Rosemount Manual: NGA 2000 PMD O2 Analyzer Module SW 2.2-Rev C | Rosemount Manuals & Guides

NGA 2000

PARAMAGNETIC DETECTOR

ANALYZER MODULE

Rosemount Analytical

748361-C

OTICE

N

The information contained in this document is subject to change without notice.
Rosemount Analytical's system of NGA 2000 Modular Gas Analyzers and Controllers are patented,

under U.S. Patent 5.787.015.

Viton-A® is a registered trademark of E.I. duPont de Nemours & Co.
Paliney No. 7™ is a trademark of J.M. Ney Co.

Manual Part Number 748361-C
December 1998
Printed in U.S.A.

Rosemount Analytical Inc.

4125 East La Palma Avenue
Anaheim, California 92807-1802

C

ONTENTS

PREFACE

PURPOSE/SAFETY SUMMARY........................................................................P-1

GLOSSARY ......................................................................................................P-5

SPECIFICATIONS..............................................................................................P-7

SPECIFICATIONS - SAMPLE............................................................................P-7

SPECIFICATIONS - PHYSICAL.........................................................................P-7

CUSTOMER SERVICE, TECHNICAL ASSISTANCE AND FIELD SERVICE....P-8

RETURNING PARTS TO THE FACTORY.........................................................P-8

TRAINING ......................................................................................................P-8

DOCUMENTATION............................................................................................P-8

COMPLIANCES .................................................................................................P-9

S

ECTION

1.1 OVERVIEW..............................................................................................1-1

1.2 TYPICAL APPLICATIONS .......................................................................1-1

1.3 THEORY OF TECHNOLOGY...................................................................1-1

1.4 FEATURES ..............................................................................................1-2

S

ECTION

2.1 UNPACKING............................................................................................2-1

2.2 ASSEMBLY..............................................................................................2-1

2.3 LOCATION...............................................................................................2-2

2.4 GASES.....................................................................................................2-2

2.5 ELECTRICAL CONNECTIONS................................................................2-5

1. I

2. I

2.4.1 Requirements..............................................................................2-2

2.4.2 Connections................................................................................2-5

2.4.3 Leak Test....................................................................................2-5

NTRODUCTION

NSTALLATION

748361-C Rosemount Analytical December 1998

NGA 2000 Paramagnetic Detector

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ONTENTS

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SECTION 3. STARTUP AND OPERATION

3.1 OVERVIEW ............................................................................................. 3-1

3.2 DISPLAYS ............................................................................................... 3-1

S

ECTION

3.3 RUN MODE DISPLAY ............................................................................. 3-1

3.4 MENU DISPLAYS.................................................................................... 3-1

3.5 HELP DISPLAYS..................................................................................... 3-2

3.6 STARTUP PROCEDURE ........................................................................ 3-5

3.7 BINDING.................................................................................................. 3-5

3.8 CALIBRATION......................................................................................... 3-5

3.9 BACKGROUND GAS COMPENSATION................................................. 3-7

3.10 BAROMETRIC PRESSURE COMPENSATION .................................... 3-10

S

ECTION

4.1 OVERVIEW ............................................................................................. 4-1

4.2 PRINTED CIRCUIT BOARD REPLACEMENT........................................ 4-1

4.3 MODULE FAN REPLACEMENT.............................................................. 4-2

4.4 THERMAL FUSE REPLACEMENT ......................................................... 4-3

3. S

4. M

TARTUP AND OPERATION (CONTINUED

AINTENANCE AND TROUBLESHOOTING

)

4.5 FLOW SENSOR REPLACEMENT .......................................................... 4-4

4.6 POWER FUSE REPLACEMENT............................................................. 4-4

S

ECTION

5.1 REPLACEMENT PARTS......................................................................... 5-1

A

PPENDIX

ENERAL PRECAUTIONS FOR HANDLING AND STORING HIGH PRESSURE CYLINDERS

G

ARRANTY

W

IELD SERVICE AND REPAIR FACILITIES

F

5.

REPLACEMENT PARTS

A. PMD I

DENTIFICATION MATRIX

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December 1998 Rosemount Analytical 748361-CNGA 2000 Paramagnetic Detector

FIGURES

1-1 Spherical Body in Non-Uniform Magnetic Field........................................1-2

1-2 Paramagnetic Detector Technology.........................................................1-3

2-1 Analyzer Module Installation into Instrument Platform .............................2-1

2-2 PMD Front Panel Connections.................................................................2-4

2-3 PMD Back Panel Connections.................................................................2-4

2-4 Interconnection of Typical Gas Manifold to PMD Analyzer Module..........2-5

2-5 PMD Wiring Diagram................................................................................2-6

2-6 Outline and Mounting Dimensions............................................................2-7

3-1 Run Mode Display....................................................................................3-3

3-2 Main Menu Display...................................................................................3-3

3-3 Basic Controls Menu................................................................................3-3

3-4 Expert Controls and Setup Menu.............................................................3-4

3-5 Technical Level Configuration Menu........................................................3-4

3-6 Typical Help Screen.................................................................................3-4

3-7 Display Screens (1 of 5)...........................................................................3-10

3-8 Display Screens (2 of 5)...........................................................................3-11

3-9 Display Screens (3 of 5)...........................................................................3-12

3-10 Display Screens (4 of 5)...........................................................................3-13

3-11 Display Screens (5 of 5)...........................................................................3-14

4-1 PMD Module - Major Components...........................................................4-2

4-2 Module Fan Assembly..............................................................................4-2

4-3 Detector Assembly...................................................................................4-3

ONTENTS

C

TABLES

3-1 PMD Analyzer Module Alarms..................................................................3-2

3-2 Calibration Range for Various Zero Bases Operating Ranges.................3-6

3-3 Oxygen Equivalents of Common Gases...................................................3-9

748361-C Rosemount Analytical December 1998

NGA 2000 Paramagnetic Detector

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ONTENTS

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NOTES

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December 1998 Rosemount Analytical 748361-CNGA 2000 Paramagnetic Detector

P

REFACE

PURPOSE/SAFETY SUMMARY

The purpose of this manual is to provide the procedures for the installation, operation
and maintenance of this NGA 2000 module.

Some sections may describe equipment not used in your NGA 2000 system
configuration. The user should become thoroughly familiar with the operation of this
module before operating it. Read this instruction manual completely.

To avoid explosion, loss of life, personal injury and damage to this equipment
and on-site property, all personnel authorized to install, operate and service the
this equipment should be thoroughly familiar with and strictly follow the
instructions in this manual. SAVE THESE INSTRUCTIONS.

If this equipment is used in a manner not specified in these instructions, protective
systems may be impaired.

DANGER is used to indicate the presence of a hazard which will cause severe
personal injury, death, or substantial property damage if the warning is ignored

WARNING is used to indicate the presence of a hazard which can cause severe
personal injury, death, or substantial property damage if the warning is ignored.

CAUTION is used to indicate the presence of a hazard which will or can cause minor
personal injury or property damage if the warning is ignored.

NOTE is used to indicate installation, operation, or maintenance information which is
important but not hazard-related.

WARNING: ELECTRICAL SHOCK HAZARD

Do not operate without covers secure. Servicing requires access to live parts
which can cause death or serious injury. Refer servicing to qualified personnel.

For safety and proper performance this instrument must be connected to a
properly grounded three-wire source of power.

748361-C Rosemount Analytical December 1998

NGA 2000 Paramagnetic Detector

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WARNING: POSSIBLE EXPLOSION HAZARD

This equipment is not designed for and should not be used in the analysis of
flammable samples. Use of this equipment in this way could result in explosion
and death.

Note
Apply leak test liquid to cell or detectors only as a last resort.

WARNING: POSSIBLE EXPLOSION HAZARD

Verify that all gas connections are made as labeled and are leak free. Improper
gas connections could result in explosion or death. See Section 2.4.3 for Leak
test procedure.

WARNING: PARTS INTEGRITY

Tampering or unauthorized substitution of components may adversely affect
safety of this product. Use only factory documented components for repair

WARNING: OVER-VOLTAGE SPIKING

If this Analyzer Module is used with a non-Rosemount Analytical power supply,
adding Rosemount Analytical PN 90331 Current Protector in series with the 24 V
positive line will prevent over-voltage spiking and resultant fuse blowing when
powering up the instrument.

CAUTION: PRESSURIZED GAS

This module requires periodic calibration with a known standard gas. See
General Precautions for Handling and Storing High Pressure Gas Cylinders in
the rear of this manual.

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December 1998 Rosemount Analytical 748361-CNGA 2000 Paramagnetic Detector

REFACE

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CAUTION: HAND INJURY HAZARD

Do not place hands or fingers in Platform front handles when the front panel is
open. Dropping front panel while hand or fingers are inside either handle can
cause serious injury.

CAUTION: OVERBALANCE HAZARD

This Analyzer Module may tip instrument over if it is pulled out too far and the
Platform is not properly supported.

748361-C Rosemount Analytical December 1998

NGA 2000 Paramagnetic Detector

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NOTES

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December 1998 Rosemount Analytical 748361-CNGA 2000 Paramagnetic Detector

GLOSSARY

NALYZER MODULE

A

Self contained analysis modules that are designed to be installed into the NGA 2000
System. One Analyzer Module can be installed into a Single Enclosure containing the
Platform Module. Two Analyzer Modules can be installed into a Dual Enclosure. The
simplest NGA 2000 System consists of one Analyzer Module.

ACKPLANE

B

The interconnect circuit board which the Controller Board, Power Supply Board, I/O
Board(s) and Expansion Board(s) are plugged into the Backplane

ONTROL MODULE

C

The operator interface plus the Controller Board.

REFACE

P

ONTROLLER BOARD

C

The Controller Board in the Platform which runs the software program that operates
the Display, Keypad and Network Manager. The Controller Board plugs into the
Backplane.

ISTRIBUTION ASSEMBLY

D

The Distribution Assembly consists of the Backplane and the card cages in the
Platform Module that contain I/O Module(s) and Expansion Module(s).

XPANSION BOARD

E

The Expansion Board performs special features not related to I/O functions. The
Expansion Board plugs into the Backplane from the Platform front.

I/O M

An auxiliary module that provides some sort of interface to the outside world. I/O
modules may include analog outputs, relay contacts, and digital interfaces. In general,
they are mounted in platforms as options.

ODULE

PERATOR INTERFACE

O

The Display and Keyboard of the Platform.

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NGA 2000 Paramagnetic Detector

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P

LATFORM

P

Any combination of the NGA case, the display and computer board, power supply, and
I/O modules. In general, it could be considered to be anything in the NGA system
other than the analyzer modules.

OWER SUPPLY

P

Any of a variety of components that provide conditioned power to other NGA 2000
components, from the Power Supply Board that plugs into the Backplane in a stand­alone instrument to several larger ones that can power larger collections of modules
and components.

RIMARY VARIABLE

P

The measured species concentration value from an Analyzer Module.

ECONDARY VARIABLE

S

The current status data placed on the network by an Analyzer Module. This includes
sample flow, source voltage and other diagnostic information.

OFTKEYS

S

The five function keys located below the front panel display. The menu function for
each softkey is displayed directly above it and is controlled by the software.

YSTEM

S

A NGA 2000 System consisting of one (or more) Analyzer Modules, an optional
Platform, one or more optional I/O Boards, an optional Expansion Board and an
optional Supplemental Power Supply.

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December 1998 Rosemount Analytical 748361-CNGA 2000 Paramagnetic Detector

SPECIFICATIONS

MEASUREMENT SPECIES:
RANGES:
R

EPEATABILITY

M

INIMUM DETECTABLE LEVEL

N
L

:

OISE

INEARITY

RESPONSE TIME:

D

RIFT (ZERO AND SPAN

E

FFECT OF TEMPERATURE

E

NVIRONMENT

A

MBIENT TEMPERATURE

E

FFECT OF FLOW

P

OWER REQUIREMENTS

:

:

:

:

REFACE

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Oxygen

0 to 100% oxygen; four fullscale selections, including
suppressed zero ranges in 1% increments

±1% of fullscale (at constant temperature)

0.01% oxygen

:

<1% of fullscale, peak-to-peak; <±1% for suppressed ranges
±1% of fullscale

0 to 90% of fullscale in 20 seconds (±2 seconds)
<±1% of fullscale/24 hours, <±2% of fullscale/week at constant

):

:

:

:

temperature;
<±2% of fullscale/24 hours, <±4% of fullscale/week of range for

99 to 100% (at constant temperature)
<±1% of fullscale over any 10°C interval for rate of change no

greater than 10°C per hour
Location - Class B controlled, indoor, non-hazardous

0 to 45°C (32 to 113°F)
<±1% of range when sample flow rate is changed by 20 ml/min.

24 VDC ±5%, 50 W max.; ripple and noise: <100 mV
peak-to-peak; line and load regulations: <±1%

SPECIFICATIONS – SAMPLE

T

EMPERATURE

F

LOW RATE

E

XHAUST PRESSURE

P

ARTICLES

D

EWPOINT

M

ATERIALS IN CONTACT WITH

S

AMPLE

:

:

:

:

:

:

Non-flammable;: 10 to 66°C (50 to 150°F)
800 to 1400 ml/min.

-345 to 690 hPa-gauge (-5 to 10 psig)
filtered to <2 microns
below 43°C (110°F), no entrained liquid

Glass, 316 stainless steel, titanium, Paliney No. 7, epoxy
resin, Viton A, platinum, nickel, rhodium and MgF

SPECIFICATIONS - PHYSICAL

C

ASE CLASSIFICATION

D

IMENSIONS

W

EIGHT

M

OUNTING

M

AXIMUM LENGTH OF

C

ABLE

See the Preface section of the Platform Components manual for specifications regarding Platform­related components (e.g., case dimensions) and the Preface of the I/O Module manual for specifications
regarding I/O (e.g., relay outputs).

:

:

:

:

:

LON

General purpose for installation in weather-protected
areas

See Outline and Mounting Dimensions, Figure 2-4
8 kg (17.6 lbs.
Inside a Platform or custom-installed in a panel

1600 m (1 mile) between Analyzer Module and Platform

2

748361-C Rosemount Analytical December 1998

NGA 2000 Paramagnetic Detector

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CUSTOMER SERVICE, TECHNICAL ASSISTANCE AND FIELD SERVICE

For order administration, replacement Parts, application assistance, on-site or factory
repair, service or maintenance contract information, contact:

Rosemount Analytical Inc.

Process Analytical Division

Customer Service Center

1-800-433-6076

RETURNING PARTS TO THE FACTORY

Before returning parts, contact the Customer Service Center and request a Returned
Materials Authorization (RMA) number. Please have the following information when
you call: Model Number, Serial Number, and Purchase Order Number or Sales Order

Number.

Prior authorization by the factory must be obtained before returned materials will be
accepted. Unauthorized returns will be returned to the sender, freight collect.

When returning any product or component that has been exposed to a toxic, corrosive
or other hazardous material or used in such a hazardous environment, the user must
attach an appropriate Material Safety Data Sheet (M.S.D.S.) or a written certification
that the material has been decontaminated, disinfected and/or detoxified.

Return to:

Rosemount Analytical Inc.

4125 East La Palma Avenue

Anaheim, California 92807-1802

TRAINING

A comprehensive Factory Training Program of operator and service classes is
available. For a copy of the Current Operator and Service Training Schedule contact
the Technical Services Department at:

Rosemount Analytical Inc.

Phone: [phone]

FAX: [phone]

D

OCUMENTATION

The following NGA 2000 Paramagnetic Detector instruction materials are available.
Contact Customer Service or the local representative to order.

748361 Instruction Manual (this document)

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December 1998 Rosemount Analytical 748361-CNGA 2000 Paramagnetic Detector

9

6

COMPLIANCES

This product may carry approvals from several certifying agencies, including Factory
Mutual and the Canadian Standards Association (which is also an OSHA accredited,
Nationally Recognized Testing Laboratory), for use in non-hazardous, indoor locations

Certified

REFACE

P

®

NRTL /C

Rosemount Analytical Inc. has satisfied all obligations from the European
Legislation to harmonize the product requirements in Europe.

This product complies with the standard level of NAMUR EMC.
Recommendation (May 1993).

This product satisfies all obligations of all relevant standards of the EMC framework in
Australia and New Zealand.

EN 61010-1/1993

97-C219

NAMUR

748361-C Rosemount Analytical December 1998

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NGA 2000 Paramagnetic Detector

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NOTES

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December 1998 Rosemount Analytical 748361-CNGA 2000 Paramagnetic Detector

I

NTRODUCTION

1

1.1 OVERVIEW

This manual describes the Paramagnetic Detector (PMD) Analyzer Module of
Rosemount Analytical's NGA 200 Series of gas analysis components.

The PMD Analyzer Module is designed to continuously determine the concentration
of oxygen in a flowing gaseous mixture. The concentration is expressed in ppm or
percent volume O2.

The entire Analyzer Module is designed as a slide-in module (if configured in stand­alone instrument fashion), removable from the front of the Platform, with gas
connections made from the rear. All electronics relative to sample detection and
conditioning are included in this module.

1.2 TYPICAL APPLICATIONS

PMD Analyzer Module applications include:

• process control

• continuous emissions monitoring systems (CEMS)

• industrial gas production

• fermentation process monitoring

1.3 THEORY OF TECHNOLOGY

Oxygen is strongly paramagnetic (i.e., capable of becoming a temporary magnet when
placed in a magnetic field) while most other common gases are weakly diamagnetic
(i.e., tend to be non-magnetic). See Figure 1-1.

The Magnetic susceptibility of the flowing gas sample is sensed in the
detector/magnet assembly. As shown in Figure 1-2, a dumbbell shaped, nitrogen­filled, hollow gas test body is suspended on a platinum/nickel alloy ribbon in a non­uniform magnetic field.

Because of a "magnetic buoyancy" effect, the spheres of the test body are subjected
to displacement forces, resulting in a displacement torque proportional to the magnetic
susceptibility of the gas surrounding the test body.

748361-C Rosemount Analytical December 1998

NGA 2000 Paramagnetic Detector

1-1