PASCO OS-8542 User Manual

Includes
and
Typical
Experiment Results
Instruction Manual and
012-07105B
Experiment Guide for the
PASCO scientific
Model OS-8542
BLACK BODY LIGHT SOURCE
FOR THE OS-8539 EDUCATIONAL
SPECTROPHOTOMETER
Black Body Instruction Manual 012–07105B
The exclamation point within an equilateral triangle is intended to alert the user of the presence of important operating and maintenance (servicing) instructions in the literature accompanying the device.
012–07105B Black Body Instruction Manual
Table of Contents
Section Page
Copyright, Warranty, and Equipment Return ................................................................................. ii
Introduction .................................................................................................................................. 1
Theory ...................................................................................................................................... 2-4
Setup ........................................................................................................................................ 5-8
Calibration ....................................................................................................................................9
Procedures .............................................................................................................................9-10
Experiment ........................................................................................................................... 10-11
Data Collection and Analysis ..................................................................................................... 12
Teacher’s Guide ................................................................................................................... 13-15
Troubleshooting ..........................................................................................................................16
Parts and Replacements .............................................................................................................17
Technical Support .......................................................................................................Back Cover
i
Copyright, Warranty, and Equipment Return
Please—Feel free to duplicate this manual subject to the copyright restrictions below.
Copyright Notice
The PASCO scientific 012-07105A manual is copyrighted and all rights reserved. However, permission is granted to non-profit educational institutions for reproduction of any part of the manual providing the reproductions are used only for their laboratories and are not sold for profit. Reproduction under any other circumstances, without the written consent of PASCO scientific, is prohibited.
Limited Warranty
PASCO scientific warrants the product to be free from defects in materials and workmanship for a period of one year from the date of shipment to the customer. PASCO will repair or replace at its option any part of the product which is deemed to be defective in material or workmanship. The warranty does not cover damage to the product caused by abuse or improper use. Determination of whether a product failure is the result of a manufacturing defect or improper use by the customer shall be made solely by PASCO scientific. Responsibility for the return of equipment for warranty repair belongs to the customer. Equipment must be properly packed to prevent damage and shipped postage or freight prepaid. (Damage caused by improper packing of the equipment for return shipment will not be covered by the warranty.) Shipping costs for returning the equipment after repair will be paid by PASCO scientific.
Equipment Return
Should the product have to be returned to PASCO scientific for any reason, notify PASCO scientific by letter, phone, or fax BEFORE returning the product. Upon notification, the return authorization and shipping instructions will be promptly issued.
NOTE: NO EQUIPMENT WILL BE
ACCEPTED FOR RETURN WITHOUT AN AUTHORIZATION FROM PASCO.
When returning equipment for repair, the units must be packed properly. Carriers will not accept responsibility for damage caused by improper packing. To be certain the unit will not be damaged in shipment, observe the following rules:
The packing carton must be strong enough for the
item shipped.
Make certain there are at least two inches of packing
material between any point on the apparatus and the inside walls of the carton.
Make certain that the packing material cannot shift in
the box or become compressed, allowing the instrument come in contact with the packing carton.
Address: PASCO scientific
10101 Foothills Blvd. Roseville, CA 95747-7100
Phone: (916) 786-3800
FAX: (916) 786-3292
email: support@pasco.com
web: www.pasco.com
ii
012–07105B Black Body Instruction Manual
Introduction
About this Manual
This manual describes setup, operational, and procedure guidelines for conducting a black body experiment using the OS-8537 Educational Spectrophotometer, OS-8542 Black Body Light Source and the OS-8543 Black Body Prism with Infrared Filter.
The Black Body Prism comes with the necessary accessories for mounting the prism onto the spectrophotometer table of the PASCO OS-8537 Educational Spectrophotometer. The Black Body Prism is designed to convert the PASCO Model OS-8539 Educational Spectrophotometer from a grating to a prism spectrophotometer. A prism spectrophotometer has two advantages over a grating spectrophotometer: a) it eliminates overlap of orders observed with a grating (When a grating is used, second order visible wavelengths overlap first order infrared wavelengths.), and b) the spectrum is brighter because it does not spread over several orders or in both directions.
Equipment Required:
OS-8542 Black Body Light Source
OS-8543 Black Body Prism with infrared filter, filter bracket and beveled stop piece
PASCO
BLACK BODY PRISM
OS-8543
Black body light source Prism mount with prism
Also Required:
• Educational Spectrophotometer System (OS-8539)
Filter bracket (with filter) for the infrared light sensor
infrared filter
0-10 VDC Power Supply (1 A) (SE-9720) Or Power Amplifier (CI-6552)
Science Workshop Interface (Model 750 or 700)
Stop piece for the light sensor arm
PASCO Infrared Sensor (CI-6628)* Or High Sensitivity Light Sensor (CI-604)**
DataStudio™ software
Setup CD for the Black Body experiment
1 package containing 10 tungsten light bulbs (9 for replacement in the black body light source)
*Use the infrared sensor for black body experiments or when you want to measure infrared wavelengths.
**Use the high sensitivity light sensor for experiments in which only visible wavelengths are desired and a linear response is not needed.
1
Black Body Instruction Manual 012-07105B
Theory
The 60-degree prism is mounted so that the back face is perpendicular to the incoming light, as shown in Figure 1. A schematic of the prism and the path of light is shown in Figure 2 below. Since the prism angle is 60 degrees, it can be shown that
(1) θ2+ θ3=60°
And using Snell’s law at each interface,
(2) sin (60°) = n sin (θ2) and
(3) sin (θ) = n sin(θ3)
Combining equations (3) and (1) yields
(4) sin (θ) = n sin (60° θ2)
which, using the double angle formula becomes
black body light
light sensor
aperture slits
collimating slits
collimating lens
prism mount with prism
GAIN
1
10
100
direction of light
Figure 1: Path of Light Through the Prism Spectrophotometer
(5) sin (θ) = n{ sin (60°) cos (θ2) – sin (θ2) cos (60°)}
Now use a trig identity to change from cos to sin, and (5) becomes
1
(6) sin θ = n sin 60° 1 – sin2θ
2
– n sin θ2cos 60°
2
= sin 60° n2–n2sin2θ
If we now use (2), equation 6 becomes
1
(7) sin(θ) = sin(60°)[n2– sin2(60°)]
2
– sin(60°)cos(60°)
Solving (7) for n gives
(8) n =
sinθ
+ cos602+ sin260
sin60
And finally, if we simplify,
path of light
The Cauchy equation gives the relationship between the wavelength and the index of refraction.
(10) n(λ)=
A
+ B
2
λ
where A and B depend on the type of glass.
1 2
– n sin θ2cos 60°
2
θ
3
θ
2
60°
n
60°
Figure 2: Schematic of a Prism
θ
2
012–07105B Black Body Instruction Manual
Table 1 shows the values for the prism used. The graph in Figure 3 shows an inverse square fit of the data.
Thus, we get the values of A=13,900 and B=1.689 with the wavelength given by
Thus, the final equation for the wavelength (in nanometers) is
Table 1: Prism Coefficients
ataD,stneiciffeoCmsirP
)mn(htgnelevaWxednInoitcarfeR
007.404677.1
008.534267.1
000.084847.1
001.684647.1
001.6454
006.785827.1
008.346227.1
003.656127.1
005.607717.1
001.258907.1
000.4101307.1
37.1
Figure 3: Relationship between refraction index and wavelength for light passing through a prism
Determination of the Wavelength from the Angle (using DataStudio)
In DataStudio, the equation for determining the wavelength is listed in the Definition box in the Calculator window, as follows:
Wavelength = filter (0,8000, (13900/(((1.1547*sin ((Init - Angle)/Ratio))^2 + 0.75)^0.5 - 1.689))^0.5)
where 0,8000 is the filtering range for the infrared light (0-8000 nm)
13,900 is constant A, as described above.
1.689 is constant B, as described above.
1.1547 is
2
3
Init - is the initial angle reading measured during data collection Angle - is the angle measured by the rotary motion sensor Ratio - is the ratio of the disk radius to the pin radius
3
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