the analyzer is sorting. When finished, the display will return to the Program Manage menu screen.
Page 43
Configuring the Printout
Print Current Program
To print the parameters of the current program as shown in the top left corner of the Program Manage menu screen:
§ From the Program Manage menu, press the 6 key. The current program will be printed.
Print Program List
To print the entire list of programs:
§ From the Program Manage menu, press the 7 key. The list of programs will be printed.
Print All Programs
To print all programs with parameters:
§ From the Program Manage menu, press the 8 key. The list of programs with parameters will be printed.
43
Page 44
Data Log
The analyzer will store the last 999 test results. Results can easily be sorted, viewed on the display or printed. In addition, you can perform statistical analysis on sorted or selected results for viewing or printing. Sorted data may be also downloaded.
Note
The default setting for the data log is Off. To store data to the data log, it must be turned On first. Results in the data log are saved when dowd loading a new software version.
To enter the data log:
§ From the Standby screen, press the Setup soft key to display the Setup menu screen.
§ Press the 2 key or highlight “Data log” and press the Enter key to display the Data Log menu.
To enable data to enter the data log:
§ From the Data Log menu, press the On|Off soft key to toggle data log to On.
To prevent data from entering the data log:
§ From the Data Log menu, press the On|Off soft key to toggle data log to Off.
To view data log results:
§ From the Data Log menu, press the 1 key to display the data log.
§ Use the soft keys to move through the data:
Up Moves to more recent data Down Moves to older data
To manually select data log results to form a group:
§ From the Data Log menu, press the 5 key to display the data log selection screen. The last group selected is still retained.
44
1)View data log
2)Statistics
3)Select by date range
4)Select by module
5)Select data points
n
O :gol at
aD
Number of points in log:495
Data log menu
05/01/2011 02:43 PM
On/Off
Page 45
§ Toggle the Select All or Clear All soft key to select or deselect all data in order to define a known starting point.
§ Use the navigation keys to scroll through the data: right arrow to page down, left arrow to page up.
§ Highlight a test result and press the Enter key to show STAT. Continue for all desired results to form the group.
To print the data group:
§ From the data log selection screen, press the Print Stat soft key to print the selected group results.
To print the entire data log:
§ From the data log selection screen, press the Print All soft key to print all the data log results.
To print statistics for a group:
§ After selecting a group from the data log selection screen, press the Arrow soft key to return to the Data Log menu while retaining the group.
§ From the Data Log menu, press the 2 key to view statistics of the selected results. The display will show statistics including the average, standard devia­tion, relative standard deviation, the highest value and the lowest value.
§ To print the statistics, press the Print soft key. Use the Arrow soft key to return to the Data Log menu.
To select by date range:
§ From the Data Log menu screen, press the 3 key for Select by date range to go to the Select data range screen.
§ Press the 1 key and set a start date
§ Press the 2 key and set an end date
§ Press the Arrow soft key to sort the
data log for this date range.
All data in the data log tested on and between these dates will be retained as a group. The display will return to the Data Log menu screen. From here you can perform statistics on the group by pressing the 2 key for Statistics, or view selected data by pressing the 5 key for Select data points. All data in this group will be displayed when you press STAT. From here you may print this group by pressing the Print soft key.
45
Page 46
Modify Operators
our analyzer may be programmed with a custom list of operators specific for your company. Operators can be alphanumeric and contain various characters.
To change or set operator names:
§ Press the 3 key from the Setup menu to display the current list of operators.
§ Use the arrow soft keys, then press Enter for any operator slot to display the alphanumeric entry screen. You may also press the Edit soft key for the highlighted name.
§ Enter the desired name, then press the Enter key to return to the Set Users/Operators Menu.
§ Line 20 is a blank line that cannot be edited.
§ When finished, press the Arrow soft key to return to
the Setup menu.
Note
To enable the use of Operators and to have the operator name on the result printout, Operator must first be activated in the Results Printout Format menu. When Operator is activated, then the User soft key will be available from the Standby menu to select an operator from the list of operators.
Note
Operator names will be deleted when downloading a new version of software.
46
••
••
••
••
••
••
••
Operator setup
Edit Clear
05/01/2011 02:24 PM
Page 47
Graphing
Your analyzer is able to display and print a graph of the current or last test.
Three styles of graphs are available: – Percent|time – Weight|time – Temperature|time
To view the percent|time graph during
a test:
§ From the Test in Progress screen,
press the Graph soft key. The display
will show the Result|Time graph.
The graph automatically updates and
scales until the test is completed.
When the test has been completed it
will automatically scale one more time.
To view the weight|time graph during
a test:
§ From the Percent|Time graph, press the
Weight soft key.
To view the Temperature|Time graph
during a test:
§ From either the Percent|Time or
Weight|Time graphs, press the Temp
soft key.
To return to the Percent|Time graph:
§ From either the Weight|Time or Temp|Time graphs, press the % (result) soft key.
To return to the Test in Progress screen during a test:
§ From any graph screen, press the Test soft key.
To view a graph from the Test Done or Standby screen after a test is com­pleted:
§ Prior to running a new test, press the Graph soft key.
To print any graph: After the test is completed, from the Test Done screen, press the Print soft key while displaying any of the three graphs.
47
Page 48
Results Printout Format
The printout format is used with the internal printer (optional) or the serial communications port.
The printout format may be customized by choosing the specific content regarding the analyzer or your testing conditions that may be important to your testing program. The default printout format is shown below:
To change the printout format:
§ From the Setup Menu screen press the 4 key or highlight Results Printout format using the naviga­tion keys and press Enter to display the Results Printout menu.
48
Results Printout Menu
On/Off
05/01/2011 02:44 PM
1.Header
2.Analzyer Info
3.Operator
4.Sample number
5.Calibration Info
6.Program name
7.Program info
8.Interval print
9.Weight info
0.Signature line
On On Off Off Off On On Off On Off
LMP110S Moisture Analyzer Module 1: M30604026 Program 1: Default UNITS: Moisture MODE: Standard START DELAY: 0 sec M2 TEMP1: 105C, Std TIME1: Off TEMP2: Off TIME2: Off SLOPE: Window: 1.0 %IW: 0.05 Actual STANDBY: 60C IDEAL WT: 5.0 grams LOCK: Off RESULT on 05/15/2011 at 10:24 AM Elapsed time: 07:13
52.46 %M
Initial Weight = 5.167 grams Final Weight = 2.456 grams Weight Loss = 2.711 grams
Page 49
49
§ Press the number key corresponding to the content to be added to the Result Printout format.
§ The following content is either On or Off: Analyzer info Operator Calibration info Program name Program info Weight info Signature line
§ The following content requires a selection or input: Header Sample number Interval print
A complete printout format is shown to the left:
Header line 1 Header line 2 Header line 3 LMA110S Moisture Analyzer Module 1: M30604026 Operator: John Smith Sample ID: 1 Calibration external: 06/01/2011 09:00 AM Last temp cal: 05/13/2011 08:20 AM Program 1: Titon X UNITS: Moisture FACTOR: 1.00, 0.00 MODE: Standard START DELAY: 9 sec M2 TEMP1: 105C, Std TIME1: Off TEMP2: Off TIME2: Off SLOPE: Window: 1.0 %IW: 0.05 Actual STANDBY: 60C IDEAL WT: 5.0 grams LOCK: Off TARGETS: MIN: 45.00 MAX: 55.00 Time Temp Weight Data Units
- - - - - - - - - - - - - - - - - - - - - - - - - -
- - - -
0:00 61C 5.167 0.00 %M
RESULT on 06/15/2011 at 10:24 AM Elapsed time: 07:13
52.46 %M
Target: PASS Initial Weight = 5.167 grams Final Weight = 2.456 grams Weight Loss = 2.711 grams
Signature:
Page 50
50
To edit or change header lines:
§ From the Results Printout menu press the 1 key.
§ From the Header screen press the number key 1, 2
or 3 to edit or change any of the three header lines.
§ Press the Enter key when finished editing each header line.
§ Press the Enter key from the Header screen to return to the Results Printout menu.
To select a sample number format:
§ From the Results Printout menu press the 4 key to display the Sample Number screen.
§ Press the number for the format desired. The display will return to the Results Printout menu screen. (If Numeric Increment is selected you will be prompted to enter a starting number before return­ing to the Results Printout menu screen.)
To set a print interval:
§ From the Results Printout menu, press the 8 key.
§ Select an interval in seconds. The screen will return
to the Results Printout menu.
1.Header line 1
2.Header line 2
3.Header line 3
Header
05/01/2011 02:24 PM
Header line 1
Lower
Symbol
Sartorius
Clear all
A
Clear one
05/01/2011 02:39 PM
Select sample number: Off
1.Numeric
2.Numeric increment ( 1 )
3.Batch
Sample Number
05/01/2011 02:39 PM
Page 51
51
Setting the Time and Date
The time and date along with the date format will need to be set to your local time on setup. The date will automatically roll to the next year. The analyzer will set the day of the week automatically.
To set the time and date (and format):
§ From the Setup Menu screen, press the 5 key or highlight Time and Date using the navigation keys and press Enter to display the Time and Date screen.
To set the time:
§ From the Time and Date screen, press the 1 key for Set time.
§ At the Time screen, press the Format soft key to select the 12- or 24-hour clock.
§ Use the numeric keys to type in the local time.
§ If you want to use the 12-hour clock, press the
AM|PM soft key to select AM or PM.
§ Press the Enter key to return to the Time and Date screen.
To set the date:
§ From the Time and Date screen, press the 2 key for Set date.
§ At the Date screen, press the Format soft key to select format.
§ Use the numeric keys to type in the date. The day is automatically shown.
§ Press the Enter soft key to return to the Time and Date screen.
1. Set time 02:14 PM
2. Set date 05/01/2011
Day: Monday
Time and Date
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Communication Ports
The LMA110S offers four unique modes to communicate to other Sartorius moisture analyzers, a PC, with a net­work or to the optional internal printer.
§ Serial – Transfer programs between moisture analyzers (LMA110S [Mark 3] or Mark 2) or interface with a PC
§ USB – For Sartorius Service only
§ Ethernet – connect to a network
To set up serial communications to match peripheral device:
§ From the Setup Menu screen, press the 6 key or highlight the Communication Ports menu using the navigation keys and press the Enter key.
§ Press the 1 key for Serial Port to display the Serial Port menu screen.
§ Press the 1 key or On|Off soft key to toggle the serial port On.
§ Press the 2 key for Select baud rate and then the appropriate key to select either 300, 1200, 2400, 4800, 9600, 19200, 57600, or 115200. The screen will return to the Serial Port menu screen.
§ Press the 3 key for Set up serial port to make final selections: – 8, no parity, 1 stop bit – 7, even parity, 1 stop bit – 7, odd parity, 1 stop bit
§ Finally, press the 4 key to toggle CTS On or Off.
To turn the optional internal printer Off, press the 4 key from the Communi­cation Ports menu, or highlight Printer On and toggle the On|Off soft key to display Printer Off.
Note
To download or upload drying pro­grams from another Sartorius product (Mark 3, Mark 2, Omni 1) refer to operating instructions Transfer Programs on page 61.
Serial Command Set
Through specific serial commands entered via a personal computer inter­faced to the LMA110S, all setup and operational functions of the analyzer can be performed from the computer.
For a complete set of serial commands, please contact Sartorius.
Pin Assignment Chart
Pin Configuration of 9 pin DE-9S
Pin Remark 1 Shorted with pins 4 and 6 2 TxD (out) 3 RxD (in) 4 Shorted with pins 1 and 6 5 GND
(tied to shell and digital ground) 6 Shorted with pins 1 and 4 7CTS 8RTS 9 No connection
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Serial Command List
Command Format Limit Description Response Format Range
Test Setting Commands
SET UNITS MOISTURE UNITS MOISTURE
SOLIDS UNITS SOLIDS VOLATILES UNITS VOLATILES MOISTURE/DRY UNITS MOISTURE/DRY
WEIGHT UNITS WEIGHT SET TEMP1 + Float (0-210) 0=OFF TEMP1 x 25-210C SET TEMP2 + Float (0-210) 0=OFF TEMP2 x 25-210C SET TIME1 xx.x Float (0-99.9) 0=OFF TIME1 xx.x 0=99.9 minutes, 0=OFF SET TIME2 xx.x Float (0-99.9) 0=OFF TIME2 xx.x 0=99.9 minutes, 0=OFF SET FACTOR x.xxx Float FACTOR x.xxx SET OFFSET x.xxx Float OFFSET x.xxx SET PLACES x Integer (2 or 3) PLACES x 2,3 SET SLOPE x.xxx Float (0.0 - 9.99) SLOPE x.xxx 0-9.99%, 0=OFF SET SLOPETIME x.xx Float (0.1 - 99.99) SLOPETIME x.xx 0-9.99 minutes, 0=OFF SET CALC ACTUAL “ACTUAL”/”CALC1”/
”CALC2”/”CALC3” CALC ACTUAL CALC1 CALC CALC1 CALC2 CALC CALC2 CALC3 CALC CALC3
SET DELAY x Integer (0 - 9) DELAY x 0-9 sec SET STANDBY x Integer (<165) STANDBY x 25-165C SET IDEALWEIGHT xx.x Float (0.1 - 99.0) IDEALWEIGHT xx.x 0-99 grams SET IDEAL PERCENT xx.x Float (0.1 - 10.0) IDEAL PERCENT xx.x 1-10 SET IDEALLOCK ON “ON”/”OFF” IDEALLOCK ON
OFF IDEALLOCK OFF SET TARGETUPPER xxx.x Float (0 - 100.0) TARGETUPPER xxx.x 0-100 SET TARGETLOWER xxx.x Float (0 - 100.0) TARGETLOWER xxx.x 0-100 SET TARGETLIMIT ON “ON”/”OFF” TARGETLIMIT ON
OFF TARGETLIMIT OFF SET MODE STANDARD “STANDARD”/
”CONCENTRATION” MODE STANDARD
CONCENTRATION MODE CONCENTRATION SET PROGRAMNAME string String PROGRAMNAME string Max: 15 characters GET TEMP1 Float (0-210) 0=OFF TEMP1 x GET TEMP2 Float (0-210) 0=OFF TEMP2 x
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Command Format Limit Description Response Format Range
GET TIME1 Float (0-99.9) 0=OFF TIME1 xx.x GET TIME2 Float (0-99.9) 0=OFF TIME2 xx.x GET FACTOR Float FACTOR x.xxx GET OFFSET Float OFFSET x.xxx GET PLACES Integer (2 or 3) PLACES x GET SLOPE Float (0.0 - 9.99) SLOPE x.xxx GET SLOPETIME Float (0.1 - 99.99) SLOPETIME x.xx GET CALC “ACTUAL”/”CALC1”/
”CALC2”/”CALC3” CALC ACTUAL GET DELAY Integer (0 - 9) DELAY x GET STANDBY Integer (<165) STANDBY x GET IDEALWEIGHT Float (0.1 - 99.0) IDEALWEIGHT xx.x GET IDEAL PERCENT Float (0.1 - 10.0) IDEAL PERCENT xx.x GET IDEALLOCK “ON”/”OFF” IDEALLOCK ON GET TARGETUPPER Float (0 - 100.0) TARGETUPPER xxx.x GET TARGETLOWER Float (0 - 100.0) TARGETLOWER xxx.x GET TARGETLIMIT “ON”/”OFF” TARGETLIMIT ON GET MODE “STANDARD”/”SYRINGE”/
”CONCENTRATION” MODE STANDARD GET PROGRAMNAME String PROGRAMNAME string
System Commands
SET SN xxxxxxxx Set controller SN SN M3123005A 9 characters SET MN xxxxxxxx Set module SN MN M3123005A 9 characters SET TCD mm/dd/yyyy TCD 12/28/2004 mm/dd/yyyy SET BCD mm/dd/yyyy BCD 12/28/2004 mm/dd/yyyy SET LCT EXTERNAL LCT EXTERNAL
INTERNAL LCT INTERNAL NONE LCT NONE
SET SLEEP ON SLEEP ON
OFF SLEEP OFF SET SLEEPTIME hh:mm pm SLEEPTIME hh:mm pm hh:mm am or hh:mm pm SET WAKE ON WAKE ON
OFF WAKE OFF SET WAKETIME hh:mm pm WAKETIME hh:mm pm hh:mm am or hh:mm pm SET SLEEPDAY 1-7 SLEEPDAY 1-7 ON/OFF 1=Monday…7=Sunday SET WAKEDAY 1-7 WAKEDAY 1-7 ON/OFF 1=Monday…7=Sunday SET CONSERVE x CONSERVE x 0-60 minutes SET TIME xx:xx AM/PM TIME 01:00 PM hh:mm am or hh:mm pm SET DATE mm/dd/yyyy DATE 01/18/2005 mm/dd/yyyy SET TIMEFORMAT 0-1 TIMEFORMAT 0 0=AM/PM, 2=24 hr
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Command Format Limit Description Response Format Range
SET DATEFORMAT 0-1 DATEFORMAT 0 SET PASSNUM xxxxx PASSNUM xxxxx SET ACCESS 1-9 ON ACCESS 1-9 ON/OFF Security access 1-9
correspond to menu items 1-9
1-9 OFF
SET OP X string OP x string Operator Names:
1-19, 15 character max. (OPTIONAL) SET PRINTER ON Printer ON (OPTIONAL) SET PRINTER OFF Printer OFF
GET SN SN M3123005A GET MN MN M3123005A GET TCD TCD: mm/dd/yyyy
hh:mm AM/PM
GET BCD BCD: mm/dd/yyyy
hh:mm AM/PM GET LCT LCT: EXTERNAL GET SLEEP SLEEP OFF GET SLEEPTIME SLEEPTIME 00:00 AM GET WAKE WAKE OFF GET WAKETIME WAKETIME 00:00 AM GET SLEEPDAY 1-7 SLEEPDAY 1-7 ON/OFF GET WAKEDAY 1-7 WAKEDAY 1-7 ON/OFF GET CONSERVE CONSERVE 0 GET TIME HH:MM:SS GET DATE MM/DD/YYYY
GET TIMEFORMAT TIMEFORMAT 0 GET DATEFORMAT DATEFORMAT 0 GET PASSNUM PASSNUM xxxxxx GET ACCESS 1-8 ACCESS X ON/OFF GET OP X OP 1-19 string GET STATS Prints stats (OPTIONAL) GET PRINTER Printer ON/OFF GET READING x.xxxx xxC (Weight Temp) GET WINDOW WINDOW Window string GET RESULT STATUS followed
by result lines GET DATALOG Data Log format
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Command Format Limit Description Response Format Range
Results Printout Commands
sretcarahc 51 :xaMgnirts 1 REDAEHgnirts 1 REDAEH TES sretcarahc 51 :xaMgnirts 2 REDAEHgnirts 2 REDAEH TES sretcarahc 51 :xaMgnirts 3 REDAEHgnirts 3 REDAEH TES
NO REDAEHTNIRPNO REDAEHTNIRP TES
FFO REDAEHTNIRPFFO
NO OFNINO OFNI TES
FFO OFNIFFO
NO ROTAREPONOROTAREPO TES
FFO ROTAREPOFFO
CIREMUN ONPMASCIREMUN ONPMAS TES
CNI ONPMASCNI
HCTAB ONPMASHCTAB
FFO ONPMASFFO
NO OFNILACNO OFNILAC TES
FFO OFNI
LACFFO
NO EMANGORPNOEMANGORP TES
FFO EMANGORPFFO
NO OFNIGORPNOOFNIGORP TES
FFO OFNIGORPFFO
NO STHGIEWNOSTHGIEW TES
FFO STHGIEWFFO
NO ERUTANGISNOERUTANGIS TES
FFO ERUTANGISFFO
,FFO=0 :lavretnI tnirP03 LAVRETNIx LAVRETNI TES
2, 5, 10, 30, 60 seconds
CORPORATION SUIROTRAS :1 redaeh tnirP1 REDAEH TEG
YN ,AIMEHOB:2 redaeh tnirP2 REDAEH TEG
:3 redaeh tnirP3 REDAEH TEG
800-635-2906
NO REDAEHTNIRPREDAEHTNIRP TEG
NO OFNIOFNI TEG
NO ROTAREPOROTAREPO TEG
NO
ONPMAS + CNI ONPMASONPMAS TEG
FFO OFNILACOFNILAC TEG
weN EMANMARGORPEMANGORP TEG
NO OFNIGORPOFNIGORP TEG
NO STHGIEWSTHGIEW TEG
NO ERUTANGISERUTANGIS TEG
03 LAVRETNILAVRETNI TEG
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Command Format Limit Description Response Format Range
System DO Commands
DO TRANSFER MARK3 DO TRANSFER MARK2 DO CAL EXTERNAL Calibration Complete DO WEIGHT RAISE DO WEIGHT LOWER DO PROGRAMS CLEAR PROGRAMS CLEAR DO PROGRAMS SAVE PROGRAMS SAVE DO PROGRAMS ALPHABETIZE PROGRAMS ALPHABETIZE DO RECALL XXX RECALL XXX DO ARCHIVE SAVE ARCHIVE SAVE DO ARCHIVE LOAD ARCHIVE LOAD DO TARE TARING DO CLROPERATORS CLROPERATORS DO CLRDATALOG CLRDATALOG DO KEY 0 KEY 0 DO KEY 1 KEY 1 DO KEY 2 KEY 2 DO KEY 3 KEY 3 DO KEY 4 KEY 4 DO KEY 5 KEY 5 DO KEY 6 KEY 6 DO KEY 7 KEY 7 DO KEY 8 KEY 8 DO KEY 9 KEY 9 DO KEY . KEY . DO KEY PF (Paper Feed) KEY PF (Paper Feed) DO KEY START (Start/Stop) KEY START (Start/Stop) DO KEY UP KEY UP DO KEY DOWN KEY DOWN DO KEY LEFT KEY LEFT DO KEY RIGHT KEY RIGHT DO KEY SOFT1 KEY SOFT1 DO KEY SOFT2 KEY SOFT2 DO KEY SOFT3 KEY SOFT3 DO KEY SOFT4 KEY SOFT4 DO KEY ENTER KEY ENTER
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Mark 3 LTE Program Download Format
Introduction: This document details the program output format for the Mark 3 LTE
Moisture Analyzer. The analyzer has the capability to transfer program settings to another Mark LTE 3 or a PC. The analyzer can also be downloaded with settings from a PC. This text format is used to transfer all the information necessary to control the test conditions of a moisture analysis test.
Field Description 1 Program Number (#XXX)
2 Program Name (15 characters max.) 3 Units (0=Moisture, 1=Solids, 2=Volatiles, 3=Moisture dry,
4=PPM Moisture, 5=Weight, 6=mg/L) 4 Slope Time (X.X minutes) 5 Slope Percentage (X.XXX) 6 Slope Calculation (0=Actual, 1=Calc 1, 2=Calc 2, 3=Calc 3) 7 Standby Temperature (165C max) 8 Equilibration Time (X minutes) 9 Ideal Weight (XX.X grams) 10 Ideal Weight % (XX.X) 11 Ideal Weight Lock (0=OFF, 1=ON) 12 Target Limit: Upper (X.XXX %) 13 Target Limit: Lower (X.XXX %) 14 Target Limit: Usage (0=OFF, 1=ON) 15 Test Resolution (2=X.XX%, 3=X.XXX%) 16 Scale Factor (X.XXX) Default=1.000 17 Scale Offset (X.XXX) Default=0.000 18 Temperature 1 (XXX) 19 Ramp 1 (0=Standard) 20 Time 1 (XX.X) 21 Temperature 2 (XXX) 22 Ramp 2 (0=Standard) 23 Time 2 (XX.X) 24 Test Mode (0=Standard, 1=Concentration, 2=Fat) 25 Start Delay (seconds)
Output Example: # 1,Default,0,1.0,0.050,0,60,0,5.0,10.0,0,100.00,0.000,0,3,1.000,0.000,105,0,0.0,0,0,
0.00,128/r/n
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Mark 2 Program Download Format
Field Description 1 Program Number (#XXX)
2 Units (M,S,W,V,L) 3 Ideal Weight (XX.X, Negative value indicates ideal wt. loading locked 90-110%) 4 Temp 1 (XXX) 5 Temp 2 (XXX) 6 Time 1 (Seconds) 7 Time 2 (Seconds) 8 Standby Temp (XXX) 9 Slope Mode (0=Actual, 1=Calc1, 2=Calc2, 3=Calc3) 10 Slope Time (Tenths of minutes, example: 50=5.0 minutes) 11 Slope % (XX.XXX) 12 Start Delay of Initial Wt. Capture* 13 Program Name (19 characters)
Output Example (Factory Defaults): # 1,M, 5.0,105, 0, 0, 0, 60,0,10, 0.050,65,FACTORY 1 # 2,M,30.0,110, 0, 120, 0,110,0,20, 0.010,65,FACTORY 2 # 3,S, 2.0,135, 0, 0, 0,130,0,10, 0.100,65,FACTORY 3 # 4,W, 5.0,105,130, 300, 300, 60,0, 0, 0.000,65,FACTORY 4 # 5,L, 2.0,135, 0, 0, 0,100,0,10, 0.050,65,FACTORY 5 /r/n
* Field 12 - Start Delay of Initial Wt. Capture Bit 0...Sample ID 0=Off 1=On
Sample ID Off Sample ID On Time(s) Value Hex Time (s) Value Hex
0 0 0000 0000 0 1 0000 0001 1 16 0001 0000 1 17 0001 0001 2 32 0010 0000 2 33 0010 0001 3 48 0011 0000 3 49 0011 0001 4 64 0100 0000 4 65 0100 0001 5 80 0101 0000 5 81 0101 0001 6 96 0110 0000 6 97 0110 0001 7 112 0111 0000 7 113 0111 0001 8 128 1000 0000 8 129 1000 0001 9 144 1001 0000 9 145 1001 0001
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Conserve Mode
The Conserve Mode allows the analyzer to manage the heating elements to be turned Off when the analyzer is not in use. In addition, a time schedule can be set for each day of the week for a Sleep mode and a Wake mode.
To edit or change the Conserve Mode period:
§ From the Setup Menu screen, press the 7 key or highlight the Conserve mode using the navigation keys and press Enter to display the Conserve Mode screen.
§ Press the 1 key for Conserve to show the Conserve screen.
§ Use the numeric keys to type in a period of time up to 60 minutes and press Enter to return to the Conserve Mode screen.
Note
To turn Conserve Off, meaning the analyzer will maintain the standby temperature while the analyzer is not being used, enter 0 minutes.
To set or change the sleep and wake mode:
§ From the Conserve Mode screen press 2 or 3 key to show the Sleep mode or Wake up mode screen.
§ From the Sleep mode or Wake up mode screen, type in the desired time (use AM|PM key to set correctly) and press the Enter key.
§ Press the Day soft key. Then select the days of the week that the Sleep mode or Wake up mode is to be used. You will need to press the appropriate number key for each day to toggle it either On or Off.
§ Press the Enter key to return to the Wake up or Sleep mode screen.
§ Press the Enter again to return to the Conserve Mode screen. To manually wake the analyzer, press the Enter key.
1.Conserve 60 minutes
2.Sleep mode Off
3.Wake up mode Off
Conserve mode
On/Off
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Security
The security mode allows the analyzer to be pass code protected from making unauthorized changes or to access selectable features including the setup configuration, programs, the data log and other areas. The security mode is also where important actions can be taken, including clearing the data log or operators, as well as managing program storage or restoring the analyzer to original or factory default settings.
To edit or change any parameter under Security menu:
§ From the Setup menu screen, press the 8 key or highlight, Security mode using the navigation keys and press Enter to display the Security menu.
Activate and Deactivate Security
To activate security:
§ From the Security menu screen the press 1 for Set Security On. The display will change to the Pass Code screen.
§ Type a pass code up to 6 digits using the numeric keys and press the Enter key. The analyzer will now be secured as set in the “Set up security access” menu. The display will return to the Setup menu.
1.Set security On
2.Set up security access
3.Clear data log
4.Clear operators
5.Restore factory defaults
6.Manage program storage
Security menu
On/Off
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To deactivate security:
§ From the Setup menu screen press the 8 key or highlight Security and press the Enter key.
§ Type the set pass code and press the Enter key. The security protection of the analyzer will now be deactivated.
Setup Security Access
Sections of the analyzer setup configuration and other features can be security protected with the pass code at the discretion of the primary operator.
To set up security access:
§ If security is On, first deactivate security as described above.
§ From the Security menu screen, press the 2 key or highlight “Set up security access” and press the Enter key to display the Security access screen.
§ From the list of features, select either On or Off to activate or deactivate, respectfully, each feature.
§ Press the respective number key to toggle On or Off, or highlight the selection and press the On|Off soft key.
§ Press the Arrow soft key to return the Security menu.
§ Security must be set On in the Security menu to
activate.
Note
If a selection from the Security access list is activated (showing On next to the listing in the Security access screen) and the security mode has been enabled under “Set pass code On|Off,” then when an operator tries to enter this selection, the Pass code screen will appear. The only way to enter this selection is to enter the correct pass code which deactivates security.
Security access
On/Off
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1)Progam manage:
2)Data log:
3)Modify operators:
4)Results printout format:
5)Time and date
6)Communication ports:
7)Conserve mode:
9)Audio & video:
0)Service:
On On On On On On On On On
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Clear Data Log
The data log holds 999 results. Periodically it may become full or you may elect to clear all current results in the data log. Security must be deactivated to perform this function.
To clear the data log:
§ From the Security Menu screen, press the 3 key or highlight Clear data log and press the Enter key to display a confirmation screen.
§ Press the 1 key for Yes to clear all results in the data log.
Note
Clearing the data log causes a permanent loss of data.
Clear Operators
At times you may want to clear all operators. Operator 20 will always remain a blank line. Security must be deactivated to perform this function.
To clear all operators:
§ From the Security Menu screen, press the 4 key or highlight Clear operators and press the Enter key to display a confirmation screen.
§ Press the 1 key for Yes to clear all operators in the Operator list.
Note
Clearing the operators causes a permanent loss of operator names.
Erase all results in data log?
1) Yes
2) No
Clear Data Log
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Restore Factory Defaults
At some time it may be necessary to return the analyzer to factory default settings. Security must be deactivated to perform this function.
To restore factory defaults:
§ From the Security Menu screen, press the 5 key or highlight Restore factory defaults and press the Enter key to display a confirmation screen.
§ Press the 1 key for yes to restore all factory settings
Note
Restoring factory default settings will cause a permanent loss of results in the data log as well as clear all programs and any user setup parameters.
Manage Program Storage
The analyzer has the capacity to store a custom set of programs in memory. In the event that the user selectable programs become altered, the stored custom set of programs may be re-loaded. This sec­tion also all programs to be cleared or reload saved programs to be reloaded from an archive or another analyzer. Security must be deactivated to perform this function.
1) Clear all programs
2) Save user programs to archive
3) Load user programs from archive
4) Transfer programs
Manage program storage
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Clear All Programs
To clear all programs:
§ From the Security Menu screen, press the 6 key or highlight Manage program storage and press the Enter key to dis­play the Manage program storage screen.
§ Press the 1 key to Clear all programs and display the confirmation screen. Press the 1 key to permanently clear all programs.
Note
Clearing all programs will cause a per­manent loss of all programs.
Save User Programs to Archive
The analyzer has the storage capacity to store a backup set of the current pro­grams in memory.
To save user programs to archive:
§ From the Security Menu screen, press the 6 key or highlight Manage program storage and press the Enter key to dis­play the Manage program storage screen.
§ Press the 2 key for Save user programs to archive and display the confirmation screen.
Note
Saving user programs to archive will overwrite any existing programs that may have previously been stored to this archive.
Load User Programs
If the user selectable programs become altered, the last stored backup set of programs may be re-loaded from the archive.
To re-load user programs from the archive:
§ From the Security Menu screen, press the 6 key or highlight Manage program storage and press the Enter key to dis­play the Manage program storage screen.
§ Press the 3 key for Load user programs to archive and display the confirmation screen.
§ Press the 1 key to save user programs to archive.
Note
Loading user programs from archive will overwrite any existing programs that may have previously been stored to the user selectable list of programs.
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Transfer Programs
The analyzer has been designed for easy uploading or downloading of all programs from other Sartorius moisture analyzers to the Mark 3 LTE. The fol­lowing combination of analyzers with the appropriate cable is capable of transferring programs: Mark 3 to Mark 3 (serial to serial, null modem cable) mark 3 to Mark 2 (serial to serial, see Accessories on page 83)
Set the same communication parameters on both analyzers:
§ Suggested settings: 9600 baud, 8 bits, No parity, and 1 stop bit, CTS Off
To download programs from a Mark 3 LTE to another analyzer:
§ Install the appropriate cable between the analyzers.
§ Turn the serial port On in serial port menu (page 53).
§ From the Security Menu screen, press the 6 key or highlight Manage program storage and press the Enter key to dis­play the Manage program storage screen.
§ (Mark 2 only—press Setup, Setup 2 menu, Prg Xmit and External input)
§ Press the 4 key for transfer programs.
§ Press the 1 key for Mark 3 to Mark 3 or
2 key for Mark 3 to Mark 3. After a con­firmation screen, the display will show the program transfer in progress.
§ Check the transfer in the receiving ana­lyzer under Recall.
To upload programs to your Mark 3 LTE from another analyzer, follow instruc­tions on the downloading analyzer:
§ Install the appropriate cable between the analyzers.
§ Turn the serial port On in serial port menu (page 53).
§ (Mark 2 only—press Setup, Setup 2 menu, Prg Xmit and Output Programs)
§ The Mark 3 LTE will automatically recognize receipt of the programs.
§ Check the transfer in the receiving analyzer under Recall.
1) Mark 3 to Mark 3
2) Mark 3 to Mark 2
Program transfer
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Audio, Video and Language
The analyzer audio and video appearance may to adjusted to your desired taste or lighting conditions.
Audio Adjustments
An audio beep may be activated or turned off for a keystroke, when adding sample during the test mode or at the end of a test. If the key press beep is acti­vated, a beep will occur every time a key is pressed. If the ideal weight beep is activated, a pulsating beep will occur when the weight of the sample being added is within the ideal weight limits.
To change the audio format:
§ From the Setup Menu screen, press the 9 key or highlight Audio & Video using the navigation keys and press Enter to display the Audio & Video screen.
To change the key press audio beep:
§ From the Audio & Video screen, press the 1 key to toggle On or Off, or highlight Key press beep and press the On|Off soft key.
To change the ideal weight audio beep:
§ From the Audio & Video screen, press the 2 key to toggle On or Off, or highlight Ideal weight beep and press the On|Off soft key.
To change end of test beep:
§ From the Audio & Video screen, press the 3 key to toggle On or Off, or highlight End of test beep and press the On|Off soft key.
1)Key press beep On
2)Ideal weight beep On
3)End of test beep On
4)Video contrast Level 5
5)Video color scheme Black on eti
hw
Audio & Video
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On/Off
6)Language
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Video Contrast Adjustment
To change the video contrast:
§ From the Audio & Video screen, press the 4 key for Video contrast to display the Video contrast screen.
§ Press a number key between 1 and 9 to change. A smaller number will make the screen appear lighter, while a larger number will make the screen appear darker.
§ Press the Arrow soft key to save the contrast selec- tion and return the Audio & Video screen.
Video Color Scheme
The screen may be set in either of two color schemes: black lettering on a white background or white lettering on a black background.
To change the video color scheme:
§ From the Audio & Video screen, press the 5 key for Video color scheme to select either black on white or white on black.
Setting the Language
– 6 languages are available for display of the
information:
– English – Spanish – German – French – Italian – Portuguese
§ To change the language, press the 6 key in the “Audio & Video” menu. Then select the required language.
1)Level 1 (lightest)
2)Level 2
3)Level 3
4)Level 4
5)Level 5 (normal)
6)Level 6
7)Level 7
8)Level 8
9)Level 9 (darkest)
Video contrast
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Language
1)English
2)Spanish
3)German
4)French
5)Italian
6)Portuguese
05/01/2011
02:40 PM
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Service
For best performance and reliable usage, the analyzer requires periodic cleaning (see the chapter on “Cleaning”). The analyzer contains a wide variety of features related to calibrating and troubleshooting. The Service menu is where you have access to:
§ Calibrating the balance
§ Adjusting the temperature
§ Establishing a calibration schedule
§ Troubleshooting and diagnostics
(Factory secured area, under the guidance of Sartorius Service personnel only)
System
This screen will display important information about your analyzer including model, serial number, soft­ware version, dates of last calibration and adjust­ment, installation date and MAC address.
To view the system screen:
§ From the Setup menu screen, press the “.” key or highlight Service using the navigation keys and press Enter to display the Service menu screen.
To view and print system information:
§ From the System menu press the 1 key to display System screen.
§ Press the Print soft key to print this screen.
Mark 3 LTE Moisture Analyzer SN: M3114045B Control sw: 2.00.00 Module sw: 2.00.00 Last bal cal: 04/13/2011 01:37 PM Last temp cal: 04/13/2011 10:42 AM Installation Control sn: 04/01/2011
MAC address: 0040d53114045
System
Print
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1.System
2.Calibrate balance
3.Adjust temperature
4.Advanced
Service menu
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Calibration | Adjustment Functions
Calibrate Balance
The balance of the analyzer should be calibrated and adjusted on installation and then periodically at some interval consistent with your quality program (one year is typical). The balance may be calibrated manually with a known external calibration weight. The analyzer also allows you to set a calibration interval that will remind you when calibration is due.
To access the balance calibration and other balance test features:
§ From the Service menu screen, press the 2 key for “Calibrate Balance.”
1)Calibrate external weight
2)Schedule calibration
Calibrate balance
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§ Press Print to obtain a calibration report or Arrow key to exit to the Service menu. The date of last balance calibration on the System screen is also updated.
To calibrate and adjust using an external calibration weight:
§ From the Calibrate balance screen, press the 1 key for Calibrate external weight to display the Calibrate external screen.
§ The balance will automatically re-zero.
§ At the prompt, “Add cal weight”, add the calibration
weight to the pan support and close the hood. The analyzer will automatically recognize hood clo­sure, wait for stability and begin the calibration and adjustment procedure.
Note
Permissible external calibration weights include: 10, 20 and 30 g. Weights must be within 2% of tolerance.
§ When this procedure has been completed, the display will show “Calibration complete” when finished.
§ Press Print to obtain a calibration report or Arrow key to exit to the Service menu. The date of last balance calibration on the System screen is also updated.
Calibrate external
Zero Cal
5.389 g
Add external calibration weight
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02:40 PM
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To schedule calibration/adjustment:
§ From the Calibrate balance screen, press the 2 key for Schedule calibration to display the Schedule calibration screen.
§ Press the number key for the interval of choice.
§ When done, press the Arrow key to accept the
changes. The display will return to the Calibrate balance menu and will reset the calibrations sched­ule. When this interval expires, the operator will be prompted on the screen to calibrate the analyzer. However, this message will not prevent testing a sample or any other operation of the analyzer.
Note
When the new calibration has been completed, the analyzer will automatically reschedule the same interval from the time the calibration is completed.
1)Off
2)1 day
3)7 days
4)30 days
5)90 days
6)180 days
7)365 days
Schedule calibration
Calibration schedule: Off
05/01/2011 02:40 PM
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Heater Adjustment
Adjust Temperature or Verify Temperature
The temperature of the analyzer should be verified and adjusted as needed periodically at some interval consistent with your quality program (one year is typical). To perform an adjustment the optional temperature calibration and adjustment kit is needed.
Installation of the temperature bowl:
§ Open the heater hood and wear gloves to carefully remove the pan support and the pan shield since it may be hot.
Caution
The pan support and pan shield will be hot. Only remove these items if you are wearing protective gloves. Otherwise, leave the heater hood open and let these items cool down before attempting to remove them.
§ Place the temperature bowl (“fixture”) in the same place as the pan shield.
§ Press the leads coming off the temperature bowl into the connectors in the rear of the temperature chamber for the automatic temperature calibration.
§ Lower the heater hood.
Perform temperature adjustment:
§ From the Service menu, press the 3 key to display the Adjust Temperature screen.
1)Manual temp cal
2)Verify temperature
3)Adjust schedule
4)Reference fixture: 1255
5)Automatic temp cal
Adjust temperature
05/01/2011 02:44 PM
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§ To initiate an automatic temperature calibration and adjustment, press the 5 for Automatic Temp Cal. The screen will change to the Temperature screen.
§ The analyzer will automatically begin at two temperatures (80°C and 150°C). Each of Cal 1 and Cal 2 temperature steps will take 20 minutes. The time elapsed is shown on the screen. As soon as the Cal 1 temperature phase has expired, Cal 2 will begin automatically.
§ When the Cal 2 phase has elapsed, the screen will change to show that adjustment has been completed.
§ The analyzer will then verify the adjustment by checking at 130°C for 20 minutes. The entire temp calibration and adjustment process takes 60 minutes.
§ The “Temp adjust done” screen will show both the pre-adjusted temperature, along with the postad­justed temperature for both calibration temperatures.
§ The time and date of last temperature calibration and adjustment is automatically updated on System menu.
§ Pressing the Arrow soft key anytime during the temperature adjustment will abort the “auto temp cal” process. The screen will return to the “Auto temp cal” screen without adjusting the analyzer temperature calibration.
Auto temp cal
Cal 1
Current
80 71
1.5 minutes
Cal Bowl Temp: 75
Time = 20 minutes
05/01/2011 02:40 PM
Auto temp cal
Standby
Current
60
124
Coefficients set
Calibration passed verification
Calibration passed
05/01/2011 02:44 PM
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§ The automatic temperature adjustment report is printed after the adjustment process.
To verify an adjustment temperature:
§ From the Service menu, press the 3 key to display the Adjust Temperature screen.
§ Press the 2 for Verify temperature. The screen will change to the Verify temperature screen.
§ The default verifies temperature is 130°C. Press the “Temp” soft key to begin. The screen will change to the Temp verify in process screen and show the selected temperature. After 20 minutes, the screen will change to the Temp verify done screen and will display the expected selected temperature and the actual temperature that was measured by the temperature bowl (“fixture”).
§ Press the Print soft key to print a temperature verification report (optional).
§ If the agreement of the selected temperature and the actual temperature are not within 2 degrees for any of the selected temperatures, it is recommended that you perform the temperature calibration and adjustment procedure.
Automatic Temperature Adjustment Report
- - - - - - - - - - - - - - - - - - - - - - - - - -
Fixture number 1234 Temperature 80C: 82C Temperature 150: 150C Mark 3 LTE Moisture Analyzer Module SN: M3085010B Calibration passed 05/10/11 02:05 PM
Signature:
__________________________
Preadjust 80: 79 Adjusted 80: 80
Preadjust 150: 144 Adjusted 150: 150
Temp adjust done
05/01/20112 02:43 PM
Print
Ad-
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To change the temperature adjustment schedule:
§ From the Service menu, press the 3 key to display the Adjust Temperature screen.
§ Press the 3 for Adjust schedule. The screen will change to the Schedule temp adjust screen.
§ Select the desired period of time. When this period expires, a warning will appear in the warning box indicating that a new verification or temperature adjustment should be performed.
To enter a reference fixture number:
§ From the Adjust Temperature screen, press the 4 for Reference fixture. The screen will change to have you enter the reference fixture number that is marked on your temperature bowl. The number will then appear on both the temperature adjustment or verification reports.
1)Off
2)1 day
3)7 days
4)30 days
5)90 days
6)180 days
7)365 days
Schedule calibration
Calibration schedule: Off
05/01/2011 02:50 PM
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Concentration Mode
The Mark 3 LTE is able to determine Total Suspended Solids in low solids samples, such as for wastewater sam­ples. The sample solids are first concen­trated onto a filter pad placed into a vacuum apparatus. During the test mode the operator will be prompted to enter the number of milliliters of sample that was filtered. Results are displayed in mg/l.
Wet wt of filter pad (mg) – dry wt of filter pad (mg) Entered milliliters of sample / 1000
To select the concentration mode:
§ Press the 9 key from the Program menu to display the Mode screen.
§ Press the 2 key for Concentration. The display will return to the Program menu.
To test samples in the Concentration mode:
§ Open the heater hood, place the filter pad onto a pan and close the hood.
§ Press the Start|Stop key to begin a test.
§ The analyzer will automatically tare the
pan and filter pad.
§ Open the hood, remove the filter pad and place it into the vacuum apparatus. Pour a known volume of sample into the vacuum apparatus. When finished, remove the sample pad and return it to the pan in the heater module and close the hood.
§ At the prompt, enter the number of milliliters of sample that were put through the vacuum apparatus and then press the Enter key.
§ The analyzer will enter the test mode. When the test is done, the results will be reported in mg/l.
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Status
Result
}
Temperature info
Test Done
Test Done
DRY MILK POWDER
Recall Setup
Users
Service
Press START key to begin test
Standby
3.45 % M
60 97
Current
Standby
7.48 % M
60 60
Current
1
3
05/01/2011 02:40 PM
Multi-module Mode
The multi-module mode allows one operator to simultaneously control up to two heater modules connected to a single Control Module. This is possible by connecting each heater module to a Mod Comm port on the back of the Control Module.
To initiate an additional heater module:
§ Connect the inter-module cable.
§ Power off and back on again the heater
module that powers the control module (press Enter to override Warm-up).
§ On power up, a scan is initiated to determine which Mod Comm ports have a heater module attached. If more than one is connected, the screen will display in the Multi-module mode. Note that a double set of bars shows the active heater module.
Multi-module screen description:
§ Heater module icon: Separate display of heater module information including:
§ Status: warm-up, test done, pass/fail, minutes in test
§ Test result
§ Current temperature and temperature
status
§ Program name: current program for active heater module
§ Time and date
§ Recall soft key: Select program for
active heater module
§ Setup soft key: Access to global setup
§ Service soft key: Access to specific
functions for active heater module
§ Users soft key: Access to list of users for active heater module
§ Warning box: Messages specific to active heater module
Multi-module key functions:
§ Navigational keys (right and left Arrows): Moves double bars to activate
heater module (or press keys 1–4).
§ Start|Stop: Initiates test for active heater module
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Each heater module can run a test inde­pendent from the other heater modules by recalling a program from the pro­gram list and initiating a test. The pro­gram list is common for all heater mod­ules. When a test is initiated, the display will show test screens from the single module mode, such as entering an ID number and bar graph prompt to add the ideal sample size.
To test a sample in multi-mode:
§ Press the navigational right or left arrow key to move the double bars to
the desired heater module.
§ Check current program. To change program, press Recall and select a new program if desired.
§ Press the Start|Stop key to initiate a test. (the screens and functionality are the same as in the single module mode).
§ After the initial weight is captured, the display will return to the multi-mode screen. The status line will show the elapsed time of the test to indicate a test is in progress.
§ At the end of the test, the status line will display “Test Done” (or Pass or Fail if target limits have been entered in this program). The printer (optional) will also print the result at the end of the test.
Note
Certain functions are not available in the multi-module mode including: Interval print and graphing. However, in the multi-module mode, one can test one or more samples and still have access to service for another heater module which is not testing a sample.
To perform service options on any heater module such as: – Balance calibration
– Temperature adjustment
§ From the multi-module screen, press the navigational right or left arrow key to move the double bars to activate the desired heater module.
§ Press the Service soft key to display the Service menu.
§ Press the number key of the desired option and press the Enter key. The display will show these screens as in the single module mode.
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Cleaning
Recommended care
For best performance and reliable usage, the analyzer requires periodic cleaning.
Danger
Before beginning the cleaning process:
§ The analyzer must be disconnected from the power source.
§ Allow the analyzer to cool down for 30 minutes.
§ Take care during cleaning not to spill any liquid into the analyzer.
§ The I/O connections on the back of the analyzer may not come into contact with liquids.
§ Do not immerse the analyzer in water or any other cleaning solution.
Regular cleaning of the analyzer with a mild detergent and a soft cloth should include the following:
§ Clean the outer surface of the analyzer.
§ Carefully remove and clean the pan
support and pan shield.
§ Keep all warning labels clean.
§ Wipe dust from the interior of the
stainless steel heater housing.
§ Remove and clean the recessed area under the pan shield: – Remove the pan support and pan
shield.
– Remove the two screws holding the
perforated plate.
– Be careful not to spill liquid or solid
debris down the center hole where the balance pan receiver protrudes.
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Disposal
Packaging that is no longer required must be disposed of at the local waste disposal facility. The packaging is made of environmentally friendly materials that can be
used as secondary raw materials.
The equipment, including accessories and batteries, does not belong in your regular household waste. The EU legis­lation requires its Member States to col­lect electrical and electronic equipment and dispose of it separately from other unsorted municipal waste with the aim of recycling it.
In Germany and many other countries, Sartorius AG takes care of the return and legally compliant disposal of its electrical and electronic equipment on its own. These products may not be placed with household waste or brought to collection centers run by local public disposal operations – not even by small commercial operators.
In countries that are not members of the European Economic Area (EEA) or where no Sartorius affiliates, sub­sidiaries, dealers or distributors are located, please contact your local authorities or a commercial disposal operator.
Prior to disposal and/or scrapping of the equipment, any batteries should be removed and disposed of in local collec­tion boxes.
Sartorius AG and Sartorius, its affili­ates, subsidiaries, dealers and distrib­utors will not take back equipment contaminated with hazardous mate­rials (ABC contamination) – either for repair or disposal. Please refer to the accompanying leaflet/manual or visit our website (www.sartorius.com) for comprehen­sive information that includes our service addresses to contact if you plan to send your equipment in for repairs or proper disposal.
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Specifications
Display of Results 0.001 % Balance Resolution 0.001 grams Balance Capacity 40 grams
Reproducibility of the Sample weight = 1g : 0.1% measurement Sample weight = 5g : 0.02%
Balance Repeatability ±1.0 mg Method of Measurement Loss on Drying Modular Configuration Control and heater modules (optional: up to 2 heater modules) Heat Source Four parallel infrared quartz cylinders Temperature Setting/Control 30–210°C in one-degree increments/RTD sensor, ±1°C Temperature Steps Programmable, one or two Temperature Adjustment Optional fixture for internal electronic two-point adjustment Standby Temperature 30–160°C in one degree increments Temperature Display Display of both target and current temp at each stage of drying and standby Conserve Mode Clock Programmable time by day of week to shut down and wake up analyzer Balance Calibration External manual Ideal Weight Audio and visual display for programmable target sample weight addition Target Limit Alert Minimum and maximum programmable limits and screen alert when test done Program Storage 60 programs with unique settings, alphanumeric naming Result Storage 999 results with statistics: average, SD, RSD, high and low Units of Measure of Results Weight, %moisture, %solids, %volatiles, mg Endpoint Determination Actual slope, Calculation and Windows of Time modes Sample ID Numeric, Numeric incrementing, alphanumeric or turned off Modes of Operation Standard Test, Syringe or Concentration modes Operator Names Twenty alphanumeric operator names Security Mode Selectable setup and operation protection with pass code Graph Mode Graph of Temperature/Time and Percent/Time Display Quarter VGA with contrast adjustment (black on white or white on black) Keypad Sealed membrane with audible tactile feedback External Input|Output Serial Internal Clock Date and Time: U.S. or International, Military or AM|PM Audio Beep Key stoke, ideal weight met and end of test, selectable on or off System Status Indicator Lights Two tri-color LEDs (balance & heater) on front of heater module Power Requirements 100–120/200–240 V~ ~5A T Dimensions (L + W + H) 41.3 + 49.5 + 23.5 cm (16 1/4” + 19 1/2” + 9 1/4”) modules combined Weight 10 kg (22 lbs.)
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Moisture analyzer accessories are available for purchase directly from Sartorius or the local distributor that you purchased the Mark 3 LTE Moisture Analyzer from.
Description Sample filter pad, 90mm round Box/200 6906941
Mark 3 Lg Volume Sample Pan Box/10 69MA0349 Calibrated Mark 3 RTD Bowl YTM09MA Mark 3 to PC (serial) cable YCC01-MK1 Mark 3 to PC (USB) cable YCC01-MK3 Mark 3 to Mark 3 serial download cable YCC01-MK4 Mark 2 to Mark 3 upload cable YCC01-MK5 Mark 3 to PC Ethernet cable YCC01-MK2 Extra long Inter-Module cable, 30” (4th HM) 69TC0131 Large Pan Support 69TC0289 Mark 3 Cal/Val Kit YVK02MA 8 ml Pipette Box/400 YAT02MA 8 ml Pipette (New Style) Box/500 YAT04MA Calibrate DMM 84Y200 Calibrate Temperature Bowl 84Y201 Digital Multi-Meter 6738-63 DMM with calibration 6738-63C Large Tweezers YCC01-MK6 Small Tweezers YCC01-MK7 Mark 3 Carrying Case YDB09MA 4”Mark 1, 2 & 3 Sample Pan Box/200 69TC0479 4” Higrade Filter pad Box/200 69MA0327 20 gr weight, class 1 WT20GCLS1 OIC Version WinWedge 32 Std v3.0 YSW04-MK1 OIC Custom WinWedge files (included) Information
available on request
Accessories (Options)
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Regulatory Compliance
C Marking
The Mark 3 LTE moisture analyzer complies with the following EC Directives and European Standards:
Council Directive 2004/108/EEC: “Electromagnetic compatibility (EMC)”
Applicable European Standards: Limitation of emissions: In accordance with product standard EN 61326-1 Class B (residential area)
Defined immunity to interference: in accordance with product standard EN 61326-1 (minimum test requirements, un-monitored operation)
!
Class A Warning Warning: This is a class A product. In a domestic environment this product may cause radio interfer­ence in wich case the user may be required to take adequate measures.
CSA Marking
Certificate: 2416856 Master Contact: 167555 Equipment Class 1 Pollution Degree 2 Installation Category II
CLASS 8721 05 - LABORATORY EQUIPMENT - Electrical
CLASS 8721 85 - ELECTRICAL EQUIPMENT FOR LABORATORY USE
- Certified to US Standards
Note: The operator shall be responsible for any modifications to Sartorius equipment and for connections of cables not sup­plied by Sartorius and must check and, if necessary, correct these modifications. On request, Sartorius will provide information on the minimum operating specifications in accordance with the standards listed above for defined immunity to interference.
Council Directive 2006/95/EC: “Electrical equipment designed for use within certain voltage limits”
Applicable European Standards:
EN61010-1: 2001 Safety requirements for electrical equipment for measurement, control and laboratory use Part 1: General requirements
If you use electrical equipment in installations and under ambient condi­tions subject to stricter safety standards than those described in the manual, you must comply with the provisions as specified in the applicable regulations for installation in your country.
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Notes
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86
Notes
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87
Page 88
JW · W3A000.CP · KT Publication No.: 98040-699-09 Rev. D
Sartorius Corporation 5 Orville Dr. Bohemia, NY 11716
info@sartorius-omnimark.com www.sartorius.us
Tel (800) 835-3211 Fax (631) 253-5263
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