Rosemount Analytical 398, 396, 396VP, 398VP Operating Manual

Instruction Manual

IQ-MAN-396-396VP-397-398-398VP

L

Rev. M

March 2017

Rosemount

pH/ORP Sensors

™

396/396VP/397/398/398VP

asgkas

h

Essential Instructions

Read this page before proceeding!

Emerson designs, manufactures and tests its products to meet many national and international stan-

dards. Because these sensors are sophisticated technical products, you MUST properly install, use,

nd maintain them to ensure they continue to operate within their normal specifications. The

a
following instructions MUST be adhered to and integrated into your safety program when installing,
using, and maintaining Rosemount products. Failure to follow the proper instructions may cause
any one of the following situations to occur: loss of life; personal injury; property damage; damage
to this sensor; and warranty invalidation.

• Read all instructions prior to installing, operating, and servicing the product.

• If you do not understand any of the instructions, contact your Emerson representative for
clarification.

• Follow all warnings, cautions, and instructions marked on and supplied with the product.

• Inform and educate your personnel in the proper installation, operation, and maintenance
of the product.

• Install your equipment as specified in the Installation Instructions of the appropriate
Instruction Manual and per applicable local and national codes. Connect all products to
the proper electrical and pressure sources.

• To ensure proper performance, use qualified personnel to install, operate, update,
program, and maintain the product.

• When replacement parts are required, ensure that qualified people use replacement parts
specified by Emerson. Unauthorized parts and procedures can affect the product's
performance, place the safe operation of your process at risk, and VOID YOUR WARRANTY.
Third-party substitutions may result in fire, electrical hazards, or improper operation.

• Ensure that all equipment doors are closed and protective covers are in place, except when
maintenance is being performed by qualified persons, to prevent electrical shock and
personal injury.

The information contained in this document is subject to change without notice.

DANGER

Hazardous Area InstallationN

This sensor is not Intrinsically Safe. or Explosion Proof. Installations near flammable liquids or in
hazardous area locations must be carefully evaluated by qualified on site safety personnel.

To secure and maintain an intrinsically safe installation, an appropriate transmitter/safety
barrier/sensor combi nation must be used. The installation system must be in accordance with the
governing approval agency (FM, CSA or BASEEFA/CENELEC) hazardous area classification require­ments. Consult your transmitter instruc tion manual for details.

Proper installation, operation and servicing of this sensor in a Hazardous Area Instal lation is entirely
the responsibility of the user.

CAUTION

Sensor/Process Application Compatibility

The wetted sensor materials may not be compatible with process composition and operating
conditions. Application compatibility is entirely the responsibility of the user.

About This Document

This manual contains instructions for installation and operation of the Rosemount 396, 396VP, 397,
398, and 398VP pH/ORP Sensors.

The following list provides concerning all revisions of this document.

Rev. Level Date Notes

0 03/99 This is the initial release of the product manual. The manual has been

reformatted to reflect the Emerson documentation style and updated

to reflect any changes in the product offering.
A 12/01 Revised wiring diagram on page 24.
B 2/02 Added info to page 1.
C 6/02 Updated multiple drawings.
D 8/02 Added drawing #40105549, rev. D.
E 10/02 Revised drawing #40039601, rev. J, on page 10.
F 4/03 Revised Model 397 specs on page 2, and revised drawing on page 27.
G 8/03 Added Silcore information.
H 3/04 Added Xmt wiring drawings.
I 10/04 Added 5081 wiring drawing and updated 1055 wiring.
J 2/06 Changed drawing 40039603 rev. C, on page 13. Added a note on

page 15.

K 1/07 Miscellaneous revisions.
L 11/10 Removed mention of patents and updated dnv logo.
M 03/17 Updated Ordering Information, Wiring Diagrams, Accessories, Emerson

Logo and Address. Also, added FM Installation drawing and EC

Declaration of Conformity

Instruction Manual Table of Contents

LIQ-MAN-396-396VP-397-398-398VP March 2017

Contents

Section 1: Description and Specifications

1.1 TUpH Features and Applications ..........................................................................1

1.2 Specifications ......................................................................................................3

1.3 Product Certifications ..........................................................................................4

1.4 Ordering Information...........................................................................................6

Section 2: Installation

2.1 First Time Installation ..........................................................................................9

2.2 Unpacking and Inspection .................................................................................10

2.3 Mounting...........................................................................................................10

2.4 Electrical Installation..........................................................................................17

Section 3: Startup and Calibration

3.1 Sensor Preparation ............................................................................................33

3.2 Calibration Using Buffer Solution or Grab Sample...............................................33

Section 4: Maintenance

4.1 Electrode Cleaning.............................................................................................35

4.2 Automatic Temperature Compensator...............................................................36

Section 5: Troubleshooting..................................................................................37

Section 6: Accessories

6.1 Accessories........................................................................................................39

EC Declaration of Conformity.............................................................................41

Intrisicallly Safe Sensor Installation Drawing - FM ................................43

Table of Contents i

Table of Contents Instruction Manual

March 2017 LIQ-MAN-396-396VP-397-398-398VP

ii Table of Contents

Instruction Manual Description and Specifications

LIQ-MAN-396-396VP-397-398-398VP March 2017

Section 1: Description and Specifications

1.1 TUpH Features and Applications

The low maintenance and disposable Rosemount 396, 396VP, 397, 398, and 398VP TUpH sensors
offer long life and high performance in measuring pH or ORP in aqueous solutions in pipelines, open
tanks, or ponds.

These TUpH sensors feature a large area reference junction for maximum resistance to process
coatings, generally found in dirty, high solid applications. In addition, the secondary helical reference
pathway serves as added protection from poisoning ions. The simplified construction, designed
with user convenience in mind, does not require electrolyte replenishment or any component
replacement. All models feature a large glass bulb for increased resistance to the effects of aging for
longer life.

1.1.1 Rosemount 396 and 396VP Sensor Features and Applications

Rosemount 396/396VP sensors are constructed of
polypropylene and stainless steel and are completely
sealed by EP (ethylene propylene) to eliminate process
intrusion.

Sesnors are specially designed for improved life in harsh,
dirty applications such as lime slurry waste treatment
and paper machine headbox and pigment/dye
applications where large quantities of suspended solids
are present. Installation is easily achieved through a wide
variety of mounting configurations.

1.1.2 Rosemount 397 Sensor Features and Applications

The Rosemount 397 is housed in a highly chemical resistant
polypropylene body and completely sealed with EP to
eliminate process intrusion. The Rosemount 397 body is
specifically designed for use with the Quik-Loc Kit which
consists of an adapter and coupler. The PEEK (poly
etheretherke tone) adapter enables the Rosemount 397
sensor to fit into a 1 in. MNPT Dixon coupler for quick and
easy removal without sensor cable twisting. The 316 stain
less steel DIxon coupler is sealed with EP an features locking
arms. The Quik-Loc Kit is not recommended for use in
processes with hazardous, corrosive, or strong oxidizing
chemicals due to a risk of spray and bodily hazards.

1.1.2 Rosemount 398 and 398VP Sensor Features and Applications

The chemical-resistant construction of Tefzel, titanium, and the TUpH reference junction make the
Rosemount 398 and 398VP the ideal sensors for measuring pH in harsh process liquids. Use these
sensors to measure pH in sour water strippers, in pulp bleaching towers that use chlorine dioxide,
and in process streams containing a variety of organic solvents.

Rosemount 398 and 398VP sensors use the highest quality materials to provide superior chemical
resistance. The sensors are housed in a titanium tube and features an optional 1 inch MNPT process
connector for insertion, submersion, or flow-through applications. The molded Tefzel TUpH
construction is offered with a choice of seals (Viton, EPDM, or Kalrez).

Description and Specifications 1

Description and Specifications Instruction Manual

March 2017 LIQ-MAN-396-396VP-397-398-398VP

Figure 1-1: Cross Section Diagram of the TUpH Reference Technology

All TUpH sensors are designed with a large area reference junction, helical reference pathway, and an
AccuGlass pH glass bulb. This sensor technology ensures superior performance while only requiring
minimal maintenance.

2 Description and Specifications

Instruction Manual Description and Specifications

LIQ-MAN-396-396VP-397-398-398VP March 2017

1.2 Specifications

Table 1-1: Percent linearity over pH

396, 396VP, 397, 398, 398VP 396, 396VP, 397, 398, 398VP

pH Range GPHT Hemi GPLR Hemi

0-2 pH 94% 93%

-12 pH

2

12-13 pH 97% 95%

13-14 pH 92% --

Table 1-2: Rosemount 396, 396VP, 397, 398 and 398VP Specifications

Rosemount 396

396VP

Measured Ranges 0 to 14 pH 0 to 14 pH

ORP: -1500 mV to 1500 mV

Available pH

ACCUGLASS Types

GPHT hemi bulb or

GPLR flat bulb

9%

9

Rosemount 398

398VP

GPHT hemi bulb or

GPLR flat bulb GPHT hemi bulb

Rosemount 397 Quik-loc Kit

0 to 14 pH

8%

9

_

_

316 SST,

Wetted Materials

Process Connection

Temperature Range 0-100 °C (32-212 °F) 0-100 °C (32-212 °F) 0-100 °C (32-212 °F)

Pressure Range-

Hemi bulb

Pressure Range-

Flat bulb

Minimum

Conductivity

Preamplifier Options Remote Remote Remote

Weight/Shipping

Weight

Polypropylene, EPDM, glass

None, use 1 in. NPT
process connector,

PN 23166-00 or 23166-01

(sold separately)

100-1136 kPa abs

(0-150 psig)

100-790 kPa abs

(0-100 psig)

75 µS/cm, nominal 75 µS/cm, nominal 75 µS/cm, nominal

0.45 kg/0.9 kg (1 lb/2 lb) 0.45 kg/0.9 kg (1 lb/2 lb) 0.45 kg/0.9 kg (1 lb/2 lb) 0.45 kg/0.9 kg

Titanium, Tefzel, glass,

choice of Kalrez, Viton, or

EPDM (platinum: ORP only)

None, use 1 in. NPT

process connector,

PN 23166-00 or 23166-01

(sold separately)

100-1825 kPa abs

(0-250 psig)

100-790 kPa abs

(0-100 psig)

Polypropylene, EP, glass 316 SST, EP, PEEK

None, must use Quik-Loc

kit which includes 1 in.

MNPT process

connection

100-790 kPa abs

(0-100 psig)

_ _

1-in. MNPT

_

(1 lb/2 lb)

Description and Specifications 3

Description and Specifications Instruction Manual

March 2017 LIQ-MAN-396-396VP-397-398-398VP

1.3 Product Certifications

Please see online certificates for further details.

osemount 396/396VP:

R

IECEx

Sensors without preamp (pH and ORP) – Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C)

Sensors with SMART preamp (pH only) – Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C)

Sensors with standard preamp (396P only) – Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +80 °C) or
Ex ia IIC T5 Ga (-20 °C ≤ Ta ≤ +40 °C)

Per standards IEC60079-0 : 2011, IEC 60079-11 : 2011

ATEX

Sensors without preamp (pH and ORP) – II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C)

Sensors with SMART preamp (pH only) – II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C)

Sensors with standard preamp (396P only) – II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +80 °C) or

II 1 G Ex ia IIC T5 Ga (-20 °C ≤ Ta ≤ +40 °C)

Per standards EN 60079-0: 2012+A11:2013, EN 60079-11:2012

FM

See online FM Certificate of Compliance for applicable sensor options:

Intrinsically Safe for use in Class I, II, and III, Division 1, Groups A, B, C, D, E, F, and G; Temperature
Class T6 Ta = -20 °C to +60 °C

Intrinsically Safe for use in Class I, Zone 0, AEx ia IIC T6 Ta = -20 °C to +60 °C

Nonincendive for use in Class I, Division 2, Groups A, B, C, and D; Temperature Class T6 Ta = -20 °C
to +60 °C

Suitable for use in Class II and III, Division 2, Groups E, F, and G; Temperature Class T6 Ta = -20 °C
to +60 °C Hazardous (Classified) Locations

IS/I,II,III/1/ABCDEFG/T6 Ta = 60 °C - 1400332; Entity; I/0/AEx ia IIC/T6 Ta = 60 °C - 1400332; Entity;
NI/I/2/ABCD/T6 Ta = 60 °C; S/II,III/2/EFG/T6 Ta = 60 °C

Per standards 3600:1998, 3610:2010, 3611:2004, 3810:2005

CSA

See online CSA Certificate of Compliance for applicable sensor options:

Sensors with preamp – Intrinsically Safe:

Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups
ABCD; Ambient temperature rating -20 °C to +60 °C; Ex ia IIC; T6

Sensors without preamp – Intrinsically Safe and Non-Incendive:

Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups
ABCD; Ex ia IIC; T6; Ambient temperature rating -20 °C to +60 °C: (Simple Apparatus)

Per standards C22.2 No. 0-10, C22.2 No. 0.4-M2004, C22.2 No. 94-M1991, C22.2 No. 142 – M1987,
C22.2 No 157 – M1992, CAN/CSA E60079-0:07, CAN/CSA E60079- 11:02, UL50 11th Ed, UL508
17th Ed, UL913 7th Ed,, UL 60079-0: 2005, UL 60079-11: 2002

4 Description and Specifications

Instruction Manual Description and Specifications

LIQ-MAN-396-396VP-397-398-398VP March 2017

Rosemount 397/398/398VP:

IECEx

Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C)

er standards IEC60079-0 : 2011, IEC 60079-11 : 2011

P

ATEX

II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C)

Per standards EN 60079-0: 2012+A11:2013, EN 60079-11:2012

FM

Intrinsically Safe for use in Class I, II, and III, Division 1, Groups A, B, C, D, E, F, and G; Temperature
Class T6 Ta = -20 °C to +60 °C

Intrinsically Safe for use in Class I, Zone 0, AEx ia IIC T6 Ta = -20 °C to +60˚C

Nonincendive for use in Class I, Division 2, Groups A, B, C, and D; Temperature Class T6 Ta = -20 °C
to +60 °C

Suitable for use in Class II and III, Division 2, Groups E, F, and G; Temperature Class T6 Ta = -20 °C to
+60 °C Hazardous (Classified) Locations

IS/I,II,III/1/ABCDEFG/T6 Ta = 60 °C - 1400332; Entity; I/0/AEx ia IIC/T6 Ta = 60 °C - 1400332; Entity;
NI/I/2/ABCD/T6 Ta = 60 °C; S/II,III/2/EFG/T6 Ta = 60 °C; Entity Parameters

Per standards 3600:1998, 3610:2010, 3611:2004, 3810:2005

CSA

Intrinsically Safe and Non-Incendive:

Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups
ABCD; Ex ia IIC; T6; Ambient temperature rating -20°C to +60°C: (Simple Apparatus)

Per standards C22.2 No. 0-10, C22.2 No. 0.4-M2004, C22.2 No. 94-M1991, C22.2 No. 142 – M1987,
C22.2 No 157 – M1992, CAN/CSA E60079-0:07, CAN/CSA E60079- 11:02, UL50 11th Ed, UL508
17th Ed, UL913 7th Ed, UL 60079-0: 2005, UL 60079-11: 2002

Description and Specifications 5

Description and Specifications Instruction Manual

March 2017 LIQ-MAN-396-396VP-397-398-398VP

1.4 Ordering Information

The Rosemount 396 pH sensor features either a standard hemi bulb or flat glass electrode. The
sensor is housed in a stainless steel body and must be used with a 1 inch MNPT threaded process
connector (sold separately). The Rosemount 396 is not available with an integral preamplifier and
comes standard with a 15 ft integral cable.

Table 1-3: Rosemount 396 ordering information

Model Sensor type

96

3

Transmitter/TC Compatibility

50 3K TC
54 Pt-100

Cable Option

_ No Selection
62 Cable without BNC

Electrode Option

_ No Selection
71 pH - GPHT Flat Glass

Typical Model Number: 396-54-62-71

H/ORP Sensor

p

1)

(

(2)

(3)

1. For use with legacy transmitter models 1181, 1050, and 1003.

2. For wiring to Rosemount 1056, 1066, 1057, 56, and 5081 transmitters.

3. No selection will configure the sensor with a standard hemi bulb glass electrode.

The Rosemount 396VP sensor features a Variopol cable connection for use with a mating Variopol
interconnecting cable (sold separately).

Table 1-4: Rosemount 396VP ordering information

Model Sensor type

396VP pH/ORP Sensor

Temperature Compensation

50 3K TC
54 Pt-100
55 Pt-100 (for SMART Preamp)

(1)

(2)

Electrode Option

_ No Selection
71 pH - GPHT Flat Glass

(3)

Preamplifier Option

_ No Selection
70 SMART Preamplifier

Typical Model Number: 396VP-55-71-70

1. For use with legacy transmitter models 1181, 1050, 1003.

2. Must be selected with Option 70 for SMART Preamplifier.

3. No selection will configure the sensor with a standard hemi bulb glass electrode.

4. Must be selected with Option 55.

(4)

6 Description and Specifications

Instruction Manual Description and Specifications

LIQ-MAN-396-396VP-397-398-398VP March 2017

The Rosemount 398 sensor is housed in a titanium tube and made with a Tefzel reference junction.
Sensors must be used with a 1 inch MNPT process connector (sold separately). These sensors come
with a standard 15 ft. integral cable. A preamplifier must be used if the sensor is installed more than
15 ft. from the connected transmitter.

able 1-5: Rosemount 398 ordering information

T

Model Sensor type

398 pH/ORP Sensor

Measuring Electrode Type

10 pH - GPHT Glass
12 ORP
13 pH - GPLR Flat Glass

O-ring Material

30 EPDM
31 Viton
32 Kalrez

Transmitter/TC Compatibility

1)

50 3K TC
54 Pt-100

Cable Option

_ No Selection
62 Cable without BNC

Typical Model Number: 398-10-30-54-62

(

(2)

1. For use with legacy transmitter model 1181. Not available with option 62. If selected with ORP, sensor will not come with TC.

2. For use with Rosemount transmitter models 1056, 1066, 1057, 56, and 5081. Only available with option 54.

The Rosemount 398VP sensor features a Variopol cable connection for use with a mating Variopol
interconnecting cable (sold separately).

Table 1-6: Rosemount 398VP ordering information

Model Sensor type

398VP pH/ORP Sensor

Measuring Electrode Type

10 pH - GPHT Glass
12 ORP
13 pH - GPLR Flat Glass

O-ring Material

30 EPDM
31 Viton
32 Kalrez

Transmitter/TC Compatibility

50 3K TC
54 Pt-100

Typical Model Number: 398VP-10-30-54

1. For use with legacy transmitter model 1181. If selected with ORP, sensor will not come with TC.

(1)

Description and Specifications 7

Description and Specifications Instruction Manual

March 2017 LIQ-MAN-396-396VP-397-398-398VP

The Rosemount 397 pH sensor is housed in a polypropylene body and is designed to be used with

he Quik-Loc Kit (sold separately).

t

Table 1-7: Rosemount 397 ordering information

Model Sensor type

397 pH/ORP Sensor

Preamplifier/Cable

02 Without Integral Preamplifier, 15 ft (4.6 m) Cable

Measuring Electrode Type

10 pH - GPHT Glass
12 ORP

Transmitter/TC Compatibility

50 3K TC
54 Pt-100

Other Options

_ No Selection
62 Cable without BNC
64 Tefzel Body Material

Typical Model Number: 397-02-10-54-62

(1)

(2)

1. For use with legacy transmitter model 1181.

2. For use with Rosemount transmiter models 1056, 1066, 1057, 56, and 5081.

8 Description and Specifications

Instruction Manual Installation

LIQ-MAN-396-396VP-397-398-398VP March 2017

Section 2: Installation

2.1 First Time Installation

For first time Rosemount 397 installations, using the following guide is recommended:

1. Quik-Loc Mounting (required for all first time installations)

Choose one: PN 23757-00, Quik-Loc Kit: for use in 1 in. tees; insertion depth 1.4 in. (35 mm)

2. Remote Junction Boxes (optional, recommended for sensor to analyzer distances of more
than 15 ft)

Choose one: PN 23555-00 includes preamplifier

3. Extension cables (used with remote junction boxes)

Choose one: PN 23646-01, 11 conductor, shielded, prepped

PN 9200273, 11 conductor, shielded, unprepped

For first time Rosemount 396/396VP/398/398VP installations, using the following guide is
recommended:

1. Process Connector Accessories (required for all first time installations with 1-inch process
connection threads)

Choose one: PN 23166-00, 316 SST, 1 in. x 1 in. NPT process connector, with EPDM O-ring

PN 23166-01, Titanium, 1 in. x 1 in. NPT process connector, with EPDM O-ring

PN 9510066, Nylon, 1 in. x 1 in. NPT process connector (submersion only)

Choose one (optional process connector o-rings)

PN 9550220, Kalrez o-ring, 2-214

PN 9550099, Viton o-ring, 2-214

2. Variopol Cable (required for all first time installations) of Models 396VP and 398VP

Choose one: PN 24281-00, 15 ft cable with mating VP connector

PN 24281-06, 10 ft cable with mating VP connector

3. Mounting Accessories (optional)

Choose one: PN 915240-03 PVC flow through tee, 3/4 in. NPT process connection

PN 915240-04 PVC flow through tee, 1 in. NPT process connection

PN 915240-05 PVC flow through tee, 1 1/2 in. NPT process connection
PN 11275-01 Sensor handrail mounting assembly
PN 2002011 1-1/2 in. CPVC Tee with 1 in. FNPT connection
PN 24091-00 Low Flow Cell

4. Remote Junction Boxes (optional, recommended for sensor to analyzer distances of more
than 15 ft)

Choose one: PN 23555-00 includes preamplifier

5. Extension cables (used with remote junction boxes)

Choose one: PN 23646-01, 11 conductor, shielded, prepped

PN 9200273, 11 conductor, shielded, unprepped

Installation 9