Rosemount 1055 pH Analzyer Manuals & Guides

Page 1
Model Solu Comp®II
Dual Input pH Analyzer
Model Options 1055-22-32 and 1055-22
Instruction Manual
PN 51-1055pH/rev.M February 2006
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READ THIS PAGE BEFORE PROCEEDING!
Your purchase from Rosemount Analytical, Inc. has resulted in one of the finest instruments available for your particular application. These instruments have been designed, and tested to meet many national and international standards. Experience indicates that its performance is directly related to the quality of the installation and knowledge of the user in operating and maintaining the instrument. To ensure their continued operation to the design specifications, personnel should read this manual thoroughly before proceeding with installation, commissioning, operation, and main­tenance of this instrument. If this equipment is used in a manner not specified by the manufacturer, the pro­tection provided by it against hazards may be impaired.
• Failure to follow the proper instructions may cause any one of the following situations to occur: Loss of life; personal injury; property damage; damage to this instrument; and warranty invalidation.
• Ensure that you have received the correct model and options from your purchase order. Verify that this manual covers your model and options. If not, call 1-800-854-8257 or 949-757-8500 to request correct manual.
• For clarification of instructions, contact your Rosemount representative.
• Follow all warnings, cautions, and instructions marked on and supplied with the product.
• Use only qualified personnel to install, operate, update, program and maintain the product.
• Educate your personnel in the proper installation, operation, and maintenance of the product.
• Install equipment as specified in the Installation section of this manual. Follow appropriate local and national codes. Only connect the product to electri­cal and pressure sources specified in this manual.
• Use only factory documented components for repair. Tampering or unauthorized substitution of parts and procedures can affect the performance and cause unsafe operation of your process.
• All equipment doors must be closed and protective covers must be in place unless qualified personnel are performing maintenance.
• If this equipment is used in a manner not specified by the manufacturer, the protection provided by it against hazards may be impaired.
WARNINGS
RISK OF ELECTRICAL SHOCK
Equipment protected throughout by double insulation.
• Installation of cable connections and servicing of this product require access to shock hazard voltage levels.
• Main power and relay contacts wired to separate power source must be disconnected before servicing.
• Do not operate or energize instrument with case open!
• Signal wiring connected in this box must be rated at least 240 V.
• Non-metallic cable strain reliefs do not provide grounding between conduit connections! Use grounding type bush­ings and jumper wires.
• Unused cable conduit entries must be securely sealed by non-flammable closures to provide enclosure integrity in compliance with personal safety and environmental pro­tection requirements. Unused conduit openings must be sealed with NEMA 4X or IP65 conduit plugs to maintain the ingress protection rating (NEMA 4X).
• Electrical installation must be in accordance with the National Electrical Code (ANSI/NFPA-70) and/or any other applicable national or local codes.
• Operate only with front and rear panels fastened and in place over terminal area.
• Safety and performance require that this instrument be connected and properly grounded through a three-wire power source.
Proper relay use and configuration is the responsibility
of the user.
CAUTION
This product generates, uses, and can radiate radio fre­quency energy and thus can cause radio communication interference. Improper installation, or operation, may increase such interference. As temporarily permitted by regulation, this unit has not been tested for compliance within the limits of Class A computing devices, pursuant to Subpart J of Part 15, of FCC Rules, which are designed to provide reasonable protection against such interference. Operation of this equipment in a residential area may cause interference, in which case the user at his own expense, will be required to take whatever measures may be required to correct the interference.
WARNING
This product is not intended for use in the light industrial, residential or commercial environments per the instrument’s certification to EN50081-2.
Emerson Process Management
Rosemount Analytical Inc.
2400 Barranca Parkway Irvine, CA 92606 USA Tel: (949) 757-8500 Fax: (949) 474-7250
http://www.raihome.com
© Rosemount Analytical Inc. 2005
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QUICK START GUIDE
FOR MODEL SOLU COMP II pH/ORP ANALYZER
(Model Options 1055-22-32 and 1055-22)
1. Refer to Section 2.0 for installation instructions.
2. Wire pH (or ORP) sensor(s) to the analyzer. See the drawings below. Refer to the sensor instruction sheet for details. Make alarm, output, and power connections as shown below.
CONTINUED ON THE FOLLOWING PAGE
3. Once connections are secured and verified, apply power to the analyzer.
Wiring Connections for Solu Comp II Model 1055-01-10
(Panel Mount with 115/230 Vac Power)
Wiring Connections for Solu Comp II Model 1055-02-10
(Panel Mount with 24 Vdc Power)
Wiring Connections for Solu Comp II Model 1055-01-11
(Surface/Pipe Mounting with 115/230 Vac Power)
Wiring Connections for Solu Comp II Model 1055-02-11
(Surface/Pipe Mounting with 24 Vdc Power)
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5. Choose the desired language. Choose >> to show more choices.
6. Choose the number of sensors wired to the analyzer.
NOTE
If One sensor is selected, only
S1 will be available. S2 cannot be disabled.
7. Choose the measurement for sensor 1.
8. Choose the measurement for sensor 2.
9. Choose temperature units.
10. The main display appears. The outputs and alarms are assigned to default val­ues. To change settings, refer to Section 5.0, Programming the Analyzer. To reinstall factory settings and return to Quick Start, see Section 5.10.
# of sensors?
One
TTwwoo
Temperature in?
*
CC
*
F
S1 Measure?
ppHH
Redox ORP
S2 Measure?
ppHH
Redox ORP
4. When the analyzer is powered up for the first time, Quick Start screens appear. Using Quick Start is easy.
a. A blinking field shows the position of the cursor.
b. Use the  or  key to move the cursor left or right. Use the or key to move the cursor up or down or to
increase or decrease the value of a digit. Use the or key to move the decimal point.
c. Press ENTER to store a setting. Press EXIT to leave without storing changes. Pressing EXIT also returns the
display to the previous screen.
EEnngglliisshh
Fran ais
Espa ol >>
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QUICK REFERENCE GUIDE
MENU TREE FOR pH/ORP/REDOX MEASUREMENTS
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About This Document
This manual contains instructions for installation and operation of the Solu Comp II Model 1055 Dual Input pH Analyzer.
The following list provides notes concerning all revisions of this document.
Rev
. Level
Date Notes
0 7/00 This is the initial release of the product manual. The manual
has been reformatted to reflect the Emerson documentation style and updated to reflect any changes in the product offering.
A 2/02 Update specs (p. 2).
B 7/02 Added UL specs info
C 9/02 Fixed minor typos throughout
D 10/02 deleted option code -41 reference of p. 3
E 2/03 Revised specs & maintenance info (p. 5, 9, 45, 46)
F 4/03 Update CE specs info (p. 2, 9)
G 2/04 Update H
2SO4
specs info & recommended sensors (p. 4)
H 5/04 Updated list of compatible sensors
I 9/04 Update pipe and surface mounting drawings
J 11/04 Update panel mounting drawing
K 12/04 Revise USP references
L 4/05 Revise mounting drawing on p.12
M 2.06 Revise Case and Analog Output specifications on page 2.
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i
MODEL SOLU COMP II TABLE OF CONTENTS
MODEL SOLU COMP II DUAL INPUT pH ANALYZER
TABLE OF CONTENTS
Section Title Page
1.0 DESCRIPTION AND SPECIFICATIONS ................................................................ 1
1.1 Features and Applications........................................................................................ 1
1.2 Specifications........................................................................................................... 2
1.3 Ordering Information and Accessories..................................................................... 8
2.0 INSTALLATION ....................................................................................................... 11
2.1 Unpacking and Inspection........................................................................................ 11
2.2 Installation................................................................................................................ 11
3.0 WIRING.................................................................................................................... 15
3.1 Preparing Conduit Openings.................................................................................... 15
3.2 Power, Alarm, Output, and Sensor Connections ..................................................... 15
4.0 DISPLAY AND OPERATION ................................................................................... 18
4.1 Display ..................................................................................................................... 18
4.2 Keypad..................................................................................................................... 18
4.3 Programming and Calibrating the Solu Comp II - Tutorial ....................................... 19
4.4 Security .................................................................................................................... 20
4.5 Using Hold ............................................................................................................... 20
5.0 PROGRAMMING THE ANALYZER ........................................................................ 21
5.1 General .................................................................................................................... 21
5.2 Changing StartUp Settings....................................................................................... 21
5.3 Configuring and Ranging the Outputs...................................................................... 23
5.4 Configuring Alarms and Assigning Setpoints ........................................................... 25
5.5 Selecting Type of Measurement and Activating Solution Temperature Correction .. 28
5.6 Choosing Temperature Units and Manual/Automatic Temperature Compensation . 30
5.7 Setting a Security Code ........................................................................................... 31
5.8 Noise Rejection........................................................................................................ 31
5.9 Single Sensor or Dual Sensor Input......................................................................... 32
5.10 Resetting Factory Calibration and Factory Default Settings .................................... 32
5.11 Selecting a Default Screen, Language, and Screen Contrast ................................. 33
6.0 CALIBRATION ........................................................................................................ 35
6.1 Introduction .............................................................................................................. 35
6.2 Calibrating Temperature........................................................................................... 35
6.3 Two-Point Buffer Calibration (Auto Calibration) ....................................................... 37
6.4 Two-Point Buffer Calibration (Manual Calibration) ................................................... 39
6.5 Making the Analyzer Reading Match a Second Instrument (Standardization) ......... 41
6.6 Entering a Known Slope .......................................................................................... 42
6.7 ORP Calibration ....................................................................................................... 43
7.0 MAINTENANCE ..................................................................................................... 44
7.1 Overview .................................................................................................................. 44
7.2 Replacement Parts .................................................................................................. 44
8.0 TROUBLESHOOTING ............................................................................................ 47
8.1 Overview .................................................................................................................. 47
8.2 Troubleshooting Using Fault Codes......................................................................... 47
8.3 Troubleshooting When No Error Message is Showing ............................................ 48
8.4 Simulating Inputs ..................................................................................................... 51
8.5 Simulating Temperature ........................................................................................... 52
8.6 Measuring Reference Voltage.................................................................................. 53
9.0 RETURN OF MATERIAL ........................................................................................ 54
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MODEL SOLU COMP II TABLE OF CONTENTS
TABLE OF CONTENTS CONT’D
LIST OF FIGURES
Number Title Page
2-1 Panel Mount Installation ........................................................................................... 12
2-2 Pipe Mount Installation ............................................................................................. 13
2-3 Surface Mount Installation........................................................................................ 14
3-1 Removing the Knockouts ......................................................................................... 15
3-2 Wiring Connections for Solu Comp II Model 1055pH-01-10 ....................................
(Panel Mount with 115/230 Vac Power).................................................................... 16
3-3 Wiring Connections for Solu Comp II Model 1055pH-02-10 ....................................
(Panel Mount with 24 Vdc Power) ............................................................................ 16
3-4 Wiring Connections for Solu Comp II Model 1055pH-01-11 ....................................
(Wall/Pipe Mounting with 115/230 Vac Power)......................................................... 17
3-5 Wiring Connections for Solu Comp II Model 1055pH-02-11 ....................................
(Wall/Pipe Mounting with 24 Vdc Power) ................................................................. 17
4-1 Displays During Normal Operation........................................................................... 18
4-2 Solu Comp II Keypad ............................................................................................... 18
5-1 Assigning Outputs 1 and 2 ...................................................................................... 23
5-2 High Alarm Logic ..................................................................................................... 25
5-3 Low Alarm Logic ....................................................................................................... 25
6-1 Calibration Slope and Offset .................................................................................... 37
7-1 Exploded View of Solu Comp II (Panel Mount Version) ........................................... 45
7-2 Exploded View of Solu Comp II (Pipe/Surface Mount Version) ................................ 46
8-1 Simulating Inputs When the Preamplifier is in the Analyzer ..................................... 51
8-2 Simulating pH Input When the Preamplifier is in the Sensor.................................... 52
8-3 Three-Wire RTD Inputs ............................................................................................ 52
8-4 Simulating RTD Inputs.............................................................................................. 53
8-5 Checking for a Poisoned Reference Electrode ........................................................ 53
LIST OF TABLES
Number Title Page
5-1 Default Settings ........................................................................................................ 22
7-1 Replacement Parts for Solu Comp II (Panel Mount Version) ................................... 45
7-2 Replacement Parts for Solu Comp II (Pipe/Surface Mount Version) ........................ 46
ii
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1
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
SECTION 1.0.
DESCRIPTION AND SPECIFICATIONS
1.1 FEATURES AND APPLICATIONS
1.2 SPECIFICATIONS
1.3 ORDERING INFORMATION AND ACCESSORIES
1.1 FEATURES AND APPLICATIONS
The Solu Comp II analyzers offer the choice of sin­gle or dual sensor input with measurement choices of pH/ORP, resistivity/conductivity/TDS, % concen­tration, ratio conductivity, total and free chlorine, dis­solved oxygen, dissolved ozone, flow and tempera­ture. Dual measurement analyzers offer a wide choice of measurement combinations thus reducing the cost per loop and needed panel space.
FIELD COMMISSION OPTION: The Solu Comp II can be ordered with the ability to commission meas­urements in the field. This added flexibility can greatly reduce the number of spare instruments required for field servicing.
QUICK START PROGRAMMING: Exclusive Quick Start screens appear the first time the Solu Comp II is powered up. Screen prompts direct the user to register the number of sensors, the measurement unit(s) and the language to display. Some measure­ment specific prompts are also displayed. The measurement loop is ready for use in a matter of minutes.
MENUS: Menu screens for calibrating and register­ing choices are simple and intuitive. Plain language prompts guide the user through the procedures. There are no service codes to enter before gaining access to menus.
DUAL SENSOR INPUT AND OUTPUT: The Solu Comp II accepts single or dual sensor input. The two 4-20 mA outputs can be independently pro­grammed to correspond to any selected measure­ment or temperature. Output damping and linear or log output may also be field selected.
ALARMS: The Solu Comp II has three fully pro­grammable alarm relays that can be assigned to any selected measurement or temperature. Alarms can be configured as high, low, or USP1. The third relay has the additional choice of fault alarm opera­tion. When selected, a fault alarm will activate the relay when a sensor or analyzer fault occurs.
ENCLOSURE: The panel mount version fits stan­dard ½ DIN panel cutouts, and its shallow depth is ideally suited for easy mounting in Hoffman-type enclosures. A panel mount gasket is included to maintain the weather rating of the panel. Surface/pipe mount enclosure includes self-tapping screws for surface mounting. A pipe mounting accessory kit is available for mounting to a 2-inch pipe.
DISPLAY: The two-line, 16-character, back-lit dis­play can be customized to meet user requirements. All operations and descriptive messages can be field selected for English, French, German, Italian, Spanish, or Portuguese. Informative screens, which permit data not shown in the regular display, may be seen at the push of a button.
TEMPERATURE: Most measurements (except ORP and flow) require temperature compensation. The Solu Comp II will automatically recognize either a Pt100 or Pt1000 RTD, normally built into the sen­sor. When this RTD is present, the Solu Comp II can be set up to display the temperature in °C or °F as well as set any one or more of the alarms and/or outputs to respond to this sensor input. If two meas­urements with temperature are present either can be chosen for each alarm and output selected.
1
USP alarm applies to conductivity/resistivity only.
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2
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
1.2 SPECIFICATIONS - General
Case: ABS (panel-mount), polycarbonate (pipe- and
surface-mount). All versions are NEMA 4X/CSA 4 (IP65).
Dimensions
Panel (code -10): 6.10 x 6.10 x 3.72 in. (155 x
155 x 94.5 mm) Surface/Pipe (code -11): 6.23 x 6.23 x 3.23 in.
(158 x 158 x 82 mm); see page 5 for dimensions of pipe mounting bracket.
Conduit openings: Accepts PG13.5 or 1/2 in. con-
duit fittings
Display: Two line, 16-character, back-lit display.
Character height: 4.8 mm. Display can be cus­tomized to meet individual requirements. Depending on number of sensors, as many as 14 display screens are available.
Ambient temperature and humidity: 0 to 50°C, (32
to 122°F) RH 5 to 95% (non-condensing) Note: The analyzer is operable from -20 to 60°C
(-4 to 140°F) with some degradation in display performance.
Power:
Code -01:
115/230 Vac
±15%, 50/60 Hz ±6%, 8.0W
Code -02*: 24 Vdc ±15%, 6.0W
Installation Category II
*
For +24Vdc Power Supply use only devices meeting NEC Class II or UL recognized (UL 1950).
Equipment protected throughout by double insula­tion.
Hazardous Location:
Class I, Division 2, Groups A, B, C, & D
POLLUTION DEGREE 4: Extended Environment
Outdoor use where conductive contamination such as rain, snow, or dust may be present.
(Hazardous Location only)
RFI/EMI: EN-61326 LVD: EN-61010-1
Input: Choice of single or dual sensor input with
measurement choices of pH/ORP, conductivity/ resistivity, toroidal conductivity, flow, chlorine, dis­solved oxygen, and dissolved ozone. Field-com­missioned units allow user to change measure­ments on either or both inputs. See combination guide for valid combinations. For contacting con­ductivity measurements, temperature element must be a Pt 1000 RTD. For other measure­ments, use either a Pt100 RTD, Pt1000 RTD, or 22k NTC (D.O. only).
Outputs: Two 4-20 mA or 0-20 mA isolated outputs.
Continuously adjustable. Linear or logarithmic. Maximum load 500 ohms. Output dampening with time constant of 5 sec is user-selectable.
Alarms: Three alarm relays for process measure-
ment(s) or temperature. Alarm 3 can be configured as a fault alarm, instead of a
process alarm. Each relay can be configured independently. Alarm logic (high or low activation or USP*) and deadband are user-programmable. The USP* alarm can be programmed to activate when the conductivity is within a user-selectable percentage of the limit.
*conductivity/resistivity measurement only
Relays: Form C, single pole double throw, epoxy sealed
Terminal Connections Rating: 26-14 AWG wire size
Weight/Shipping weight (rounded up to nearest lb or
nearest 0.5 kg): 3 lb (1.5 kg)/4 lb (2.0 kg)
Resistive Inductive
28 Vdc 5.0 A 3.0 A 115 Vac 5.0 A 3.0 A 230 Vac 5.0 A 1.5 A
Ordinary Location: (-68 only)
POLLUTION DEGREE 2: Normally only non-con­ductive pollution occurs. Occasionally, however, a temporary conductivity caused by condensation must be expected.
12RN
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MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
Measures conductivity in the range 0 to 20,000 µS/cm. Display choices are conductivity, resistivity, and TDS (total dissolved solids). Three temperature corrections are available: high purity water (dilute sodium chlo­ride), cation conductivity (dilute hydrochloric acid), and adjustable linear temperature coefficient (0 to
5.00%/°C). Temperature correction can be disabled, allowing the analyzer to display raw conductivity.
PERFORMANCE SPECIFICATIONS -
ANALYZER (CONDUCTIVITY INPUT)
Accuracy (Resistivity)**: 0.9% of reading
Accuracy (Temperature)**: ±0.1°C between 5°C and
100°C; ±1°C between 101°C and 200°C
Stability: 0.5% of reading/month
Ambient Temperature Effect: ±0.05% of reading/°C
Output Accuracy: ±0.1 mA
Temperature correction: High purity water (dilute
sodium chloride), cation conductivity (dilute hydrochloric acid), linear temperature coefficient (0.0 to 5.00%/°C), or none. High purity water and cation conductivity temperature correction apply between 0 and 100°C. Linear temperature coeffi­cient can be applied between -5 and 200°C.
Measurement Range: 0.0 to 20,000 µS/cm, 0.05 to
20 M-cm, or 0 to 10,000 ppm TDS
Temperature Range: -5°C to 200°C (23°F to 392°F)
1
whichever is greater
2
Accuracy values pertain to Endurance Model 400 Series conductivity sensors only
RECOMMENDED SENSORS FOR CONDUCTIVITY:
The Solu Comp II is intended for use with the ENDURANCE Model 400 series conductivity sensor (Pt 1000 RTD).
Model 400 Screw-in/Insertion
Model 400VP Screw-in/Insertion with 6.0 VP connector
Model 401 Screw-in/Insertion (except 401-15)
Model 402 Retractable
Model 402VP Retractable with 6.0 VP connector
Model 403 Sanitary Flanged
Model 403VP Sanitary Flanged with 6.0 VP connector
Model 404 Flow-Through
The analyzer can also be used with Rosemount Analytical conductivity sensor Models 140, 141, 142, and 150 having a Pt 100 RTD.
Refer to the table to select the appropriate cell constant.
Ratio Conductivity (Codes -20-30):
The dual conductivity Solu Comp II can function as a ratio analyzer or recovery device (% passage or % rejection). Product sensor 2’s conductivity reading is always displayed.
Ratio
%Pass
%Reject
CONTACTING CONDUCTIVITY (Codes -20 and/or -30)
Range Cell constant (/cm) Accuracy
1,2
0.055 - 9.99 µS/cm 0.01 0.9% of reading or ±0.002 µS/cm
10 - 50 µS/cm 0.01 ±2% of reading
0.055 - 500 µS/cm 0.1 ±2% of reading or ±0.1 µS/cm
0.055 - 5000 µS/cm 1.0 ±2% of reading or ±1 µS/cm
0 - 5 mS/cm 1.0 ±2% of reading
or ±0.001 mS/cm
0 - 20 mS/cm 10 ±2% of reading
or ±0.01 mS/cm
Range, µµS/cm Cell constant, /cm
0.0 to 50 0.01 5 to 500 0.1
50 to 5,000 1.0
500 to 20,000 10
12.34 µS/cm 40.3 C
7.34pH 25.3 C
Ratio .3325
S2 4.621 µS/cm
%Passage 12.1
S2 4.621 µS/cm
%Reject 87.9
S2 4.621 µS/cm
3
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4
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
When used with Model Series 200 Toroidal Conductivity Sensors, display choices are conductiv­ity, resistivity, and percent concentration. The per­cent concentration selection includes the choice of four common solutions (0-12% NaOH, 0-15% HCl, and 0-25% or 96-99.7% H2SO4). The conductivity­concentration algorithms for these solutions are fully temperature compensated. For other solutions, a simple-to-use menu allows the customer to enter his own data. The analyzer accepts as many as five (5) data points and fits either a linear (two [2] points) or a quadratic function (three [3] or more points) to the data. Reference temperature and linear temperature slope may also be adjusted for optimum results.
PERFORMANCE SPECIFICATIONS -
Measurement Range: see table below
Accuracy: ± 1% of reading and ± 0.01 mS/cm
Repeatability: ± 0.5% of reading and ± 0.005 mS/cm
Stability: ± 0.25% of reading and ± 0.005 mS/cm/month,
noncumulative
Ambient Temperature Effect: ± 0.05% of reading/°C
Temperature Compensation: -15 to 200°C (5 to
392°F) automatic or manual. Automatic requires a Pt100/1000 RTD
Temperature correction: Linear temperature
coefficient (0.0 to 5.00%/°C) neutral salt (dilute sodium chloride) or none
RECOMMENDED SENSORS:
Model 222 Flow-through conductivity sensor
Model 225 Clean-in-place conductivity sensor
Model 226 Large bore conductivity sensor
Model 228 Toroidal conductivity sensor
Model 242 Flow-through conductivity sensor
Model 247 Economy conductivity sensor
TOROIDAL CONDUCTIVITY (Codes -21 and/or -31)
FULL SCALE MICROSIEMENS/cm
INDUCTIVE SENSORS
Conductivity Sensor
Model Number 226 228 225 222 (1in.) 222 (2 in.)
Cell Constant* 1.0 3.0 3.0 6.0 4.0
Minimum Range 50 250 250 500 500
Maximum Range 1,000,000 2,000,000 2,000,000 2,000,000 2,000,000
* Typical
S1 1027mS/cm 100 C
S2 847.1µS/cm 100 C
Page 13
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
For use with any standard pH or ORP sensor and all Uniloc sensors and junction boxes with built-in diag­nostic style preamplifiers, display choices are pH, ORP or Redox. The automatic buffer recognition fea­ture uses stored buffer values and their temperature curves for the most common buffer standards avail­able worldwide. The analyzer will recognize the value of the buffer being measured and perform a self stabi­lization check on the sensor before completing the calibration. Manual or automatic temperature compen­sation is keypad selectable. Change in pH due to process temperature can be compensated using a programmable temperature coefficient or isopotential point. Measurement and display of pH glass and ref­erence impedance helps alert the user to sensor maintenance needs.
*reference impedance is suppressed with amperometric/pH combinations (-24, -25, -26)
PERFORMANCE SPECIFICATIONS ­ANALYZER (pH INPUT)
Measurement Range [pH]: 0 to 14 pH
Accuracy: ±0.01 pH
Repeatability: ±0.01 pH
Stability: ±0.01 pH/month, non-cumulative
Temperature Coefficient: ±0.003 pH/°C
Temperature Compensation: Pt100/Pt1000 RTD,
Automatic or Manual -15 to 100°C (5 to 212°F)
Temperature Correction: Choose from standard
measurement compensation, solution temperature correction for high purity or dilute base solutions, and custom temperature correction.
PERFORMANCE SPECIFICATIONS ­ANALYZER (ORP INPUT)
Measurement Range [ORP]: -1400 to +1400 mV
Accuracy: ±2.0 mV
Repeatability: ±1.0 mV
Stability: ±1.0 mV/month, non-cumulative
Temperature Coefficient: ± 0.2 mV/°C
Temperature Measurement: -15 to 100°C
(5 to 212°F)
Temperature Correction: none required
RECOMMENDED SENSORS FOR pH:
Model 320B Flow Through pH Model 320HP High Purity pH Model 328A Steam Sterilizable pH Model 370 and 371 EuroSenz pH Model 381+ Insertion/Submersion/Flow Through pH Model 385+ Insertion/Submersion/Retractable pH Model 389 Insertion/Submersion pH Model 396 Insertion/Submersion pH Model 396VP Insertion/Submersion pH with VP 6.0 connector Model 396P Insertion/Submersion pH Model 396PVP Insertion/Submersion pH with VP 6.0 connector Model 396R Retractable pH Model 396RVP Retractable pH with VP 6.0 connector Model 397 Quik Disconnect pH Model 398 Insertion/Submersion pH Model 398VP Insertion/Submersion with VP 6.0 connector Model 398R Retractable pH Model 398RVP Retractable pH with VP 6.0 connector Model 399 Insertion/Submersion pH Model Hx338 Steam Sterilizable pH Model Hx348 Steam Sterilizable pH
RECOMMENDED SENSORS FOR ORP:
Model 330 Flow Through ORP Model 371 EuroSenz ORP Model 381+ Insertion/Submersion/Flow Through ORP Model 385+ Insertion/Submersion/Retractable pH Model 389 Insertion/Submersion ORP Model 396P Insertion/Submersion ORP Model 396PVP Insertion/Submersion ORP with VP 6.0 connector Model 396R Retractable ORP Model 398 Insertion/Submersion ORP Model 398VP Insertion/Submersion with VP 6.0 connector Model 398R Retractable ORP Model 398RVP Retractable ORP with VP 6.0 connector
When used with conductivity (-20-32 or -22-30):
Model 320HP High Purity ORP Model 381+ Insertion/Submersion/Flow Through ORP Model 385+ Insertion/Submersion/Retractable ORP Model 396P Insertion/Submersion ORP Model 396PVP Insertion/Submersion ORP with VP 6.0 connector Model 396R Retractable ORP Model 396RVP Retractable ORP with VP 6.0 connector
pH/ORP (Codes -22 and/or -32)
S1 4.34pH 25 C
S2 12.34pH 27 C
5
Page 14
6
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
When used with a chlorine specific membrane-covered amperometric sensor, display choices are free chlorine or total chlorine. (Total chlorine measurement requires the use of the Model SCS921 or other sample condi­tioning system). Because the permeability of the mem­brane is a function of temperature, a correction is nec­essary when the sensor is used at a temperature dif­ferent from the one at which it was calibrated. The Solu Comp II automatically applies the temperature correction factor. The process temperature is meas­ured by an RTD in the sensor. An input filter allows the user to configure the analyzer for rapid response or low noise. The low noise option is recommended for samples containing less than 0.1 ppm chlorine.
pH is also a factor in the measurement of free chlo­rine. An aqueous solution of free chlorine is a mixture of hypochlorous acid and hypochlorite ion. The rela­tive amount of each depends on the temperature and pH. Generally, increasing the pH and temperature reduces the amount of hypochlorous acid in the mix­ture. Because the response of the sensor to hypochlorous acid is greater than its response to hypochlorite, accurate determination of chlorine requires knowledge of the pH and temperature of the sample. If the pH is relatively constant, a fixed pH cor­rection factor can be entered into the analyzer. If the pH is greater than 7 and fluctuates by more than 0.2, continuous measurement of the pH and automatic pH correction is necessary. For automatic pH correction, select code -32 and an appropriate pH sensor.
PERFORMANCE SPECIFICATIONS
Measurement Range: 0-20 ppm (mg/L) chlorine
(as Cl2)
Resolution: 0.001 ppm Automatic pH Correction (requires Code -32): 5.0
to 9.5 pH
Temperature Correction: Automatic (with Pt100 RTD
in sensor) or manual 0-50°C. Can be disabled if desired.
Input filter: time constant 1 - 999 sec
RECOMMENDED SENSORS
Chlorine: 499A CL-01 Free Chlorine or 499A CL-02
Total Residual Chlorine (requires sample condi­tioning)
pH: 399-09-62, 399VP-09, 399-14
For use with most pulse signal flow sensors, the Solu Comp II's user selectable units of measure include flow rates in GPM (Gallon per minute), LPM (liters per minute), or m3/hr (cubic meters per hour), and veloci­ty in ft/sec or m/sec. When configured to measure flow, the unit also acts as a totalizer in the chosen unit (gallons, liters, or cubic meters).
Dual flow instruments can be configured as a % recovery device or a flow difference device.
PERFORMANCE SPECIFICATIONS
Frequency Range: 0.5 - 4000 Hz Flow Rate: 0 - 9999 GPM, LPM, m3/hr Totalized Flow: 0 - 9,999,999 Gallons;
37,850,000 Liters; 37,850 m3
Accuracy: ±1% (±1.5% from 3000 to 4000 Hz) Repeatability: ±1%
RECOMMENDED SENSORS
+GF+ Signet 515 Rotor-X Flow sensor Model
515/8510-XX (PN P51530-PO)
Fluidyne Flow Sensor Model 2300A
(PN Hydro-Flow-2300-A-10-5R-3-1-1)
Consult factory for other pulse type sensor compatibility.
FREE AND TOTAL CHLORINE (Code -24)
FLOW
(Standard on all models or stand alone, Code -23 and/or -33)
S2 12.34 GPM
S2 47.25K Gal
12.34 ppm
26.3 C 8.34pH
Page 15
7
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
When used with an oxygen permeable membrane­covered amperometric sensor, display choices are ppb or ppm dissolved oxygen or % saturation. Because the permeability of the membrane is a func­tion of temperature, a correction is necessary when the sensor is used at a temperature different from the one at which it was calibrated. The Solu Comp II automatically applies the temperature correction fac­tor. The process temperature is measured by an RTD in the sensor. Calibrating the analyzer is as simple as exposing the sensor to air and keying in the baromet­ric pressure. If removing the sensor from the process is impractical, the analyzer can also be calibrated against a standard instrument. Solubility correction factors for liquids containing high concentrations of electrolytes can be registered into the analyzer. The Solu Comp II automatically calculates ppb/ppm dis­solved oxygen taking into account the high salt con­centration.
PERFORMANCE SPECIFICATIONS
Measurement Range: 0-20 ppm (mg/L) dissolved
oxygen; 0- 250% saturation
Resolution: 0.01 ppm; 0.1 ppb for 499A TrDO sensor
(when O2<1.00 ppm); 0.1%
Temperature Correction for Membrane Permeability:
Automatic (with Pt100 RTD in sensor) or manual 0-50°C. Can be disabled if desired.
Input filter: 1- 255 samples
RECOMMENDED SENSORS
Model 499A DO Dissolved Oxygen Sensor Model 499A TrDO Trace Dissolved Oxygen Sensor Model Hx438 Steam Sterilizable Dissolved Oxygen
Sensor
Model Gx438 Steam Sterilizable Dissolved Oxygen
Sensor
Model Bx438 Steam Sterilizable Dissolved Oxygen
Sensor
DISSOLVED OXYGEN (Code -25)
For use with an ozone permeable membrane-covered amperometric sensor. Because the permeability of the membrane is a function of temperature, a correction is necessary when the sensor is used at a temperature different from the one at which it was calibrated. The Solu Comp II automatically applies the temperature correction factor. The process temperature is meas­ured by an RTD in the sensor. The Solu Comp II is calibrated taking a measurement of the ozone level in the process by an independent chemical method and setting the display equal to the measured value. An input filter allows the user to configure the analyzer for rapid response of low noise. The low noise option is recommended for samples containing less than 0.1 ppm dissolved ozone.
PERFORMANCE SPECIFICATIONS
Measurement Range: 0-10 ppm (mg/L) Resolution: 0.001 ppm dissolved ozone Temperature Correction for Membrane Permeability:
Automatic (with Pt100 RTD in sensor) or manual 0-35°C. Can be disabled if desired.
Input filter: time constant 1 - 999 sec
RECOMMENDED SENSOR
Model 499A OZ Dissolved Ozone Sensor
LOOP SPECIFICATIONS WITH A MODEL
499A OZ SENSOR
Loop Accuracy: ±5% of reading or ± 3 ppb at 25°C,
whichever is greater
Repeatability: ±2% of reading at a constant tempera-
ture
DISSOLVED OZONE (Code -26)
10.34 ppm
29.3 C 12.34mA
10.34 ppm
29.3 C 12.34mA
Page 16
8
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
1.3 ORDERING INFORMATION
The Solu Comp II analyzers offer the choice of single or dual sensor input with measurement choices of pH/ORP, conductivi-
ty/resistivity, toroidal conductivity, flow, chlorine, dissolved oxygen, and dissolved ozone. See combination guide (on the fol­lowing page) for valid combinations. Standard features include two isolated outputs, three alarm relays, customizable two-line display, and temperature correction.
MODEL 1055 SOLU COMP II ANALYZER
CODE MEASUREMENT 2 (Optional)
30 Contacting Conductivity 31 Toroidal Conductivity 32 pH/ORP 33 Flow
CODE FIELD-COMMISSIONED SUITES (Optional) see tables below
S1 Suite 1 - Field Commissioned Measurement
(basic)
S1A Suite 1 - Field Commissioned Measurement
(includes amperometric)
S2 Suite 2 - Field Commissioned Measurement
(basic)
S2A Suite 2 - Field Commissioned Measurement
(includes amperometric)
CODE OPTIONAL
68 UL Approval
CODE POWER
01 115/230 Vac, 50/60 Hz 02 24 Vdc
CODE MEASUREMENT 1 (Required Selection)
20 Contacting Conductivity 21 Toroidal Conductivity 22 pH/ORP 23 Flow 24 Chlorine 25 Dissolved Oxygen 26 Ozone
CODE MOUNTING
10 Panel mounting enclosure 11 Pipe/Surface mounting enclosure
(Pipe mounting requires accessory kit PN 23820-00)
MODEL 1055 SOLU COMP II ANALYZER
CODE POWER
01 115/230 Vac, 50/60 Hz 02 24 Vdc
CODE MOUNTING
10 Panel mounting enclosure 11 Pipe/Surface mounting enclosure
(Pipe mounting requires accessory kit PN 23820-00)
CODE OPTIONAL
DM Dual Measurement
CODE OPTIONAL
68 UL Approval
Field Commisssioned Suites option offers the user the ability to commission the Solu Comp II to any valid measurement combination. This feature provides the benefit of a reduction in the number of spare instruments required to meet emergency inventory needs. Please refer to the Suites tables (on the following page) for valid measurement combinations. Suites include a complete set of instrument wiring labels.
Page 17
9
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
COMBINATION GUIDE
* For D.O. sensors with 22k thermistor,
use Suite 1 only.
Page 18
10
MODEL SOLU COMP II SECTION 1.0
DESCRIPTION AND SPECIFICATIONS
ACCESSORIES (Weights are rounded up to nearest whole lb or 0.5 kg)
PART NUMBER DESCRIPTION WEIGHT SHIPPING WT.
23820-00 Pipe mounting kit, includes U-bolts, mounting bracket, nuts, 2 lb (1.0 kg) 4 lb (2.0 kg)
washers, and screws (complete)
23554-00 Gland fittings, PG 13.5, 5 per package 1 lb (0.5 kg) 2 lb (1.0 kg)
9240048-00 Tag, stainless steel (specify marking) 1 lb (0.5 kg) 1 lb (0.5 kg)
pH INPUT
9210012 Buffer Solution, 4.01 pH, 16 oz. 1 lb (0.5 kg) 2 lb (1.0 kg)
9210013 Buffer Solution, 6.86 pH, 16 oz. 1 lb (0.5 kg) 2 lb (1.0 kg)
9210014 Buffer Solution, 9.18 pH, 16 oz. 1 lb (0.5 kg) 2 lb (1.0 kg)
CONDUCTIVITY INPUT
SS-1 Conductivity Standard, 1409 µS/cm at 25°C, 1 quart (945 mL) 2 lb (1.0 kg) 4 lb (2.0 kg)
SS-1A Conductivity Standard, 1409 µS/cm at 25°C, 1 gallon (3785 mL) 9 lb (4.0 kg) 11 lb (5.0 kg)
SS-5 Conductivity Standard, 1000 µS/cm at 25°C, 1 quart (945 mL) 2 lb (1.0 kg) 4 lb (2.0 kg)
SS-5A Conductivity Standard, 1000 µS/cm at 25°C, 1 gallon (3785 mL) 9 lb (4.0 kg) 11 lb (5.0 kg)
SS-6 Conductivity Standard, 200 µS/cm at 25°C, 1 quart (945 mL) 2 lb (1.0 kg) 4 lb (2.0 kg)
SS-6A Conductivity Standard, 200 µS/cm at 25°C, 1 gallon (3785 mL) 9 lb (4.0 kg) 11 lb (5.0 kg)
SS-7 Conductivity Standard, 5000 µS/cm at 25°C, 1 quart (945 mL) 2 lb (1.0 kg) 4 lb (2.0 kg)
SS-7A Conductivity Standard, 5000 µS/cm at 25°C, 1 gallon (3785 mL) 9 lb (4.0 kg) 11 lb (5.0 kg)
Page 19
11
SECTION 2.0.
INSTALLATION
MODEL SOLU COMP II SECTION 2.0
INSTALLATION
2.1 UNPACKING AND INSPECTION
2.2 INSTALLATION
Type of Mounting Section
Panel 2.2.2
Pipe 2.2.3
Surface 2.2.4
2.1 UNPACKING AND INSPECTION
Inspect the shipping container. If it is damaged, contact the shipper immediately for instructions. Save the box. If there is no apparent damage, unpack the container. Be sure all items shown on the packing list are present. If items are missing, notify Rosemount Analytical immediately.
2.2 INSTALLATION
2.2.1 General Information
1. Although the analyzer is suitable for outdoor use, do not install it in direct sunlight or in areas of extreme tem­peratures.
2. Install the analyzer in an area where vibrations and electromagnetic and radio frequency interference are min­imized or absent.
3. Keep the analyzer and sensor wiring at least one foot from high voltage conductors. Be sure there is easy access to the analyzer.
4. AC power and relay wiring should not enter via top conduit openings and should be kept separated from other wiring in the analyzer after installation.
5. The analyzer is suitable for panel, pipe, or surface mounting. Refer to the table below.
6. See Section 3.1 for removal of conduit knockouts.
7. To reduce the likelihood of stress on wiring connections, the hinged front panel (-11 models) shall not be removed from the base during wiring installation, and there shall be sufficient wire leads to avoid stress on con­ductors.
8. For UL-approved models (-68), the clear wiring shield must be installed prior to operation.
Page 20
12
MODEL SOLU COMP II SECTION 2.0
INSTALLATION
FIGURE 2-1. Panel Mount Installation
Access to the wiring terminals is through the rear cover. Four screws hold the cover in place.
2.2.2 Panel Mounting.
MILLIMETER
INCH
Page 21
MODEL SOLU COMP II SECTION 2.0
INSTALLATION
FIGURE 2-2. Pipe Mount Installation
The front panel is hinged at the bottom. The panel swings down for access to the wiring terminals.
2.2.3 Pipe Mounting.
MILLIMETER
INCH
13
Page 22
MODEL SOLU COMP II SECTION 2.0
INSTALLATION
14
FIGURE 2-3. Surface Mount Installation
The front panel is hinged at the bottom. The panel swings down for access to the wiring terminals.
2.2.4 Surface Mounting.
MILLIMETER
INCH
Page 23
15
3.2 POWER, ALARM, OUTPUT, AND SENSOR CONNECTIONS
The Solu Comp II is available in two mounting configurations.The positions of the power, alarm, output, and sen­sor terminal blocks are different in each. Refer to the table to find the correct drawing.
For best EMI/RFI protection use shielded output signal cable enclosed in an earth-grounded metal conduit. Connect the shield to earth ground at termi­nal 4 on TB1.
AC wiring should be 14 gauge or greater. Provide a switch or breaker to disconnect the analyzer from the main power supply. Install the switch or breaker near the analyzer and label it as the disconnecting device for the analyzer.
Keep sensor and output signal wiring separate from power wiring. Do not run sensor and power wiring in the same conduit or close together in a cable tray.
Refer to the sensor manual or wiring sheet to identify the sensor wire colors and functions.
MODEL MOUNTING POWER FIGURE
1055pH-01-10 Panel 115/230 Vac 3-2 1055pH-02-10 24 Vdc 3-3 1055pH-01-11 Surface/Pipe 115/230 Vac 3-4 1055pH-02-11 24 Vdc 3-5
WARNING: RISK OF ELECTRICAL SHOCK
AC connections and grounding must be in compliance with UL 508 or local electrical code. DO NOT apply power to the analyzer until all electrical connections are verified and secure.
SECTION 3.0.
WIRING
3.1 PREPARING CONDUIT OPENINGS
3.2 POWER, ALARM, OUTPUT, AND SENSOR CONNECTIONS
MODEL SOLU COMP II SECTION 3.0
WIRING
3.1 PREPARING CONDUIT OPENINGS
The number of conduit openings and the location depend on the model.
Conduit openings accept 1/2-inch conduit fittings or PG 13.5 cable glands. To keep the case watertight, block unused openings with NEMA 4X or IP65 conduit plugs.
NOTE
Use watertight fittings and hubs that comply with the requirements of UL514B. Connect the conduit hub to the conduit before attaching the fitting to the analyzer (UL508-
26.16).
Figure 3-1 shows how to remove the knockouts. The knockout grooves are on the outside of the case. Place the screwdriver blade on the inside of the case and align it approximately along the groove. Rap the screwdriver sharply with a hammer until the groove cracks. Move the screwdriver to an uncracked portion of the groove and continue the process until the knockout falls out. Use a small knife blade to remove the flash from the inside of the hole.
FIGURE 3-1. Removing the Knockouts
Model Description Conduit openings 1055-10 panel mount two open, three knockouts 1055-11 surface or pipe mount three open, no knockouts
Page 24
16
MODEL SOLU COMP II SECTION 3.0
WIRING
FIGURE 3-2. Wiring Connections for Solu Comp II Model 1055-01-10
(Panel Mount with 115/230 Vac Power)
FIGURE 3-3. Wiring Connections for Solu Comp II Model 1055-02-10
(Panel Mount with 24 Vdc Power)
Page 25
MODEL SOLU COMP II SECTION 3.0
WIRING
FIGURE 3-5. Wiring Connections for Solu Comp II Model 1055-02-11
(Surface/Pipe Mounting with 24 Vdc Power)
FIGURE 3-4. Wiring Connections for Solu Comp II Model 1055-01-11
(Surface/Pipe Mounting with 115/230 Vac Power)
17
Page 26
18
MODEL SOLU COMP II SECTION 4.0
DISPLAY AND OPERATION
SECTION 4.0
DISPLAY AND OPERATION
4.1 DISPLAY
4.2 KEYPAD
4.3 PROGRAMMING AND CALIBRATING THE SOLU COMP II - TUTORIAL
4.4 SECURITY
4.5 USING HOLD
4.1. DISPLAY
The Solu Comp II has a two-line display. The display can be customized to meet user requirements (see Section 5.11). Figure 4-1 shows some of the displays available during normal operation. View A is the default screen for a single sen­sor. View B is the default screen for dual sensors.
The Solu Comp II has information screens that supplement the data in the main display. Press or to view the information screens. The last informa-
tion screen is the software version.
During calibration and programming, key presses cause different displays to appear. The displays are self-explanato­ry and guide the user step-by-step through the procedure.
4.2 KEYPAD
Figure 4-2 shows the Solu Comp II key­pad.
FIGURE 4-1. Displays During Normal Operation
Screen A shows pH, temperature, and current output for sensor 1. Screen B shows pH for sensors 1 and 2. Although screens A and B are the most useful, other screens can be selected. For example, screen C shows the pH, temperature, and glass and reference impedance for sensor 1. If screen C were for sensor 2, S2 would appear in the display. See Section
5.9 for more details.
FIGURE 4-2. Solu Comp II Keypad
Four arrow keys move the cursor around the screen. A blinking word or numeral show the position of the cursor. The arrow keys are also used to change the value of a numeral. Pressing ENTER stores numbers and set­tings and moves the display to the next screen. Pressing EXIT returns to the previous screen without storing changes. Pressing MENU always causes the main menu screen to appear. Pressing MENU followed by EXIT causes the main display to appear.
Page 27
19
MODEL SOLU COMP II SECTION 4.0
DISPLAY AND OPERATION
4.3 PROGRAMMING AND CALIBRATING THE SOLU COMP II
- TUTORIAL
Setting up and calibrating the Solu Comp II is easy. The following tutorial describes how to move around in the programming menus. For practice, the tutorial also describes how to assign conductivity values to the 4 and 20 mA outputs for sensor 1.
1. If the MENU screen (shown at the left) is not already showing, press
MENU. Calibrate is blinking, which means the cursor is on Calibrate.
2. To assign pH values to current outputs, the Program sub-menu must be open. Press . The cursor moves to Program (Program blinking). Press ENTER. Pressing ENTER opens the Program sub-menu.
3. The Program sub-menu permits the user to set outputs, alarms, auto­matic or manual temperature compensation, and a security code. When the sub-menu opens, Outputs is blinking, which means the cursor is on Outputs. Press or (or any arrow key) to move the cursor around the display. Move the cursor to >> and press ENTER to cause a second screen with more program items to appear. There are three screens in the Program menu. Pressing >> and ENTER in the third screen causes the display to return to the first screen (Outputs, Alarms, Measurement).
4. For practice, assign pH values to the 4 and 20 mA outputs for sensor 1. Move the cursor to Outputs and press ENTER.
5. The screen shown at left appears. The cursor is on Output Range (blink­ing). Output range is used to assign values to the low and high current outputs. Press ENTER.
6. The screen shown at left appears. The Solu Comp II has two outputs, out­put 1 and output 2. Move the cursor to the desired output and press ENTER. For purposes of the example, choose Output 1.
7. The screen shown at left appears. Out1 S1 in the top line means output 1 (Out1) is assigned to sensor 1 (S1). Either output can be assigned to either sensor (sensor and output assignments are made under the Output Configure menu shown in step 5). Use the Out1 S1 Range? screen to assign a pH value to the 4 mA output.
a. Use the arrow keys to change the pH to the desired value. Press
or to move the cursor from digit to digit. Press or to increase or decrease the value of the digit. Holding or down causes the numeral to continuously scroll up or down.
b. To move the decimal point, press or until the cursor is on the
decimal point. Press to move the decimal point to the right. Press
to move the decimal point to the left.
c. Press ENTER to store the setting.
8. The screen shown at left appears. Use this screen to assign a full scale pH value to the 20 mA output. Use the arrow keys to change the pH to the desired value. Press ENTER to store the setting.
9. The screen shown at left appears. To assign pH values to the low and high currents for output 2, select Output 2 and follow the prompts.
10. To return to the main menu, press MENU. To return to the main display press MENU then EXIT, or press EXIT repeatedly until the main display appears. To return to the previous display press EXIT.
NOTE
To store values or settings, press ENTER before pressing EXIT.
CCaalliibbrraattee
Hold
Program Display
Calibrate Hold
PPrrooggrraamm
Display
OOuuttppuuttss
Alarms
Measurement >>
OOuuttppuutt RRaannggee
Output Configure
Output Range?
OOuuttppuutt11
Output2
Out1 S1 Range?
4mA
00
.00pH
Out1 S1 Range?
20mA
11
4.00pH
Output Range?
OOuuttppuutt11
Output2
Page 28
MODEL SOLU COMP II SECTION 4.0
DISPLAY AND OPERATION
1. If a security code has been programmed, pressing MENU causes the security screen to appear.
2. Enter the three-digit security code.
3. If the entry is correct, the main menu screen appears. If the entry is incor­rect, the Invalid Code screen appears. The Enter Security Code screen reappears after 2 seconds.
Enter Security
Code
000000
Invalid Code
Calibrate
HHoolldd
Program Display
Hold Outputs and
Alarms?
YYeess
No
20
4.4 SECURITY
4.4.1 How the Security Code Works
Use the security code to prevent accidental or unwanted changes to program settings, displays, and calibration.
4.4.2 Bypassing the Security Code
Enter 555. The main menu will open.
4.4.3 Setting a Security Code
See Section 5.6.
4.5 USING HOLD
4.5.1 Purpose
The analyzer output is always proportional to measured pH. To prevent unwanted alarms and improper operation of control systems or dosing pumps, place the analyzer in hold before removing the sensor for calibration and
maintenance. Be sure to remove the analyzer from hold once calibration is complete. During hold, both outputs remain at the last value. Once in hold, the analyzer remains there indefinitely. While in hold, the screen shown to the left appears periodically.
HHoolldd
4.5.2 Using the Hold Function
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Hold.
2. The Hold Outputs and Alarms ? screen appears. Choose Yes to place the analyzer in hold. Choose No to take the analyzer out of hold.
3. The main display screen will appear.
Page 29
21
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
SECTION 5.0
PROGRAMMING THE ANALYZER
5.1 GENERAL
5.2 CHANGING STARTUP SETTINGS
5.3 CONFIGURING AND RANGING THE OUTPUTS
5.4 CONFIGURING ALARMS AND ASSIGNING SETPOINTS
5.5 SELECTING THE TYPE OF MEASUREMENT AND ACTIVATING SOLUTION TEMPERATURE CORRECTION
5.6 CHOOSING TEMPERATURE UNITS AND MANUAL OR AUTOMATIC TEM­PERATURE COMPENSATION
5.7 SETTING A SECURITY CODE
5.8 NOISE REJECTION
5.9 SINGLE SENSOR OR DUAL SENSOR INPUT
5.10 RESETTING FACTORY DEFAULT SETTINGS
5.11 SELECTING A DEFAULT SCREEN, LANGUAGE, AND SCREEN CONTRAST
5.1 GENERAL
This section describes how to do the following:
1. configure and assign values to the current outputs
2. configure and assign setpoints to the alarm relays
3. choose pH, ORP, or redox
4. choose temperature units and manual or automatic temperature compensation
5. set a security code
6. tell the analyzer the frequency of the ac power (needed for optimum noise rejection)
7. tell the analyzer the number of sensors being used
8. reset the analyzer to factory calibration and default settings
9. select a default display screen
Default settings are shown in Table 5-1 on the following page. To change a default setting, refer to the section list­ed in the table. To reset default settings, see Section 5.10.
5.2 CHANGING STARTUP SETTINGS
When the Solu Comp II is powered up for the first time, startup screens appear. The screens prompt the user to identify the number of sensors being used and whether pH, ORP, or redox is being measured. If incorrect settings were entered at startup, enter the correct settings now. To change the number of sensors refer to Section 5.9. To change the measurement, refer to Section 5.5.
FOR BEST RESULTS, ENTER THE NUMBER OF SENSORS BEING USED (SECTION 5.9) AND WHETHER pH, ORP, OR REDOX IS BEING MEASURED (SECTION 5.5) BEFORE MAKING OTHER PROGRAM SETTINGS.
Page 30
22
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
TABLE 5-1. DEFAULT SETTINGS
1. SENSOR-OUTPUT ASSIGNMENTS (pH, ORP, or redox is selected during Quick Start)
6. MISCELLANEOUS SETTINGS
Section
Language English 5.11
Hold off 4.5
Security code 000 (no security code) 5.7
ac power frequency 60 Hz 5.8
5. TEMPERATURE RELATED SETTINGS
Section
Units °C 5.6
Automatic temperature compensation On 5.6
Solution temperature correction Off 5.5
Isopotential pH 7.00 5.5
3. OUTPUT RANGES (pH, ORP, or redox is selected during Quick Start)
Measurement Range Section
pH 0 to 14 5.3
ORP/Redox -1400 to 1400 mV 5.3
Temperature 0 to 100°C 5.3
Sensor(s) Output 1 Output 2 Section
Single sensor pH/ORP/Redox Temperature 5.3 and 5.9
Dual sensor pH/ORP/Redox for sensor 1 pH/ORP/Redox for sensor 2 5.3 and 5.9
2. OTHER OUTPUT SETTINGS
Output Dampening 0 or 4 mA Mode Section
1 off 4 linear 5.3
2 off 4 linear 5.3
4. ALARM CONFIGURATION AND SETPOINTS
Alarm
1 2 3 Section
Assigned to Sensor 1 Sensor 1 (note) Fault 5.4
High or low High High NA 5.4
Deadband 0 0 NA 5.4
Setpoint (pH) 14 (high); 0 (low) 14 (high); 0 (low) NA 5.4
Setpoint (ORP/Redox) 1400 mV (high); -1400 mV (low) 1400 mV (high); -1400 mV (low) NA 5.4
Note: For dual sensor input, alarm 2 is assigned to sensor 2.
Page 31
23
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.3 CONFIGURING AND RANGING THE OUTPUTS.
5.3.1 Purpose
The Solu Comp II accepts inputs from two pH or ORP sensors and has two current outputs. This section describes how to configure and range the outputs. CONFIGURE THE OUTPUTS FIRST.
1. Configuring an output means
a. Selecting either a 4-20 mA or 0-20 mA output,
b. Assigning a sensor and a measurement (pH, ORP, or redox potential) to output 1 and output 2,
c. Turning on or turning off output current dampening.
d. Choosing a linear or logarithmic output.
2. Ranging the outputs means assigning values to the low (0 or 4 mA) and high (20 mA) outputs.
5.3.2 Definitions
1. CURRENT OUTPUTS. The analyzer provides either a continuous 4-20 mA or 0-20 mA output current directly proportional to pH, ORP, redox potential, or temperature. The low and high current outputs can be set to any value in the table.
Measurement Range Recommended Range
pH 0 to 14 NA
ORP/Redox -2000 to 2000 mV NA
Temperature -99 to 999°C or °F -5 to 200°C
2. ASSIGNING OUTPUTS. Figure 5-1 shows the ways in which the outputs can be assigned.
3. DAMPEN. Output dampening smooths out noisy readings. It also increases the response time of the output. With output dampening the time to reach 63% of final reading following a step change is 5 sec. Output damp­ening does not affect the response time of the display.
4. MODE. The current output can be made directly proportional to the displayed value (linear mode) or directly proportional to the common logarithm of the displayed value (log mode).
FIGURE 5-1. Assigning Outputs 1 and 2
Page 32
24
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.3.3. Procedure: Configure Outputs.
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose Outputs.
3. Choose Output Configure.
4. Choose Output1 or Output2.
5. Choose Sensor1 or Sensor2. Either sensor can be assigned to either
output.
6. Choose Measurement or Temp . The output will be pH (or Redox or ORP) if Measurement is selected or the temperature if Temp is select- ed.
7. Make the appropriate settings:
a. Choose 4-20 mA or 0-20 mA.
b. Choose Yes or No for output dampening.
c. Choose Linear or Log output.
8. The display returns to the Output Config? screen. Select the other out­put or press EXIT to return to the previous screen. To return to the main display, press MENU followed by EXIT.
5.3.4. Procedure: Assigning Values to the Low and High Current Outputs (Output Ranging)
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose Outputs.
3. Choose Output Range. Choose Output1 or Output2.
4. Make the appropriate settings.
a. Assign a value to the low current (0 mA or 4 mA) output.
b. Assign a value to the high current (20 mA) output.
5. The display returns to the Output Range screen. Select the other output or press EXIT to return to the previous screen. To return to the main dis­play, press MENU followed by EXIT.
Calibrate Hold
PPrrooggrraamm
Display
Output Config?
OOuuttppuutt11
Output2
OutM is for?
SSeennssoorr11
Sensor2
OutM is for?
MMeeaassuurreemmeenntt
Temp
Output Range
OOuuttppuutt CCoonnffiigguurree
OOuuttppuuttss
Alarms
Measurement >>
Calibrate Hold
PPrrooggrraamm
Display
OOuuttppuutt RRaannggee
Output Configure
OOuuttppuuttss
Alarms
Measurement >>
Page 33
25
Alarm relays are single pole-double throw (SPDT). When an alarm is activated, the coil is energized.
When an alarm activates, AL1, AL2, or AL3 (as appropriate) appears periodically in the display.
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.4 CONFIGURING ALARMS AND ASSIGNING SETPOINTS
5.4.1 Purpose
This section describes how to do the following:
1. assign an alarm relay to a sensor,
2. set the alarm logic to high or low,
3. assign values to the alarm setpoints,
4. set the alarm deadbands.
ALARM RELAYS MUST BE CONFIGURED BEFORE ASSIGNING SETPOINTS.
5.4.2 Definitions
1. ASSIGNING ALARMS. There are three alarms (AL1, AL2, and AL3). Alarms 1 and 2 can be assigned to any sensor. For example, AL1 and AL2 can be assigned to sensor 1 with, perhaps, one alarm configured as a high alarm and the other as a low alarm, and AL3 can be assigned to sensor 2. Alarms are for pH, ORP, redox, or temperature. Alarm 3 can be assigned to either sensor or used as a fault alarm. The fault alarm activates when a fault exists in a sensor or the analyzer.
2. FAULT ALARM. A fault condition exists when the Solu Comp II detects a problem with a sensor or with the ana­lyzer that is likely to cause seriously erroneous readings. If Alarm 3 was programmed as a fault alarm, the alarm 3 relay will activate. The word Fault will appear alternately in the display with the reading.
3. ALARM LOGIC, SETPOINTS, AND DEADBANDS. See Figures 5-2 and 5-3.
FIGURE 5-2. High Alarm Logic
The alarm activates when the pH exceeds the high setpoint. The alarm remains activated until the reading drops below the value determined by the deadband.
FIGURE 5-3. Low Alarm Logic
The alarm activates when the pH drops below the low setpoint. The alarm remains activated until the reading increases above the value determined by the deadband.
Page 34
26
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.4.3 Procedure: Configuring Alarms
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose Alarms.
3. Choose Alarm Configure.
4. Choose Alarm 1 (AL1), Alarm 2 (AL2), or Alarm 3 (AL3).
5. For AL1 or AL2
a. Choose Sensor 1 or Sensor 2. For a single input configuration, the
Sensor 1 Sensor 2 screen does not appear.
b. Choose Measurement or Temp.
c. Choose High or Low.
d. Set the alarm Deadband.
6. The display returns to the Alarm Configure? screen. Select another
alarm or press EXIT to return to the previous screen. To return to the main display, press MENU followed by EXIT.
7. For AL3
a. Choose Sensor1, Sensor2, or Fault.
b. For Sensor1, select High or Low and set the deadband.
c. Choosing Fault means AL3 will activate when a sensor or analyzer
fault exists. There is no user setting to make.
8. The display returns to the Alarm Configure? screen. Select another
alarm or press EXIT to return to the previous screen. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
PPrrooggrraamm
Display
Alarm Setpoints
AAllaarrmm CCoonnffiigguurree
Alarm Config?
AALL11
AL2 AL3
AL1 is for?
SSeennssoorr11
Sensor2
AL1 S1 is for?
MMeeaassuurreemmeenntt
Temp
Outputs
AAllaarrmmss
Measurement >>
AL3 is for?
FFaauulltt
Sensor1 Sensor2
Page 35
27
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.4.4 Procedure: Programming Alarm Setpoints
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose Alarms.
3. Choose Alarm Setpoints.
4. Choose Alarm 1 (AL1), Alarm 2 (AL2), or Alarm 3 (AL3).
5. The display shows the alarm selected (AL1) and the configuration. The alarm is for Sensor 1 (S1), and the logic is high. Use the arrow keys to change the alarm setpoint.
6. The display returns to the Select Alarm? screen. Select another alarm or press EXIT to return to the previous screen. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
PPrrooggrraamm
Display
AAllaarrmm SSeettppooiinnttss
Alarm Configure
Select Alarm?
AALL11
AL2 AL3
AL1 S1 Setpoint?
High
11
4.00pH
Outputs
AAllaarrmmss
Measurement >>
Page 36
28
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.5 SELECTING THE TYPE OF MEASUREMENT AND ACTIVATING SOLUTION TEMPERATURE CORRECTION
5.5.1 Purpose
This section describes how to do the following:
1. Program the Solu Comp II to measure pH, ORP, or redox potential.
2. Select a solution temperature correction.
3. Change the analyzer isopotential point.
5.5.2 Definitions
1. ORP. ORP is oxidation-reduction potential. It is the voltage difference between a noble metal (usually plat-
inum) indicator electrode and a silver/silver chloride reference electrode.
2. REDOX. Redox is redox potential. Redox potential is measured the same way as ORP. The sign of the redox
potential is the negative of ORP.
2. SIGN CONVENTION. The ORP of a solution of 0.1 M iron (II) ammonium sulfate and 0.1 M iron (III) ammoni-
um sulfate in 1 M sulfuric acid is positive. The redox potential is negative.
4. SOLUTION TEMPERATURE CORRECTION. The pH of a solution, particularly an alkaline one, is a function
of temperature. If the temperature changes, so does the pH, even though the concentration of the acid or base causing the pH remains constant. Solution temperature compensation converts the pH at the measurement temperature to the pH at a reference temperature. The Solu Comp II corrects the pH to a reference tempera­ture of 25°C.
For an accurate solution temperature correction, the exact composition of the solution must be known. The Solu Comp II has built-in temperature corrections for high purity water and for dilute solutions of a strong base. The analyzer also accepts a custom correction.
5. CUSTOM TEMPERATURE CORRECTION. The custom temperature correction has units of pH/°C. The
example shows how the analyzer uses the custom correction. Suppose the pH of the solution being measured decreases 0.022 units for every Celsius degree rise in temperature. The temperature correction is
-0.022pH/°C. If the pH at 20°C is 8.95, the corrected pH (at 25°C) is 8.95 + (-0.022)(25 - 20) or 8.84.
6. ISOPOTENTIAL pH. The isopotential pH is the pH at which the cell voltage (the cell is the pH electrode, ref-
erence electrode, and solution being measured) is independent of temperature. Most pH cells have isopoten­tial pH reasonably close to 7.00, so the Solu Comp II assumes the cell isopotential pH is 7.00. However, cer­tain specialized electrodes have isopotential pH different from 7.00.
NOTE
Do NOT change the isopotential pH of the transmitter unless you are thoroughly familiar with the role of sensor and analyzer isopotential point in pH measure­ment, OR the sensor operating instructions specifically state the isopotential pH is a value other than pH 7.00.
Page 37
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.5.3 Procedure.
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
29
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose Measurement.
3. Choose Sensor 1 or Sensor 2. For a single input configuration, the Sensor 1 Sensor 2 screen does not appear.
4. Choose pH, Redox, or ORP.
If you chose pH, do steps 5 through 9.
If you chose ORP or Redox, do step 10.
5. Choose No if a non-glass pH sensing electrode is being used.
6. Choose Soln Temp Corr or Sensor Isoptntl.
7. For Soln Temp Corr, choose Off, UltraPure, HighpH, or Custom. For Custom, enter the desired temperature coefficient.
8. For Sensor Isoptntl, enter the desired sensor isopotential pH. Do not change the sensor isopotential pH unless the sensor is known to have an isopotential pH different from 7.00.
9. The display returns to the screen shown in step 3. Choose Sensor 2 (conductivity) and follow the prompts.
10. If Redox or ORP was selected, there are no further settings to make. The display returns to the screen shown in step 3. Choose Sensor 2 (con­ductivity) and follow the prompts.
11. The display returns to the screen shown in step 3. Press EXIT to return to the previous screen. To return to the main display, press MENU followed by EXIT.
12. If TDS was selected, there are no further settings to make.The display returns to the screen shown in step 3. Press EXIT to return to the previ­ous screen. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
PPrrooggrraamm
Display
Config?
SSeennssoorr11
Sensor2
S1Measure?
ppHH
Redox ORP
S1 SolnTempCorr?
OOffff
Ultrapure >>
Sensor Isoptntl
S1:
00
7.00pH
S1 Glass Fault
Enable? Yes
NNoo
Outputs Alarms
MMeeaassuurreemmeenntt
>>
SSoollnn TTeemmpp CCoorrrr
Sensor Isoptntl
Page 38
30
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.6.3 Procedure.
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose >>.
3. Choose Temp.
4. Choose °C/F to change temperature units. Choose Live/Manual to turn on (Live) or turn off (Manual) automatic temperature compensation.
a. If °C/F is chosen, select °C or °F in the next screen. b. If Live/Manual is chosen, select Live or Manual for sensor 1 in the
next screen.
c. If Manual is chosen, enter the temperature in the next screen. The
temperature entered in this step will be used in all subsequent meas­urements, no matter what the process temperature is.
d. The display will return to the Live/Manual screen for sensor 2. Make
the desired selections for sensor 2.
Calibrate Hold
PPrrooggrraamm
Display
Config Temp?
°
CC//FF
Live/Manual
TTeemmpp
Security
#Sensors >>
Outputs Alarms
Measurement
>>>>
5.6 CHOOSING TEMPERATURE UNITS AND MANUAL OR AUTOMATIC TEMPERATURE COMPENSATION
5.6.1 Purpose
This section describes how to do the following:
1. Choose temperature display units (°C or °F).
2. Choose automatic or manual temperature compensation.
3. Enter a temperature for manual temperature compensation
5.6.2 Definitions
1. AUTOMATIC TEMPERATURE COMPENSATION. The analyzer uses a temperature-dependent factor to con-
vert measured cell voltage to pH. In automatic temperature compensation, the analyzer measures the tem­perature and automatically calculates the correct conversion factor. For maximum accuracy, use automatic temperature compensation.
2. MANUAL TEMPERATURE COMPENSATION. In manual temperature compensation, the analyzer converts
measured voltage to pH using the temperature entered by the user. It does not use the actual process tem­perature. Do NOT use manual temperature compensation unless the process temperature varies no more than about ±2°C or the pH is between 6 and 8. Manual temperature compensation is useful if the sensor tempera­ture element has failed and a replacement sensor is not available. If manual temperature correction is select­ed, the display will not show the measured temperature. It will show the manually entered value.
Page 39
31
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.8 NOISE REJECTION
5.8.1 Purpose.
For maximum noise rejection, the frequency of the ac power must be entered in the analyzer.
5.8.2. Procedure.
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose >>.
3. Choose >>.
4. Choose Noise Rejection.
5. Enter the mains frequency, 50 Hz or 60 Hz.
6. The display returns to the Noise Rejection screen. To return to the main
menu, press EXIT. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
PPrrooggrraamm
Display
NNooiissee RReejjeeccttiioonn
ResetAnalyzer >>
OOuuttppuuttss
Alarms
Measurement >>
TTeemmpp
Security
#Sensors >>
5.7 SETTING A SECURITY CODE
5.7.1 Purpose.
This section describes how to set a security code. The security code prevents program and calibration settings from accidentally being changed. Refer to Section 4.4 for additional information.
5.7.2 Procedure.
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose >>, then Security.
3. Enter a three digit security code. The security code takes effect two min­utes after the last key stroke.
4. The display returns to the security menu screen. Press EXIT to return to the previous screen. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
PPrrooggrraamm
Display
Temp
SSeeccuurriittyy
#Sensors >>
Outputs Alarms
Measurement
>>>>
Page 40
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.10 RESETTING FACTORY DEFAULT SETTINGS
5.10.1 Purpose.
This section describes how to re-install factory default values. The process also clears all fault messages and returns the display to the first quick start screen.
5.10.2. Procedure.
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose >>.
3. Choose >>.
4. Choose ResetAnalyzer.
5.
Choose Yes or No. If Yes is selected, previous settings are cleared and the Quick Start Menu appears.
Noise Rejection
ResetAnalyzer >>
Load factory
settings?
YYeess
No
OOuuttppuuttss
Alarms
Measurement >>
TTeemmpp
Security
#Sensors >>
Calibrate Hold
PPrrooggrraamm
Display
32
5.9 SINGLE SENSOR OR DUAL SENSOR INPUT
5.9.1 Purpose
The Solu Comp II accepts input from a single sensor or from two sensors. This section describes how to program the analyzer for single or dual sensors. COMPLETE THIS SECTION BEFORE DOING OTHER PROGRAMMING.
5.9.2 Procedure.
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
1. Press MENU. The main menu screen appears. Choose Program.
2. Choose >>.
3. Choose #Sensors.
4. Choose One or Tw o. Changing from Two to One will cause some set­tings to change.
NOTE
If One sensor is selected, only
S1 will be available. S2 cannot be
disabled.
5. The display returns to the # Sensors screen. To return to the main menu, press MENU. To return to the main display, press MENU followed by EXIT.
# of sensors?
One
ΤΤωωοο
OOuuttppuuttss
Alarms
Measurement >>
TTeemmpp
Security
#Sensors >>
Calibrate Hold
PPrrooggrraamm
Display
Page 41
33
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.11.2 Procedure: Selecting a Display Screen
1. Press MENU. The main menu screen appears. Choose Display.
2. Choose Default Display.
3. Press or until the desired display appears. Press ENTER. For an explanation of abbreviations, see Section 5.11.1.
4. The display returns to the screen in step 2. To return to the main menu, press MENU. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
Program
DDiissppllaayy
DDeeffaauulltt DDiissppllaayy
Language Contrst
5.11.3 Procedure: Choosing a Language
1. Press MENU. The main menu screen appears. Choose Display.
2. Choose Language.
3. Choose English, Français, Español, Deutsch, Italiano, or Portugues.
4. The display returns to the screen in step 2. To return to the main menu, press MENU. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
Program
DDiissppllaayy
Default Display
LLaanngguuaaggee
Contrast
EEnngglliisshh
Fran ais
Espa ol >>
5.11 SELECTING A DEFAULT SCREEN, LANGUAGE, AND SCREEN CONTRAST
5.11.1 Purpose
This section describes how to do the following:
1. set a default display screen
The default display screen is the screen shown during normal operation. The Solu Comp II allows the user to choose from a large number of screens. Which screens are available depends on how the analyzer was con­figured. The following is an explanation of the abbreviations used in the screens.
In the display:
i. S means sensor. S1 is sensor 1, and S2 is sensor 2. If neither S1 nor S2 appears, then the analyzer has
been configured for a single sensor input.
ii. G is glass electrode impedance, and R is reference electrode impedance.
2. select a language
3. change the screen contrast
To choose a menu item, move the cursor to the item and press ENTER.
To store a number or setting, press ENTER.
Page 42
MODEL SOLU COMP II SECTION 5.0
PROGRAMMING THE ANALYZER
5.11.2 Procedure: Changing Screen Contrast
1. Press MENU. The main menu screen appears. Choose Display.
2. Choose Contrst.
3. Press or to increase or decrease the screen contrast. As contrast increases, the number increases.
4. The display returns to the screen shown in step 2. To return to the main menu, press MENU. To return to the main display, press MENU followed by EXIT.
Calibrate Hold
Program
DDiissppllaayy
Default Display
Units
CCoonnttrrsstt
Screen Contrast:
5500
34
Page 43
35
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
SECTION 6.0
CALIBRATION
6.1 INTRODUCTION
6.2 CALIBRATING TEMPERATURE
6.3 TWO-POINT BUFFER CALIBRATION (AUTO CALIBRATION)
6.4 TWO-POINT BUFFER CALIBRATION (MANUAL CALIBRATION)
6.5 MAKING THE ANALYZER READING MATCH A SECOND INSTRUMENT (STANDARDIZATION)
6.6 ENTERING A KNOWN SLOPE
6.7 ORP CALIBRATION
6.1 INTRODUCTION
The Calibrate Menu allows the user to calibrate the pH, ORP (or redox), and temperature response of the sensor.
For pH sensors, two-point buffer calibration is standard. In auto calibration the Solu Comp II calculates the actual pH of the buffer from the nominal value entered by the user and does not accept calibration data until readings are stable. In manual calibration the user enters buffer values and judges when readings are stable. The pH reading can also be standardized, that is, forced to match the reading from a referee instrument. Finally, if the user knows the electrode slope (at 25°C), he can enter it directly.
The ORP calibration is a single-point calibration against an ORP standard.
6.2 CALIBRATING TEMPERATURE
6.2.1 Purpose
Temperature affects the measurement of pH in three ways.
1. The analyzer uses a temperature dependent factor to convert measured cell voltage to pH. Normally, a slight inaccuracy in the temperature reading is unimportant unless the pH reading is significantly different from 7.00. Even then, the error is small. For example, at pH 12 and 25°C, a 1°C error produces a pH error less than ±0.02.
2. During auto calibration, the Solu Comp II recognizes the buffer being used and calculates the actual pH of the buffer at the measured temperature. Because the pH of most buffers changes only slightly with temperature, reasonable errors in temperature do not produce large errors in the buffer pH. For example, a 1°C error caus­es at most an error of ±0.03 in the calculated buffer pH.
3. The Solu Comp II can be programmed to calculate and display pH at a reference temperature (25°C). The maximum change in solution pH with temperature is about ±0.04 pH/°C, so a 1°C temperature error does intro­duce a small error. However, the major source of error in solution temperature compensation is using an incor­rect temperature coefficient.
Temperature affects the measurement of ORP in a complicated fashion that is best determined empirically.
Without calibration the accuracy of the temperature measurement is about ±0.4°C. Calibrate the sensor/analyzer combination if
1. ±0.4°C accuracy is not acceptable
2. the temperature measurement is suspected of being in error. Calibrate temperature by making the analyzer reading match the temperature measured with a standard thermometer.
Page 44
6.2.2 Procedure
1. Remove the sensor from the process. Place it in an insulated container of water along with a calibrated ther­mometer. Submerge at least the bottom two inches of the sensor. Stir continuously.
2. Allow the sensor to reach thermal equilibrium. For some sensors, the time constant for a change in tempera­ture is 5 min., so it may take as long as 30 min. for temperature equilibration.
3. If the sensor cannot be removed from the process, measure the temperature of a flowing sample taken from a point as close to the sensor as possible. Let the sample continuously overflow an insulated container hold­ing a calibrated thermometer.
4. Change the Solu Comp II display to match the calibrated thermometer using the procedure below.
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
a. Press MENU. The main menu screen appears. Choose Calibrate.
b. Choose Sensor1 or Sensor2. For a single input configuration, the
Sensor1 Sensor2 screen does not appear.
c. Choose Temp.
d. If the analyzer was programmed in Section 5.6 to use the actual process
temperature, the screen at left will appear. To calibrate the temperature, change the number in the second line to match the temperature meas­ured with the standard thermometer. Press ENTER. The display changes to the screen in step f.
If the analyzer was programmed to use a temperature entered by the user, the screen shown in step e will appear.
e. If the analyzer was programmed in Section 5.6 to use the temperature
entered by the user, the screen at left will appear. Change the tempera­ture to the desired value, then press ENTER. The analyzer will use the temperature entered in this step in all measurements and calculations, no matter what the true temperature is.
f. The screen at left will appear. Press EXIT.
g. Choose the other sensor and enter the temperature.
h. To return to the main display, press MENU followed by EXIT.
CCaalliibbrraattee
Hold
Program Display
CalSensor1?
Measurement
TTeemmpp
CalSensor1?
Measurement
TTeemmpp
Calibrate?
Sensor1
SSeennssoorr22
Calibrate?
SSeennssoorr11
Sensor2
Live 25.0°C
CalS1
++
25.0°C
ManualTemp?
S1: +25.0°C
36
Page 45
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
6.3 TWO-POINT BUFFER CALIBRATION (AUTO CALIBRATION)
6.3.1 Purpose
1. New sensors must be calibrated before use. Regular recalibration is also necessary.
2. Use auto calibration instead of manual calibration. Auto calibration avoids common pitfalls and reduces errors.
6.3.2 Definitions
1. AUTO CALIBRATION. The analyzer recognizes the buffers and uses temperature-corrected pH values in the calibration. The table lists the buffers the Solu Comp II recognizes.
Note 1: NIST is National Institute of Standards, DIN is Deutsche Institute für Normung, JSI is Japan Standards Institute, and BSI is British Standards Institute.
Note 2: pH 7 buffer is not a standard buffer. It is a popular commercial buffer in the United States.
The Solu Comp II also measures noise and drift and does not accept calibration data until readings are sta­ble. Calibration data will be accepted as soon as the pH reading is constant to within 0.02 units for 10 sec­onds. The stability settings cannot be changed.
2. SLOPE AND OFFSET. Once the Solu Comp II suc­cessfully completes the calibration, it calculates and displays the calibration slope and offset. The slope is reported as the slope at 25°C. Figure 6-1 defines the terms.
6.3.3 Procedure
1. Obtain two buffer solutions. Ideally the buffer pH val­ues should bracket the range of pH values to be meas­ured.
2. Remove the sensor from the process liquid. If the process and buffer temperatures are appreciably dif­ferent, place the sensor in a container of tap water at the buffer temperature. Do not start the calibration until the sensor has reached the buffer temperature. Thirty minutes is usually adequate.
3. Calibrate the sensor by using the procedure on the following page.
pH at 25°C Standard(s)
(nominal pH)
1.68 NIST, DIN 19266, JSI 8802, BSI (see note 1)
3.56 NIST, BSI
3.78 NIST
4.01 NIST, DIN 19266, JSI 8802, BSI
6.86 NIST, DIN 19266, JSI 8802, BSI
7.00 (see note 2)
7.41 NIST
9.18 NIST, DIN 19266, JSI 8802, BSI
10.01 NIST, JSI 8802, BSI
12.45 NIST, DIN 19266
FIGURE 6-1. Calibration Slope and Offset
37
Page 46
38
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
a. Press MENU. The main menu screen appears. Choose Calibrate.
b. Choose Sensor 1 or Sensor 2. For a single input configuration, the
Sensor1 Sensor2 screen does not appear.
c. Choose Measurement.
d. Choose BufferCal.
e. Choose Auto.
f. Rinse the sensor with water and place it in buffer 1. Be sure the glass bulb
and reference junction are completely submerged. Swirl the sensor.
g. Choose Buffer1.
h. The screen at left is displayed until the reading is stable (<0.02 pH change
in 10 sec). When the reading is stable, the screen in step i appears. To bypass automatic stabilization, press ENTER at any time.
i. The top line shows the actual reading (S1Live). The analyzer also identifies
the buffer and displays the nominal buffer value (buffer pH at 25°C). If the displayed value is not correct, press or to select the correct value. The nominal value will change, for example, from 7.01 pH to 6.86 pH. Press ENTER.
j. The screen shown at left appears.
k. Remove the sensor from buffer 1, rinse it with water, and place it in buffer
2. Swirl the sensor. Choose Buffer2.
l. The screen at left is displayed until the reading is stable (<0.02 pH change
in 10 sec). When the reading is stable, the screen in step m appears. To bypass automatic stabilization, press ENTER at any time.
m. The top line shows the actual reading (S1Live). The analyzer also identifies
the buffer and displays the nominal buffer value (buffer pH at 25°C). If the displayed value is not correct, press or to select the correct value. The nominal value will change, for example, from 7.01 pH to 6.86 pH. Press ENTER to accept the nominal value.
n. If the calibration was successful, the analyzer will display the offset and
slope (at 25°C).
o. If the calibration was successful and if two sensors are wired to the analyz-
er, the Calibrate? screen appears. Choose the other sensor and repeat steps d through m.
p. If the slope is out of range (less than 45 mV/pH or greater than 60 mV/pH),
an error screen appears. The display then returns to step f. Repeat the cal­ibration.
q. To return to the main display, press MENU followed by EXIT.
CCaalliibbrraattee
Hold
Program Display
Calibrate?
SSeennssoorr11
Sensor2
Calibrate?
SSeennssoorr11
Sensor2
CalSensor1?
MMeeaassuurreemmeenntt
Temp
S1BufferCal?
AAuuttoo
Manual
S1AutoCal?
BBuuffffeerr11
Buffer2
S1AutoCal?
BBuuffffeerr11
Buffer2
S1 Standardize
Slope
BBuuffffeerrCCaall
S1Live 7.00pH
AutoBuf1
WWaaiitt
S1Live 7.00pH
AutoBuf1
77..0011ppHH
S1Live 7.00pH
Buf2
WWaaiitt
S1Live 7.00pH
AutoBuf2
77..0011ppHH
S1Offset 6mV
Slope 59.16 25
°C
Calibration
Error
S1AutoCal?
Buffer1
BBuuffffeerr22
Page 47
39
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
6.4 TWO-POINT BUFFER CALIBRATION (MANUAL CALIBRATION)
6.4.1 Purpose
1. New sensors must be calibrated before use. Regular recalibration is also necessary.
2. Use manual calibration if non-standard buffers are being used; otherwise, use auto calibration. Auto calibra­tion avoids common pitfalls and reduces errors.
6.4.2 Definitions
1. MANUAL CALIBRATION. In auto calibration the analyzer recognizes the buffer and uses the temperature-cor­rected pH value in the calibration. The analyzer also measures noise and drift and does not accept calibration data until readings are stable. During manual calibration, the user must judge when readings are stable and look up and enter the buffer values.
2. SLOPE AND OFFSET. Once the Solu Comp II successfully completes the calibration, it calculates and dis­plays the calibration slope and offset. The slope is reported as the slope at 25ºC. Figure 6-1 defines the terms.
6.4.3 Procedure
1. Obtain two buffer solutions. Ideally, the buffer pHs should bracket the range of pH values to be measured. Also obtain a thermometer. The pH of most buffer solutions is a function of temperature. To calibrate the sensor properly, the pH of the buffer at the measurement temperature must be entered in the analyzer.
2. Remove the sensor from the process liquid. If the process and buffer temperature are appreciably different, place the sensor in a container of tap water at the buffer temperature. Do not start the calibration until the sen­sor has reached the buffer temperature. Thirty minutes is usually adequate.
3. Calibrate the sensor using the procedure on the following page.
Page 48
40
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
a. Press MENU. The main menu screen appears. Choose Calibrate.
b. Choose Sensor 1 or Sensor 2. For a single input configuration, the
Sensor1 Sensor2 screen does not appear.
c. Choose Measurement.
d. Choose BufferCal.
e. Choose Manual.
f. Choose Buffer1.
g. Rinse the sensor with water and place it in buffer 1. Be sure the glass bulb
and junction are completely submerged. Swirl the sensor. Also place a thermometer in the buffer. Press ENTER
h. The top line shows the actual buffer reading (S1 Live). Wait until the read-
ing is stable, then note the temperature. Change the pH in the second line to the pH of the buffer at the measured temperature. Press ENTER.
i. The screen at left appears. Choose Buffer2. Rinse the sensor and ther-
mometer with water and place them in buffer 2. Be sure the bulb and junc­tion are submerged. Swirl the sensor.
j. The top line shows the actual buffer reading (S1 Live). Wait until the read-
ing is stable, then note the temperature. Change the pH in the second line to the pH of the buffer at the measured temperature. Press ENTER.
k. If the calibration was successful, the analyzer will display the offset and
slope (at 25°C).
l. If the calibration was successful and if two sensors are wired to the ana-
lyzer, the Calibrate? screen appears. Choose the other sensor and repeat steps c through j.
m. If the slope is out of range (less than 45 mV/pH or greater than 60 mV/pH),
an error screen appears. The display then returns to step g. Repeat the calibration.
n. To return to the main display, press MENU followed by EXIT.
CCaalliibbrraattee
Hold
Program Display
Calibrate?
SSeennssoorr11
Sensor2
Calibrate?
Sensor1
SSeennssoorr22
CalSensor1?
MMeeaassuurreemmeenntt
Temp
S1BufferCal?
Auto
MMaannuuaall
S1ManualCal?
BBuuffffeerr11
Buffer2
S1 Standardize
Slope
BBuuffffeerrCCaall
S1Live 7.00pH
Buf1
00
7.00pH
S1Live 10.00pH
Buf2
11
0.00pH
S1Offset 6mV
Slope 59.16 25
°C
Calibration Error!
S1ManualCal?
Buffer1
BBuuffffeerr22
Page 49
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
6.5 MAKING THE ANALYZER READING MATCH A SECOND INSTRUMENT
(STANDARDIZATION)
6.5.1 Purpose
1. The pH measured by the Solu Comp II analyzer can be changed to match the reading from a second or ref­eree instrument. The process of making the two readings agree is called standardization.
2. During standardization, the difference between the two pH values is converted to the equivalent voltage. The voltage, called the reference offset, is added to all subsequent measured cell voltages before they are con­verted to pH. If a standardized sensor is placed in a buffer solution, the measured pH will differ from the buffer pH by an amount equivalent to the standardization offset.
6.5.2 Procedure
1. Install the sensor in the process liquid.
2. Once readings are stable, measure the pH of the liquid using a referee instrument.
3. Because the pH of the process liquid may change if the temperature changes, measure the pH of the grab sample immediately after taking it.
4. For poorly buffered samples, it is best to determine the pH of a continuously flowing sample from a point as close as possible to the sensor.
5. Standardize the Solu Comp II analyzer by following the steps below.
CCaalliibbrraattee
Hold
Program Display
Calibrate?
SSeennssoorr11
Sensor2
CalSensor1?
MMeeaassuurreemmeenntt
Temp
Invalid Input!
Max: 14.00pH
S1
SSttaannddaarrddiizzee
Slope BufferCal
S1
SSttaannddaarrddiizzee
Slope BufferCal
Live 7.00pH
CalS1
00
7.00pH
a. Press MENU. The main menu screen appears. Choose Calibrate.
b. Choose Sensor1 or Sensor2. For a single input configuration, the
Sensor1 Sensor2 screen does not appear.
c. Choose Measurement.
d. Choose Standardize.
e. The top line shows the present pH reading. Change the pH reading in the
second line to match the referee instrument. Press ENTER.
f. The screen at left appears if the entered pH was greater than 14.00. The
display then returns to step e. Repeat the standardization.
g. If the entry was accepted, the screen at left appears. To verify that the
new pH was accepted, return to the main display by pressing MENU fol­lowed by EXIT.
h. To standardize the second sensor, repeat steps a through e.
i. To return to the main display, press MENU followed by EXIT.
41
Page 50
42
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
6.6 ENTERING A KNOWN SLOPE VALUE
6.6.1 Purpose
If the electrode slope is known from other measurements, it can be entered directly in the Solu Comp II analyzer. The slope must be entered as the slope at 25°C. To calculate the slope at 25°C from the slope at temperature t°C, use the equation:
slope at 25°C = (slope at t°C)
Changing the slope overrides the slope determined from the previous buffer calibration.
6.6.2 Procedure
CCaalliibbrraattee
Hold
Program Display
Calibrate?
SSeennssoorr11
Sensor2
CalSensor1?
MMeeaassuurreemmeenntt
Temp
pH Slope 25°C?
S1: 59.16mV/pH
Changing slope
overrides bufcal.
Invalid Input!
S1 Standardize
SSllooppee
BufferCal
S1 Standardize
SSllooppee
BufferCal
1. Press MENU. The main menu screen appears. Choose Calibrate.
2. Choose Sensor1 or Sensor2. For a single input configuration, the Sensor1 Sensor2 screen does not appear.
3. Choose Measurement.
4. Choose Slope.
5. The screen at left appears briefly.
6. Change the slope to the desired value. Press ENTER.
7. The slope must be between 45 and 60 mV/pH. If the value entered is out­side this range, the screen at left appears.
8. If the entry was accepted, the screen at left appears.
9. To enter the slope for the other sensor, press EXIT twice. Choose the other sensor and repeat steps 3 through 6.
10. To return to the main display, press MENU followed by EXIT.
298
t°C + 273
Page 51
MODEL SOLU COMP II SECTION 6.0
CALIBRATION
6.7 ORP CALIBRATION
6.7.1 Purpose
1. For process control, it is often important to make the measured ORP agree with the ORP of a standard solu­tion.
2. During calibration, the measured ORP is made equal to the ORP of a standard solution at a single point.
6.7.2 Preparation of ORP standard solutions
ASTM D1498-93 gives procedures for the preparation of iron (II) - iron (III) and quinhydrone ORP standards. The iron (II) - iron (III) standard is recommended. It is fairly easy to make, is not particularly hazardous, and has a shelf life of about one year. In contrast, quinhydrone standards contain toxic quinhydrone and have only an eight-hour shelf life.
Iron (II) - iron (III) standard is available from Rosemount Analytical as PN R508-16OZ. The ORP of the standard solution measured against a silver-silver chloride reference electrode is 476±20mA at 25°C. The redox potential is
-476±20mA at 25°C.
6.7.3 Procedure
CCaalliibbrraattee
Hold
Program Display
Calibrate?
SSeennssoorr11
Sensor2
CalSensorN?
MMeeaassuurreemmeenntt
Temp
Live 600mV
CalSN
++
0000mV
1. Press MENU. The main menu screen appears. Choose Calibrate.
2. Choose Sensor1 or Sensor2. For a single input configuration, the Sensor1 Sensor2 screen does not appear.
3. Choose Measurement.
4. The top line shows the actual ORP or redox potential (S1Live). Once the reading is stable, change the number in the second line to the desired value. Press ENTER.
5. The display returns to the Cal Sensor screen. Press EXIT. Choose the other sensor and repeat steps 2 through 4.
43
Page 52
44
MODEL SOLU COMP II SECTION 7.0
MAINTENANCE
SECTION 7.0
MAINTENANCE
7.1 OVERVIEW
7.2 REPLACEMENT PARTS
7.1 OVERVIEW
The Solu Comp II analyzer needs little routine maintenance. The calibration of the analyzer and sensor should be checked periodically. To recalibrate the analyzer and sensor, see Section 6.0.
Clean the analyzer case and front panel by wiping with a clean soft cloth dampened with water ONLY. Do not use solvent, like alcohol, that might cause a buildup of static charge.
7.2 REPLACEMENT PARTS
Many components of the analyzer are replaceable. Refer to the table below to find the correct parts diagram.
Model Description See Figure
1055pH-10 Panel mounting enclosure 7-1
1055pH-11 Pipe/surface mounting enclosure 7-2
Page 53
45
MODEL SOLU COMP II SECTION 7.0
MAINTENANCE
Location in Shipping
Figure 7-1 PN Description Weight
1 23823-00 Panel mounting kit, includes four brackets and 2 lb/1.0 kg
four set screws
2 note Enclosure, front, for panel mount version, includes keypad
3 33654-00 Gasket, front, for panel mount version 2 lb/1.0 kg
4 note Screw, 2-56 x 0.187 in., with integral washer
5 note Display board, LCD
6 note PCB, microprocessor
7 note Screw, self-tapping, #4 x 0.375 in.
8 note PCB, power supply, 115/230 Vac or 24 Vdc
9 note Screw, 4-40 x 0.31 in., with integral washer
10 33658-00 Gasket, rear cover, for panel mount version 2 lb/1.0 kg
11 note Enclosure cover, rear, for panel mount version, 115/230 Vac
11 note Enclosure cover, rear, for panel mount version, 24 Vdc
12 note Self-tapping screws, #6 x 1.25 in.
TABLE 7-1. Replacement Parts for Solu Comp II (Panel Mount Version)
FIGURE 7-1. Exploded View of Solu Comp II (Panel Mount Version)
Note: Information about circuit boards and size of screws and washers is for information only. Circuit boards, enclosure, display board, and screws and washers cannot be purchased from Rosemount Analytical. Shipping weights are rounded up to the nearest whole lb or 0.5 kg.
Page 54
46
MODEL SOLU COMP II SECTION 7.0
MAINTENANCE
Location in Shipping
Figure 7-2 PN Description Weight
1 note Screw, 6-32 x 1.38 in.
2 note Washer
3 note Enclosure, front, for pipe/surface mount version,
includes keypad and hinge
4 33655-00 Gasket for pipe/surface mount version 2 lb/1.0 kg
5 note Screw, 2-56 x 0.187 in., with integral washer
6 note Display board, LCD
7 note PCB, microprocessor
8 note Self-tapping screw, #4 x 0.375 in.
9 note PCB, power supply, 115/230 Vac or 24 Vdc
10 note Screw, 4-40 x 0.31 in., with integral washer
11 note Enclosure, rear, for pipe/surface mount version,
includes standoffs and hinge brackets
not shown 23833-00 Surface mount kit; consists of four self-tapping 1 lb/0.5 kg
screws #6 x 1.75 in. and four O-rings
TABLE 7-2. Replacement Parts for Solu Comp II (Pipe/Surface Mount Version)
FIGURE 7-2. Exploded View of Solu Comp II (Pipe/Surface Mount Version)
Note: Information about circuit boards and size of screws and washers is for information only. Circuit boards, enclosure, display board, and screws and washers cannot be purchased from Rosemount Analytical. Shipping weights are rounded up to the nearest whole lb or 0.5 kg.
Page 55
47
MODEL SOLU COMP II SECTION 8.0
TROUBLESHOOTING
SECTION 8.0
TROUBLESHOOTING
8.1 OVERVIEW
8.2 TROUBLESHOOTING USING FAULT CODES
8.3 TROUBLESHOOTING WHEN NO ERROR MESSAGE IS SHOWING
8.4 SIMULATING INPUTS
8.5 SIMULATING TEMPERATURE
8.6 MEASURING REFERENCE VOLTAGE
8.1 OVERVIEW
The Solu Comp II continuously monitors itself and the sensor for faults. When the analyzer detects a fault, the word fault appears in the display alternately with the measurement. If alarm 3 was configured as a fault alarm, the alarm relay will energize. The outputs do not change during a fault condition. They continue to reflect the measured pH, ORP, or temperature. Press "to display the fault codes.
8.2 TROUBLESHOOTING USING FAULT CODES
8.2.1 Absolute Value of Measured Voltage Exceeds 2500 mV
The voltage of a pH cell is usually between 600 mV and -600 mV, and the voltage of an ORP cell is between 2000 and -2000 mV. Readings outside the range -2500 mV to 2500 mV usually indicate a problem with sensor wiring or analyzer electronics.
A. If the sensor is being installed for the first time, check the wiring connections. See Section 3.3. If a junction
box is being used, be sure to check all connections at the junction box, too.
B. If the preamplifier is in a junction box, verify that the wires supplying the power (±5 Vdc) to the preamplifier are
connected at the analyzer and junction box.
C. Verify that the sensor is completely submerged in the process liquid.
8.2.2 pH Sensitive Glass Membrane is Broken
The Solu Comp II continuously measures the impedance between the sensor solution ground and the inside of the pH-sensing electrode. If the glass membrane is intact, the impedance is normally between 10 Mand 1000 MΩ. If the membrane is cracked or broken, the impedance drops below 10 M. If the membrane is cracked or broken, the sensor must be replaced.
8.2.3 RTD for Sensor 1 or Sensor 2 Open or Shorted.
There is an open or short in the sensor RTD or wiring. A. If sensor is being installed for the first time, check the wiring connections. See Section 3.0. B. Disconnect the sensor from the analyzer and measure the resistance between the RTD lead wires. See the
sensor manual to identify the RTD leads. If there is an open or short circuit, replace the sensor.
C. If there is no open or short, check the analyzer. See Section 8.4.
Fault Code Explanation See Section
S1 or S2 Out of Range Absolute value of measured voltage exceeds 2500 mV 8.2.1 S1 or S2 Broken Glass pH sensitive glass membrane is broken 8.2.2 TC1 Open or TC2 Open RTD for sensor 1 or sensor 2 is open 8.2.3 TC1 Shorted or TC2 Shorted RTD for sensor 1 or sensor 2 is shorted 8.2.3 S1 or S2 Sense Line Open RTD sense line for sensor 1 or sensor 2 is open 8.2.4 EEPROM Failure EEPROM failure 8.2.5
Page 56
48
MODEL SOLU COMP II SECTION 8.0
TROUBLESHOOTING
8.2.4 RTD Sense Line for Sensor 1 or Sensor 2 is Open.
The Solu Comp II measures temperature using a three-wire RTD inside the sensor. See Figure 8-3. The in and return leads connect the RTD to the measuring circuit in the analyzer. A third wire, called the sense line, is con­nected to the return line. The sense line allows the analyzer to correct for the resistance of the in and return leads and to correct for changes in lead wire resistance with temperature.
A. Verify that all wiring connections are secure.
B. The analyzer can be operated with the sense line open. The measurement will be less accurate because the
analyzer can no longer correct for lead wire resistance and for changes in lead wire resistance with ambient temperature. However, if the sensor is to be used at approximately constant temperature, the lead wire resist­ance error can be eliminated by calibrating the sensor at the measurement temperature. Errors caused by changes in lead wire resistance with changes in ambient temperature cannot be eliminated.To make the error message disappear, connect the RTD sense and return terminals with a jumper.
8.2.5 EEPROM Failure.
Call the factory at (800) 854-8257.
8.3 TROUBLESHOOTING WHEN NO ERROR MESSAGE IS SHOWING.
Problem See Section
New temperature during calibration more than 2-3°C different from the live reading 8.3.1
Calibration Error warning during two-point calibration 8.3.2
Calibration Error warning during standardization 8.3.3
Invalid Input while manually entering slope 8.3.4
Sensor does not respond to known pH changes 8.3.5
Calibration was successful, but process pH is slightly different from expected value 8.3.6
Calibration was successful, but process pH is grossly wrong and/or noisy 8.3.7
Current output too low 8.3.8
Alarm relays do not operate when alarm setpoint is exceeded 8.3.9
Display is unreadable -- too faint or all pixels dark 8.3.10
8.3.1 Difference Between Solu Comp II and Standard Thermometer is Greater Than 3°C.
If an error message appears during a temperature calibration, check the following:
A. Is the standard thermometer, RTD, or thermistor accurate? General purpose liquid-in-glass thermometers, par-
ticularly ones that have been mistreated, can have surprisingly large errors.
B. Is the temperature element in the pH sensor completely submerged in the test liquid?
C. Is the standard temperature sensor submerged to the correct level?
D. Review Section 6.2.2.
Page 57
MODEL SOLU COMP II SECTION 8.0
TROUBLESHOOTING
8.3.2 Calibration Error During Two-Point Calibration
Once the two-point (manual or automatic) calibration is complete, the Solu Comp II automatically calculates the sensor slope (at 25°). If the slope is greater than 60 mV/pH or less than 45 mV/pH, the analyzer displays the Calibration Error screen and does not update the calibration. Check the following:
A. Are the buffers accurate? Inspect the buffers for obvious signs of deterioration, such as turbidity or mold
growth. Neutral and slightly acidic buffers are highly susceptible to molds. Alkaline buffers (pH 9 and greater), if they have been exposed to air for long periods, may also be inaccurate. Alkaline buffers absorb carbon diox­ide from the atmosphere, which lowers the pH. If a high pH buffer was used in the failed calibration, repeat the calibration using a fresh buffer. If fresh buffer is not available, use a lower pH buffer. For example, use pH 4 and 7 buffer instead of pH 7 and 10 buffer.
B. Was adequate time allowed for temperature equilibration? If the sensor was in a process substantially hotter
or colder than the buffer, place it in a container of water at ambient temperature for at least 20 minutes before starting the calibration. Using auto calibration avoids calibration errors caused by temperature drift. The ana­lyzer will not update readings until the drift is less than 0.02 pH over 10 seconds.
C. Were correct pH values entered during manual calibration? Using auto calibration eliminates errors caused by
improperly entering data.
D. Is the sensor properly wired to the analyzer? Check the sensor wiring including any connections in a junction
box. See Section 3.0.
E. Is the sensor dirty or coated? See the sensor instruction manual for cleaning instructions.
F. Is the sensor faulty? With the main display showing, use or to scroll through
the information screens until the electrode impedance screen (at left) is displayed. Refer to the table for an interpretation of the impedance readings.
Another way of checking for a faulty sensor is to replace it with a new one. If the new sensor can be calibrat­ed, the old sensor has failed.
G. Is the analyzer faulty? The best way to check for a faulty analyzer is to simulate pH and temperature inputs.
See Section 8.4.
8.3.3 Calibration Error during Standardization.
During standardization, the millivolt signal from the pH cell is increased or decreased to force it to agree with the pH reading from a referee instrument. A unit change in pH requires an offset of about 59 mV. The Solu Comp II limits the offset to ±1400 mV. If the standardization causes an offset greater than ±1400 mV, the analyzer will dis­play the Calibration Error screen. The standardization will not be updated. Check the following:
A. Is the referee pH meter working and properly calibrated? Check the response of the referee sensor in buffers.
B. Is the process sensor working properly? Check the process sensor in buffers.
C. Is the sensor fully immersed in the process liquid? If the sensor is not completely submerged, it may be meas-
uring the pH of the liquid film covering the glass bulb and reference element. The pH of this film may be dif­ferent from the pH of the bulk liquid.
SRef Imp 123k^
Glass Imp 123M^
REFERENCE IMPEDANCE (Ref Imp)
less than 40 k Normal reading, reference junction is clean.
between 40 and 140 k Reference junction is fouled or dirty.
greater than 140 k Reference junction is blocked or electrolyte is depleted. Sensor has failed.
GLASS IMPEDANCE (Glass Imp)
less than 10 M Glass bulb is cracked or broken. Sensor has failed.
between 10 and 1000 M Normal reading.
greater than 1000 M pH sensor may be nearing the end of its service life.
49
Page 58
50
MODEL SOLU COMP II SECTION 8.0
TROUBLESHOOTING
D. Is the sensor fouled? The sensor measures the pH of the liquid adjacent to the glass bulb. If the sensor is
heav-ily fouled, the pH of liquid trapped against the bulb may be different from the bulk liquid.
E. Has the sensor been exposed to poisoning agents (sulfides or cyanides) or has it been exposed to extreme
temperature? Poisoning agents and high temperature can shift the reference voltage many hundred millivolts. To check the reference voltage, see Section 8.6.
8.3.4 Invalid Input While Manually Entering Slope.
If the sensor slope is known from other sources, it can be entered directly into the analyzer. The Solu Comp II will not accept a slope (at 25°C) outside the range 45 to 60 mV/pH. See section 8.3.2 for troubleshooting sensor slope problems.
8.3.5 Sensor Does Not Respond to Known pH Changes.
A. Did the expected pH change really occur? If the process pH reading was not what was expected, check the
performance of the sensor in buffers. Also, use a second pH meter to verify the change.
B. Is the sensor properly wired to the analyzer?
C. Is the glass bulb cracked or broken? Check the glass electrode impedance. See Section 8.3.2.
D. Is the analyzer working properly. Check the analyzer by simulating the pH input.
8.3.6 Buffer Calibration Is Acceptable, Process pH Is Slightly Different from Expected Value.
Differences between pH readings made with an on-line instrument and a laboratory or portable instrument are nor­mal. The on-line instrument is subject to process variables, for example ground potentials, stray voltages, and ori­entation effects that may not affect the laboratory or portable instrument. To make the process reading agree with a referee instrument, see Section 6.5.
8.3.7 Calibration Was Successful, but Process pH Is Grossly Wrong and/or Noisy.
Grossly wrong or noisy readings suggest a ground loop (measurement system connected to earth ground at more than one point), a floating system (no earth ground), or noise being brought into the analyzer by the sensor cable. The problem arises from the process or installation. It is not a fault of the analyzer. The problem should disappear once the sensor is taken out of the system. Check the following:
A. Is a ground loop present?
1. Verify that the system works properly in buffers. Be sure there is no direct electrical connection between the buffer containers and the process liquid or piping.
2. Strip back the ends of a heavy gauge wire. Connect one end of the wire to the process piping or place it in the process liquid. Place the other end of the wire in the container of buffer with the sensor. The wire makes an electrical connection between the process and sensor.
3. If offsets and noise appear after making the connection, a ground loop exists.
B. Is the process grounded?
1. The measurement system needs one path to ground: through the process liquid and piping. Plastic pip­ing, fiberglass tanks, and ungrounded or poorly grounded vessels do not provide a path. A floating system can pick up stray voltages from other electrical equipment.
2. Ground the piping or tank to a local earth ground.
3. If noise still persists, simple grounding is not the problem. Noise is probably being carried into the instru­ment through the sensor wiring.
C. Simplify the sensor wiring.
1. Disconnect all sensor wires at the analyzer except pH/mV IN, REFERENCE IN, RTD IN and RTD RE­TURN. See the wiring diagrams in Section xx.xx. If the sensor is wired to the analyzer through a remote junction box containing a preamplifier, disconnect the wires at the sensor side of the junction box.
2. Tape back the ends of the disconnected wires to keep them from making accidental connections with other wires or terminals.
Page 59
MODEL SOLU COMP II SECTION 8.0
TROUBLESHOOTING
3. Connect a jumper wire between the RTD RETURN and RTD SENSE terminals (see wiring diagrams in Section 3.2). Connect a second jumper wire between the REFERENCE IN and SOLUTION GROUND ter­minals.
4. If noise and/or offsets disappear, the interference was coming into the analyzer through one of the sensor wires. The system can be operated permanently with the simplified wiring.
D. Check for extra ground connections or induced noise.
1. If the sensor cable is run inside conduit, there may be a short between the cable and the conduit. Re-run the cable outside the conduit. If symptoms disappear, there is a short between the cable and the conduit. Likely a shield is exposed and touching the conduit. Repair the cable and reinstall it in the conduit.
2. To avoid induced noise in the sensor cable, run it as far away as possible from power cables, relays, and electric motors. Keep sensor wiring out of crowded panels and cable trays.
3. If ground loops persist, consult the factory. A visit from an experienced technician may be required to solve the problem.
8.3.8 Current Output Too Low.
Load resistance is too high. Maximum load is 600 Ω.
8.3.9 Alarm Relays Do Not Work
A. Verify the relays are properly wired. B. Replace power supply PCB (PN 23818-00)
8.3.10 Display is Unreadable.
While holding down the MENU key, press or until the display has the correct contrast.
8.4 SIMULATING INPUTS
8.4.1 General
This section describes how to simulate a pH input into the Solu Comp analyzer. To simulate a pH measurement, connect a standard millivolt source to the transmitter. If the transmitter is working properly, it will accurately meas­ure the input voltage and convert it to pH. Although the general procedure is the same, the wiring details depend on the location of the preamplifier.
8.4.2 Simulating pH input when the preamplifier is in the analyzer.
1. Turn off automatic temperature correction and solution temper-
ature correction. From the Program menu, choose Temp. Then choose Live/Manual and enter 25°C. See Section 5.6 for details.
2. Disconnect the sensor and connect a jumper wire between the pH IN and REFERENCE IN terminals.
3. From the display menu choose the pH/temperature/mV screen. The measured voltage should be 0 mV and the pH should be
7.00. Because calibration data stored in the analyzer may be offsetting the input voltage, the displayed pH may not be exact­ly 7.00.
4. If a standard millivolt source is available, disconnect the jumper wire between pH IN and REFERENCE IN and connect the volt­age source as shown in Figure 8-1. Be sure to jumper the ref­erence and solution ground terminals.
FIGURE 8-1. Simulating Inputs When
the Preamplifier is in the Analyzer
51
Page 60
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MODEL SOLU COMP II SECTION 8.0
TROUBLESHOOTING
5. Calibrate the analyzer using the procedure in Section 6.3. Use 0.0 mV for Buffer 1 (pH 7.00) and -177.4 mV for Buffer 2 (pH 10.00). If the analyzer is working properly it should accept the calibration. The slope should be 59.16 mV/pH and the offset should be zero.
6. To check linearity, return to the main display and the pH/temperature/mV screen. Set the voltage source to the values shown in the table and verify that the pH and millivolt readings match the values in the table.
8.4.3 Simulating pH input when the preamplifier is in a
junction box.
The procedure is the same as described in section 8.4.2. Keep the connections between the analyzer and the junction box in place. Disconnect the sensor at the sensor side of the junction box and connect the voltage source as shown in Figure 8-2.
8.4.4 Simulating pH input when the preamplifier is in
the sensor.
The preamplifier in the sensor simply converts the high impedance signal into a low impedance signal without amplifying it. To simulate pH values, follow the procedure in Section 8.4.2.
8.5 SIMULATING TEMPERATURE
8.5.1 General.
The Solu Comp II accepts either a Pt100 or a Pt1000 RTD in a three-wire configuration. See Figure 8-3.
Voltage (mV) pH (at 25°)
295.8 2.00
177.5 4.00
59.2 6.00
-59.2 8.00
-177.5 10.00
-295.8 12.00
FIGURE 8-2. Simulating pH Input When the
Preamplifier is in the Sensor.
FIGURE 8-3. Three-Wire RTD Configuration.
Although only two wires are required to connect the RTD to the analyzer, using a third (and some­times fourth) wire allows the analyzer to correct for the resistance of the lead wires and for changes in the lead wire resistance with tempera­ture.
Page 61
MODEL SOLU COMP II SECTION 8.0
TROUBLESHOOTING
8.5.2 Simulating temperature
To simulate the temperature input, wire a decade box to the analyzer or junction box as shown in Figure 8-4.
To check the accuracy of the temperature measure­ment, set the resistor simulating the RTD to the values indicated in the table and note the temperature read­ings. The measured temperature might not agree with the value in the table. During sensor calibration an off­set might have been applied to make the measured temperature agree with a standard thermometer. The offset is also applied to the simulated resistance. The Solu Comp II is measuring temperature correctly if the difference between measured temperatures equals the difference between the values in the table to with­in ±0.1°C.
For example, start with a simulated resistance of
103.9 , which corresponds to 10.0°C. Assume the
offset from the sensor calibration was -0.3 Ω. Because of the offset, the analyzer calculates tem­perature using 103.6 . The result is 9.2°C. Now change the resistance to 107.8 , which corre­sponds to 20.0°C. The analyzer uses 107.5 to cal­culate the temperature, so the display reads 19.2°C. Because the difference between the displayed tem­peratures (10.0°C) is the same as the difference between the simulated temperatures, the analyzer is working correctly.
8.6 MEASURING REFERENCE VOLTAGE
Some processes contain substances that poison or shift the potential of the reference electrode. Sulfide is a good example. Prolonged exposure to sulfide converts the reference electrode from a silver/silver chloride electrode to a silver/silver sulfide electrode. The change in reference voltage is several hundred millivolts. A good way to check for poisoning is to compare the voltage of the reference electrode with a silver/silver chloride electrode known to be good. The reference electrode from a new sensor is best. See Figure 8-5. If the reference electrode is good, the voltage difference should be no more than about 20 mV. A poisoned reference electrode usually requires replacement.
Temp. (°C) Pt 100 (Ω) Pt 1000 (Ω)
0 100.0 1000 10 103.9 1039 20 107.8 1078 25 109.7 1097 30 111.7 1117 40 115.5 1155 50 119.4 1194 60 123.2 1232 70 127.1 1271 80 130.9 1309 85 132.8 1328 90 134.7 1347
100 138.5 1385
FIGURE 8-4. Simulating RTD Inputs.
FIGURE 8-5. Checking for a Poisoned
Reference Electrode.
Refer to the sensor wiring diagram to identify the reference leads. A laboratory silver/silver chloride
electrode can be used in place of the second sensor.
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54
MODEL SOLU COMP II SECTION 9.0
RETURN OF MATERIAL
SECTION 9.0
RETURN OF MATERIAL
9.1 GENERAL.
To expedite the repair and return of instruments, proper communication between the customer and the factory is important. Before returning a product for repair, call 1-949-757-8500 for a Return Materials Authorization (RMA) number.
9.2 WARRANTY REPAIR.
The following is the procedure for returning instruments still under warranty:
1. Call Rosemount Analytical for authorization.
2. To verify warranty, supply the factory sales order number or the original purchase order number. In the case of individual parts or sub-assemblies, the serial number on the unit must be supplied.
3. Carefully package the materials and enclose your “Letter of Transmittal” (see Warranty). If possible, pack the materials in the same manner as they were received.
4. Send the package prepaid to:
Emerson Process Management, Liquid Division Liquid Division 2400 Barranca Parkway Irvine, CA 92606
Attn: Factory Repair
RMA No. ____________
Mark the package: Returned for Repair
Model No. ____
9.3 NON-WARRANTY REPAIR.
The following is the procedure for returning for repair instruments that are no longer under warranty:
1. Call Rosemount Analytical for authorization.
2. Supply the purchase order number, and make sure to provide the name and telephone number of the individ­ual to be contacted should additional information be needed.
3. Do Steps 3 and 4 of Section 9.2.
NOTE
Consult the factory for additional information regarding service or repair.
9.1 GENERAL
9.2 WARRANTY REPAIR
9.3 NON-WARRANTY REPAIR
Page 63
WARRANTY
Seller warrants that the firmware will execute the programming instructions provided by Seller, and that the Goods manufactured or Services provided by Seller will be free from defects in materials or workmanship under normal use and care until the expira­tion of the applicable warranty period. Goods are warranted for twelve (12) months from the date of initial installation or eighteen (18) months from the date of shipment by Seller, whichever period expires first. Consumables, such as glass electrodes,
membranes, liquid junctions, electrolyte, o-rings, catalytic beads, etc., and Services are warranted for a period of 90 days from the date of shipment or provision.
Products purchased by Seller from a third party for resale to Buyer ("Resale Products") shall carry only the warranty extended by the original manufacturer. Buyer agrees that Seller has no liability for Resale Products beyond making a reasonable commercial effort to arrange for procurement and shipping of the Resale Products.
If Buyer discovers any warranty defects and notifies Seller thereof in writing during the applicable warranty period, Seller shall, at its option, promptly correct any errors that are found by Seller in the firmware or Services, or repair or replace F.O.B. point of man­ufacture that portion of the Goods or firmware found by Seller to be defective, or refund the purchase price of the defective por­tion of the Goods/Services.
All replacements or repairs necessitated by inadequate maintenance, normal wear and usage, unsuitable power sources, unsuit­able environmental conditions, accident, misuse, improper installation, modification, repair, storage or handling, or any other cause not the fault of Seller are not covered by this limited warranty, and shall be at Buyer's expense. Seller shall not be obli­gated to pay any costs or charges incurred by Buyer or any other party except as may be agreed upon in writing in advance by an authorized Seller representative. All costs of dismantling, reinstallation and freight and the time and expenses of Seller's per­sonnel for site travel and diagnosis under this warranty clause shall be borne by Buyer unless accepted in writing by Seller.
Goods repaired and parts replaced during the warranty period shall be in warranty for the remainder of the original warranty peri­od or ninety (90) days, whichever is longer. This limited warranty is the only warranty made by Seller and can be amended only in a writing signed by an authorized representative of Seller. Except as otherwise expressly provided in the Agreement, THERE ARE NO REPRESENTATIONS OR WARRANTIES OF ANY KIND, EXPRESS OR IMPLIED, AS TO MERCHANTABILITY, FIT­NESS FOR PARTICULAR PURPOSE, OR ANY OTHER MATTER WITH RESPECT TO ANY OF THE GOODS OR SERVICES.
RETURN OF MATERIAL
Material returned for repair, whether in or out of warranty, should be shipped prepaid to:
Emerson Process Management
Liquid Division
2400 Barranca Parkway
Irvine, CA 92606
The shipping container should be marked:
Return for Repair Model
_______________________________
The returned material should be accompanied by a letter of transmittal which should include the following information (make a copy of the "Return of Materials Request" found on the last page of the Manual and provide the following thereon):
1. Location type of service, and length of time of service of the device.
2. Description of the faulty operation of the device and the circumstances of the failure.
3. Name and telephone number of the person to contact if there are questions about the returned material.
4. Statement as to whether warranty or non-warranty service is requested.
5. Complete shipping instructions for return of the material.
Adherence to these procedures will expedite handling of the returned material and will prevent unnecessary additional charges for inspection and testing to determine the problem with the device.
If the material is returned for out-of-warranty repairs, a purchase order for repairs should be enclosed.
Page 64
Credit Cards for U.S. Purchases Only.
The right people, the right answers, right now.
ON-LINE ORDERING NOW AVAILABLE ON OUR WEB SITE
http://www.raihome.com
Specifications subject to change without notice.
Emerson Process Management
Liquid Division
2400 Barranca Parkway Irvine, CA 92606 USA Tel: (949) 757-8500 Fax: (949) 474-7250
http://www.raihome.com
© Rosemount Analytical Inc. 2005
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