Oxford Instruments X-MET8000 User Manual

X-MET8000 Series User Manual
Contents
Welcome...................................................................................................................5
Who Is This Guide For?...................................................................................................................................................5
X-MET8000 Series Operator’s Guide...........................................................................6
The X-MET8000 Series...................................................................................................................................................6
The X-MET8000 Series Components....................................................................................................................6
The X-MET8000 Series External Connections.......................................................................................................7
Safety First!....................................................................................................................................................................8
Safety Symbols....................................................................................................................................................8
Caution X-Rays.....................................................................................................................................................8
Caution Beryllium................................................................................................................................................9
Caution Lanyard Use............................................................................................................................................9
How To Operate The X-MET8000 Series.......................................................................................................................10
The Control Panel...............................................................................................................................................10
The Touch Screen...............................................................................................................................................11
The Virtual Keyboard..........................................................................................................................................11
The Menu Screen...............................................................................................................................................12
The Status Bar...................................................................................................................................................12
The Tools Menu..................................................................................................................................................13
Take The First Measurement.........................................................................................................................................13
Switch On The X-MET8000 Series......................................................................................................................14
Add A Sample Name..........................................................................................................................................16
Take A Measurement..........................................................................................................................................16
The Results Screen.............................................................................................................................................18
Delete A Poor Measurement...............................................................................................................................19
Print Result From Result Screen To Bluetooth Printer.........................................................................................19
Switch Off The X-MET8000 Series......................................................................................................................20
Average A Batch Of Measurements..............................................................................................................................20
Sample And Batch Names..................................................................................................................................20
Which Method?..................................................................................................................................................20
Auto Select Modes Make Analysis Easy..............................................................................................................21
How Long For A Measurement?..........................................................................................................................23
Add The Sample And Batch Names....................................................................................................................24
Choose A Method...............................................................................................................................................24
Set The Measurement Time...............................................................................................................................25
Check The Status Bar.........................................................................................................................................26
Set The Batch Size.............................................................................................................................................27
Take Averaged Measurements...........................................................................................................................28
The Average Results Screen...............................................................................................................................28
Search The Results History................................................................................................................................29
Delete The Results History.................................................................................................................................32
Generate Report to Printer.................................................................................................................................35
Generate Report to Network Share....................................................................................................................37
The X-MET8000 Series User Manual and USB Driver ...................................................................................................38
Save The X-MET8000 Series User Manual and USB Driver ................................................................................39
Operation With A PC.....................................................................................................................................................40
Connect To A PC And Login................................................................................................................................40
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About The Report Generator..............................................................................................................................42
Wireless Network Use Cases..............................................................................................................................48
X-MET Application Programming Interface.........................................................................................................80
X-MET8000 Series Settings..........................................................................................................................................82
Set The Date And Time......................................................................................................................................83
Set The Language..............................................................................................................................................84
Make Safe Measurements............................................................................................................................................85
Handle The X-MET8000 Series Carefully............................................................................................................85
Safe, Reliable Measurements.............................................................................................................................87
Use The Correct Accessory................................................................................................................................89
X-MET8000 Series For Hot Samples...................................................................................................................91
Battery Usage....................................................................................................................................................92
Maintenance and Troubleshooting...............................................................................................................................92
Recommended Daily Maintenance.....................................................................................................................93
Recommended Weekly Maintenance.................................................................................................................93
Battery Maintenance..........................................................................................................................................94
Troubleshooting..................................................................................................................................................97
Recertification....................................................................................................................................................98
End Of Life.........................................................................................................................................................98
Technical Specifications...............................................................................................................................................99
Technical Specifications, X-MET8000 Series.......................................................................................................99
Technical Specifications, Battery........................................................................................................................99
Technical Specifications, Battery Charger..........................................................................................................99
Technical Specifications, DC Power Supply......................................................................................................100
EC Declaration of Conformity, X-MET8000.................................................................................................................100
X-MET8000 Series Supervisor’s Guide.....................................................................102
Users And Security.....................................................................................................................................................102
Set Passwords..................................................................................................................................................102
Switch User......................................................................................................................................................103
Advanced Use............................................................................................................................................................104
Sample Preparation..........................................................................................................................................104
Choose The Right Method................................................................................................................................105
Analyze And Report Results.............................................................................................................................107
Modify The Results Screen.........................................................................................................................................115
About Results Screen Formats.........................................................................................................................116
A Custom Results Screen.................................................................................................................................117
About The Grade Table.....................................................................................................................................134
About Pseudo Elements...................................................................................................................................138
Wireless Network Use Cases......................................................................................................................................141
Wireless Connections.................................................................................................................................................141
Add A Bluetooth Connection............................................................................................................................143
Add A Bluetooth Keyboard...............................................................................................................................145
Check GPS Information....................................................................................................................................147
Connect the X-MET8000 series to a company network....................................................................................149
Add A Broadcast Wi-Fi Connection...................................................................................................................149
Add A Hidden Wi-Fi Connection........................................................................................................................153
Wireless Printing........................................................................................................................................................158
Configure A Printer...........................................................................................................................................158
Print A Test Page..............................................................................................................................................161
Generate Report to Printer...............................................................................................................................162
Wireless File Transfers................................................................................................................................................164
Configure Network Share Settings...................................................................................................................164
Write Test File To Network................................................................................................................................165
Generate Report to Network Share..................................................................................................................166
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VNC connection to the X-MET8000 series..................................................................................................................167
Configure VNC Server Settings........................................................................................................................168
Setup a VNC connection on a PC.....................................................................................................................168
Control the X-MET8000 series using an iPad..............................................................................................................170
Setup an iPad to control the X-MET8000 series................................................................................................170
Control the X-MET8000 series using an iPad....................................................................................................172
Manage Backups........................................................................................................................................................175
Create A Backup..............................................................................................................................................175
Restore A Backup.............................................................................................................................................177
Delete A Backup...............................................................................................................................................179
Configuration.............................................................................................................................................................180
Set The Power Saving......................................................................................................................................181
Choose Sounds................................................................................................................................................182
Configure Camera Settings..............................................................................................................................183
Disable the Proximity Safety Sensor................................................................................................................185
Calibration Adjustments.............................................................................................................................................186
Auto-Select Mode Calibration Adjustments......................................................................................................186
Empirical Calibration Adjustments...................................................................................................................191
Fundamental Parameter Calibration Adjustments............................................................................................194
About The Energy Calibration..........................................................................................................................196
Operation With A PC...................................................................................................................................................197
Connect To A PC And Login..............................................................................................................................198
About The Report Generator............................................................................................................................200
Software Installation........................................................................................................................................214
Operation With A GPS................................................................................................................................................221
Bluetooth.........................................................................................................................................................221
X-MET8000 series Internal GPS........................................................................................................................221
Nokia LD-3W Bluetooth GPS.............................................................................................................................221
Trimble Field Computer and GPS......................................................................................................................222
Major Differences Internal GPS vs. Nokia LD-3W vs. Trimble Field Computer...................................................222
Setup and use the Internal GPS.......................................................................................................................223
Setup and use the Nokia LD-3W Bluetooth GPS...............................................................................................225
Setup and use a Trimble Field Computer and GPS...........................................................................................234
Troubleshooting GPS........................................................................................................................................246
X-MET Application Programming Interface.......................................................................................................247
Additional Troubleshooting.........................................................................................................................................250
Missing Menus Or Methods..............................................................................................................................250
Do A Test Measurement...................................................................................................................................250
Radiation Specifications.............................................................................................................................................253
Primary Beam Intensity....................................................................................................................................254
Primary Beam Direction...................................................................................................................................254
Scattered Radiation Profile...............................................................................................................................254
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Welcome
This guide covers several products, and uses ‘X-MET8000 series’ to refer to them. The X-MET8000 series can analyze all elements between Magnesium and Uranium.
Oxford Instruments wishes to ensure that every customer is able to get the maximum benefit from their use of the X-MET8000 series. There are two booklets to help operators:
This booklet helps operators to make safe, reliable and accurate measurements. When and how to use the right accessories. How to
Safe, Accurate Measurements With The X-MET8000 Series maintain the X-MET8000 series to get the maximum benefit from it, and
basic troubleshooting information. This booklet also includes safety, regulatory and compliance information, technical specifications and the EC Declaration of Conformity.
This booklet demonstrates how to use the X-MET8000 series. How the software works. It shows how to make typical measurements which
How To Use The X-MET8000 Series
every customer is likely to need, and how to search the results. How to save the X-MET8000 Series User Manual to a USB memory device.
The X-MET8000 Series User Manual is stored within the X-MET8000 series, and has more in depth information, and how to use the X-MET8000 series in some specific situations. It shows how a supervisor can prepare the X-MET8000 series for an operator to use.
Oxford Instruments Industrial Analysis Tubney Woods, Abingdon, Oxfordshire, OX13 5QX, UK
Who Is This Guide For?
This guide is for the operators and supervisors who are trained to analyze samples with X-ray fluorescence. The local Oxford Instruments representative can train personnel in the safe and accurate use of the X-MET8000 series, or give advice about how to train personnel.
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X-MET8000 Series Operator’s Guide
The X-MET8000 Series
These are the main components and features of the X-MET8000 series, and the external connections to it.
The X-MET8000 Series Components
The X-MET8000 series includes a rugged transit case as standard. This contains the following items:
1. X-MET8000 series analyzer
2. Slot for lanyard
3. Slot for wrist lanyard
4. Operator’s Manuals on a CD
5. Spare protective film windows
6. Spare battery
7. Battery, inside handle
8. USB cable
9. Background plate (optional accessory)
10. Slot for optional light radiation shield or weld adapter
11. DC power supply with cable and plug adapter
12. Desktop battery charger
13. Alloy CRM sample
14. Sample boxes
The included accessories depend upon the version of the X-MET8000 series. The background plate, the light radiation shield, and the weld adapter are optional accessories. The DC power supply (battery charger) includes international plug adapters.
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The X-MET8000 Series Features
These are the main features of the X-MET8000 series.
1. Measurement window
2. Proximity window
3. Hot surface protection
4. Control panel
5. Proximity and X-Ray On indicators
6. Touch screen display
7. Trigger
8. Battery cover
9. Battery cover release
10. Ring for lanyard
11. Connector cover
The control panel contains the Power On button and the Home button. The labels include safety information and the serial number. Open the connector cover to access the external connections.
Check both batteries before use. Refer to: Battery Maintenance on page 94.
The X-MET8000 Series External Connections
The X-MET8000 series has four external connections that are underneath the display. Open the plastic connector cover to access them.
1. USB A connector.
2. DC supply connector.
3. Extension connector.
4. USB Micro-AB connector.
Use the USB Micro-AB connector to connect the X-MET8000 series to a PC with the USB cable. Use the USB A connector for a USB memory device or an external display. Use the DC supply connector to connect the external DC power supply to charge or power the X-MET8000 series.
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Only use the included DC power supply to charge or power the X-MET8000 series and it's batteries. Use of incompatible DC power supply and/or charger might result in damage or personal injury.
The extension connector is designed for X-MET8000 series accessories and is not compatible with generic consumer devices. Connecting incompatible devices to the extension port might damage the X-MET8000 series and/or the device(s) connected to it.
Safety First!
The X-MET8000 series is designed to meet rigorous safety requirements, and is safe to operate in accordance with these instructions.
If the X-MET8000 series is used in a manner not specified by Oxford Instruments, the safety features of the X-MET8000 series can be impaired.
Many regulatory organizations require each customer to register the X-MET8000 series. The local Oxford Instruments representative can assist with the specific regulatory requirements.
The X-MET8000 has regulatory approval as Type Number: XMDS 2770.
Safety Symbols
These symbols appear on the X-MET8000 series and in the documentation.
Caution; X-Rays: This symbol is a warning about X-ray generation.
Caution; X-Rays (Ca): This symbol is a warning about X-ray generation for use in Canada.
Caution; Toxic Material: This symbol is a warning about the presence of toxic material.
Caution; Electricity: This symbol is a warning about the presence of electricity.
Caution: This symbol provides a general warning.
Caution X-Rays
The X-MET8000 series generates X-ray radiation when it is energized.
Caution; X-Rays: Do not misuse or abuse the X-MET8000 series because of the risk of direct exposure to X-ray radiation above permissible levels. Prolonged direct exposure to X-ray radiation can cause serious personal injury.
Contact the local Oxford Instruments representative for advice about X-ray radiation, or for X-ray safety training.
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Caution Beryllium
The detector has a thin beryllium window. Beryllium is a toxic compound, however, the beryllium window poses no health hazard when it is intact.
Caution; Toxic Material: Do not puncture, break or damage the beryllium window in any way. This can produce airborne particles. Prolonged inhalation of beryllium can cause cancer.
Do not allow the detector to come into contact with moisture, or condensation from high humidity. This can corrode the beryllium window, in particular if chlorine, sulphates, copper or iron is also present.
Contact the local Oxford Instruments representative for advice about beryllium, or if the beryllium window is pierced, broken, damaged or corroded.
Caution Lanyard Use
The X-MET8000 series includes a lanyard. This is only applicable for use at ground level.
Caution: Do not use the X-MET8000 series lanyard as a safety lanyard for work at height because of the risk of a fall. This can result in serious personal injury.
The anchor for the lanyard on the underside of the X-MET8000 series is applicable for use with a tool safety lanyard for work at height.
X-MET8000 Series Safety Features
The X-MET8000 series includes these 10 key safety features to protect the operator.
Power On Button And Indicator
Safety Feature: Press and hold the Power On button for 5 seconds to switch the X-MET8000
series on or off.
Password Protection
Safety Feature: An operator must have the correct password to use the X-MET8000 series.
Safety Feature: The supervisor can change the passwords.
Proximity Sensors
Safety Feature: The sample must cover the proximity window before the X-MET8000 series
can generate an X-ray beam.
Safety Feature: When the sample covers the proximity window, the proximity indicators change to green.
Safety Feature: The X-MET8000 series switches the X-ray beam off if there is no return signal from the sample.
Trigger And X-Ray On Indicators
Safety Feature: An operator must pull the trigger for the X-MET8000 series to generate an
X-ray beam.
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Safety Feature: The X-Ray On indicators blink red when the X-MET8000 series generates an X-ray beam.
Safety Feature: If one of the X-Ray On indicators fails, the X-MET8000 series will not generate an X-ray beam.
X-ray shutter
Safety Feature: The shutter state is indicated on the X-MET8000 series screen "Shutter
open/Shutter closed".
How To Operate The X-MET8000 Series
Use the control panel and touch screen display to operate the X-MET8000 series. The touch screen display includes a virtual keyboard to type text and numbers. There is a Menu screen and a status bar to access the main functions and the configuration, and a Tools menu can appear for some screens.
The Control Panel
The control panel contains the Power On button and the Home button.
1. Home button
2. Power On button
Press the Home button to immediately leave the current screen and cancel an operation.
Home button
The symbol on the Home button is lit white when the X-MET8000 series is on.
The symbol on the Power On button is lit white when the X-MET8000 series is on.
Power On button
Press and hold the Power On button for 5 seconds to switch the X-MET8000 series on or off.
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The Touch Screen
Use these finger movements to control the X-MET8000 series.
FlickSlideTap
Tap a button or arrow to select or activate it.
Press and Slide to scroll a list up or down.
Flick a screen to left or right to display the previous or next screen.
The Virtual Keyboard
Use the virtual keyboard to type text into a text box. Tap the character, and it will pop up above the other keys. Release the character, and it appears in the text box. Tap the arrows on either side of the text box to move the cursor to the left or right.
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The Menu Screen
Tap Menu in the bottom right of the screen and the Menu screen appears. This gives access to the main functions of the X-MET8000 series.
The Menu screen is always available. Tap Menu, and then tap Home to immediately leave the current screen and cancel an operation.
The Status Bar
Tap the status bar at the top of the screen and the status bar screen appears. This contains information about the configuration and provides quick access to these settings. The status bar is always available.
1. Method name
2. Measurement time
3. Proximity indicator
4. Time
5. User level
6. Bluetooth and Wi-Fi
7. Battery level
The user level is shown as:
Operator: two people
Supervisor: one person
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The Tools Menu
When available, Tools appears in the middle at the bottom of the screen because a Tools menu is available. Not every screen requires a Tools menu. Tap Tools to make the Tools menu appear. The function of the Tools menu varies with the screen that it supports. These are two examples.
Take The First Measurement
The X-MET8000 series has factory settings which are applicable to many measurements. It is a good idea to give each sample a name, because it is easier to find it in the results history if it has one. Follow these instructions to take the first measurement.
Remember that the booklet ‘Safe, Accurate Measurements With The X-MET8000 Series’ contains important safety information, as well as guidance for accurate measurements.
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Switch On The X-MET8000 Series
Take the X-MET8000 series out of the transit case, and then follow these steps to switch it on.
1. Press and hold the Power On button for 5 seconds.
The X-MET8000 series powers on, and the Safety screen appears.
2. Tap Login in the bottom left of the Safety screen.
The Login screen appears, with the numeric keypad.
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3. Tap the numbers to type the password.
The factory settings are:
Operator: 1111
Supervisor: 0000
The supervisor should change the passwords. Refer to the X-MET8000 Series User Manual .
4. Tap Done.
The main screen appears. If the Proximity Safety Sensor has been disabled a warning message is shown. The Proximity Safety Sensor can be re-enabled by tapping Yes.
If it is necessary to set the date, time or language, refer to: X-MET8000 Series Settings on page
82.
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Add A Sample Name
Follow these steps to name the sample.
1. Tap Menu, and then tap Sample Name.
The Sample Information screen appears.
2. Tap Set Sample Name.
The Set Sample Name screen appears, with the virtual keyboard.
3. Use the virtual keyboard to type the Sample Name, and then tap Done.
4. Tap Done again to return to the main screen.
Take A Measurement
Follow these steps to measure the sample.
1. Carefully hold the X-MET8000 series so that it touches the sample, and that both the proximity
and measurement windows are covered.
Do not press the X-MET8000 series into the sample.
The proximity indicators change to green.
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2. Pull and hold the trigger firmly.
The X-ray On indicators blink red.
3. Keep the X-MET8000 series upright and steady during the measurement.
Use both hands to hold the X-MET8000 series and keep them away from the sample.
The Results screen refreshes approximately every 2 seconds.
4. At the end of the measurement time, the X-MET8000 series makes a ‘ping’ sound. Release the
trigger to stop the measurement.
The measurement stops, and the X-MET8000 series displays the result.
It is possible to release the trigger and stop the measurement before the ‘ping’ sound.
Follow these steps again to make the next measurement.
Flick the screen to left or right to access other results.
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The Results Screen
The Results screen has this information.
1
7
6
5
4
3
2
8
1. Sample name
2. Grade ID
3. Match level
4. The number of potential
matches
5. Element
6. % or PPM
7. +/-
8. Limit
This is defined in Add A Sample Name on page 16.Sample name
The grade or trade name for the sample. Tap the arrow on the left or right of the grade ID to display the next or previous possible match.
Grade ID
‘Good Match’ or ‘Possible Match’.Match level
There can be more than one match for the sample. The best match is always shown first.
The number of potential matches
The chemical symbol. If an element has a red background it is because it is outside the required limits for that grade.
Element
The measurement unit, for example %(percentage) or PPM(parts per million).
% or PPM
This indicates the precision(2 sigma) of the measurement. The lower the +/- value, the greater the precision.
+/-
The required limits for the grade.Limit
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Delete A Poor Measurement
Occasionally a poor measurement will occur. This can be because the sample is badly positioned, or because the measurement time is too short. The booklet ‘Safe, Accurate Measurements With The X-MET8000 Series’ contains guidance for accurate measurements. Follow these steps to delete a measurement from the Results screen.
1. Tap Tools when a result is visible.
The Results screen Tools menu appears.
2. Tap Delete Measurement.
A Warning dialog box appears.
3. Do one of the following:
Tap OK to delete the measurement.
Tap Cancel to not delete the measurement.
Print Result From Result Screen To Bluetooth Printer
Before printing the results, it is necessary to configure a Bluetooth Printer and select Connect as Printer option from the Tools menu in the Bluetooth Settings screen. Please refer to the Supervisor
manual to set this up. Follow these steps to print a measurement from the Results screen to a Bluetooth Printer.
1. Tap Tools when a result is visible.
The Results screen Tools menu appears.
2. Tap Print Result.
Device begins to send the result for the printing. In few seconds, result is printed at the Bluetooth Printer.
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Switch Off The X-MET8000 Series
Press and hold the Power On button for 5 seconds. The X-MET8000 series powers off.
Average A Batch Of Measurements
Sometimes it is necessary to average a batch of measurements on a larger, mixed sample. It is important that all measurements use the same conditions:
The same method
The same measurement time.
When all the measurements are complete, it is very easy to switch between the various results. The X-MET8000 series also provides comprehensive search facilities to find a series of measurements from the results history.
Sample And Batch Names
The X-MET8000 series automatically increments an index number appended to the sample name, and uses a separate name for a batch of measurements. For example, ‘Sample Batch’ could include ‘Sample 1’, ‘Sample 2’,’Sample 3’ and so on.
Which Method?
The method defines how the X-MET8000 series analyses the sample. The available methods depend upon the version of the X-MET8000 series.
Some of the method names include ‘FP’, for example Alloy FP, Mining FP or Soil FP. This refers to ‘fundamental parameters’, which is a complex mathematical algorithm to analyse materials.
The X-MET8000 series can include auto select modes, with a ‘Mode’ suffix. If an applicable mode is available, this is the first choice for the operator. These appear at the top of the method list, and include Alloy Mode, Alloy LE Mode, Mining Mode and RoHS Mode. Modes chose the most applicable calibration for the sample.
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The X-MET8000 series can include empirical calibrations. These are calibrations of specific elements with a specific concentration range, and include stainless steel, copper, titanium, iron and many other elements. An operator will not see these in the list of available methods. Only a supervisor can see these. An auto select mode can chose the correct empirical calibration for the sample, which makes analysis easier for the operator.
The X-MET8000 includes ‘LE’ in some of the method names, for example Stainless LE, Alloy LE FP or Alloy LE Mode. The LE refers to ‘light elements’, and these methods can analyse alloys that include magnesium, aluminum, silicon, phosphorous and sulfur.
Sometimes a mode is not able to fully measure a sample, because some of the concentrations in the sample are outside the limits for that method. If this occurs, a greater than, >, or less than, <, indicator appears next to the concentration.
When this occurs, the operator should choose an applicable ‘FP’ method. These work with a wider range of concentrations and sample types, and is the second choice for the operator.
Auto Select Modes Make Analysis Easy
Auto select modes make use of both empirical and fundamental parameter calibrations. Use the numbers in the illustrations to follow how Alloy LE Mode analyzes first stainless steel and then gold. It uses an empirical calibration for stainless steel, and a fundamental parameter calibration for gold. All steps happen automatically, and can make life very easy for an operator!
Alloy LE Mode, Empirical For Stainless Steel
These steps show how Alloy LE Mode uses an empirical calibration to analyze a stainless steel sample, and return the grade.
1. The X-MET8000 series acquires a spectrum to identify the sample.
2. It compares the identification spectrum with all the empirical calibrations to obtain a match.
3. It finds a match with the stainless steel empirical calibration, shown in green.
4. It uses the stainless steel calibration to analyze the sample and then display the results.
5. It compares the results with the grade library and finds SS316 is the best match.
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Alloy LE Mode, Empirical For Stainless Steel
Alloy LE Mode, Fundamental Parameter For Gold
These steps show how Alloy LE Mode uses a fundamental parameter calibration to analyze a gold sample, and return the grade.
1. The X-MET8000 series acquires a spectrum to identify the sample.
2. It compares the identification spectrum with all the empirical calibrations to obtain a match.
3. It does not find a match with any empirical calibration, all shown in red.
4. It switches to a fundamental parameter calibration and uses the internal calculator to analyze the
sample, compute and then display the results.
5. It compares the results with the grade library and finds 24 carat gold is the best match.
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Alloy LE Mode, Fundamental Parameter For Gold
How Long For A Measurement?
The factory set measurement time of 15 seconds is applicable for many measurements. Quicker measurements for iron, copper, nickel and similar alloys require as little as 5 seconds. Magnesium and aluminum alloys need longer measurement times, for example 30 seconds or more. Complex alloys also require longer measurement times to analyze all the trace elements.
Longer measurements will always give more precise results. However, the X-MET8000 series can provide excellent results in only a few seconds. The standard deviation, STD, figures indicate the measurement precision. The longer the measurement time, the lower the standard deviation figures, the greater the precision.
At the end of the measurement time, the X-MET8000 series makes a ‘ping’ sound. It is also possible to use the internal timer to fully control the measurement. This is known as ‘Timed Assay’. The operator
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pulls the trigger, and then releases it to start the measurement. The internal timer automatically stops the measurement.
When Timed Assay is off, the operator must release the trigger when the ‘ping’ sounds to stop the measurement. The Results screen refreshes approximately every 2 seconds, and the operator can decide to release the trigger before the ‘ping’ sounds to stop the measurement immediately.
Timed Assay is very useful for longer measurements and measurements with the bench-top stand. It is also useful to make sure that a batch of measurements all have the same measurement time.
It is possible to set the measurement time to zero. There is no ‘ping’ sound, and the operator must decide when to stop the measurement. If Timed Assay is off, the operator pulls the trigger to start the measurement, and then releases the trigger to stop the measurement. If Timed Assay is on, the operator pulls and releases the trigger to start the measurement, and then pulls and releases it again to stop the measurement.
Add The Sample And Batch Names
Follow the Add A Sample Name on page 16 steps to name the sample. Make sure that the sample name has a single word, then a space, then a number. For example, ‘Steel 1’ or ‘Alloy 1’, but not ‘Steel alloy 1’.
Follow the Add A Sample Name on page 16 steps again, but tap Set Average Result Name. Use the virtual keyboard to type the batch name.
Choose A Method
Follow these steps to choose a method.
1. Tap Menu, and then tap Method.
The Method screen appears.
2. Tap a method to choose it from the list of available methods. If the list of Methods is long, press
and slide the list to scroll it up or down.
The first preference is for a Mode, and these appear at the top of the list.
The second preference is for a method with an ‘FP’ suffix.
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3. Tap Done to return to the main screen.
Set The Measurement Time
Follow these steps to set the measurement time.
1. Tap Menu, and then tap Time.
The Measurement Time Settings screen appears.
2. For an average of a batch of measurements, tap Timed Assay ON.
Make sure that a tick appears in the correct Timed Assay tick box.
3. Tap Measurement Time.
The Set Measurement Time screen appears, with the numeric keypad.
4. Use the numeric keypad to type the measurement time, in seconds, and then tap Done.
5. Tap Done again to return to the main screen.
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Check The Status Bar
The status bar at the top of the screen shows the Method and Measurement Time. Check that the values shown are correct.
1. Tap the status bar to access the Method and Measurement Time.
The Status Bar screen appears.
2. Do one of the following:
If it is necessary to change one or the other, tap Method or Measurement Time to navigate
straight to the applicable settings.
Tap the status bar again to close it.
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Set The Batch Size
To assist an average of a batch of measurements, it is possible to set the number of measurements to average. Follow these steps to set the number of measurements.
1. Tap Menu, and then tap Settings.
The Settings screen appears.
2. Tap Result View Settings.
The Result View Settings screen appears.
3. Tap Average, and make sure that the tick appears in the box.
4. Tap Edit (pencil) next to Average.
The Set Number Of Measurements screen appears, with the numeric keypad.
5. Use the numeric keypad to type the number of measurements to average, and then tap Done.
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6. Tap Done twice again to return to the main screen.
Take Averaged Measurements
Follow the steps in Take A Measurement on page 16, but pull the trigger firmly, then release it. When Timed Assay is on, the internal timer controls the measurement and stops it automatically. When it is complete, the X-MET8000 series displays the result. The display includes both the individual result, and an average of all the results in the batch. Flick the screen to left or right to access other results.
The Average Results Screen
The Average Results screen has this information.
1. Sample name
2. Grade ID
3. Match level
4. The number of potential
matches
5. Average name
6. Average result
7. Element
8. % or PPM
9. Average
10. +/-
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This is defined in Add The Sample And Batch Names on page 24.Sample name
The grade or trade name for the sample. Tap the arrow on the left or right of the grade ID to display the next or previous possible match.
Grade ID
‘Good Match’ or ‘Possible Match’.Match level
There can be more than one match for the sample. The best match is always shown first.
The number of potential matches
This is defined in Add The Sample And Batch Names on page 24.Average name
The result number within the batch and the batch size.Average result
The chemical symbol. If an element has a red background it is because it is outside the required limits for that grade.
Element
The measurement unit, for example %(percentage) or PPM(parts per million).
% or PPM
The average concentration of the element across the batch.Average
This indicates the precision(2 sigma) of the measurement. The lower the +/- value, the greater the precision.
+/-
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Search The Results History
The X-MET8000 series has a search facility to find results with a specific name, date, or method. Follow these steps to search and manage the results history.
1. Tap Menu, and then tap History.
The History screen appears.
2. Tap Tools.
The History screen Tools menu appears.
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3. Tap one of the following Filter Results By options.
Name
Time
Method
The Search History screen appears, with the virtual keyboard when Name or Method is selected. And Set Date Range screen appears when Time is selected.
4. Use the virtual keyboard to type the item to search for, and then tap Go.
The History screen appears with search results.
5. Tap a measurement in the list to display the results.
The History Results screen appears.
6. To restore all the results to the History screen, tap Tools and then Restore.
The Tools menu now includes Filter Results By option.
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