Rosemount NGA 2000 FID User Manual

NGA 2000
F
LAME IONIZATION
A
NALYZER
D
ETECTION
ODULE
Rosemount Analytical
N
OTICE
HE INFORMATION CONTAINED IN THIS DOCUMENT IS SUBJECT TO CHANGE WITHOUT NOTICE
T
.
OSEMOUNT ANALYTICAL'S
R
UNDER
Teflon® is a registered trademark of E.I. duPont de Nemours and Co., Inc. Kynar® is a registered trademark of Pennwalt, Inc.
U.S. P
ATENT
NGA 2000
5.787.015.
SYSTEM OF MODULAR GAS ANALYZERS AND CONTROLLERS ARE PATENTED
,
Manual Part Number 748331-E November 1998 Printed in U.S.A.
Rosemount Analytical Inc.
4125 East La Palma Avenue Anaheim, California 92807-1802
C
ONTENTS
P
REFACE
PURPOSE/SAFETY SUMMARY........................................................................P-1
GLOSSARY ......................................................................................................P-4
SPECIFICATIONS - GENERAL..........................................................................P-7
SPECIFICATIONS - GAS REQUIREMENTS .....................................................P-8
SPECIFICATIONS - PHYSICAL.........................................................................P-9
SPECIFICATIONS - GAS CONNECTIONS........................................................P-9
CUSTOMER SERVICE, TECHNICAL ASSISTANCE AND FIELD SERVICE ....P-10
RETURNING PARTS TO THE FACTORY .........................................................P-10
TRAINING ......................................................................................................P-10
DOCUMENTATION............................................................................................P-10
COMPLIANCES..................................................................................................P-11
S
ECTION
1.1 OVERVIEW ..............................................................................................1-1
1.2 TYPICAL APPLICATIONS........................................................................1-1
1.3 THEORY OF TECHNOLOGY...................................................................1-1
1.4 GAS SAFETY FEATURES.......................................................................1-3
1.5 FUEL GAS OPTION .................................................................................1-3
S
ECTION
2.1 UNPACKING.............................................................................................2-1
2.2 ASSEMBLY...............................................................................................2-1
2.3 LOCATION ...............................................................................................2-2
2.4 GASES .....................................................................................................2-3
1. I
2. I
2.4.1 Overview.....................................................................................2-3
NTRODUCTION
NSTALLATION
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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C
ONTENTS
2.4.2 Connections................................................................................2-4
2.4.3 Specifications .............................................................................2-5
2.4.4 Leak Test....................................................................................2-7
2.5 ELECTRICAL CONNECTIONS................................................................2-7
S
ECTION
3.1 OVERVIEW..............................................................................................3-1
3.2 DISPLAYS................................................................................................3-1
3.3 RUN MODE DISPLAY..............................................................................3-1
3.4 MENU DISPLAYS....................................................................................3-1
3.5 HELP DISPLAYS .....................................................................................3-2
3.6 STARTUP PROCEDURE.........................................................................3-6
3.7 BINDING ..................................................................................................3-9
3.8 CALIBRATION .........................................................................................3-9
3.9 ROUTINE OPERATION...........................................................................3-10
3.10 SAFETY SYSTEM....................................................................................3-11
S
ECTION
4.1 BURNER DISASSEMBLY AND CLEANING.............................................4-1
4.2 COMPONENT REPLACEMENT...............................................................4-3
3. S
4. M
TARTUP AND OPERATION
AINTENANCE AND TROUBLESHOOTING
4.3 BURNER STARTUP TROUBLESHOOTING ...........................................4-3
S
ECTION
5.1 REPLACEMENT PARTS ..........................................................................5-1
A
PPENDIX
ENERAL PRECAUTIONS FOR HANDLING
G
ARRANTY
W
IELD SERVICE AND REPAIR FACILITIES
F
5. R
5.1.1 Electronics..................................................................................5-1
5.1.2 Electro-Mechanical.....................................................................5-1
5.1.3 O-Rings and Gaskets.................................................................5-1
5.1.4 Burner Assembly and Components............................................5-2
5.1.5 Pneumatics.................................................................................5-2
EPLACEMENT PARTS
A. FID I
DENTIFICATION MATRIX
TORING HIGH PRESSURE CYLINDERS
& S
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November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
F
IGURES
1-1 Flame Ionization Detection Technology....................................................1-1
1-2 NGA 2000 Flame Ionization Detection Module - Top View.......................1-2
2-1 Analyzer Module Installation Into Platform ...............................................2-1
2-2 Back Panel Connections...........................................................................2-2
2-3 FID Module Flow Diagram........................................................................2-4
2-4 Front Panel Connections, Controls and Indicators...................................2-5
2-5 Outline and Mounting Dimensions............................................................2-8
2-6 FID Wiring Diagram..................................................................................2-9
3-1 Run Mode Display....................................................................................3-2
3-2 Main Menu Display...................................................................................3-2
3-3 Basic Controls Menu Display....................................................................3-3
3-4 Expert Controls and Setup Menu Display.................................................3-3
3-5 Technical Configuration Menu Display.....................................................3-3
3-6 Typical Help Screen..................................................................................3-4
3-7 Typical Curves of Module Response vs. Pressure Setting on Sample
Pressure Regulator........................................................................3-5
3-8 Typical Curves of Module Response vs. Pressure Setting on Fuel
Pressure Regulator........................................................................3-5
3-9 Typical Curves of Module Response vs. Pressure Setting on Air
Pressure Regulator........................................................................3-6
3-10 Front Panel Torquing Sequence...............................................................3-12
3-11 Display Screens (1 of 5)...........................................................................3-13
3-12 Display Screens (2 of 5)...........................................................................3-14
3-13 Display Screens (3 of 5)...........................................................................3-15
3-14 Display Screens (4 of 5)...........................................................................3-16
3-15 Display Screens (5 of 5)...........................................................................3-17
4-1 FID Burner Assembly................................................................................4-2
C
ONTENTS
T
ABLES
1-1 Analyzer Characteristics Relative to Fuel Gas...........................................1-5
3-1 FID Analyzer Module Alarms....................................................................3-4
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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C
ONTENTS
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OTES
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November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
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REFACE
P
URPOSE/SAFETY SUMMARY
The purpose of this manual is to provide information concerning the components, functions, installation and maintenance of this particular NGA 2000 module.
Some sections may describe equipment not used in your configuration. The user should become thoroughly familiar with the operation of this module before operating it. Read this instruction manual completely.
To avoid explosion, loss of life, personal injury and damage to this equipment and on-site property, all personnel authorized to install, operate and service this equipment should be thoroughly familiar with and strictly follow the instructions in this manual. Save these instructions.
If this equipment is used in a manner not specified in these instructions, protective systems may be impaired.
DANGER
personal injury, death, or substantial property damage if the warning is ignored.
WARNING
personal injury, death, or substantial property damage if the warning is ignored.
CAUTION
personal injury or property damage if the warning is ignored.
NOTE
important but not hazard-related.
is used to indicate the presence of a hazard which
is used to indicate the presence of a hazard which
is used to indicate the presence of a hazard which
is used to indicate installation, operation or maintenance information which is
will
cause
can
cause
will or can
cause
severe
severe
minor
WARNING: ELECTRICAL SHOCK HAZARD
Operate this equipment only when covers are secured. Servicing requires access to live parts which can cause death or serious injury. Refer servicing to qualified personnel.
For safety and proper performance, this module must be connected to a properly grounded three-wire source of electrical power.
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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REFACE
WARNING: POSSIBLE EXPLOSION HAZARD
This equipment is used in the analysis of sample gases which may be flammable, and the burner fuel used in the ionization process is flammable. A continuous dilution purge system is factory-installed (in accordance with Standard ANSI/NFPA 496-1993, Chapter 6, and it must be functional at all times during operation. DO NOT DISABLE THIS PURGE SYSTEM.
WARNING: FLAMMABLE SAMPLES
Consult the factory if flammable samples will be measured.
WARNING: PARTS INTEGRITY
Tampering with or unauthorized substitution of components may adversely affect safety of this product. Use only factory-approved components for repair.
WARNING: POSSIBLE EXPLOSION HAZARD
Ensure that all gas connections are made as labeled and are leak free. Improper gas connections could result in explosion and death.
CAUTION: PRESSURIZED GAS
This module requires calibration with a known standard gas. See General Precautions for Handling and Storing High Pressure Gas Cylinders at the rear of this manual.
CAUTION: OVERBALANCE HAZARD
This Analyzer Module may tip instrument over if it is pulled out too far and the Platform is not properly supported.
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REFACE
CAUTION: HAND INJURY HAZARD
Dropping the front panel of the Platform while hand or fingers are inside either case handle can cause serious injury.
CAUTION: PURGE AIR REQUIREMENT
This Analyzer Module must be used in conjunction with a device (Platform or PC Interface) that can actively monitor network variables related to pressure or flow of the continuous dilution purge, or the front panel LEDs of the Analyzer Module, as installed, must be visible. The purpose of this requirement is to maintain adherence to ANSI/NFPA 496 standard which assures the continued viability of the purge system. Under no circumstances should any pressure or flow indicator be connected to the PURGE AIR OUT outlet of the Analyzer Module because this may affect the sealing performance of the module.
CAUTION: OVER-VOLTAGE SPIKING
If this Analyzer Module is used with a non-Rosemount Analytical power supply, adding Rosemount P/N 903341 Current Protector in series with the 24 V positive power line will prevent over-voltage spiking and resultant fuse blowing when powering up the instrument.
Note This Analyzer Module is completely leak-tested at the factory for gas leakage.
The user is responsible for testing for leakage at the inlet and outlet fittings on the rear panel (with a test procedure chosen by the user). The user is also responsible for leak-testing periodically and if any internal pneumatic components are adjusted or replaced. See leak test instructions in section 2.4.4.
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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REFACE
G
LOSSARY
NALYZER MODULE
A
The module that contains all sensor/detector components for development of a Primary Variable signal; includes all signal conditioning and temperature control circuitry.
ACKPLANE
B
The interconnect circuit board which the Controller Board, Power Supply, Analyzer Module power and network cables, I/O Modules and Expansion Modules plug into.
ONTROL MODULE
C
The Operator Interface plus the Controller Board.
ONTROLLER BOARD
C
The computer board that serves as the Network Manager and operates the Display and Keypad.
ISTRIBUTION ASSEMBLY
D
The Backplane and the card cages that hold I/O and Expansion Modules.
XPANSION MODULE
E
A circuit board that plugs into the Backplane from the front of the Platform and performs special features not related to I/O functions.
I/O M
A circuit board that plugs into the Backplane from the rear of the Platform. Has a connector terminal for communication with external data acquisition devices and provides an input/output function.
O
The Display and Keyboard.
P
Any workable collection of the following: Controller Board, Power Supply, Distribution Assembly, Enclosure and Operator Interface.
P
ODULE
PERATOR INTERFACE
LATFORM
OWER SUPPLY
Any of a variety of components that provides conditioned power to other NGA 2000 components, from the Power Supply Board that plugs into the front of the Backplane in a stand-alone instrument to several larger ones that can power larger collections of modules and components.
P-4
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REFACE
RIMARY VARIABLE
P
The measured species concentration value from an Analyzer Module.
ECONDARY VARIABLE
S
Data placed on the network by a module regarding current status, e.g., sample flow, source voltage and other diagnostic information.
OFTKEYS
S
The five function keys located below the front panel display; they assume the function displayed directly above each on the display, a function dictated by software.
YSTEM
S
Any collection of Analyzer Module(s), Platform(s), I/O Module(s) and Expansion Module(s).
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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REFACE
N
OTES
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REFACE
S
PECIFICATIONS
M
EASUREMENT SPECIES
R
ANGES
H2/H
E FUEL
H2
FUEL OPTION
R
EPEATABILITY
M
INIMUM DETECTABLE LEVEL
N
OISE
L
INEARITY
R
ESPONSE TIME
CEMS ICEE
Z
ERO DRIFT
S
PAN DRIFT
E
FFECT OF TEMPERATURE
O
PERATING TEMPERATURE
P
OWER REQUIREMENTS
- G
ENERAL
Total hydrocarbons
0 to 100 ppm (output scalable down to 0-2 ppm fullscale)
low range: 0 to 4 ppm CH4, through 0 to 1% CH high range:: 0 to 50 ppm CH4, through 0 to <5% CH
low range: 0 to 1 ppm CH4, through 0 to 2500 ppm CH high range:: 0 to 10 ppm CH4, through 0 to 2% CH
1% of fullscale at a constant temperature, sample flow and fuel, burner
4
4
4
4
air and sample pressure
0.04 ppm H2/He fuel
0.01 ppm H2 fuel
1% of fullscale, peak to peak
1% of fullscale for H2/He fuel and He fuel
≤ ±
30 sec. For 10% to 90% of fullscale, with sample bypass flow at 0.5
L/min. (non-flammable sample)
1 sec. For 10% to 90% of fullscale, with sample bypass flow at 0.5
L/min. (non-flammable sample)
1% of fullscale/24 hours at constant temperature, hydrocarbon
≤ ±
concentration of supply gases, sample flow and fuel, burner air and sample pressure
1% of fullscale/24 hours at constant temperature, hydrocarbon
≤ ±
concentration of supply gases, sample flow and fuel, burner air and sample pressure
2% of fullscale for any temperature change of 10°C and rate of
≤ ±
change less than 10°C/hour
32°F to 113°F (0°C to 45°C)
+24 VDC ±5%, 120 W max.. direct to analyzer module; Ripple and Noise: <100 mV peak to peak Line and Load Regulations: <±1%
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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P
REFACE
S
PECIFICATIONS
B
URNER AIR
F
LOW RATE
THC S
UPPLY PRESSURE
F
UEL GAS (STANDARD
F
LOW RATE
THC S
UPPLY PRESSURE
Unless this Analyzer Module is factory- or field-configured specifically for using 100% hydrogen fuel, DO NOT USE PURE HYDROGEN FUEL. An explosion resulting in severe personal injury or death could occur. Also, each Analyzer Module is factory-configured for either mixed or pure hydrogen fuel, and cannot use the fuel for which it was not configured unless field reconfiguration is done.
- G
AS REQUIREMENTS
Zero-grade air 350 to 400 ml/min
ppm, CH
4
1725 to 3450 hPa-gauge (25 to 50 psig)
)
Premixed 40% hydrogen and 60% helium 75 to 80 ml/min.
0.5 ppm, CH
4
2415 to 3450 hPa-gauge (35 to 50 psig)
WARNING: POSSIBLE EXPLOSION HAZARD
F
UEL GAS
S
AMPLE
P
URGE AIR
(H
OPTION
2
F
LOW RATE
THC S
UPPLY PRESSURE
F
LOW RATE
THC S
UPPLY PRESSURE
T
EMPERATURE
P
ARTICULATES
D
EWPOINT
F
LOW RATE
S
UPPLY PRESSURE
)
Zero-grade hydrogen 35 to 40 ml/min.
0.5 ppm, CH
4
2415 to 3450 hPa-gauge (35 to 50 psig) Non-flammable (below 100% of LEL)
0.5 to 40 ml/min.
0.5 ppm, CH
4
483 to 1035 hPa-gauge (7 to 15 psig) 32°F to 132°F (0°C to 55°C), <20°C variance/24 hours,
<10°C variance/hour Filtered to <2 microns
<45°C Instrument air, nitrogen or other non-flammable gas (refer
to ANSI/NFPA 496 for the requirements for the Protective Gas System)
16 to 18 L/min. 689 to 1378 hPa-gauge (10 to 20 psig)
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REFACE
S
PECIFICATIONS
M
ATERIALS IN CONTACT
WITH SAMPLE
D
IMENSIONS
W
EIGHT
M
OUNTING
C
ASE CLASSIFICATION
MAX. S
FROM PLATFORM
S
PECIFICATIONS
S B F
UEL IN
P P B B
P V
EPARATION
AMPLE IN URNER AIR IN
URGE AIR IN URGE AIR OUT YPASS OUT URNER EXHAUST OUT
RESSURE RELIEF ALVE
- P
HYSICAL
Stainless steel, Teflon, glass-filled Teflon, brass, neoprene, Kynar
See Figure 2-5, Outline and Mounting Dimensions
10.43 kg (23 lbs.) Horizontal, inside a Platform or custom installed in a panel General Purpose for installation in weather protected area 1600 m (1 mile)
- G
AS CONNECTIONS
1/4 inch O.D. tube fitting 1/4 inch O.D. tube fitting 1/4 inch O.D. tube fitting 3/8 inch O.D. tube fitting 3/8 inch O.D. tube fitting 1/4 inch O.D. tube fitting 1/2 inch O.D. tube connection, tygon or equivalent (this
connection shall slope downward 6° minimum from horizontal)
CAUTION: PRESSURE RELIEF
See the Preface Section of the Platform manual for specifications regarding Platform related components.
748331-E Rosemount Analytical November 1998
VALVE RESTRICTION
No connection shall be made to this fitting. If this caution is ignored, damage to the case seals may occur, and the instrument will not operate properly.
NGA 2000 Flame Ionization Detection Module
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REFACE
C
USTOMER SERVICE
For order administration, replacement Parts, application assistance, on-site or factory repair, service or maintenance contract information, contact:
R
ETURNING PARTS TO THE FACTORY
Before returning parts, contact the Customer Service Center and request a Returned Materials Authorization (RMA) number. Please have the following information when you call:
Number.
Prior authorization by the factory must be obtained before returned materials will be accepted. Unauthorized returns will be returned to the sender, freight collect.
When returning any product or component that has been exposed to a toxic, corrosive or other hazardous material or used in such a hazardous environment, the user must attach an appropriate Material Safety Data Sheet (M.S.D.S.) or a written certification that the material has been decontaminated, disinfected and/or detoxified.
Model Number, Serial Number, and Purchase Order Number or Sales Order
, T
ECHNICAL ASSIST ANCE AND FIELD SERVICE
Rosemount Analytical Inc.
Process Analytical Division
Customer Service Center
1-800-433-6076
Return to:
Rosemount Analytical Inc.
4125 East La Palma Avenue
Anaheim, California 92807-1802
T
RAINING
A comprehensive Factory Training Program of operator and service classes is available. For a copy of the the Technical Services Department at:
D
OCUMENTATION
The following NGA 2000 Flame Ionization Detection Module instruction materials are available. Contact Customer Service or the local representative to order.
748331 Instruction Manual (this document)
Current Operator and Service Training Schedule
Rosemount Analytical Inc.
Phone: 1-714-986-7600
FAX: 1-714-577-8006
contact
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November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
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9
6
OMPLIANCES
This product may carry approvals from several certifying agencies, including Factory Mutual and the Canadian Standards Association (which is also an OSHA accredited, Nationally Recognized Testing Laboratory), for use in non-hazardous, indoor locations
P
REFACE
FM
APPROVED
Rosemount Analytical Inc. has satisfied all obligations from the European Legislation to harmonize the product requirements in Europe.
This product complies with the standard level of NAMUR EMC. Recommendation (May 1993).
This product satisfies all obligations of all relevant standards of the EMC framework in Australia and New Zealand.
®
97-C219
NAMUR
N
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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REFACE
N
OTES
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November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
I
NTRODUCTION
1
1.1 OVERVIEW
This manual describes the Flame Ionization Detector (FID) Analyzer Module of Rosemount Analytical's NGA 2000 Series of gas analysis components. See Figures 1-1 and 1-2.
The FID Analyzer Module is designed to continuously determine the concentration of hydrocarbons in a flowing gaseous mixture. The concentration is expressed in parts-per-million or percent of volume.
The entire FID Analyzer Module is designed as a slide-in module (if configured in stand-alone instrument fashion), removable from the front of the Platform, with gas connections made from the rear. All electronics relative to sample detection and conditioning are included in this module.
1.2 TYPICAL APPLICATIONS
The monitoring of atmospheric air for low-level hydrocarbon contaminants and determining the hydrocarbon content of exhaust emissions from internal combustion engines are examples of typical applications for the FID Analyzer Module.
1.3 THEORY OF TECHNOLOGY
This Analyzer Module uses the flame ionization method of detection. The sensor is a burner in which a regulated flow of sample gas passes through a flame sustained by regulated flows of a fuel gas (hydrogen or a hydrogen/diluent mixture) and air.
Within the flame, the hydrocarbon components of the sample stream undergo a complex ionization that produces electrons and positive ions. Polarized electrodes collect these ions, causing current to flow through an electronic measuring circuit.
Negative Ion Collection Ring
+90V
Sample
F
IGURE
1-1. F
D
LAME IONIZATION
ETECTION
Signal Conditioning
Positive Carbon Ions
Air Fuel
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
1-1
NTRODUCTION
I
The ionization current is proportional to the rate at which carbon atoms enter the burner, and is therefore a measure of the concentration of hydrocarbons in the sample. This measure of concentration is placed on the network, where it is can be shown on the Platform Display or on other data acquisition devices.
Gas Lines (See Figure 2-2)
Purge Air
Fuel Shutoff Solenoid Valve
Pressure Regulator
Capillary
Case Heater Silicon Pad (On Base)
Purge Air Flow Switc h Fuel Pressure Sensor
Air Pressure Sensor
Ignite/Operate Mode Burner-Air Flow Solenoid Valve
Air Circulation Fan
Purge Air Heater Cartridge
Sample Press u re Sensor
Purge Air Outlet Pressure Switch
Preamp Board (In Shield)
Detector (Burner)
Computer Board
Sample Bypass Flow Sensor
DC-DC Converter
Safety Board
Burner Air and Fuel Regulators (Stacked Vertically)
Sample Back Pressure Regulators
F
IGURE
1-2. NGA 2000 F
1-2
Manual Ignite Switch
LAME IONIZATION DETECTION MODULE
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
Power Supply Board
Network & Power Module
- T
OP VIEW
1.4 GAS SAFETY FEATURES
The FID Analyzer Module is designed with a factory installed continuous dilution purge system in accordance with standard ANSI/NFPA 496 - 1993, Chapter 6. Front-panel LEDs indicate that the burner flame is lit and that the purge system is enabled. In addition, fuel gas is automatically shut off when a flame-out condition occurs or the safety system is disabled.
The purge system is enabled only if there is proper purge gas flow in, purge gas pressure, and internal case pressure, and after five times the case volume has been exchanged.
All tubing ahead of the burner is rigid metallic tubing assembled with ferrule/nut type compression fittings. However, should an internal fuel leak occur, a worst-case leak would be dissipated below 25% of the LEL of hydrogen through the combination of an inlet fuel flow restrictor and purge gas flow.
NTRODUCTION
I
This module is designed to use 100% hydrogen fuel or 40% H
2
/60% He fuel at a maximum inlet pressure of 3446 hPa-gauge (50 psig). A different flow restrictor is used for each fuel type.
A standard FID Analyzer Module is only equipped to analyze a non-flammable sample, below 100% of the LEL.
WARNING: POSSIBLE EXPLOSION HAZARD
Protection against explosion depends upon a special fuel flow restrictor in the fuel inlet fitting. Do not remove fuel inlet restrictor. Use the correct fuel flow restrictor for the fuel being used. Do not use 100% hydrogen fuel in a 40% H2/60% He configured Analyzer Module. Replace only with factory supplied fitting.
1.5 FUEL GAS OPTION
The standard FID Analyzer Module requires 40% hydrogen/60% helium burner fuel gas. As an option, the analyzer module can be equipped to use 100% hydrogen fuel. The particular application and characteristics of the sample gas to be measured will dictate the preferred type of fuel. The following guidelines can be used f or determining fuel gas type:
1. For measuring low-level hydrocarbons in ambient air or in other sample gas with
relatively constant oxygen content, 100% hydrogen is preferable. It provides the highest obtainable sensitivity and maximum stability. Zero drift caused by ambient temperature variations of the fuel cylinder is somewhat lower for 100% hydrogen than for mixed fuel. (With either fuel, it is desirable to maintain a constant cylinder temperature.)
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
1-3
NTRODUCTION
I
2. For monitoring internal combustion exhaust emissions or other sample gas with varying oxygen content, mixed fuel is preferable. In fact, a hydrogen/helium mixture is more desirable than a hydrogen/nitrogen mixture. With this type of sample, the use of mixed fuel gas minimizes the error introduced by oxygen synergism.
An effective way to reduce the effect of internal oxygen is to dilute it with an inert gas. This can be accomplished with a constant dilution of sample and calibration gases upstream from the burner. But it is simpler and more accurate to provide that diluent in the form of premixed fuel. Both nitrogen and helium have been used as a diluent, but helium has proven to be most effective in improving the quality of response to the various species of hydrocarbons.
As indicated earlier the flame output signal is optimum when the ratio of hydrogen flow to inert flow is about 40/60. Therefore, this is the chosen composition for hydrogen/helium premixed fuel.
The sample flow is kept low to maximize the dilution effect while still providing adequate sensitivity. The burner air flow is normally about four times the fuel flow, and changes have little effect on signal strength. For a given flow, the signal can be optimized by adjusting the fuel flow rate.
Typical flow rates with premixed fuel:
Fuel 100 cc/min Sample 7 cc/min Air 400 cc/min
Note that with a 40/60 premixed fuel, the above flow rates amount to 40 cc (8%) hydrogen, 67 cc (13%) inert plus sample and 400 cc (79%) air, which compare closely to the 30 cc (8%) hydrogen, 45 cc (12%) inert/sample and 300 cc (80%) air noted earlier for straight hydrogen fuel.
Since sample flow in the case of mixed fuel operation is only about 1/6 of that with straight hydrogen fuel, higher sensitivity is obtained with the latter. However, in any application where the sample contains more than one species of hydrogen and/or a varying concentration of oxygen, mixed fuel is preferred.
The mixed fuel is recommended, not only for sample containing variable concentrations of oxygen, but also for a specific pure gas application. If straight oxygen samples are used with straight hydrogen fuel, the mixture entering the burner is essentially 40% H2/60% O2, which tends to produce an unstable signal. The mixed fuel works better. Note that the choice of fuel determines certain analyzer characteristics, as shown in Table 1-1.
1-4
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
ANALYZER FUEL GAS
CHARACTERISTICS 100% H
FULLSCALE SENSITIVITY FUEL CONSUMPTION O
PERATING RANGE
1 ppm, CH4 to 2%, CH 35 to 40 cc/min 75 to 80 cc/min 276 to 345 hPa-gauge
2
(4 to 5 psig)
NTRODUCTION
I
40% H2/60% HE
4
4 ppm, CH4 to <5%, CH
4
207 to 345 hPa-gauge (3 to 5 psig)
T
ABLE
1-1. A
NALYZER CHARACTERISTICS RELATIVE TO FUEL GAS
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
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NTRODUCTION
I
N
OTES
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November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
I
NSTALLATION
2
2.1 UNPACKING
If the FID Analyzer Module is received as a separate unit, carefully examine the shipping carton and contents for signs of damage. Immediately notify the shipping carrier if the carton or contents is damaged. Retain the carton and packing material until all components associated with the Analyzer Module are operational.
2.2 ASSEMBLY
If the Analyzer Module requires assembly with other components (e.g., the Platform and associated I/O Modules), do so at this time. Following the guides on the bottom left and bottom center of the Platform, carefully slide the Analyzer Module halfway into place.
CAUTION: HAND INJURY HAZARD
Do not place hands or fingers in Platform front handles when the front panel is open. Dropping front panel while hand or fingers are inside either handle can cause serious injury.
ANALYZER MODULE GUI DES
PIN SEATS
DISENGAGED FRONT PANEL
F
IGURE
2-1. A
NALYZER MODULE INSTALLATION INTO PLATFORM
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
2-1
NSTALLATION
I
Lift the spring loaded pins on the front of the module, and carefully slide it the rest of the distance. Secure the module in position by releasing the pins, which seat in the available holes in the bottom of the case (see Figure 2-1). If the module and Platform are difficult to assemble, remove the module, ensure the top cover of the module is firmly seated on the hold down screws, and repeat the assembly procedure.
Connect the network cable to either the NETW ORK 1 or NETWORK 2 connection on the Analyzer Module (see Figure 2-4), and the NETWORK connection on the Backplane (see Platform manual). Connect the power cable to both the Analyzer Module front panel and to the Backplane.
Install I/O Module(s) according to guidelines in the I/O manual. After startup and calibration have been performed, secure the Front Panel with the six screws provided.
2.3 LOCATION
Install the Analyzer Module in a clean, weather-proofed, non-hazardous, vibration free location free from extreme temperature variations. For best results, install the Analyzer Module near the sample stream to minimize sample transport time.
MIXED
FUEL
IN
F
IGURE
2-2. B
PURGE
AIR OUT
SAMPLE
PRESSURE
RELIEF
VALVE
PURGE
AIR IN
ACK PANEL CONNECTIONS
BURNER
AIR IN
IN
BYPASS OUT
VENT TO SAFE AREA
SLOPE DOWNWARD
6° MINIMUM
MAXIMUM INPUT PRESSURE
FUEL: 50 PSIG (3450 hPa)
BURNER AIR: 50 PSIG (3450 hPa)
SAMPLE: 15 PSIG (1035 hPa)
PURGE AIR: 20 PSIG (1378 hPa)
BURNER EXHAUST OUT
WARNING: INSTALLATION RESTRICTIONS
For safety, the Analyzer Module should be installed in a non-confined, ventilated space. Do not block any of the rear panel outlets as they are part of the safety system.
Operating ambient temperature is 0°C to 45°C, limited to temperature changes of less than 10°C/hr. Acceptable dew point range is less than 95% relative humidity, but not in excess of 45°C wet bulb temperature.
2-2
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
The cylinders of fuel, air, and calibration gas(es) and the source of purge air should be located in an area of relatively constant ambient temperature.
2.4 GASES
NSTALLATION
I
2.4.1 O
VERVIEW
During normal operation, the Analyzer Module requires fuel and air to maintain the burner flame as well as suitable standard gases for calibration and instrument air for purge requirements. Criteria for selection of these gases follow in section 2.4.3.
After initial startup or after startup following a prolonged shutdown, the analyzer may display baseline drift for a considerable period of time, particularly on the most sensitive range. Commonly, the drift is caused by small amounts of hydrocarbons in the inner walls of the tubing in both the internal flow system and the external gas supply system. Drift results from any factor influencing the equilibrium of these absorbed hydrocarbons, such as temperature or pressure.
Note that this type of drift occurs only when the flame is burning. If drift occurs when the flame is extinguished, the electronic circuitry is at fault. To minimize drift, use clean fuel and air, keep the analyzer clean, and locate the gas cylinders in an area of relatively constant ambient temperature.
The cylinders supplying all gases each should be equipped with a clean, hydrocarbon free, two stage regulator and a shutoff valve.
All new external gas tubing (except for PURGE IN/OUT and SAMPLE BYPASS) is strongly recommended, preferably pre-cleaned, stain-less steel, gas chromatograph grade tubing. Thoroughly clean before use. if a hydrocarbon based cleaning solvent such as acetone is used, purge tubing with dry nitrogen or helium for several minutes before using.
Gas line connections are compression fittings. Do not use pipe thread tape. Since the oxidation of hydrogen is accompanied by the formation of water vapor, the
Exhaust tubing always should be slanted downward at least 6 degrees from horizontal. Otherwise, water may accumulate in the line, causing back pressure and noisy readings, or may back up in the line and flood the burner.
If the sample is toxic or noxious, or is to be reclaimed, connect the Bypass outlet to a suitable disposal system. Do not use any device that may cause back pressure in the line.
Purge air and burner air should be supplied from separate sources.
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
2-3
NSTALLATION
I
2.4.2 C
BURNER
EXHAUST
OUT
REGULATOR
Restrictor
ONNECTIONS
Reference Figure 2-2. Connect inlet and outlet lines for sample, burner fuel and air, exhaust, bypass, and purge to appropriately labeled fittings on the rear panel. All connections are 1/4 inch ferrule type compression fittings except the PURGE AIR IN and OUT connections, which are 3/8 inch compression fittings. The BURNER EXHAUST OUT is a 1/2 inch connection. Burner exhaust, bypass and purge air out must be vented at atmospheric pressure to a non-classified location in accordance with ANSI/NFPA-496.
Bulkhead 3/8T Brass
PURGE AIR
Plug 1/4MPT Brass
Run Tee 1/4T - 1/8MPT Brass
Tubing, Teflon 1/4” OD
PURGE
FLOW
SWITCH
Tubing, Copper 1/4” OD
Union 1/4T Brass
Diffuser
Tubing, SS 3/8” OD
PURGE AIR HEATER
PURGE AIR
IN
Elbow 3/8T - 1/4MPT Brass
Tubing, Viton 1/4” OD
PURGE
PRESS
SENSOR
Elbow 1/4T - 1/4MPT Kynar
SAMPLE
PRESS
SENSOR
Elbow 1/8T - 1/4MPT SS
SAMPLE
IN
CAPILLARY
Branch Tee 1/8T - 1/8FPT SS
SAMPLE
BACK PRESS
REGULATOR
SAMPLE
Elbow 1/8T - 1/8MPT Kynar
Connector 1/8T - 1/8MPT Kynar
BYPASS
OUT
Bulkhead Reducer 1/4T - 1/8T Brass
FLOW
SENSOR
Tubing, Teflon 1/8” OD
Elbow 1/8T - 1/4MPT SS
BURNER
AIR IN
Tubing, Teflon 1/8” OD
BURNER AIR PRESSURE REGULATOR
Connector 1/8T - 3/8MPT SS
Filter
Bulkhead Reducer 1/4T - 1/8T SS
GA
IN OUT
BURNER
AIR
PRESS
SENSOR
Bulkhead 3/8T - 1/4MPT Brass
COM
3-WAY VALVE
NO
Air Measurement Restrictor 1/8T - 1/8MPT SS
PURGE AIR
Run Tee 1/4T - 1/4FPT Brass
Connector 1/8T - 1/8MPT SS
Air Ignite Restrictor 1/8T - 1/8MPT SS
NC
Run Tee 1/8T - 1/8MPT SS
Bulkhead Connector
OUT
1/4T - 1/8NPT SS
Purge Exit Restrictor
BURNER
Fuel Restrictor
Tubing, Viton 1/4” OD
PRESS
SW
Connector 1/16T - 1/8MPT SS
Fuel Restrictor
MIXED FUEL
IN
SOLENOID
VALVE
Connector 1/8T - 1/8MPT SS
GA
IN OUT
FUEL
PRESS
SENSOR
FUEL PRESSURE REGULATOR
Connector 1/8T - 3/8MPT SS
F
IGURE
2-3. FID M
ODULE FLOW DIAGRAM
2-4
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
NSTALLATION
A
A
I
F
IGURE
2-4. F
BURNER
AIR
FUEL
WARNING
!
TTENTIO
!
SAMPLE
FUEL OVERRIDE
RONT PANEL CONNECTIONS
POWER
HEAT
FLAME
, C
LON
1
LON
ON
PURGE
1 +
AIR
2 -
3 GND T 6A 260V
2
IGNITE
ONTROLS AND INDICATORS
FID
WARNING
!
TTENTION
!
NETWORK 1
NETWORK 2
POWER
FUSE
It is recommended that no connection be made to the PURGE AIR OUT port. If, however, the analyzer's location requires interconnection with a venting system, the 3/8" O.D. line should be kept as short as possible, and no longer than four feet.
CAUTION: POSSIBLE INSTRUMENT DAMA GE
No connection should be made to the PRESSURE RELIEF VALVE fitting. Doing so may cause damage to the instrument.
2.4.3 S
PECIFICATIONS
UEL GAS
F
Standard analysis usually requires mixed fuel, i.e., 40% (±2%) hydrogen and 60% helium. H2/He mixed fuel is recommended over H2/N2 fuel because of better linearity in concentration output. Such blends are supplied by many gas vendors specifically for this use, with a guaranteed maximum total hydrocarbon content of 0.5 ppm, measured as methane. This specification should be used when obtaining these mixtures.
Note The fuel restrictor is marked with a red dot, and the sample capillary is marked with a
red or green dot for mixed fuel applications. Some applications require the use of 100% hydrogen fuel. When using this option,
always ensure that sample pressure (4 to 5 psig) is present when fuel flow is present. Otherwise, the detector tip may be damaged.
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
2-5
NSTALLATION
I
Note The fuel restrictor and sample capillary are marked with a white dot for 100%
hydrogen fuel applications.
URNER AIR
B
In order to ensure a low background signal, burner air should contain less than 1 ppm maximum total hydrocarbon content. An alternate source for burner air and zero gas (see CALIBRATION GASES below) is a combination diaphragm pump and heated palladium catalyst. This process continuously removes moderate amounts of hydrocarbons and carbon monoxide from ambient air.
URGE AIR
P
Instrument quality air, nitrogen, or other nonflammable gas is required for the saf ety purge system.
ALIBRATION GASES
C
Calibration method and gases depends on the type of fuel gas used, the operating range, and the desired measurement accuracy. In all methods, zero and span gases are used, and are introduced through the sample inlet at the rear of the module.
ERO GAS
Z
- Analysis is affected by the background gas of the sample. Therefore, it is
recommended to use zero gas with as close to the background composition of the sample as possible. Normally less than 0.5 THC as CH4 is sufficient.
If the burner fuel is 100% hydrogen, the zero gas, background gas of the sample or background gas of the span gas cannot be hydrogen or oxygen. These gases combined with pure hydrogen fuel would generate excessive heat in the burner, causing deterioration of the internal components of the burner.
PAN GAS
S
- Span gas consists of a specified concentration of methane or other
hydrocarbon in a background gas such as nitrogen. Analysis is affected by the background gas of the sample. Therefore, span gas containing the same background gas as the sample is recommended. Then, the background effect is canceled out.
AMPLE GAS
S
- Sample gas should be nonflammable (below 100% of the sample's
LEL). For high sensitivity applications requiring background gas compensation, contact the factory.
LOW RATE
F
- The sample flow rate must be between 0.5 L/min. and 2 L/min. Flow rate
for purge air should be 16 to 18 L/min.
RESSURIZATION/FILTRATION
P
the range of 483 to 1035 hPa-gauge (7 to 15 psig), and internally, should be 345
2-6
- Sample pressure at the SAMPLE inlet should be within
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
NSTALLATION
I
hPa-gauge (5 psig) nominally. Burner fuel pressures should be: 1725 to 3450 hPa-gauge (25 to 50 psig) for cylinder regulator, 1518 to 1723 hPa-gauge (22 to 25 psig) internal. Burner air pressures should be: 1725 to 3450 hPa-gauge (25 to 50 psig) for cylinder regulator, 965 to 1103 hPa-gauge (14 to 16 psig) internal. Purge air (external supply) pressure should be between 689 and 1378 hPa-gauge (10 and 20 psig), 689 to 827 hPa-gauge (10 to 12 psig) nominal. The internal purge air regulator pressure is factory preset at a nominal setting of 551 hPa-gauge (8 psig) with a supply pressure of 689 hPa-gauge (10 psig). Noncompliance with these specifications, particularly those concerning purge air, could cause over-pressure damage to the module. The nominal internal case pressure is about 0.5 to 1.0 inch of water, and the pressure relief valve is set at 1/3 psig (nominal).
At the very least, the module's safety system, which requires a certain volume of purge air flowing through the case before allowing burner ignition, will not allow the instrument to operate.
All internal pressure settings are preset at the factory, but the operator should check for accuracy. Sample should be filtered for particulates down to two microns.
2.4.4 LEAK TEST
The Analyzer Module is completely tested at the factory for gas leakage. The user is responsible for testing for leakage at the inlet and outlet fittings on the rear panel. The user is also responsible for internal leak testing periodically and if any internal pneumatic components are adjusted or replaced (with a test procedure chosen by the user).
2.5 ELECTRICAL CONNECTIONS
Two electrical connections are required on the Analyzer Module: POWER and NETWORK. See Figure 2-4. On the Analyzer Module, two NETWORK connectors are available, either of which is appropriate for: 1) interconnection with the Backplane of the Platform or 2) "daisy-chaining" with other NGA 2000 components. Connect Analyzer Module POWER to Backplane POWER or external 24 VDC power source.
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
2-7
NSTALLATION
[
]
[
]
[
]
[
]
[
]
[
]
I
8.2
[208.2]
FID
4.3
[109.7]
.25
[6.3]
Dimensions:
1.9
[49.4]
1.1
27.9
.9
[22.5]
[152.4]
17.75
[450.9]
20.0
[510.0]
6.0
5.7
143.6
4.3
109.1
2.9
73.6
1.4
35.6 .8
[20.9]
1.8
[46.3]
1.7
43.4
3.1
[78.0]
INCHES
[MM]
F
IGURE
2-5. O
UTLINE AND MOUNTING DIMENSIONS
2-8
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
C
A
CABLE ASSEMBLY, FLAT 24COND
CARTRIDGE HEATER
P6 J6
J1
P1
POWER SUPPLY BOARD
J4
P4
J5
P5
CABLE ASSEMBLY, FLAT 3 COND
P9
J9
OVEN HEATER
FUEL SOL.
++ +
J10
P10
YEL
GRN
BRN
RED
ORN
NSTALLATION
I
OVEN
HEAT
JP1
J3
FLAME ON
PURGE AIR
P2
J2
POWER MODULE
ASSEMBLY
J4
LED INDICATOR
ASSEMBLY
PWR MOD
J1 J1
SWITCH ASSEMBLY, MANUAL IGNITE
J6
J5 +10V REF
CABLE ASSEMBLY,
LON/POWER
MODULE
J5 P5
P3
J2
P2
J3
J8
P8
J11
AIR
BLU
P15
P11
J7
P7
BLK
BLK
RED
RED
J15
AIR
SENSOR,
3-WAY SOLENOID
CASE TEMP
E2 24VOLTE1E3
BLK
RED
J14
P14
RTN
GRN
FLAT 10 COND
HARNESS, CHASSIS
HEATER
FAN
ASSEMBLY
THERMOSTAT
POWER
J6
J1 J2
P1
RTN
P3
ABLE SSEMBLY,
FLAT 3
COND
CABLE ASSEMBLY, FLAT 16 COND
HARNESS, GLOW PLUG
P4
J4
SAFETY BOARD
J3 P3
CABLE ASSEMBLY, FLAT 20COND
P6
J6
COMPUTER
ANALYSIS
J5
P5
P4
BOARD
J4
J2P2J3
J1 P1
SENSOR
AIR
J11
P11
PRESS
2-WAY
SOLENOID
J16
P16
FUEL IN
ASSY,
PRESS
SWITCH
PRESSURE
SWITCH
CABLE
P2
J2
1 2 3 4 5 6 7 8
FLO
SW
J1
P1
POWER RESISTOR
MTG STUD
P7
J7
P3
GND STRAP
FLOW
SENSOR
CASE
FLO
SW
FLO
SW
FLO SEN
HARNESS
POL VOL
GRY
EI
PUR
E2
PREAMP
J1
SHIELD
BOARD
CHASSIS GND
CABLE ASSEMBLY, CATHODE
P1
SHIELD
E3
R37
R38
J13
P13
SENSOR, FLAME-OUT
SENSOR
FUEL
J10
P10
PRESS
SENSOR SAMPLE
J12
P12
PRESS
BURNERGND
CABLE ASSEMBLY, ANODE
GLOW PLUG ASSEMBLY
J1
P1
CATHODE
BURNER ASSEMBLY
ANODE
F
IGURE
2-6. FID W
IRING DIAGRAM
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
2-9
NSTALLATION
I
N
OTES
2-10
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
S
TARTUP AND OPERATION
3
3.1 OVERVIEW
Prior to initial startup, the user should leak test the module as outlined in Section 2. For the remainder of this section, Analyzer Module interconnection with a Platform or
some interfacing component will be assumed. Display and Keypad information shall refer to that which the user can expect to see and do with regard to the Front Panel of the Platform.
(For a complete description of Platform Front Panel controls and indicators, see Section 1 of the Platform instruction manual.)
3.2 DISPLAYS
Three kinds of Display screens are available to the user:
Run Mode
Menu
Help
3.3 RUN MODE DISPLAY
The Run Mode is the normal mode of operation. In this mode, the display (see Figure 3-1) will show current gas measurement, the component of interest, user-selectable (up to four) secondary variables, the current operations of the softkeys, and a graphic bar representing the displayed concentration as a percent of fullscale.
If more than one Analyzer Module is connected to the system, another Run Mode display will show up to four gas measurements at once. Ala rm messages m ay also appear on the display (See Table 3-1).
3.4 MENU DISPLAYS
The Menu structure enables the user to access data and functions, and put information onto the network.
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
3-1
TARTUP AND OPERATION
S
The Main Menu (see Figure 3-2) is subdivided into three levels of control based generally on which personnel is likely to use it: Basic Controls, Expert Controls, and Technical Controls. (See Figures 3-3 through 3-5.) Many layers of the menu structure are described at appropriate places throughout this manual.
From the Run Mode display, press the MENUS softkey to gain access to the Main Menu. (See Figure 3-2.)
See Figures 3-11 through 3-15 for flow charts depicting menu screens related to this Analyzer Module.
3.5 HELP DISPLAYS
The Help structure is intended to be an on-line "tutorial," context-sensitive and topic-interconnected, so that the user can practically operate NGA 2000 without need of an instruction manual. (See Figure 3-6.)
F
IGURE
3-1. R
23.2 ppm HC
Display Parms. Menu Dual Info
F1
UN MODE DISPLAY
23.2 ppm HC Analyzer XXXXXXXX
Basic Controls
Expert controls and setup ...
Technical level configuration ...
Analyzer PQ 322-14
F2 F3 F4 F5
Main Menu
Delete alarm message!
Display Parms. Info
F1
F
IGURE
3-2. M
AIN MENU DISPLAY
3-2
F2 F3 F4 F5
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
g
p
p
23.2 ppm HC Analyzer XXXXXXXX Basic Controls
Measurement range numbers:
Range upper limit: 10 ppm Range and functional control: Local Bypass sample flow: 1000 ml/min Ranges with valid calibration 1&2 Calibration status: Ready If it won’t calibrate… Flame condition: On Light flame…
Home Escape Zero Span Info
TARTUP AND OPERATION
S
F
IGURE
F
IGURE
3-3. B
3-4. E
F1
F2 F3 F4 F5
ASIC CONTROLS MENU DISPLAY
23.2 ppm HC Analyzer XXXXXXXX Ex
ert controls and set u
Expert analyzer controls ...
Auxiliary module controls ... System set up ... Analyzer module set up ... Auxiliary module set up ... Local I/O set up ...
Home Escape Info
F1 F2 F3 F4 F5
XPERT CONTROLS AND SETUP MENU DISPLAY
23.2 ppm HC Analyzer XXXXXXXX
Home Escape Cal Info
F1 F2 F3 F4 F5
F
IGURE
748331-E Rosemount Analytical November 1998
3-5. T
ECHNICAL CONFIGURATION MENU DISPLAY
Technical confi
System set up .. .
Service menus... Diagnostic menus... Other module diagnostic menus... listing of all modules...
uration menu
NGA 2000 Flame Ionization Detection Module
3-3
TARTUP AND OPERATION
p
S
23.2 ppm HC Analyzer XXXXXXXX Main Menu Hel
The Main Menu for the analyzer system. Note that this menu refers to the particular analyzer selected from t he run screen, when used in a system. The softkey marked “HOME” will always return you to this screen. Help menu system... Help on help... Keyboard controls... Editing controls.. .
Home Escape Map
F1 F2 F3 F4 F5
F
IGURE
3-6. T
YPICAL HELP SCREEN
DISPLAY MESSAGE DESCRIPTION TYPE
AIR FET FID Air FET current WARNING AIR PRESS FID Air Pressure WARNING BAIR FLOW Burner Air Flow WARNING BAROMETER System Barometer WARNING BFUEL FLOW Burner Fuel Flow WARNING BLOCK FET Heater current WARNING CASE TEMP Case Temperature WARNING CRUDE NOISE Ca lculated Noise WARNING CURRENTRNGHI Current, High Range WARNING CURRENTRNGLO Current, Low Range WARNING CURRENTSFAC Current Range WARNING FLAME TEMP Flame Temperature WARNING FUEL PRES Fuel Pressure WARNING LIN ERROR Linearizer Error WARNING N15 VOLTS Power Supply -15V WARNING P10 VOLTS Power Supply +10V REF WARNING P15 VOLTS Power Supply +15V WARNING POL VOLTS Polarizing Volts WARNING SAMP PRES Sample Pressure WARNING CALRESULT Calibration Error FA ILURE PURGE AIR FID Purge Air FAILURE SW ERROR Software Error FAILURE
T
ABLE
3-1. FID A
NALYZER MODULE ALARMS
3-4
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
RESPONSE
A
)
A
)
A
)
(100 ppm CH
fullscale )
4
1.0
0.8
0.6
0.4
0.2
TARTUP AND OPERATION
S
SAMPLE: 100 ppm CH4 in N FUEL: 25 psig (1726 hPa) H AIR: 25 psig (1726 hPa)
2
2
F
IGURE
3-7. T
RESPONSE
(100 ppm CH
0
0
2
13.76
3
20.64
27.52
SAMPLE PRESSURE
YPICAL CURVES OF MODULE RESPONSE VS
S
AMPLE PRESSURE REGULATOR
1.0
0.8
0.6
fullscale )
4
0.4
0.2
4
5
34.4
6
41.28
psig
hPa
. P
RESSURE SETTING ON
IR: 30 psig (2064 hPa
IR: 20 psig (1376 hPa
IR: 10 psig (688 hPa
SAMPLE: 100 ppm CH4 in N
at 5 psig (344 hPa)
7
48.16
2
F
IGURE
748331-E Rosemount Analytical November 1998
3-8. T
F
YPICAL CURVES OF MODULE RESPONSE VS
UEL PRESSURE REGULATOR
0
0
5
344
10
688
15
1032
20
1376
25
1726
30
2064
psig
FUEL PRESSURE
NGA 2000 Flame Ionization Detection Module
hPa
. P
RESSURE SETTING ON
3-5
TARTUP AND OPERATION
psig (
S
1.0
F
IGURE
RESPONSE
(100 ppm CH
3-9. T
A
FUEL: 30
0.8 FUEL: 25 psig (1726 hPa) H
FUEL: 20 psig (1376 hPa) H
SAMPLE: 10 0 ppm CH
10
AIR PRESSURE
15
1032
4
fullscale)
0.6
0.4
0.2
0
0
5
344
688
YPICAL CURVES OF MODULE RESPONSE VS
IR PRESSURE REGULATOR
2064 hPa) H
at 5 psig (344 hPa)
20
1376
psig
hPa
. P
RESSURE SETTING ON
2
2
2
4
25
1726
in N
2
3.6 STARTUP PROCEDURE
Apply power to the FID Analyzer Module. If it is associated with a Platform, do this by plugging in the Platform to a power source. The Platform has no ON/OFF power button. Once power has been supplied to the Platform, the FID Analyzer Module will be energized.
30
2064
If the user's system contains only one Analyzer Module, all system components, the Controller Board and the network "self-install" (bind together) during initial startup. If the system contains more than one Analyzer Module, the startup sequence will interrogate the network to locate and identify all components on the network. The user will have to bind appropriate combinations of components after the startup sequence (see section 3.7).
After the warm-up period (about one hour for the FID Analyzer module), all modules are completely functional.
Before introducing gases to the FID, the user should check the general health of the analyzer module's electronics by reviewing the results of its self test sequence. These test results can be found by selecting the following from the Main Menu: Technical Level Configuration, Diagnostic Menus, Analyzer Module Diagnostics, Self Test. All tested parameters should indicate "Pass."
3-6
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
TARTUP AND OPERATION
S
Descriptions of the tests performed follow:
EEPROM test - Checks the EEPROM on the Analysis Computer PCB.
EPROM test - Checks the EPROM on the Analysis Computer PCB.
RAM test - Checks the RAM on the Analysis Computer PCB.
Power supply test - Verifies that all internal DC voltages are within the
required tolerances.
Network test - Checks the internal network interface.
20 bit ADC test - Checks the 20-bit ADC on the Analysis Computer PCB by
sending a DC signal through the Preamp PCB and reading the signal back with the 20-bit ADC.
12 bit ADC test - Checks the 12-bit ADC on the Analysis Computer PCB by sending a DC signal and reading the signal back with the 12-bit ADC.
Power Supply PCB test - Checks the presence of the Power Supply PCB by activating the 3-way air solenoid.
Safety PCB test - Checks the presence of the Safety PCB by sending a command and reading it back.
Case temperature test - Compares the temperature read between the Preamp temperature sensor and the case temperature sensor. They must be within 10°C of each other. This test sometimes fails if the case is opened. The sensor in the Preamp will take longer to cool off since it is in an enclosure. Re-running the self-test after thermal equilibrium will produce a positive result if the sensors are working properly.
The self-test can be repeated at any time by activating the TEST softkey in the Self Test Results menu.
Set the Range Number (Expert Controls sub-menu) to the desired setting (see Figure 3-12). Introduce all gases at suitable pressures (see Specifications page in the Preface section of this manual).
Check/set internal pressure regulators according to the following specifications:
INTERNAL PRESSURE
REGULATOR
TYPICAL OPERATING PRESSURES
B
URNER AIR
F
UEL
S
AMPLE
S
AMPLE (MIXED FUEL
748331-E Rosemount Analytical November 1998
(100% H2)
965 to 1103 hPa-gauge (14 to 16 psig) 1516 to 1723 hPa-gauge (22 to 25 psig) 276 to 345 hPa-gauge (4 to 5 psig)
)
207 to 345 hPa-gauge (3 to 5 psig)
NGA 2000 Flame Ionization Detection Module
3-7
TARTUP AND OPERATION
S
Purge air of the following specifications must be present:
Flow: 16 to 18 L/min. Supply Pressure: 689 to 1378 hPa-gauge (10 to 20 psig).
Noncompliance could cause damage to the module. At the very least, the module's safety system, which requires a certain volume of purge air flowing through the case before allowing burner ignition, will not allow the instrument to operate. The lowest purge air flow/pressure setting possible during burner operation is preferable. Thus, the user should set the external purge air pressure initially at 689 hPa-gauge (10 psig). Check the Miscellaneous Control Parameters screen under Technical Diagnostics, and note whether the Purge Gas (switch) variable is "ON." If it is "OFF," increase purge air supply by 69 hPa-gauge (1 psig), and recheck the Purge Gas variable until it reads "ON." DO NOT EXCEED 1378 hPa-GAUGE (20 PSIG). If the maximum setting is reached, and the Purge Gas variable does not read "ON," contact factory. If the safety system is initiated successfully (Purge Gas variable is "ON"), continue with the remainder of the startup procedure.
Note Do not restrict the PURGE OUT port and the pressure relief valve. They must be
vented to atmospheric pressure.
Two methods of burner ignition are possible: auto-ignition and manual ignition. Note the four LEDs on the front panel of the Analyzer Module. They provide necessary information for either ignition procedure. The LEDs, when illuminated, denote the following information:
Green - unit powered on Amber - constant illumination indicates case temp. is within 5% of operating
temp. setpoint (i.e., 50°C with burner off, 54°C with burner
on);otherwise, LED will blink Green - Flame on Green - purge air system intact (it has filled five volumes of the module
interior)
Auto-ignition provides fuel override and three attempted ignitions (default setting), if necessary. Manual ignition requires that the Platform front panel, if used, be disengaged.
CAUTION: HAND INJURY HAZARD
Do not place hands or fingers in Platform front handles when the front panel is open. Dropping front panel while hand or fingers are inside either handle can cause serious injury.
3-8
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
TARTUP AND OPERATION
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The manual ignition switch on the Analyzer Module front panel must be manipulated in the following ways:
Press up and hold for one minute. This opens burner fuel and air solenoids.
Press down to ignite burner glow plug for up to 10 seconds.
Repeat as necessary (if fuel and air sources are farther away than 10 feet,
several more attempts may be necessary).
Flame on is defined true when the flame temperature exceeds 115°C (239°F).
If the flame has been lit, but the flame temperature increases slowly, perform
the following steps:
# After igniting flame, release switch for 2 sec. # Press switch down for 2 sec. # Repeat release switch and press down steps as necessary.
3.7 BINDING
To achieve full coordination between Analyzer Modules and associated I/O Modules, the user must bind those components together in the System Set Up portion of the Technical Configuration Menu in software. (See Figures 3-11 through 3-15 and section 1.5 of the I/O Modules manual for binding instructions.)
3.8 CALIBRATION
See section 2.3.3 for a description of the method for choosing calibration zero and span gases.
To calibrate the Analyzer Module, introduce zero gas into the SAMPLE INLET, and do the following:
1. If more than one Analyzer Module is functional and the split Run Mode display is shown, press the DISPLAY softkey until the desired Analyzer's Run Mode display is acquired.
2. Press the MENUS softkey to enter the Main Menu.
3. Verify the fuel type in the Miscellaneous Control Parameters menu (under the Technical Configuration menu structure, select the following from the Main Menu: Diagnostic menus, Analyzer Module Diagnostics and then Miscellaneous Control Parameters).
4. Verify the capillary type in the Analyzer Manufacturing Data menu (under the Technical Configuration menu structure, select the following from the Main Menu: Technical Level Configuration, Service Menus, Manufacturing Data, Analyzer Module Data).
5. In the Calibration Gas List menu (from the Main Menu, select Expert Controls and
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
3-9
TARTUP AND OPERATION
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Setup, Analyzer Module Setup, then Calibration Gas List), enter necessary data, including the Operational Sample Pressure and the Calibration Gas HC Response Factor. Common HC factors are: methane (CH4), 1.0, ethane (C2H6), 1.90, propane (C3H8), 3.00. These factors are not used to compensate the reading, but are used to select the proper preamp sense resistor.
6. Press HOME to re-enter the Main Menu, enter the Basic Controls menu, introduce zero gas and allow its response to stabilize, press the ZERO softkey to enter the Analyzer Zero menu, press ZERO ag ain and w ait.
7. Press the SPAN softkey to enter the Analyzer Span menu, introduce span gas and allow its response to stabilize, press SPAN again and wait.
8. Press the HOME softkey to re-enter the Main Menu.
9. Press DISPLAY softkey for the Run Mode display.
If the user is unable to calibrate the Analyzer Module (i.e., when ZERO or SPAN is initiated, nothing happens), several possible solutions present themselves. One solution relates to the use of an incorrect gas for zeroing or spanning (e.g., using a high concentration gas to zero or a zero gas to span the Analyzer Module). Simply recalibrating with the appropriate gas(es) will not correct the problem because the ZERO OFFSET or SPAN FACTOR has been set to an extreme value in the process.
To remedy the problem, do the following:
1. Verify that correct zero and span calibration gases are being used properly. If so, attempt to recalibrate according to instructions at the beginning of this section, ensuring that case temperature and displayed measurement reading are stable before initiating the calibration routine. If incorrect gases were used in the initial, failed calibration, skip to Step 2.
2. Make the following selections from the Main Menu: Expert Controls and Setup, Analyzer Module Setup, then Calibration Parameters. Disable Calibration Adjustment Limits.
3. Recalibrate the analyzer module according to instructions at the beginning of this section, ensuring that case temperature and displayed measurement reading are stable before initiating the calibration routine.
4. Enable Calibration Adjustment Limits in the Calibration Parameters menu.
3.9 ROUTINE OPERATION
After binding and calibration, proceed as follows: Supply sample gas to SAMPLE INLET. Adjust external flow controller or throttle valve
so that flow discharged from the BYPASS outlet is between 0.5 and 2.0 L/min. The reading on the SAMPLE BYPASS pressure gauge should be the same as that used during adjustment of the span control. Adjust, if necessary.
Adjust the Range Number setting. The Analyzer Module will now automatically and continuously output the measured hydrocarbon content of the sample. Output is in
3-10
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
TARTUP AND OPERATION
S
terms of the particular hydrocarbon present in the span gas. Note that readings obtained during operation depend on the concentration of total hydrocarbons in the sample.
If maximum sensitivity is required from the FID Analyzer Module, use an optimum combination of settings on the SAMPLE, FUEL, and AIR pressure regulators. Settings must be determined experimentally, but the curves in Figures 3-7, 3-8 and 3-9 may be used as guides.
The Analyzer Module will not allow the user to increase the upper limit of a range beyond the "maximum range" software setting. To change the "maximum range" value, select the following from the Main Menu: Technical Configuration Menu, Service Menus, Manufacturing Data, and Analyzer Module Data. Select Maximum Range, and use the arrow keys to scroll the indicated value. The same applies for Minimum Range settings.
During shutdown, always turn off fuel gas first, then the air and sample gases. The flame can also be turned off by setting Ignition System Enable to "Off" in the Light Flame menu (under Basic Controls; see Figure 3-11). Subsequently, remember to set Ignition System Enable to "On" before attempting to ignite the flame.
After initial startup, or startup following a prolonged shutdown, the Analyzer Module requires about one day's continuous operation to stabilize. For several days afterwards, calibrate daily. The frequency of subsequent calibrations can be reduced as experience dictates, consistent with the accuracy requirements of the particular application.
3.10 SAFETY SYSTEM
The FID Analyzer Module safety system will not allow ignition or continuous burner function unless the following conditions are present:
Internal purge gas pressure is at least 380 hPa-gauge (5.5 psig). (Monitor display message, Purge Gas Pressure in Physical Measurements menu, for the proper setting.)
Internal fuel pressure is less than 2064 hPa-gauge (30 psig). (Monitor display messages, Fuel Supply Pressure in Physical Measurements menu and Fuel Pressure Status "ON" in Miscellaneous Control Parameters menu for proper settings. If the internal fuel pressure has exceeded 2064 hPa-gauge [30 psig], check that the external pressure is less than 3450 hPa-gauge [50 psig]. The +24 VDC power to the Analyzer Module must be cycled to continue operation.)
Flow rate for purge air in is at least 16 L/min. and case pressure is greater than
0.5 inch of water. (Monitor display message, Purge Gas "ON" in Miscellaneous Control Parameters menu for correct state. Proper sealing hardware must be used in order to obtain the required purge air in flow rate and case pressure.)
Five case volumes of purge air have been achieved and the three above conditions are present. The time duration to achieve a safe system is a
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
3-11
TARTUP AND OPERATION
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minimum of 6 min. The elapsed time can be monitored in the Technical Startup Analyzer menu. (Monitor the Purge Air Green LED "ON," Purge Control Status "ON," or Purge Air Alarm for indication of the state of the safety system.)
As stated above, proper sealing hardware is crucial to the successful operation of the safety system. Therefore, a specific torquing sequence (as shown in Figure 3-10) must be followed when the front panel of the module is being reinstalled after removal. All front and rear panel screws must be installed.
Note Do not over-torque rear panel screws.
Torque Sequence:
Screw #1, 4 to 5 turns Screw #2, 4 to 5 turns Screw #3, 4 to 5 turns Screw #4, 4 to 5 turns Screw #5, 4 to 5 turns Screw #6, 4 to 5 turns
614
Repeat torque sequence until all screws are tight.
F
IGURE
3
5
3-10. F
2
The gasket must fill in between the front panel plate and the enclosure.
RONT PANEL TORQUING SEQUENCE
3-12
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
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Measurement range number: 1 Range upper limit: 10 ppm Range and functional control: LOCAL Bypass s ample flow : 10 00 ml/min. Ranges with valid calibration: 1&2 Calibration status: Ready If it won’t calibrate... Flame condition: On Light flame…
Basic controls
Basic controls... Expert controls and setup... (Operational configuration) Technica l level co n figu ra tion ... (Diagnostic and manufacturing/service)
Main Menu
Basic level security
(expert,technical) Enter your security code with softkeys. Security codes are set in the system setup menu in the Technical level menus. Press five characters when Security code says READY. Press six to return to “READY”.
Security code: 54321
Expert controls and setup
Expert analyzer controls... Auxiliary module controls... System set up... Analyzer module set up... Auxiliary module set up... Local I/O set up...
Expert and Technical menus follow in succeeding flow charts.
PARMS
Technical configuration menu
System set up... Service m enus... Diagnostic menus... Other module diagnostic menus... Listing of all modules...
Current measurement parameters
Flame Condition: ON Measurement range number: 1 Range change control: Local Linearization mode: N/A Analyzer opera tiona l sta te: N ormal Analyzer alarm sta te: No rmal Alarms level reporting: Failure
MORE
Current measurement parameters
Response time: 2.0 Secs Bypass s ample flow : 10 00 ml/min. Sample press ure : 12.3 hP a Preamp Temperature : 55 .3°C Purge control s tatu s : On
ZERO
Analyzer Zero
Are you sure? You must have zero gas flowing through the analyzer. This control does NOT contr ol any auto-cal. Module bound to this analyzer! If you are sure, press ZERO again now. Press left arrow key when you are done.
Calibration status: Ready Error message for last zero: 24-08-94
F
IGURE
3-11. D
SPAN
Analyzer Span
Are you sure? You must have zero gas flowing through the analyzer. This control does NOT contr ol any auto-cal. Module bound to this analyzer! If you are sure, press SPAN again now. Press left arrow key when you are done.
Calibration status: Ready
Error message for last zero: 24-08-94
ISPLAY SCREENS
(1
Check that you are flowi ng the correct gas, and the gas concentrat ion
If it won’t calibrate...
is what it is supposed to be. Make sure that the reading is stable before starting. If you have enabled or disabl ed the lineariz er, you may hav e made it hard for the analyzer t o calibrate. If so, go to the calibrati on parameters screen under Expert c ontrols and setup, under Analyzer set up, and disable the limits checking. Recalibrated, then disable the limits check ing again. If all else fails, manually adj ust the calibrat ion factors until the readings are close to correct and t r y again.
5)
OF
Light Flame
Flame condition: On Auto-ignition: Disa bled Ignition system enable: On Number of ignition attempts s o far: 0 Time of this cycle - secs: 0 Fuel supply pre s su re: 1 3.8 hPa Burner air pres s ur e: 25 .2 h Pa Sample press ure : 12.3 hP a Flame temperature: 23 2 C Status: On
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
3-13
TARTUP AND OPERATION
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From MAIN MENU
Expert controls and setup Expert analyzer controls... Auxiliary module controls... System set up... Analyzer Module set up... Auxiliary Module set up... Local I/O set up...
Analyzer module set up... and Auxiliary module set up... outlined in the next flow chart. Local I/O set up information is included in the I/O Modules manual.
Measurement range number: 1
Expert controls
Range upper limit: 10 ppm Range settings... Linearizer: N/A
Range and functional control: LOCAL Zero/Span calibration… Ranges with valid calibration: 1&2 Physical Measurements… Flame condition: On Light Flame…
CAL
Range Settings
Minimum range: 10 ppm Maximum range: 5000 ppm Range 1 lower limit: 0 ppm Range 1 upper limit: 10 ppm Range 2 lower limit: 0 ppm Range 2 upper limit: 100 ppm Range 3 lower limit: 0 ppm Range 3 upper limit: 250 ppm Range 4 lower limit: 0 ppm Range 4 upper limit: 1000 ppm
Auxiliary module controls
This screen selects any module with a control screen. This includes any auto calibration or sample module bound to this analyzer. Module Tag Module Tag
Dependent on which auxiliary module is present on the network. See I/O Modules manual.
#1
Zero/Span Calibration
Measurement range number: 1 Zero gas concentration: 0 ppm Span gas concentration: 9.89 ppm Sample flow: 1000 ml/min. Flame condition: ON Raw measurement signal: 520000 Status: Ready Result... Calibration adjustment limits: Enabled
Front panel control... Display resolution... Auxiliary lines...
See Platform manual for a flow chart of these displays.
Physical Measurements
Bypass sample flow: 1000 ml/min. Flow lower limit: 150 cc/min. Flow upper limit: 250 cc/min. Sample pressure: 345 hPa Fuel pressure: 1690 hPa Burner air pressure: 1043 hPa Purge gas pressure: 604 hPa Case temperature: 54.0 C
System Set Up
CAL DATA
#2
Zero/Span diagnostic data
Date of last zero: 24-08-94
Error message for last zero: 24-08-94 Error percentage for last zero: 5% Raw signal at last zero: 500000 Last zero gas would read: -0.83 ppm Date of last span: 24-08-94 Error message for last span: Cal OK Error percentage for last span: 5% Raw signal at last span: 500000 The last span gas would read: 113 ppm
CAL DATA
F
IGURE
See #2 on this flow chart.
3-12. D
See #3 on this flow chart.
Are you sure? You must have zero gas flowing through the analyzer. This control does NOT control any auto­cal module bound to this analyzer! If you are sure, press ZERO again now. Press left arrow key when you are done. Calibration status: Ready Error message for last zero: 24-08-94
ISPLAY SCREENS
3-14
ZEROFACTORS SPAN
Analyzer Zero
Range 1 (2,3,4) Factors
Manufacturer’s settings
Zero offset: 0 Span factor: 0.0014
Zero offset 500000 Span factor: 0.0015
(2
Stored settings
5)
OF
Are you sure? You must have span gas flowing through the analyzer. This control does NOT control any auto­cal module bound to this analyzer! If you are sure, press SPAN again now. Press left arrow key when you are done. Calibration status: Ready Error message for last zero: 24-08-94
Analyzer Span
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
HISTORY
FACTORS
#3
Calibration Factors
Only those factors appropriate for the current range will affect the reading on the current range. Make sure you are using the correct ones! Measurement range number: 1 Range 1 factors... Range 2 factors... Range 3 factors... Range 4 factors...
Range 1 (2,3,4) Factors
Zero offset: 0
Span factor: 0.0014
Fullscale range at calibration: 10 ppm
Measurement range number: 1
Raw measurement signal: 679532
TARTUP AND OPERATION
S
From MAIN MENU
Expert controls and setup
Expert analyzer controls... Auxiliary module controls... System set up... Analyzer Module set up... Auxiliary Module set up... Local I/O set up...
For Expert analyzer controls, Auxiliary module controls, and System set up menus, see preceding flow chart.
Analyzer module set up
Calibration gas list... Calibration parameters... Gas measurement parameters... Analyzer paramete r list... Physical measurement parameters... Displayed parameters... Analyzer tag: FID
Auxiliary module set up
Select an au xiliar y module for set up Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag
Dependent on which auxiliary module is bound to the analyzer. See I/O Modules manual.
Calibration gas list
Zero gas - range 1: 0 ppm Span gas - r ang e 1 : 9.3 ppm Zero gas - range 2: 0 ppm Span gas - r ang e 2 : 19 .3 pp m Zero gas - range 3: 0 ppm Span gas - r ang e 3 : 10 1.1 p pm Zero gas - range 4: 0 ppm Span gas - r ang e 4 : 24 7.1 p pm Calibration gas HC response factor: 1 Operational sample pressure: 345 hPa Calibratio n …
Calibration Parameters
Calibration adjustment limits: Enabled Calibration averaging time: 5 Se cs Calibration failure alarm: Ye s Cal failure error allow ed : 5% Calibration time out: 60 Sec s Zero ranges : All Span ranges: SEPARATELY
Gas measurement parameters
Linearization parameters... Response time/delay parameters... Range setting... Units... Linearization functions...
See #1 in previous flow chart.
Calibration
Linearization parameters
Range 1 linear izer: En ab led if enabled, uses cu rve no.: 1 Range 2 linear izer: En ab led if enabled, uses cu rve no.: 2 Range 3 linear izer: En ab led if enabled, uses cu rve no.: 3 Range 4 linear izer: En ab led if enabled, uses cu rve no.: 4 Set coefficients…
Response time/delay parameters
Range 1 t90 time: 1 0 Se cs Range 2 t90 time: 1 Sec s Range 3 t90 time: 1 Sec s Range 4 t90 time: 1 Sec s LON update ra te: 10 x/Sec Output delay time: 0 Sec s
Range Settings
Minimum range: 10 ppm Maximum r ange: 5000 ppm Range 1 lower limit: 0 ppm Range 1 upper limit: 10 ppm Range 2 lower limit: 0 ppm Range 2 upper limit: 100 ppm Range 3 lower limit: 0 ppm Range 3 upper limit: 250 ppm Range 4 lower limit: 0 ppm Range 4 upper limit: 1000 ppm
Gas measure ment un its: p pm Pressure meas ure ment u nits : ps ig Temperature meas ure ment u nits : F Variables a re s till s e nt as t he ba s ic S I u nit.
Polynomial set up... Midpoint correction set up...
Units
Linearization functions
Linearity coefficients
Curve 1 (2,3,4) AO coefficient: 1.34523E -4 A1 coefficient: 0.98375 1 A2 coefficient: 0.11575 1 A3 coefficient: 1.11575 E-6 A4 coefficient: 7.3421E -12 Curve upper lim i t : 10 ppm Curve over-range: 10% Curve under-range: 5% Status: Enabled
Polynomial set up
Range to be linearized: 1 Current spa n g as : 9.8 9 p pm Calculated polyn omial ord er : 4 Gas values sho w n a s: P erce nt Gas concentrations... Analyzer function: Re ad y
Gas concentrations
Gas value: 0 Raw reading: 0 ppm Linearized values: 0 pp m
Gas value: 10 Raw reading: 11 ppm Linearized values: 1 0 p pm Point to be measu red : Po int 1 Analyzer function: Re ad y
Correction: Dis able d Point being meas ure d: Pt 1 Point 1 gas concentration: 100 ppm Point 2 gas concentration: 150 ppm Point 3 gas concentration: 150 ppm Point 1 reading: 1 00 pp m Point 2 reading: 1 20 pp m Point 3 reading: 1 50 pp m Span gas value: 1 00 ppm Analyzer function: Re ad y
Point 1
Point 2
Midpoint correcti on set u p
Range 1 (2,3 ,4)
See I/O Modules manual for Local I/O set up information.
F
IGURE
3-13. D
Analyzer Parameter List
Analyzer tag: FID Flame condition: On First line’s par ameter : Flow Second line’s pa ramete r: Flow Third line’s par ameter : Flow Fourth line’s p ara meter: Flow Linearization parameters...
Linearity coefficients
A0 coefficient: 1.34523E-4 A1 coefficient: 0.983751 A2 coefficient: 0.115751 A3 coefficient: 1.11575E-6 A4 coefficient: 7.3421E-12 Curve upper limit: 10 ppm
#4
Physical Measuremen t
Parameters
Sample cap illar y p re s s u re : 12 3 . hP a Sample cap illar y p re s s u re w as : 0 h Pa Fuel supply pressure: 13.8 hPa Fuel supply pressure was: 0 hPa Purge gas p res s ur e: 34 .1 h Pa Purge gas p res s ur e w as : 0 hPa Burner air pres s ur e: 25 .2 h Pa Burner air pres s ur e w as : 0 hPa Press ur e limits .. . Temperature limits...
Displayed Parameters
First line’s par ameter : Flow Second line’s pa ramete r: Flow Third line’s par ameter : Flow Fourth line’s p ara meter: Flow May be displayed on the appropriat e line of the single analyzer display screen.
ISPLAY SCREENS
NEXT
Pressure Limits
Sample cap illar y upper limit: 345 hPa Sample cap illar y lo w e r limit: 100 hPa Fuel pressure upper limit: 2070 hPa Fuel pressure lower limit: 690 hPa Burner air upp er limit: 1380 hP a Burner air lower limit: 690 hPa Purge gas upper limit: 1035 hPa Purge gas lower limit: 380 hPa Barometric press u re: 1 013 hP a
Temperature Limits
Case uppe r limit: 61.0 C Case lowe r limit: 47.0 C Flame upper l i mi t: 225 C Flame lower limit: 115 C Block upper limit: 66.0 C Block lower limit: 50.0
MORE
(3
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Analyzer Parameter List
Primary Variable Parameters Control mode: LOCAL Output delay time: 0 Se cs Range 1 upper limit: 10 ppm Range 2 upper limit: 100 ppm Range 3 upper limit: 250 ppm Range 4 upper limit: 1000 ppm Range 1 low er limit: 0 pp m Range 2 low er limit: 0 pp m Range 3 low er limit: 0 pp m Range 4 low er limit: 0 pp m
Analyzer Parameter List
Calibration Parameters Calibration averaging time: 5 Se cs Calibration failure alarm: Ye s Cal failure error allow ed : 5% Calibration time out: 60 Sec s Ranges ze roe d: All Calibrate range s : Sep ara tely Calibration adjus tment limits: En ab led
Physical Measuremen t
Parameters
Bypass sample flow: 1000 ml/min. Bypass s ample flow w as : 0 ml/min. Case tempera ture : 54.3 °C Case tempera ture w as : 0°C Flame temperature: 23 2°C Flame temperature w as : 0 °C Preamp temperature : 55 .3°C Preamp temperature w as : 0 °C
Analyzer Parameter List
Primary Variable Parameters Range 1 t90 time: 10 Secs Range 2 t90 time: 1 Secs Range 3 t90 time: 1 Secs Range 4 t90 time: 1 Secs Linearizer on ra ng e 1 : Ena bled Linearizer on ra ng e 2 : Ena bled Linearizer on ra ng e 3 : Ena bled Linearizer on ra ng e 4 : Ena bled
Analyzer Parameter List
Calibration Gase s Zero gas - ra nge 1: 0 pp m Zero gas - ra nge 2: 0 pp m Zero gas - ra nge 3: 0 pp m Zero gas - ra nge 4: 0 pp m Span gas - range 1: 9.3 ppm Span gas - range 2: 19.3 ppm Span gas - range 3: 101.1 ppm Span gas - range 4: 247.1 ppm
Calculated physical parameters
Burner air flow: 12 .3 ml/min Burner air flow w as : 0 ml/min Burner fuel flow: 153 ml/min Burner fuel flow w as : 0 ml/min
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
3-15
TARTUP AND OPERATION
S
From MAIN MENU
Technical configuration menu
System set up... Service menus... Diagnostic menus... Other module diagnostic menus... Listing of all modules...
For diagnostic menus, Other module diagnostic m enus, and listing of all modules, see succeeding flow chart.
System set up Main display configuration... Front panel control... Date and time... Module binding... System reset... Security codes... System tag: Ros emou nt
Service menus
Manufacturing data... Service history... In maintenance since: N/A Record security codes...
Main display configuration, Front panel control, and Date and time displays can be found in Platform manual.
Module binding
Analyzer module s elec ted : FID Select modu le s ... Proposed bind: View bindings... Bind sele ct ion s ! Unbind everything!
System reset
Are you sure? Re-initializ ing w ill d es tr oy a ll bin ds ! System reset! Re-initialize networks!
#5
Record security codes
Basic level security: En able d Expert level security: Enabled Technical level security: En ab led Record basic level security codes... Record expert level security codes... Record technical level security codes...
Manufacturing data
Control module data... Analyzer module data... Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag
Service history
Control module data... Analyzer module data... Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag
Record security code
Technica l level s e cu rity
see #5 above
Select I/O modules
Select the modules you wish to bind to the current analyzer. Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag
Modules Boun d
Analyzer module s elec ted : FID Auxiliary modu le : Au to 10 2 3 Auxiliary modu le : Ac al 2 3 22 Auxiliary modu le : HA RT 10 9 2 Auxiliary modu le : no n e Auxiliary modu le : no n e Auxiliary modu le : no n e Proposed new bind:
Record basic level security
(expert, technical menu the same) Press five sof tkeys in any order to def ine the code. The actual code is represented by the order in which they are pressed, and shown numerically below. Press the left arrow key when you are done. Actcual code number: 54321
Control Unit Manufacturing Data
Control unit serial number: 800002356 Manufacturing date code: 12-08-93 Hardware revision n umbe r: 1.0 0 Software revision nu mber: 2 .2 Revision notes... User tag nu mber: PV 1c
Analyzer Manufacturing Data
Analyzer module s/n: 8900189342 Manufacturing date code: 17-08­93 Hardware revision n umbe r: 1.1 3 Software revision nu mber: 2 .2 Minimum range: 10 ppm Maximum range: 5000 ppm Measured g as : HC Capillary: 13 .5 ml/min @ 5 ps ig
IO Module Manufacturing Data
See I/O Modules manual.
Control Module Service History
Manufacturing date: 12-08-93 In service date: 01- 23- 94 Last service date : 01 -23 -94 List notes... Add service date!
Analyzer Module Ser vice History
Manufacturing da te: 1 7-0 8-9 3 In service date: 21- 06 -94 Last zero ca libration da te: 2 4-0 8-9 4 Last span calibr ation da te: 24 -08 -94 Last service date : 21 -06 -94 List notes... Add service date!
I/O Module Service History
See I/O Modules manual.
F
IGURE
3-14. D
ISPLAY SCREENS
3-16
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November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
TARTUP AND OPERATION
S
From MAIN MENU
Technical configuration menu
System set up... Service menus... Diagnostic menus... Other module diagnostic menus... Listing of all modules...
For System set up and Servic e menus, see preceding flow charts.
Diagnostic menus
Control module diagnostics... Analyzer Module diagnostics... Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag
Other module diagnostics
This screen reserved for other m odules if present. Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag
Listing of all modules
Lists all modules detect ed on the network. Jumps to the module's diagnostic screen. Module Tag Module Tag Module Tag Module Tag Module Tag Module Tag
For Control Unit Di agnost ics, see the Platform manual.
#6
Analyzer Diagnostics
Power s u p ply voltag e s ... Primary variable parameters... Physical measurements parameters... Temperature control parameters... Miscellaneous control parameters... Auto ignition parameters... Self test... Software diagnostics... Startup analyzer...
For I/O diagnostics, see the I/O Modules manual.
Analyzer Diagnostics
See #6 above.
Analyzer diagnostics
Power supply voltages +15V analog is: 14.88 V +15V analog was: 14.92 V
-15V analog is : -14 .85 V
-15V analog w a s: - 14 .92 V +10V preamp refere nce is: 9 .99 V +10V preamp refere nce w as : 9.9 9 V Polarizing voltage is: 89 V Polarizing voltage was: 87.5 V
Primary variables parameters
Raw measurement signal: 679532 Signal gain setting: Low Preamp gain se tting: H igh Pk-pk noise: 0 ppm Barometric press. Compensation: Enabled Calibration factors ...
Physical measurements parameters See #4 in previous flow chart.
Temperature control
Case setpoint: 54 C Case P gain: 6.000000 Case I gain: 0.0005000 Case bias: 0.4 C Case temperature: 54.3 C Controller duty cycle: 50 %
Miscellaneous control parameters
Case heate r cu rren t: 1.7 A Burner air valve current: 1.1 A Alarm messages valid for: FAILURE Ignition command sta tus : Off Flame status: On Purge gas s w itch : On Igniter status : Off Fuel type: H2-He
Auto ignition param eters
Auto fuel override dura tion: 6 0 S Auto ignite override du ratio n: 5 S Auto ignition number of cycles: 3 Auto ignition: Disa bled Fuel enrichment sta tus : On Flame status: On
Self test results
EEPROM test: Pas s EPROM test: Pas s RAM test: Pas s Power supply test: Pass Network tes t: Pa ss 20 bit ADC test: P as s 12 bit ADC test: P as s Power supply board test: Pass Safety board test: Pass Case tempera ture tes t: Pas s
Calibration factors
See #3 in previous flow chart.
MORE
Miscellaneous control parameters
Fuel solenoid status: On Purge control s tatu s : On Fuel pressu re s ta tus : On Operational sa mple pre s s ure : 345 hPa
F
IGURE
3-15. D
ISPLAY SCREENS
748331-E Rosemount Analytical November 1998
(5
OF
5)
Software diagnostics
Last messa ge : No e rro r And: No error And: No error And: No error And: No error And: No error And: No error And: No error Edit to reset: Re por t Software error code (1=no error): 1
Analyzer starting u p
Purge gas timer- se cs : 53 0 Purge gas p res s ur e: 60 0 h Pa Purge gas s w itch : On Purge control s tatu s : On Fuel pressu re: 1 3.8 hPa Fuel solenoid status: On Igniter status : Off Flame temperature: 170 C Flame condition: On Time of this cycle-secs: 0
Re-initializing the analyzer
Are you sure? INIT will erase ALL the configuration data, but not manufacturing data, including serial number, etc. If you are sure, press INIT again.
NGA 2000 Flame Ionization Detection Module
INIT
3-17
TARTUP AND OPERATION
S
N
OTES
3-18
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
M
AINTENANCE AND TROUBLESHOOTING
4
CAUTION: QUALIFIED PERSONNEL
This equipment should not be adjusted or repaired by anyone except properly qualified service personnel.
4.1 BURNER DISASSEMBLY AND CLEANING
Disassemble the burner only if contaminants must be removed. Combustion products or other contaminants which accumulate inside the burner may form electrical leakage paths between the collector and the burner contact, resulting in noisy readings.
If the instrument is to be operated at the highest sensitivity, traces of such contaminants can cause erroneous readings. For best performance, clean the burner per the following procedure:
ISASSEMBLY
D
1. Power OFF the module.
2. Shut fuel gas, air and sample gases OFF.
3. Slide Analyzer Module from the Platform (if applicable).
CAUTION: HAND INJURY HAZARD
Do not place hands or fingers in Platform front handles when the front panel is open. Dropping the panel while hand or fingers are inside either handle can cause serious injury.
4. On the combustion chamber, disconnect the polarizing voltage cable and amplifier input cable.
5. Disconnect the four connectors attached to the burner (one to glow plug, two to preamp board , and one to thermistor).
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
4-1
NGA 2000 F
LAME IONIZATION DETECTION MODULE
6. Disconnect the four gas supply tubes (two air, one fuel and one sample).
7. Disconnect the exhaust tube.
8. Remove the burner assembly by loosening the two securing nuts.
9. Unscrew the burner cap retainer ring, and remove burner cap.
10. Loosen clamp; lifting straight up, remove combustion chamber­chimney assembly from the manifold.
Note If the old burner tip assembly is to
be used again, do not touch it with bare hands or any materials likely to contaminate it with hydrocarbons, salt, etc. Additionally, all items used for cleaning (tweezers, swabs, etc.) must be absolutely free of contamination.
GLOW PLUG
O-RING 903227
SCREW 2-56 X 3/16 LOCK WASHER NO.2 FLAT WASHER NO. 2
CLAMP
JUMPER
FLAMEOUT SENSOR
BURNER CAP NUT
BURNER CAP
CHIMNEY
ADAPTER EXHAUST
O-RING 903227
COMBUSTION CHAMBER
BURNER TIP
O-RING 903256
11. Unscrew and remove burner tip assembly.
LEANING
C
1. Clean chimney assembly, com-
TEE FITTING
MOUNTING BRACKET
BURNER FUEL RESTRICTOR
CAPILLARY
bustion chamber, and burner tip assembly with acetone or methyl ethyl ketone.
IGURE
F
SCREW (2) M3X0.5 x 6mm
4-1. FID B
URNER ASSEMBLY
2. Follow cleaning with a distilled water wash.
EASSEMBLY
R
Using care not to touch any internal parts, reassemble the burner per the following procedure.
1. Holding with clean tissue, screw burner tip assembly finger-tight into manifold.
2. Push combustion chamber/chimney assembly down onto manifold, taking care not to hit burner tip. Tighten clamp on combustion chamber chimney assembly.
4-2
Rosemount Analytical
November 1998
748331-E
M
AINTENANCE AN D TROUBLESHOOTING
3. Replace burner cap (and flameout sensor assembly), with flameout sensor assembly in-line with burner exhaust.
4. Install burner onto module base.
5. Connect all leads and tubing. Replace module cover and install module into Platform.
Note Fittings using Teflon pipe seal tape: Replace Teflon pipe seal tape to maintain a tightly sealed burner assembly.
4.2 COMPONENT REPLACEMENT
Components which may require replacement include; sample capillary, fan, fuses, EPROM, printed circuit boards and front panel LED's.
Replacement of each of these components require sliding out the bottom chassis from the enclosure.
Three fuses that may be replaced are located on; 1) the Network/Power Assembly, 2) the Safety Board and 3) the Power Supply Board. If the thermal fuse on the Safety Board or the Power Supply Board require replacement, this indicates a overheating condition, which denotes a wider problem requiring troubleshooting.
EPROM's should only be replaced by qualified electronics personnel because special tools and knowledge are required.
For accessibility when replacing printed circuit boards, the printed circuit board mounting panel has been designed to swing down.
4.3 BURNER STARTUP TROUBLESHOOTING
If unable to startup burner, check the following:
1. All supply gas cylinder pressures are within specifications (see Specifications in Preface section).
2. Correct gases are being supplied to each back panel inlet.
3. Air, not zero gas (if nitrogen), is being supplied to burner.
4. Burner exhaust is being vented to atmospheric pressure, and is not tied to either purge air exhaust or another FID exhaust.
5. Burner exhaust continuously slopes downward until reaching atmospheric pressure vent.
6. Parameters "IS/WAS" match in the Physical Measurement Parameters screen (see Figure 3-13); use NEXT softkey to view all parameters.
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
4-3
M
AINTENANCE AN D TROUBLESHOOTING
7. As a last resort, check burner fittings for leaks (purge air pressure is higher than the pressure in any of the lines connected to the burner; thus, any leak would be
the fitting rather than
into
out
of it).
4-4
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
R
EPLACEMENT PARTS
5
WARNING: PARTS INTEGRITY
Tampering with or unauthorized substitution of components may adversely affect safety of this product. Use only factory-approved components for repair.
5.1 REPLACEMENT PARTS
5.1.1 E
5.1.2 E
5.1.3 O-R
LECTRONICS
NL655588 Computer Board NL655796 Preamp Board NL655596 Safety Board NL655764 Power Supply Board NL657540 DC-DC Power Board NL813344 Fuse 6A NL903107 Fuse Thermal NL657029 LED Indicator Assembly NL657053 Switch Assembly NL656026 Case Temperature Sensor NL655468 DC-DC Converter (+5V, ±15V)
LECTRO-MECHANICAL
NL902833 Fan NL655760 Case Heater NL656347 Purge Air Heater
NL011167 O-Ring, Buna-N (LED) NL010177 O-Ring, Buna-N (Switch) NL903124 O-Ring, Buna-N (1/4" Bulkhead) NL008025 O-Ring, Buna-N (Fuel, Air Regulator, 3/8" Bulkhead) NL656167 Front Panel Gasket
INGS AND GASKETS
748331-E Rosemount Analytical November 1998
NGA 2000 Flame Ionization Detection Module
5-1
R
EPLACEMENT PARTS
5.1.4 B
NL655779 Burner Assembly, Mixed Fuel NL655784 Burner Assembly, 100% Fuel NL655803 Flameout Sensor NL655801 Glow Plug NL100194 Gasket, Connector - Sample NL810156 Fitting, Tee NL655782 Burner Cap NL656217 Burner Manifold NL656364 Chimney NL630354 Exhaust Adapter NL652995 Connector, Restrictor - Mixed Fuel NL073616 Burner Tip NL656365 Combustion Chamber NL903227 O-Ring, Viton NL903256 O-Ring, Viton
5.1.5 P
NL657448 Kit, Capillary - Mixed Fuel Low Range NL657777 Kit, Capillary - Mixed Fuel High Range NL657776 Kit, Capillary - 100% Fuel Low Range NL017154 Filter, Burner Air & Sample NL902832 Regulator, Fuel and Burner Air NL655269 Regulator, Sample - Brass NL655513 Regulator, Sample - Stainless steel NL871672 Regulator, Purge Air NL615598 Restrictor, Bulkhead - Mixed NL656890 Restrictor, Bulkhead - 100% Fuel NL655794 Restrictor, Air Ignite NL656888 Restrictor, Air Measurement NL630669 Restrictor, Burner - Mixed Fuel NL630662 Restrictor, Burner - 100% Fuel NL902931 Sensor, Flow 400- 2000 ml/min. NL656444 Sensor, Fuel Pressure NL656443 Sensor, Burner Air Pressure NL656418 Sensor, Sample Pressure NL656218 Solenoid - Fuel NL656219 Solenoid, 3-Way - Air NL657126 Switch, Flow - Purge Air NL903690 Switch, Pressure - Purge Air NL903128 Valve, Pressure Relief
URNER ASSEMBLY AND COMPONENTS
1
2
NEUMATICS
1
2
1
1
1
1
1
1 Select per application fuel. Restrictor and sample capillary must display the same color code. 2 Select per application. The sample capillary displays a green color marking. The restrictor displays a red color marking
(mixed fuel).
5-2
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
A
PPENDIX
A. FID I
DENTIFICATION
M
ATRIX
A
Each analyzer is configured per the customer sales order. Below is the FID sales matrix which lists the various configurations available.
To identify the configuration of an analyzer, locate the analyzer name-rating plate. The 12-position sales matrix identifier number appears on the analyzer name-rating plate.
F NGA 2000 FID ANALYZER MODULE
Code Language
A English X Special
Code Configuration Identifier
A10 Mixed Fuel, Calibrated Ranges: 0-10, 0-25, 0-100, 0-250 ppm
Mixed Fuel, Calibrated Ranges: 0-250, 0-1000, 0-2500, 0-10000
A20
ppm A30 Mixed Fuel, Calibrated Ranges: 0-4, 0-10, 0-40, 0-100 ppm B10 Hydrogen Fuel, Calibrated Ranges: 0-1, 0-2.5, 0-10, 0-25 ppm
C10 Mixed Fuel, Calibrated Ranges: 0-10, 0-30, 0-100, 0-300 ppm C20 C30 Mixed Fuel, Calibrated Ranges: 1000, 2500, 10000, 25000
Mixed Fuel, Calibrated Ranges: 0-300, 0-1000, 0-3000, 0-10000
ppm X99 Special Calibration Ranges
F A B10 A00 ZZZ Z EXAMPLE
748331-E Rosemount Analytical November 1998
Code Materials
A00 Brass and Neoprene Back Pressure Regulator B00 Stainless Steel and Kynar Back Pressure Regulator
ZZZ No Selection
Z No Selection
NGA 2000 Flame Ionization Detection Module
A-1
A
PPENDIX
N
OTES
A. FID I
DENTIFICATION MATRIX
A-2
November 1998 Rosemount Analytical 748331-ENGA 2000 Flame Ionization Detection Module
ENERAL PRECAUTIONS FOR HANDLING AND
G
TORING HIGH PRESSURE GAS CYLINDERS
S
Edited from selected paragraphs of the Compressed Gas Association's "Handbook of Compressed Gases" published in 1981 Compressed Gas Association 1235 Jefferson Davis Highway Arlington, Virginia 22202 Used by Permission
1. Never drop cylinders or permit them to strike each other violently.
2. Cylinders may be stored in the open, but in such cases, should be protected against extremes of weather and, to prevent rusting, from the dampness of the ground. Cylinders should be stored in the shade when located in areas where extreme temperatures are prevalent.
3. The valve protection cap should be left on each cylinder until it has been secured against a wall or bench, or placed in a cylinder stand, and is ready to be used.
4. Avoid dragging, rolling, or sliding cylinders, even for a short distance; they should be moved by using a suitable hand-truck.
5. Never tamper with safety devices in valves or cylinders.
6. Do not store full and empty cylinders together. Serious suckback can occur when an empty cylinder is attached to a pressurized system.
7. No part of cylinder should be subjected to a temperature higher than 125°F (52°C). A flame should never be permitted to come in contact with any part of a compressed gas cylinder.
8. Do not place cylinders where they may become part of an electric circuit. When electric arc welding, precautions must be taken to prevent striking an arc against the cylinder.
4125 E
AST LA PALMA AVENUE
• A
Rosemount Analytical Inc.
J
ULY
NAHEIM
ALIFORNIA
1997 • 748525-C • P
, C
92807-1802 • 714-986-7600 • FAX 714-577-8006
RINTED IN
USA
(blank)
ARRANTY
W
Goods and part(s) (excluding consumables) manufactured by Seller are warranted to be free from defects in workmanship and material under normal use and service for a period of twelve (12) months from the date of shipment by Seller. Consumables, glass electrodes, membranes, liquid junctions, electrolyte, o-rings, etc., are warranted to be free from defects in workmanship and material under normal use and service for a period of ninety (90) days from date of shipment by Seller. Goods, part(s) and consumables proven by Seller to be defective in workmanship and/or material shall be replaced or repaired, free of charge, F.O.B. Seller's factory provided that the goods, part(s) or consumables are returned to Seller's designated factory, transportation charges prepaid, within the twelve (12) month period of warranty in the case of goods and part(s), and in the case of consumables, within the ninety (90) day period of warranty. This warranty shall be in effect for replacement or repaired goods, part(s) and the remaining portion of the ninety (90) day warranty in the case of consumables. A defect in goods, part(s) and consumables of the commercial unit shall not operate to condemn such commercial unit when such goods, part(s) and consumables are capable of being renewed, repaired or replaced.
The Seller shall not be liable to the Buyer, or to any other person, for the loss or damage directly or indirectly, arising from the use of the equipment or goods, from breach of any warranty, or from any other cause. All other warranties, expressed or implied are hereby excluded.
IN CONSIDERATION OF THE HEREIN STATED PURCHASE PRICE OF THE GOODS, SELLER GRANTS ONLY THE ABOVE STATED EXPRESS WARRANTY. NO OTHER W ARRANTIES ARE GRANTED INCLUDING, BUT NOT LIMITED TO, EXPRESS AND IMPLIED WARRANTIES OR MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE.
Limitations of Remedy. SELLER SHALL NOT BE LIABLE FOR DAMAGES CAUSED BY DELAY IN PERFORMANCE. THE SOLE AND EXCLUSIVE REMEDY FOR BREACH OF WARRANTY SHALL BE LIMITED TO REPAIR OR REPLACEMENT UNDER THE STANDARD W ARRANTY CLAUSE. IN NO CASE, REGARDLESS OF THE FORM OF THE CAUSE OF ACTION, SHALL SELLER'S LIABILITY EXCEED THE PRICE TO BUYER OF THE SPECIFIC GOODS MANUFACTURED BY SELLER GIVING RISE TO THE CAUSE OF ACTION. BUYER AGREES THAT IN NO EVENT SHALL SELLER'S LIABILITY EXTEND TO INCLUDE INCIDENTAL OR CONSEQUENTIAL DAMAGES. CONSEQUENTIAL DAMAGES SHALL INCLUDE, BUT ARE NOT LIMITED TO, LOSS OF ANTICIPATED PROFITS, LOSS OF USE, LOSS OF REVENUE, COST OF CAPITAL AND DAMAGE OR LOSS OF OTHER PROPERTY OR EQUIPMENT. IN NO EVENT SHALL SELLER BE OBLIGATED TO INDEMNIFY BUYER IN ANY MANNER NOR SHALL SELLER BE LIABLE FOR PROPERTY DAMAGE AND/OR THIRD PARTY CLAIMS COVERED BY UMBRELLA INSURANCE AND/OR INDEMNITY COVERAGE PROVIDED TO BUYER, ITS ASSIGNS, AND EACH SUCCESSOR INTEREST TO THE GOODS PROVIDED HEREUNDER.
Force Majeure. Seller shall not be liable for failure to perform due to labor strikes or acts beyond Seller's direct control.
Rosemount Analytical
4125 E
AST LA PALMA AVENUE
• A
F
EBRUARY 1997 • 7485189-C • PRINTED IN USA
Rosemount Analytical Inc.
NAHEIM
, C
ALIFORNIA
92807-1802 • 714-986-7600 • FAX 714-577-8006
(blank)
IELD SERVICE AND REPAIR FACILITIES
F
Field service and repair facilities are located worldwide.
U.S.A.
To obtain field service on-site or assistance with a service problem, contact (24 hours, 7 days a week):
National Response Center
1-800-654-7768
INTERNATIONAL
Contact your local Rosemount Sales and Service office for service support.
FACTORY
For order administration, replacement Parts, application assistance, on-site or factory repair, service or maintenance contract information, contact:
Rosemount Analytical Inc.
Process Analytical Division
Customer Service Center
1-800-433-6076
RETURNING PARTS TO THE FACTORY
Before returning parts, contact the Customer Service Center and request a Returned Materials Authorization (RMA) number. Please have the following information when you call:
Model Number, Serial Number, and Purchase Order Number or Sales Order Number.
Prior authorization by the factory must be obtained before returned materials will be accepted. Unauthorized returns will be returned to the sende r, f re ight collect.
When return ing any product or compon ent that has been expo sed to a toxic, co rrosive or other hazardous material or used in such a hazardous environment, the user must attach an appropriate Material Safety Data Sheet (M.S.D.S.) or a written certification that the material has been decontaminated, disinfected and/or detoxified.
Return to:
Rosemount Analytical Inc.
4125 East La Palma Avenue
Anaheim, California 92807-1802
4125 E
AST LA PALMA AVENUE
• A
Rosemount Analytical Inc.
, C
NAHEIM
ULY 1997 • 748190-G • PRINTED IN USA
J
ALIFORNIA
92807-1802 • 714-986-7600 • FAX 714-577-8006
(blank)
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