Rosemount Analytical 385+ Operating Manual

Instruction Manual
IQ-MAN-385+
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Rev. J
Rosemount
pH/ORP Sensors
385+
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Essential Instructions
Read this page before proceeding!
Emerson designs, manufactures and tests its products to meet many national and international stan-
dards. Because these sensors are sophisticated technical products, you MUST properly install, use,
nd maintain them to ensure they continue to operate within their normal specifications. The
a following instructions MUST be adhered to and integrated into your safety program when installing, using, and maintaining Rosemount products. Failure to follow the proper instructions may cause any one of the following situations to occur: loss of life; personal injury; property damage; damage to this sensor; and warranty invalidation.
Read all instructions prior to installing, operating, and servicing the product.
If you do not understand any of the instructions, contact your Emerson representative for clarification.
Follow all warnings, cautions, and instructions marked on and supplied with the product.
Inform and educate your personnel in the proper installation, operation, and maintenance of the product.
Install your equipment as specified in the Installation Instructions of the appropriate Instruction Manual and per applicable local and national codes. Connect all products to the proper electrical and pressure sources.
To ensure proper performance, use qualified personnel to install, operate, update, program, and maintain the product.
When replacement parts are required, ensure that qualified people use replacement parts specified by Emerson. Unauthorized parts and procedures can affect the product's performance, place the safe operation of your process at risk, and VOID YOUR WARRANTY. Third-party substitutions may result in fire, electrical hazards, or improper operation.
Ensure that all equipment doors are closed and protective covers are in place, except when maintenance is being performed by qualified persons, to prevent electrical shock and personal injury.
The information contained in this document is subject to change without notice.
DANGER
Hazardous Area InstallationN
This sensor is not Intrinsically Safe. or Explosion Proof. Installations near flammable liquids or in hazardous area locations must be carefully evaluated by qualified on site safety personnel.
To secure and maintain an intrinsically safe installation, an appropriate transmitter/safety barrier/sensor combi nation must be used. The installation system must be in accordance with the governing approval agency (FM, CSA or BASEEFA/CENELEC) hazardous area classification require­ments. Consult your transmitter instruc tion manual for details.
Proper installation, operation and servicing of this sensor in a Hazardous Area Instal lation is entirely the responsibility of the user.
CAUTION
Sensor/Process Application Compatibility
The wetted sensor materials may not be compatible with process composition and operating conditions. Application compatibility is entirely the responsibility of the user.
WARNING
Retractable sensors must not be inserted nor retracted when process pressures are in excess of 64 psig (542kPa)
About This Document
his manual contains instructions for installation and operation of the Rosemount 385+
T pH/ORP Sensors.
The following list provides concerning all revisions of this document.
Rev. Level Date Notes
A 02/01 This is the initial release of the product manual. The manual has
been reformatted to reflect the Emerson documentation style
and updated to reflect any changes in the product offering. B 05/02 Drawings updated throughout C 05/03 Drawing 40385+02 updated to rev. C; added drawing
41055119 — both on page 9. D 09/04 Updated wiring diagrams and Table 5-2 E 10/04 Added 1055 single input wiring diagram. F 03/05 ORP info revision. G 05/05 Fixed LED font mis-print on page 16. H 03/06 Added a note on page 6.
I 05/09 Updated for SMART sensors.
J 03/17 Reformatted to reflect the latest Emerson documentation style
and updated the ordering information, EC Declaration of
conformity, FM Installation drawing, and Accessories.
Instruction Manual Table of Contents
LIQ-MAN-385+ March 2017
Contents
Section 1: Description and Specifications
1.1 Features and Applications....................................................................................1
1.2 Performance and Specifications ...........................................................................2
1.3 Ordering Information...........................................................................................3
1.4 Product Certifications ..........................................................................................4
Section 2: Installation
2.1 Unpacking and Inspection ...................................................................................5
2.2 Mechanical Installation ........................................................................................5
2.3 Electrical Installation..........................................................................................10
Section 3: Startup and Calibration
3.1 Startup ..............................................................................................................17
3.2 pH Calibration Using Buffer Solutions or Grab Samples ......................................17
3.3 ORP Calibration .................................................................................................17
Section 4: Maintenance
4.1 Maintenance......................................................................................................19
4.2 Sensor Removal .................................................................................................19
4.3 pH Electrode Cleaning .......................................................................................20
4.4 Platinum Electrode Cleaning..............................................................................20
4.5 Sensor Tube Replacement (Code -02).................................................................21
Section 5: Diagnostics and Troubleshooting
5.1 Model 54/3081 pH Diagnostics..........................................................................25
5.2 Troubleshooting ................................................................................................25
5.3 Rosemount 1056/1057 SMART pH Diagnostics ..................................................26
Section 6: Accessories
6.1 Accessories........................................................................................................29
EC Declaration of Conformity.............................................................................31
Intrisicallly Safe Sensor Installation Drawing - FM ................................33
Table of Contents i
Table of Contents Instruction Manual
March 2017 LIQ-MAN-385+
ii Table of Contents
Instruction Manual Description and Specifications
LIQ-MAN-385+ March 2017
Section 1: Description and Specifications
SMART enabled
Retractable version allows removal and replacement under pressure without process shut­down.
Long-life, triple junction reference electrode provides longer service life in applications where poisoning ions are present.
Disposable tefzel and titanium design provides maximum chemical resistance and econom­ical advantage where minimum troubleshooting and maintenance downtime are of prime importance.
1.1 Features and Applications
The Rosemount 385+ Sensor measures the pH or ORP (Oxidation Reduction Potential) of aqueous solutions in pipelines, open tanks, or ponds. It is suitable for applications where a low cost, industrial, disposable sensor is required. The combination electrode features a peripheral ceramic junction. The triple junction reference cell provides longer life in processes containing sugar, ammonia, chlorides, sulfides or other poisoning ions. The Rosemount 385+ body is constructed of molded, chemically resistant Tefzel in two standard body versions.
The retraction version is housed in a titanium tube, with a plug-in style surface mount preamplifier in a weatherproof junction box. It is designed for use with a standard 1-1/2 in. ball valve assembly for process mounting where a separate sample stream is difficult or impossible to provide. The entire installation process is accomplished without line depressurization and minimal process fluid loss. Upon sensor removal, from the ball valve, maintenance and replacement is easy.
The insertion/submersion version has two body configurations: 25 ft (7.6 m) integral cable and preamplifier; 15 ft (4.5) integral cable for use with remote preamplifier.
Description and Specifications 1
Description and Specifications Instruction Manual
March 2017 LIQ-MAN-385+
1.2 Performance and Specifications
able 1-1: Percent linearity over pH
T
pH Range Option 10 Option 11
0-2 pH 94% 94%
2-12 pH 99% 97%
12-13 pH 97% 98%
13-14 pH 92% 98%
Table 1-2: Rosemount 385+ sensor specifications
Measured Range
pH range 0 to 14 pH, GPHT ACCUGLASS
ORP range -1500 mV to 1500 mV
Maximum Pressure at Retraction or Insertion (ball valve version)
542 KPa abs (64 psig)
Maximum Process Pressure and Temperature
790 KPa abs (100 psig) at 100 °C (212 °F)
Temperature Compensation
(pH only) 0 to 100°C (32 to 212°F)
Wetted Materials
Tefzel, titanium, EPDM, 316 SS and Teflon (Code 02), Viton, glass, ceramic and (ORP only) platinum.
Weight/Shipping Weight
Submersion/insertion 1.6 lb/2.8 lb (0.7 kg/1.25 kg)
Retraction 6 lb/11 lb (2.7 kg/5.0 kg)
Ball Valve 5 lb/10 lb (2.25 kg/4.5 kg)
Process Connections
With ball valve 1-1/2 in.
Without ball valve 1 in.
Cable Length
Code 02 Requires interconnecting cable P/N 9200273 (Unprepped) or P/N 23646-01 (Prepped)
Code 03 25 ft. Integral Cable
Code 04 15 ft. Integral Cable
2 Description and Specifications
Instruction Manual Description and Specifications
LIQ-MAN-385+ March 2017
1.3 Ordering Information
Table 1-3: Rosemount 385+ ordering information
Model Sensor type
385+ pH/ORP Sensor
Body Configuration
02 Retractable with Sensor Head Junction Box, Preamplifier, and Process Connector 03 Insertion/Submersion with Integral Preamplifier and 25 ft. (7.6m) Cable 04 Insertion/Submersion for use with Remote Preamplifier and 15 ft.
(1) (2)
(2)
Combination Electrode
10 pH - GPLR Glass 11 High pH Glass 12 Platinum ORP
Typical Model Number: 385+-03-10
1. Preamplifier is SMART for pH options only. A standard preamplifier is used with ORP sensors.
2. First time installations require a 1 x 1 inch NPT Process Connector (see accessories).
(1)
Description and Specifications 3
Description and Specifications Instruction Manual
March 2017 LIQ-MAN-385+
1.4 Product Certifications
Please see online certificates for further details.
ECEx
I
Sensors without preamp (pH and ORP) – Ex ia IIC T4 Ga (-20°C ≤ Ta ≤ +60°C)
Sensors with preamp (pH only) – Ex ia IIC T4 Ga (-20°C ≤ Ta ≤ +60°C)
Sensors with standard preamp (ORP only) – Ex ia IIC T4 Ga (-20°C ≤ Ta ≤ +80°C) or Ex ia IIC T5 Ga
(-20°C ≤ Ta ≤ +40°C)
Per standards IEC60079-0 : 2011, IEC 60079-11 : 2011
ATEX
Sensors without preamp (pH and ORP) – II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C)
Sensors with SMART preamp (pH only ) – II 1 G Ex ia IIC T4 Ga (-20˚C ≤ Ta ≤ +60 °C)
Sensors with standard preamp (ORP only) – II 1 G Ex ia IIC T4 Ga (-20˚C ≤ Ta ≤ +80˚C) or
II 1 G Ex ia IIC T5 Ga (-20˚C ≤ Ta ≤ +40˚C)
Per standards EN 60079-0: 2012+A11:2013, EN 60079-11:2012
FM
See online FM Certificate of Compliance for applicable sensor options:
Intrinsically Safe for use in Class I, II, and III, Division 1, Groups A, B, C, D, E, F, and G; Temperature Class T6 Ta = -20 °C to +60 °C
Intrinsically Safe for use in Class I, Zone 0, AEx ia IIC T6 Ta = -20 °C to +60 °C
Nonincendive for use in Class I, Division 2, Groups A, B, C, and D; Temperature Class T6 Ta = -20 °C to +60 °C
Suitable for use in Class II and III, Division 2, Groups E, F, and G; Temperature Class T6 Ta = -20 °C to +60 °C Hazardous (Classified) Locations
IS/I,II,III/1/ABCDEFG/T6 Ta = 60°C - 1400332; Entity; I/0/AEx ia IIC/T6 Ta = 60 °C - 1400332; Entity; NI/I/2/ABCD/T6 Ta = 60 °C; S/II,III/2/EFG/T6 Ta = 60 °C
Per standards 3600:1998, 3610:2010, 3611:2004, 3810:2005
CSA
See online CSA Certificate of Compliance for applicable sensor options:
Intrinsically Safe:
Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups ABCD; Ambient temperature rating -20 °C to +60 °C; Ex ia IIC; T6
Intrinsically Safe and Non-Incendive:
Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups ABCD; Ex ia IIC; T6; Ambient temperature rating -20 °C to +60 °C: (Simple Apparatus)
Per standards C22.2 No. 0-10, C22.2 No. 0.4-M2004, C22.2 No. 94-M1991, C22.2 No. 142 – M1987, C22.2 No 157 – M1992, CAN/CSA E60079-0:07, CAN/CSA E60079- 11:02, UL50 11th Ed, UL508 17th Ed, UL913 7th Ed, UL 60079-0: 2005, UL 60079-11: 2002
4 Description and Specifications
Instruction Manual Installation
LIQ-MAN-385+ March 2017
Section 2: Installation
2.1 Unpacking and Inspection
Inspect the outside of the carton for any damage. If damage is detected, contact the carrier immediately. Inspect the instrument and hardware. Make sure all items in the packing list are present and in good condition. Notify the factory if any part is missing.
NOTICE
Save the original packing cartons and materials as most carriers require proof of damage due to mishan­dling, etc. Also, if it is necessary to return the instrument to the factory, you must pack the instrument in the same manner as it was received. Refer to Section 6.0 for instructions.
WARNING
Glass electrode must be wetted at all times (in storage and in line) to maximize sensor life.
2.2 Mechanical Installation
The Rosemount 385+ is available in two versions, the retraction version (Code 02) and the insertion/submersion version (Code 03, & 04). Please refer to the appropriate section below.
2.2.1 Retraction Option (Code option 02)
The Rosemount 385+ sensor may be installed through a weldalet or in a pipe tee or “Y”, as shown in Figure 2-1, when used with a ball valve. Insert the end of the sensor to a depth sufficient to ensure that the glass bulb is continuously wetted by the process fluid.
The sensor can also be inserted directly into the process without the use of a ball valve for applications not requiring continuous operation during sensor maintenance (Figure 2-2).
Allow sufficient room for safe retraction and insertion of the sensor. personnel should have room for stable footing while performing removal or insertion of the sensor.
The sensor must be mounted within 10-90 degrees of the horizontal with the tip pointed downward, thus keeping air bubbles out of the pH sensitive glass bulb. Bubbles settled in the glass bulb disrupt the electrical continuity between the pH sensitive glass and the silver/silver chloride measuring element.
If the retraction version is to be installed without a ball valve follow the installation procedure for insertion service (Section 2.2.2). Perform the following steps for sensor installation through a ball valve:
1. Carefully remove the liquid filled rubber boot which protects the glass electrode and keeps
the liquid junction wet during shipping and storage. Discard the liquid and boot. Make sure the lubricated O-ring is in place in the groove inside the male connector on the sensor body (Figure 4-1, item A).
CAUTION
Buffer solution, in the vinyl boot, may cause skin or eye irritation.
Installation 5
Installation Instruction Manual
March 2017 LIQ-MAN-385+
2. With the male connector on the sensor’s body, insert the sensor into the ball valve until it gently touches the closed valve. The molded electrode guard will protect the glass bulb from breakage.
3. Thread the male connector body tightly into the ball valve assembly. DO NOT tighten the hex nut on the male connector body; doing so would not allow the sensor to be inserted through the ball valve.
4. Pull back hard on the sensor assembly, as if trying to remove the sensor, to be certain that the sensor cannot come free of the ball valve assembly. The built-in retraction stop will butt against the shoulder of the male connector if properly installed.
CAUTION
The sensor must be captured by the valve assembly and the male connector so that it cannot be blown free by process pressure if mishandled during insertion or retraction.
5. After confirming that the sensor assembly is properly secured by the valve assembly, the valve may be opened and the sensor positioned into the process at the desired depth and orientation.
6. While holding the sensor in position, tighten the hex nut of the male connector to firmly secure the sensor in place. When the hex nut is tightened, the Teflon ferrule inside the compression fitting clamps the sensor tube. (See Figure 4-2.)
CAUTION
Over tightening the hex nut may damage the ferrule.
NOTICE
A stainless steel ferrule is available if the TEFLON ferrule does not inadequately grip. When using the metallic ferrule, care must be taken to avoid over tightening and damaging the sensor tube. If the male connector leaks during insertion or retraction, replace the O-ring in the male connector.
2.2.2 Submersion/Insertion Option
Code Option -03 & -04). Figure 2-3 and Figure 2-4. The Rosemount 385+ may be installed through a weldalet or a pipe tee or “Y” when used with a process connector (P/N 23166-00-01). For submersion service, a process connector (P/N 23166-00-01 or 9510066) may be used with a water tight 1 in. schedule 80 CPVC or PVDF standpipe conduit. Refer to Figure 2-5. Tapered threads in plastic tend to loosen after installation. It is therefore recommended that TEFLON tape be used on the threads and that the tightness of the connection be checked frequently to assure that no loosening has occurred. The sensor should be installed within 80° of vertical, with the electrode facing down.
6 Installation
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