REED Instruments R3000SD-KIT3, R3000SD-KIT2, R3000SD-KIT, R3000SD, R3000SD-NIST User manual

Data Logging pH/rH Meter
R3000SD
Instruction Manual
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Introduction ................................................................................................ 3
Product Quality ........................................................................................... 3
Safety ......................................................................................................... 4
Features ...................................................................................................... 4
Included ...................................................................................................... 4
Specications .......................................................................................... 4-5
Instrument Description ............................................................................... 6
Display Description .................................................................................... 7
Operating Instructions ........................................................................... 8-10
Power ON/OFF ...................................................................................... 8
pH or rH Modes ..................................................................................... 8
pH Measurement Mode (Manual Temperature Compensation) ............. 8
pH Measurement Mode (Automatic Temperature Compensation) ........ 9
mV Measurement Mode ......................................................................... 9
Data Hold ............................................................................................... 9
Recording Maximum and Minimum Readings .................................. 9-10
Backlight .............................................................................................. 10
Setup Mode ......................................................................................... 10-14
Formatting the SD Card (Sd F) ........................................................... 11
Setting the Time and Date (dAtE) ....................................................... 11
Setting the Data Logging Sampling Rate (SP-t) ................................. 12
Enabling/Disabling Auto Power Off (PoFF) ......................................... 12
Enabling/Disabling the Beeper (bEEP) ............................................... 12
Setting Data Decimal Format (dEC) .................................................... 13
Selecting the Temperature Unit of Measure (t-CF) ............................. 13
Setting pH manual Temperature Compensation Value ....................... 13
ESC .................................................................................................... 14
Verify Set Time and Date .................................................................... 14
Verify Sampling Rate .......................................................................... 14
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Data Logging ....................................................................................... 14-16
Data Recording Modes....................................................................... 14
Manual Data Logging Mode .......................................................... 14-15
Automatic Data Logging ..................................................................... 15
Transferring Data from the SD Memory Card to a Computer ........ 15-16
pH Calibration .....................................................................................16-17
Required Equipment for Calibration ................................................... 16
Calibration Procedure ...................................................................16-17
Clearing pH Calibration Data .............................................................. 17
Data Stream Output ................................................................................. 18
3.5mm Terminal to RS-232 Serial Connection ................................... 18
System Reset ........................................................................................... 19
Battery Replacement ................................................................................ 19
Applications .............................................................................................. 19
Accessories and Replacement Parts ..................................................19-20
Frequently Asked Questions (FAQ's) ........................................................ 20
Product Care ............................................................................................ 21
Product Warranty ..................................................................................... 21
Product Disposal and Recycling .............................................................. 21
Product Support ....................................................................................... 22
Introduction
Thank you for purchasing your REED R3000SD Data Logging pH/rH Meter. Please read the following instructions carefully before using your instrument. By following the steps outlined in this manual your meter will provide years of reliable service.
Product Quality
This product has been manufactured in an ISO9001 facility and has been calibrated during the manufacturing process to meet the stated product specications. If a certicate of calibration is required please contact the nearest authorized REED distributor or authorized Service Center. Please note an additional fee for this service will apply.
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Safety
Never attempt to repair or modify your instrument. Dismantling your product, other than for the purpose of replacing batteries, may cause damage that will not be covered under the manufacturer's warranty. Servicing should only be provided by an authorized service center.
Features
• Measures pH and rH levels in water
• Manual or automatic temperature compensation (with optional ATC probe, R3000SD-ATC)
• 3-point calibration ensures best accuracy
• Accepts pH/rH Electrodes with BNC connector
• Real time datalogger with integrated SD memory card (optional)
• User selectable sampling rate
• Easy-to-read backlit LCD display
• Data hold and Min/Max functions
• Tripod mount for long-term monitoring
• Low battery indicator and auto shut off
Included
• Soft Carrying Case
• Batteries
Specifications
Temperature
Automatic Temperature Compensation (ATC): Manual: 33.8 to 212°F (1 to 100°C) Optional ATC Probe (R3000SD-ATC): 32 to 149°F (0 to 65°C)
ORP (mV)
Measuring Range: -1999 to 1999mV Accuracy: ±(0.5% +2 dgt) Resolution: 1 mV
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pH
Measuring Range: 0.00 to 14.00 Accuracy: ±(0.02 pH +2 dgt) Resolution: 0.01 pH pH Electrode Compatibility: Any pH electrode with BNC connector
General Specifications
Display: Dual Display, LCD Backlit Display: Yes Data Hold: Yes Min: Yes Max: Yes Datalogging Capabilities: Yes Real-Time Clock and
Date Stamp: Yes Sampling Rate: Yes (1 second to 8 hours, 59 minutes
and 59 seconds) External Memory: Yes, expandable up to 16GB
with SD card (optional) Auto Shut-off: Yes (after 10 minutes/off) Kick Stand: Yes Tripod Mountable: Yes Low Battery Indicator: Yes Power Supply: 6 x AA batteries or AC Adapter (optional) Data Output: Yes (RS-232) Battery Life: Sampling Time Dependent Product Certications: CE Operating Temperature: 32 to 122°F (0 to 50°C) Storage Temperature: 14 to 140°F (-10 to 60°C) Operating Humidity Range: 10 to 80% Dimensions: 7 x 2.7 x 1.9" (177 x 68 x 45mm) Weight: 1.1lbs (489g)
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Instrument Description
1
pH/ORP Meter
A
HOLD
POWER
2
3
4
5
ESC
FUNCTION
SAMPLING
TIME
LOG/SET
SD Series Data logger
R3000SD
6
B
E
C
R
7
T
E
N
E
R
8
CHECK
9
1. LCD Display
2. POWER/Backlight Button
3. Up Button
4. TIME Button
5. SD Card Slot
6. HOLD/ESC Button
7. REC/ENTER Button
8. Down/FUNCTION Button
9. LOG/SET/SAMPLING CHECK Button
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14
15
10
11
12
16
17
10. RS-232 Output Jack
11. Reset Pin
12. Power Adapter Input Jack
13. Tripod Mounting Screw
14. Battery Cover
15. Kickstand
16. pH/rH Electrode Input (BNC) Jack
17. Temperature Probe Input Jack
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Display Description
10
3
1. pH/rH (mV) Measurement Reading
2. Date & Time Values/Temperature Measurement Reading
3. Date/Time Stamp
4. Data Logging Status Indicator
5. SD Card Status Indicator
6. Temperature Unit of Measure
7. Maximum and Minimum Indicator
8. Record Mode Indicator
9. Data Hold Indicator
10. Low Battery Indicator
6
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Operating Instructions
Prior to first use with the meter, the pH electrode should
be calibrated. Refer to the pH Calibration section
of this manual for further instructions.
Power ON/OFF
Turn the meter on by pressing the POWER button. To turn the meter off, press, hold and release the POWER button for 2 seconds. Note: This meter can be powered by either six (6) "AA" batteries or AC adapter (sold separately).
pH or ORP Modes
This meter offers pH and rH modes of measurement capable of measuring
0.00 to 14.00 pH and 0 to 1999 mV (rH).
pH measurements achieve better results when the temperature of the solution being tested is known and a temperature compensation factor is applied. This can be attained using manual or automatic temperature compensation.
For manual temperature compensation, an external temperature probe is not connected to the meter and the temperature of the solution under test is manually entered. The temperature compensation value appears on the lower part of the LCD display.
For automatic temperature compensation, an external temperature probe is connected to the meter (R3000SD-ATC) and inserted into the solution under test. The temperature compensation value will also appear on the lower part of the LCD display.
pH Measurement Mode (Manual Temperature Compensation)
1. Connect the Optional pH Electrode into the pH/rH Input BNC Jack.
2. Press the FUNCTION button to select pH mode.
3. Set the pH Manual Temperature Compensation value. Refer to Setup Mode for details.
4. Place the pH electrode into the measured solution, so that the tip of the electrode and junction are fully immersed and stir at a moderate, uniform rate. The top of the LCD will display the pH value while the bottom part of the LCD will display the setting for the manual temperature compensation value.
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pH Measurement Mode (Automatic Temperature Compensation)
1.
Connect the optional temperature probe into the temperature input jack.
2. Connect the optional pH electrode into the pH/rH input BNC jack.
3. Press the FUNCTION button to select pH mode.
4. Place both the temperature probe and pH electrode into the measured solution, so that the tip of the electrode and junction are fully immersed and stir at a moderate, uniform rate. The top of the LCD will display the pH value while the bottom part of the LCD will display the setting for the manual temperature compensation value.
Note: When measurements have been completed, be sure to store the pH electrode in its protective cap.
mV Measurement Mode
This meter has a built in mV (millivolt) measurement function, which enables you to make ion-selective, rH (oxidation-reduction potential) in the range of ±1999 mV.
1. Connect the Optional rH Electrode into pH/rH Input BNC Jack.
2. Press the FUNCTION button to select mV (rH) mode.
3. The top of the LCD will display the mV value.
Data Hold
1. While taking a measurement, press the HOLD button to freeze the current readings on the display.
2. While in this mode a HOLD symbol will appear.
3. Press the HOLD button again to resume normal operation.
Note: When the Data Hold feature is active all buttons except the POWER button are disabled.
Recording Maximum and Minimum Readings
1. Press the REC button to enter recording mode as indicated by "REC" on the LCD. The meter will now begin recording maximum and minimum readings.
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2. While in recording mode; A) Press the REC button once and the maximum value will appear
on the display as indicated by "REC MAX".
B) Press the REC button again and the minimum value will appear
on the display as indicated by "REC MIN".
C) To exit recording mode and resume normal operation, press and
hold the REC button for two seconds.
When in recording mode the POWER button is disabled
and the meter cannot be turned off.
Backlight
After powering the meter ON, the LCD Backlight will turn on automatically. Press the BACKLIGHT button to turn the LCD Backlight on or off.
Setup Mode
1. Press and hold the SET button for 2 seconds to enter Setup Mode.
2. Press the SET button continuously to scroll through the following parameters.
Parameter Description
Sd F Format the SD memory card dAtE Set the time and date SP-t Set the data logging sampling rate PoFF Enable or disable the auto-power off function bEEP Turn the beeper on or off dEC Set the decimal format (USA (20.00) or European (20,00)) t-CF Select the temperature unit of measure (°C or °F) t-SEt Set pH manual Temp. compensation value, pH only ESC Exit Setup mode
3. Once the appropriate parameter has been selected, follow the instructions below.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
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Formatting the SD Card (Sd F)
Follow steps 1 through 4 when "Sd F" appears on the LCD.
1.
Press the and buttons to select "YES" to format the card. Select "NO" to abort.
2. Press the ENTER button to conrm selection.
3. Press the ENTER button again to re-conrm.
4. The meter will format the SD card and automatically return to the Setup menu when formatting is complete.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation. It is recommended that new SD cards should be formatted prior to rst use. If the formatting process fails or if no card is inserted, the meter will display:
Setting the Time and Date (dAtE)
Follow steps 1 through 4 when "dAtE" appears on the LCD.
1. Press the and buttons to adjust the year as indicated by "YY."
2. Press the ENTER button to conrm selection.
3. Repeat steps 1 and 2 for month, day, hour, minute and seconds as indicated by (mm/dd/h/m/s).
4. Press the SET button to save the time stamp and jump to next parameter.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation. The internal clock will keep accurate time when the meter is powered off. When new batteries are installed the clock will have to be reset.
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Setting the Data Logging Sampling Rate (SP-t)
Follow steps 1 through 4 when "SP-t" appears on the LCD.
1. The sampling rate can be set from "0" seconds (manual log mode only) up to 8 hours, 59 minutes and 59 seconds.
2. Press the hours, minutes or seconds as indicated by (h/m/s).
3. Press the ENTER button to conrm each selection.
4. Press the SET button to save the selected sampling rate and jump to next parameter.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
and buttons to adjust the required sampling rate by
Enabling/Disabling Auto Power Off (PoFF)
Follow steps 1 through 3 when "PoFF" appears on the LCD.
1.
Press the and buttons to select between YES (enabled) or NO
(disabled). With the Auto Power OFF feature enabled, the meter will automatically switch OFF after 10 minutes of inactivity to preserve battery life.
2. Press the ENTER button to conrm selection.
3. Press the SET button to save and jump to next parameter.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
Enabling/Disabling the Beeper (bEEP)
Follow steps 1 through 3 when "bEEP" appears on the LCD.
1.
Press the and buttons to select between ON (enabled) or
OFF (disabled).
2. Press the ENTER button to conrm selection.
3. Press the SET button to save and jump to next parameter.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
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Setting Data Decimal Format (dEC)
Numeric formats vary in different countries. By default the meter is set to bASIC mode where a decimal point is used to separate units, (i.e. 20.00). The European format uses a comma (i.e. 20,00) to separate units. To change this setting, follow steps 1 through 3 when the "dEC" parameter appears on the LCD.
1. Press the
2. Press the ENTER button to conrm selection.
3. Press the SET button to save and jump to next parameter.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
and buttons to select between bASIC and Euro.
Selecting the Temperature Unit of Measure (t-CF)
Follow steps 1 through 3 when "t-CF" appears on the LCD.
1. Press the
2. Press the ENTER button to conrm selection.
3. Press the SET button to save and jump to next parameter.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
and buttons to select between °C and °F.
Setting pH manual Temperature Compensation Value
Ph measurements are more accurate when the temperature of the solution being tested is known. This can be achieved by applying a manual or automatic temperature compensation factor to the measurement. Please follow the steps below to manually set the pH temperature compensation value.
Follow steps 1 through 3 when "t-Set" appears on the LCD.
1. Press the solution being tested in °C or °F. By default, the meters temperature compensation factor is set to 25°C or 77°F.
2. Press the ENTER button to conrm selection.
3. Press the SET button to save and jump to next parameter.
Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
and buttons to select the select the temperature of the
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ESC
Press the SET button when "ESC" appears on the LCD to exit the Setup mode and resume normal operation. Note: At any time, you can press the ESC button to exit the Setup mode and resume normal operation.
Verify Set Time and Date
During normal operation, press the TIME button once to display the hour, minute, seconds. Press the button again to display the year, month and day.
Verify Sampling Rate
During normal operation, press the SAMPLING CHECK button to view the selected sampling rate.
Data Logging
Data Recording Modes
Manual Data Logging: Press the LOG button to manually log up to 99 readings on a SD memory card (see Manual Data Logging Mode for details).
Automatic Data Logging: Setup the meter parameters in order to automatically log data on a SD memory card. The number of data points is limited by the size of the memory card.
Note: It is recommended to use a class 4 SDHC memory card between 1 and 16Gb. Insert the SD memory card in the slot at the bottom of the meter. The card must be inserted with the label side facing the rear of the meter.
Manual Data Logging Mode
In manual mode, the LOG button is pressed to manually log a reading on the inserted SD card at any time. In order to setup the meter for manual data logging, follow steps 1 through 7 below.
1. Set the data logging sampling rate to "0" seconds.
2. Press the REC button and "REC" will appear on the LCD.
3. Press the LOG button to enter manual data logging function as indicated by "DATALOGGER".
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4. The meter will also display P-X (X = memory position number between 1 and 99).
5. Press the and buttons to select one of the 99 data memory positions in which to record.
6. Press the LOG button again to save a reading to memory. "DATALOGGER" will ash each time a data point is stored.
7. To exit manual data logging mode, press and hold the REC button 2 seconds to resume normal operation.
Automatic Data Logging Mode
In automatic mode the desired data logging sampling rate can be set between 1 second to 8 hours, 59 minutes and 59 seconds prior to recording. In order to setup the meter for automatic data logging, follow steps 1 through 5 below.
1. Press the REC button and "REC" will appear on the LCD.
2. Press the LOG button to enter automatic data logging function as indicated by "DATALOGGER".
3. The "DATALOGGER" icon will appear on the LCD and will ash every time a reading is stored.
4. To pause the data logging session press the LOG button and "DATALOGGER" will stop ashing. To resume press the LOG button again.
5. To end the current data logging session, press and hold the REC button for 2 seconds.
Transferring Data from the SD Memory Card to a Computer
1. While the meter is powered Off remove the SD memory card from the SD card slot.
2. Insert the SD memory card into the computer.
3. Open the le(s) with Excel. See sample below:
Position Date Time Ch1_Value Ch1_Unit Ch2_Value Ch2_Unit 1 19-07-10 11:00:39 3.45 pH 25 Degree_C 2 19-07-10 11:00:43 3.45 pH 25 Degree_C 3 19-07-10 11:00:47 3.52 pH 25 Degree_C 4 19-07-10 11:00:51 3.48 pH 25 Degree_C 5 19-07-10 11:00:55 3.5 pH 25 Degree_C 6 19-07-10 11:00:59 3.46 pH 25 Degree_C 7 19-07-10 11:01:03 3.45 pH 25 Degree_C 8 19-07-10 11:01:07 3.56 pH 25 Degree_C 9 19-07-10 11:01:11 3.45 pH 25 Degree_C 10 19-07-10 11:01:15 3.45 pH 25 Degree_C 11 19-07-10 11:01:19 3.45 pH 25 Degree_C 12 19-07-10 11:01:23 14 pH 30 Degree_C
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The raw data can be used to create a graph in Excel. See sample below:
pH Calibration
This meter has been manufactured for use with a pH electrode that generates 0mV at pH7.00 (177.4mV at pH4). If your pH electrode does not meet stated specications or is being used for the rst time, calibration procedures are necessary. Calibration also ensures accurate measurements. It is always recommended to carry out a two point calibration for better accuracy.
Required Equipment for Calibration
1. pH Electrode (See Accessories and Replacement Parts)
2.
pH Buffer Solutions (See Accessories and Replacement Parts)
Calibration Procedure
1. Prepare buffer solutions for calibration. It is recommended to start with calibration buffer pH 7.00 pH, followed by either pH 4.00 or pH 10.00 (whichever is nearest to the expected sample value). Use the pH 4.00 and pH 7.00 buffer solutions when measurements are expected to be on the lower side of the pH scale. Use the pH 7.00 and pH 10.00 buffer solutions when measurements are expected to be on the higher side of the pH scale.
2. Connect the optional pH electrode into the pH input jack
3. Turn the meter on by pressing the POWER button.
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4. Manually adjust the temperature compensation value to make it same as the temperature value of the pH buffer solution. Refer to the Setup Mode section of this manual for instructions. For automatic temperature compensation, plug in the optional ATC probe.
5. Rinse the electrode with distilled water to remove any residual solution.
6. Place the electrode into the pH 7.00 buffer solution, so that the tip of the electrode and junction are fully immersed in the buffer solution, and stir at a moderate, uniform rate. If using an ATC probe, both probes should be placed into the solution together.
7. When calibration has stabilized, a pH value will appear at the top of the display.
8. Press and hold both the REC and HOLD buttons until the screen displays "PH" at the top of the screen, and "CAL" on the lower part of the screen and release to enter the calibration mode.
9. Press the and buttons to scroll to pH 7.00 or whichever screen matches your buffer solution.
10. Press the Enter button to save your selection.
11. Repeat steps 5 through 10 for the pH 4.00 and pH 10.00 buffer solutions.
Clearing pH Calibration Data
1. While under normal, press and hold both the REC and HOLD buttons until the screen displays "PH" at the top of the screen, and "CAL" on the lower part of the screen and release to enter the calibration mode.
2. Press the and buttons to until "CLr" appears on the display.
3. Press the ENTER button to conrm and erase all calibration data.
4. The display will continuously blink while the calibration data is being erased.
5. When complete, the meter will resume normal operation.
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Data Stream Output
41050000000010 = Upper Value, +10 pH
4
RS-232 Mono Jack
Pin 2 (RX) Pin 4 (DTX)
Sleeve Tip
Using Terminal application, a data stream can be viewed from the RS-232 output, connect RS-232/USB cable between the product and terminal/PC and use the following setting to view the data stream.
Terminal Settings:
• Bits per second: 9600
• Data bits: 8
• Parity: None
• Stop bits: 1
Reading
Decimal Place 0-3
Positive (+) = 0, Negative (-) = 1
°C = 01, °F = 02, pH = 05, mV = 18
1 = Upper display value, 2 = Lower display value
3.5mm Terminal to RS-232 Serial Connection
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System Reset
If the meter becomes unresponsive or if the display freezes, the Reset pin can be used to reset the instrument.
1. Use a paper clip or any similar small object to press the Reset pin.
2. After pressing the Reset pin, power the meter back up by holding the POWER button for 2 seconds.
3. If resetting the meter does not resolve the issue, please return the meter to the nearest authorized REED distributor or authorized Service Center for repair.
Battery Replacement
When the low battery icon appears on the LCD, the batteries must be replaced.
1. Remove the two (2) Phillips screws on the back of the meter directly located above the top of the kickstand.
2. Remove the battery cover.
3. Replace 6 x "AA" batteries.
4. Secure the battery cover with the two (2) Phillips screws.
Applications
• Water conditioning
• General purpose pH measurement
• Aquariums
• Wastewater monitoring
• Beverage production
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Accessories and Replacement Parts
R3000SD-PH1 Professional pH Electrode R3000SD-PH2 General Purpose Electrode R3000SD-rH Professional rH Electrode R3000SD-ATC Automatic Temperature Compensation Probe R1404 pH Buffer Solution, 4.01, 500ml R1407 pH Buffer Solution, 7.0, 500ml R1410 pH Buffer Solution, 10.0, 500ml R1420 Electrode Storage Solution, 500ml R1425 Electrode Cleaning Solution, 500ml R1500 Tripod RSD-ADP-NA Power Supply, 110V RSD-ADP-EU Power Supply, 220V CA-05A Soft Carrying Case R8888 Deluxe Hard Carrying Case SD-4GB 4GB Class 4 SDHC Memory Card RSD-16GB 16GB Micro SD Memory Card w/ Adapter
Don't see your part listed here? For a complete list of all accessories and replacement parts visit your product page on www.REEDInstruments.com.
Frequently Asked Questions (FAQ's)
I cannot turn off my meter, do you know why?
Often times, the meter cannot be turned off because it is in recording mode ("REC" mode). Make sure to exit that function by holding down the
REC button before attempting to turn the meter off.
Can I set an alarm to go off at a specific temperature?
The meter does not have an alarm function.
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How long can I record for?
Battery life will depend on a number of factors:
• Quality of Battery
• Whether the beeper is ON or OFF
• Whether the backlight is ON or OFF
• Environmental Conditions during data logging
As a reference, using alkaline batteries with both the backlight and beeper on while automatic data logging at a 2 second sampling rate; the batteries lasted approx. 14 hours.
What is the exact ingredient of the rH probe storing solution?
The rH probe storing solution is made up of 30% Potassium Chloride & 70% Water.
Product Care
To keep your instrument in good working order we recommend the following:
• Store your product in a clean, dry place.
• Change the battery as needed.
• If your instrument isn't being used for a period of one month or longer
please remove the battery.
• Clean your product and accessories with biodegradable cleaner. Do not
spray the cleaner directly on the instrument. Use on external parts only.
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Product Warranty
REED Instruments guarantees this instrument to be free of defects in material or workmanship for a period of one (1) year from date of shipment. During the warranty period, REED Instruments will repair or replace, at no charge, products or parts of a product that proves to be defective because of improper material or workmanship, under normal use and maintenance. REED Instruments total liability is limited to repair or replacement of the product. REED Instruments shall not be liable for damages to goods, property, or persons due to improper use or through attempts to utilize the instrument under conditions which exceed the designed capabilities. In order to begin the warranty service process, please contact us by phone at 1-877-849-2127 or by email at info@REEDInstruments.com to discuss the claim and determine the appropriate steps to process the warranty.
Product Disposal and Recycling
Please follow local laws and regulations when disposing or recycling your instrument. Your product contains electronic components and must be disposed of separately from standard waste products.
Product Support
If you have any questions on your product, please contact your authorized REED distributor or REED Instruments Customer Service by phone at 1-877-849-2127 or by email at info@REEDInstruments.com.
Please visit www.REEDInstruments.com for the most
up-to-date manuals, datasheets, product guides and software.
Product specifications subject to change without notice. All rights reserved. Any unauthorized copying or reproduction of this manual is strictly prohibited without prior written permission from REED Instruments.
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