PCE Instruments PCE-WO2 10 Users guide

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© PCE Instruments
PCE-WO2 10 Oxygen Meter
User Manual
Last change: 8 August 2019
v1.0
English
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Contents
1 Safety notes ........................................................................................... 1
2 Technical specifications ...................................................................... 2
3 Delivery Scope ...................................................................................... 2
4 Installing the Batteries ......................................................................... 3
5 Display ................................................................................................... 3
6 Keypad ................................................................................................... 4
7 Filling the Electrolyte Solution ............................................................ 5
8 Connecting the Dissolved Oxygen Probe .......................................... 5
9 Switching the Tester On and Off ......................................................... 6
10 Prior to Use ............................................................................................ 6
11 Setup Menu ............................................................................................ 6
11.1 Setting the default option .................................................................................................. 7
12 Setting the salinity coefficient ............................................................. 8
13 Setting the ambient pressure .............................................................. 8
14 DO Calibration in % Saturation Mode ................................................. 9
14.1 Single point calibration - 100% saturation ......................................................................... 9
14.2 2 points calibration ........................................................................................................... 9
15 Temperature Calibration .................................................................... 10
16 Dissolved Oxygen Measurement ....................................................... 11
17 Auto-Hold ............................................................................................. 11
18 Electrode Care and Maintenance ...................................................... 12
19 Troubleshooting .................................................................................. 12
20 Addendum: Preparation of the Zero Oxygen Solution .................... 12
21 Contact ............................................................................................... 13
22 Disposal ............................................................................................... 13
© PCE Instruments
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© PCE Instruments
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1 Safety notes
Please read this manual carefully and completely before you use the device for the first time. The device may only be used by qualified personnel and repaired by PCE Instruments personnel. Damage or injuries caused by non-observance of the manual are excluded from our liability and not covered by our warranty.
• The device must only be used as described in this instruction manual. If used otherwise, this can cause dangerous situations for the user and damage to the meter.
• The instrument may only be used if the environmental conditions (temperature, relative humidity, …) are within the ranges stated in the technical specifications. Do not expose the device to extreme temperatures, direct sunlight, extreme humidity or moisture.
• Do not expose the device to shocks or strong vibrations.
• The case should only be opened by qualified PCE Instruments personnel.
• Never use the instrument when your hands are wet.
• You must not make any technical changes to the device.
• The appliance should only be cleaned with a damp cloth. Use only pH-neutral cleaner,
no abrasives or solvents.
• The device must only be used with accessories from PCE Instruments or equivalent.
• Before each use, inspect the case for visible damage. If any damage is visible, do not
use the device.
• Do not use the instrument in explosive atmospheres.
• The measurement range as stated in the specifications must not be exceeded under
any circumstances.
• Non-observance of the safety notes can cause damage to the device and injuries to the user.
We do not assume liability for printing errors or any other mistakes in this manual. We expressly point to our general guarantee terms which can be found in our general terms of
business. If you have any questions please contact PCE Instruments. The contact details can be found at
the end of this manual.
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2 Technical specifications
Measuring range oxygen content
0.0 ... 20.0 mg/l
Resolution oxygen content
0.1 mg/l
Measuring accuracy oxygen content
±0.5 mg/l
Measuring range oxygen saturation
0.0 ... 200.0 %
Resolution oxygen saturation
0.1 %
Measuring accuracy of oxygen saturation
±2.0 %
Temperature compensation
0 ... +40 °C / 32 ... 104 °F, automatic
Air pressure correction
60.0 ... 112.5 kPa, 450 ...850 mmHg
Salinity correction
0 ... 35 g/l
Sensor type
polarography
Environmental conditions
0 ... +60 °C / 32 ... 140 °F, max. 80 % r.H.
Power supply
2 x 1.5 AAA batteries
Dimension (length x radius)
175 x 40 mm / 6.8 x 1.5"
Weight
100 g / 3.5 oz
3 Delivery Scope
1 x Dissolved Oxygen Meter PCE-WO2 10 1 x Oxygen probe with measuring cable 2 x Membrane 1 x Electrolyte solution (30ml) 2 x 1.5 V AAA batteries 1 x User manual 1 x Carrying case
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4 Installing the Batteries
• Twist the electrode collar counter clockwise, pull the 6-pin connector away from the tester.
• Insert two AAA batteries into the battery compartment, note polarity.
• Align the slot on connector, gently push the connector into the tester.
• Twist the electrode collar clockwise until it is tight.
5 Display
PCE-WO2 10 pocket dissolved oxygen tester is equipped with an easy-to-read LCD display that used to show the measured values and mode icons. The following table describes the function of each icon.
INDEX:
ICON
DESCRIPTION
MEAS
Indicates the tester is in the measurement mode.
CAL
Indicates the tester is in the calibration mode.
SETUP
Indicates the tester is in the setting mode.
HOLD
Indicates the measuring value has been locked.
ATC
Indicates the temperature compensation is enabled.
When the battery is depleted, the icon will disappear.
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6 Keypad
The tester has a succinct membrane keypad, names and symbols describe each function key controls.
INDEX:
KEY
FUNCTION
MEAS/HOLD
• Switches the tester ON/OFF.
• Locks the measured value, press the key again to resume measuring.
• Exits the calibration or setting and returns to the measurement mode.
CAL
• Press the key to start the calibration.
• Press and hold the key to enter the setup menu.
• In the setting mode, press the key to select the default option.
ENTER
• Confirms the calibration or selected option.
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7 Filling the Electrolyte Solution
• Take out the dissolved oxygen probe and electrolyte solution from the packaging. Unscrew
the membrane cap.
• Fill the membrane cap halfway with electrolyte solution.
• Screw the membrane cap onto the probe, excess electrolyte solution will drain out.
• Be sure the cathode of probe makes contact with membrane cap, the electrolyte solution in
membrane cap should be without an air bubble.
8 Connecting the Dissolved Oxygen Probe
Insert the 6-pin connector of probe into the connector socket on the tester. After the connection is completed, DO NOT pull on the cable. Always make sure that the connector is clean and dry.
Cathode
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9 Switching the Tester On and Off
• Press the Meas key to switch on the tester, the display shows measured values.
• Press and hold the Meas key for 5 seconds, the tester will switch off.
• To enable the Auto-Power Off function, please refer to chapter SETUP MENU.
10 Prior to Use
Switch on the tester 10 to 15 minutes and wait for the probe to polarize.
11 Setup Menu
PCE-WO2 10 pocket dissolved oxygen tester contains an integrated setup menu that is used to customize the displayed option to meet measurement requirements.
MENU
DESCRIPTION
OPTIONS
DEFAULT
Set the salinity coefficient of sample.
Range: 0~35ppt
0.0ppt
Set the barometric pressure coefficient.
Range: 450~850mmHg
760mmHg
Set the number of calibration points.
1 point
1 point 2 points
Set the default measurement unit.
mg/L
Concentration Unit
mg/L, °C
ppm % % saturation
Degrees Celsius
Degrees Fahrenheit
Calibrate the temperature.
---
---
When the option is enabled, the tester will automatically sense a stable reading and lock the measurements.
Enable
Disable Disable
When the option is enabled, the tester will automatically switch off if no key is pressed within 8 minutes.
Enable
Disable Disable
Reset the tester to factory default settings.
Enable
Disable
Disable
Power
On
5 sec. Power Off
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11.1 Setting the default option
• Press and hold the Cal key for 3 seconds to enter the setup menu, the tester shows a menu item and default option.
• If necessary, press the Cal key again to select the desired option.
• Press the Enter key to confirm, the tester moves to the next menu item.
• Repeat the steps above until the tester returns to the measurement mode. Setting is
completed.
• During the setting process, press the Meas key, the tester will exit the setup menu and return to the measurement mode.
• If you do not want to calibrate the temperature, press the Enter key to skip the °C/CAL or °F/CAL option.
• The Reset function will restore the tester back to factory default settings. If enabled, all of the calibration data and selected parameters will be lost or reset, the tester must be recalibrated.
Option
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12 Setting the salinity coefficient
In order to get an accurate reading, the salinity of the sample should be specified which is done with the help of a coefficient. Salt dissolved in water will influences oxygen content of water. If your sample contains high levels of salinity, ensure that setting an applicable salinity coefficient prior to measurement.
• In the measurement mode, press and hold the Cal key for 3 seconds to enter the setup menu, the display shows (salinity coefficient) option.
• Press the Cal key again to set the value.
• Press the Enter key to confirm, the display shows the next menu item.
• Press the Meas key to exit the setting and return to the measurement mode.
13 Setting the ambient pressure
To ensure an accurate reading, the ambient pressure must be set in the unit mmHg. The following table will help to convert your ambient pressure into the required unit mmHg on the basis of your current height.
ALTITUDE (m)
kPa
mmHg
ALTITUDE (m)
kPa
mmHg
0
101.3
760
1600
82.9
622
100
100.1
750
1700
81.9
614
200
98.8
741
1800
80.9
607
300
97.6
732
1900
79.9
599
400
96.4
723
2000
78.9
592
500
95.2
714
2100
77.9
584
600
94.0
705
2200
76.9
577
700
92.8
696
2300
76.0
570
800
91.7
688
2400
75.0
563
900
90.5
679
2500
74.1
556
1000
89.4
671
2600
73.2
549
1100
88.3
662
2700
72.3
542
1200
87.2
654
2800
71.4
536
1300
86.1
646
2900
70.5
529
1400
85.0
638
3000
69.6
522
1500
84.0
630
3100
68.7
515
• In the measurement mode, press and hold the Cal key for 3 seconds to enter the setup menu, the display shows .
• Press the Enter key, the display shows (Barometric Pressure Coefficient) option.
• Press the Cal key to set the value.
• Press the Enter key to confirm, the display shows the next menu item.
• Press the Meas key to exit the setting and return to the measurement mode.
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14 DO Calibration in % Saturation Mode
PCE-WO2 10 pocket dissolved oxygen tester can be calibrated quickly in air. In the percentage saturation mode, the tester is able to perform either 1 or 2 points calibration. For single point calibration, we recommend that you perform 100% saturation calibration in the air-saturated water. If the 2 points calibration is selected, the zero oxygen solution needs to be used.
14.1 Single point calibration - 100% saturation
• Make sure that you have selected 1 point calibration in the setup menu.
• Press the Cal key, the tester shows “100% / CAL1”.
• Hold the dissolved oxygen probe in the air at 100% relative humidity or place the probe into the air-saturated water for 15 minutes.
• Press the Enter key. Wait for the reading to stabilize, the tester automatically shows END. Single point calibration is completed.
14.2 2 points calibration
• Make sure that you have selected 2 points calibration in the setup menu.
• Repeat the steps 1.2 to 1.4 above. When the first calibration point is completed, the display will show “0% / CAL2”. The tester prompts you to continue with second point calibration.
• Immerse the dissolved oxygen probe into the zero oxygen solution, stir the probe gently.
• Press the Enter key to confirm. Wait for the reading to stabilize (this can often take more than 10 minutes), the display automatically shows END. The tester returns to the measurement mode. Calibration is completed.
Performing a percentage saturation
calibration will simultaneously calibrate the corresponding mg/L (or ppm) concentration value.
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15 Temperature Calibration
During the measurement process, if the temperature reading displayed differs from that of an accurate thermometer, the tester needs to be calibrated.
• Press and hold the Cal key for 3 seconds to enter the setup menu.
• Press the Enter key until the tester shows °C/CAL or °F/CAL.
• Press the Cal key to enter the temperature calibration mode.
• Press the Cal key again to modify the temperature value (Resolution: 0.5°C).
• Press the Enter key to confirm, the tester shows the next menu item.
• Press the Meas key to return to the measurement mode. Calibration is completed.
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16 Dissolved Oxygen Measurement
PCE-WO2 10 pocket dissolved oxygen tester is suitable for measuring the water, wastewater, brine and other liquids. If the sample is belong to the seawater or other water containing large amounts of salt, please setting the salinity coefficient before measurement. Some gas and steam such as chloride, sulfur dioxide, sulfureted hydrogen, ammonium, carbon dioxide and iodin can permeate the membrane via diffusion. So their existence will influence the measurement of dissolved oxygen. If the sample contains the solvent, grease, sulfide and alga, the membrane on the probe will be blocked, damaged or eroded.
• Connect the dissolved oxygen probe to tester and wait for 15 minutes to polarize the probe.
• If necessary, to set the barometric pressure and salinity coefficient in the setup menu (Refer to page 5).
• Immerse the probe in the sample solution, make sure the temperature sensor on the probe is fully immersed.
• Stir the probe gently. Record the measured value when the reading is stable.
17 Auto-Hold
PCE-WO2 10 pocket dissolved oxygen tester contains an Auto-Hold function. If enabled, the tester will automatically sense a stable reading and lock the measurements. The icon appears on the display. If disabled, press the Hold key, the tester will immediately lock the displayed value. Press the Meas key to resume measuring.
Temperature sensor
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18 Electrode Care and Maintenance
• Always keep the membrane of the dissolved oxygen probe is wet or moist.
• If you do not use the probe for long periods, please screw off membrane cap and rinse
the cathode, anode and membrane with deionized water, then soak up residual water on them with filter paper. Install the probe again.
19 Troubleshooting
LCD DISPLAY
CAUSE
CORRECTIVE ACTION
DO probe does not connect to tester
Check the connector of probe.
Measured value is out of range
Check the DO membrane whether clogged, dirty or broken.
Electrolyte solution is depleted
Refilling electrolyte solution.
Zero oxygen solution is contaminated
Replace the calibration solution.
20 Addendum: Preparation of the Zero Oxygen Solution
Dissolve 500mg of sodium sulfate (Na2SO3) reagent and a small amount of cobalt (II) chloride hexahydrate (CoCl
2
• 6H
2
O) in the 250mL distilled water, mix the solution until the reagent is
completely dissolved.
Membrane cap
Cathode and Anode
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21 Contact
If you have any questions, suggestions or technical problems, please do not hesitate to contact
us. You will find the relevant contact information at the end of this user manual.
22 Disposal
For the disposal of batteries in the EU, the 2006/66/EC directive of the European Parliament applies. Due to the contained pollutants, batteries must not be disposed of as household waste. They must be given to collection points designed for that purpose.
In order to comply with the EU directive 2012/19/EU we take our devices back. We either re­use them or give them to a recycling company which disposes of the devices in line with law.
For countries outside the EU, batteries and devices should be disposed of in accordance with your local waste regulations.
If you have any questions, please contact PCE Instruments.
© PCE Instruments
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PCE Instruments contact information
Germany France Spain
PCE Deutschland GmbH PCE Instruments France EURL PCE Ibérica S.L. Im Langel 4 23, rue de Strasbourg Calle Mayor, 53 D-59872 Meschede 67250 Soultz-Sous-Forets 02500 Tobarra (Albacete) Deutschland France España Tel.: +49 (0) 2903 976 99 0 Téléphone: +33 (0) 972 3537 17 Tel. : +34 967 543 548 Fax: +49 (0) 2903 976 99 29 Numéro de fax: +33 (0) 972 3537 18 Fax: +34 967 543 542 [email protected] [email protected] [email protected] www.pce-instruments.com/deutsch www.pce-instruments.com/french www.pce-instruments.com/espanol
Germany United Kingdom Italy
PCE Produktions- und PCE Instruments UK Ltd PCE Italia s.r.l. Entwicklungsgesellschaft mbH Unit 11 Southpoint Business Park Via Pesciatina 878 / B-Interno 6 Im Langel 26 Ensign Way, Southampton 55010 Loc. Gragnano D-59872 Meschede Hampshire Capannori (Lucca) Deutschland United Kingdom, SO31 4RF Italia Tel.: +49 (0) 2903 976 99 471 Tel: +44 (0) 2380 98703 0 Telefono: +39 0583 975 114 Fax: +49 (0) 2903 976 99 9971 Fax: +44 (0) 2380 98703 9 Fax: +39 0583 974 824 [email protected] [email protected] [email protected] www.pce-instruments.com/deutsch www.pce-instruments.com/english www.pce-instruments.com/italiano
The Netherlands China Hong Kong
PCE Brookhuis B.V. PCE (Beijing) Technology Co., Limited PCE Instruments HK Ltd. Institutenweg 15 1519 Room, 6 Building Unit J, 21/F., COS Centre 7521 PH Enschede Zhong Ang Times Plaza 56 Tsun Yip Street Nederland No. 9 Mentougou Road, Tou Gou District Kwun Tong Telefoon: +31 (0)53 737 01 92 102300 Beijing, China Kowloon, Hong Kong [email protected] Tel: +86 (10) 8893 9660 Tel: +852-301-84912 www.pce-instruments.com/dutch [email protected] [email protected] www.pce-instruments.cn www.pce-instruments.cn
United States of America Turkey
PCE Americas Inc. PCE Teknik Cihazları Ltd.Şti. 711 Commerce Way suite 8 Halkalı Merkez Mah. Jupiter / Palm Beach Pehlivan Sok. No.6/C 33458 FL 34303 Küçükçekmece - İstanbul USA Türkiye Tel: +1 (561) 320-9162 Tel: 0212 471 11 47 Fax: +1 (561) 320-9176 Faks: 0212 705 53 93 [email protected] [email protected] www.pce-instruments.com/us www.pce-instruments.com/turkish
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