Successfully cementing the casing string of an oil or gas well is highly
dependent upon the characteristics of the cement slurry. Properties that
should be considered include consistency, density, the ability to quickly
develop compressive strength, rheological properties, and ltration control.
Well cements that have poor ltration control can lead to a complete failure
of the cementing operation. In addition, the invasion of ltrates into producing
zones causes formation damage, which can greatly reduce the production
potential of the reservoir. Developing cement slurries that have minimal
ltration loss prevents expensive remedial cementing operations and reduces
formation damage. The OFITE Stirred Fluid Loss Tester provides a reliable
means of determining the uid loss characteristics of a well cement.
Overview
A cement slurry is poured into the test cell, which is then placed into the
heating jacket. The gear drive system is connected to the agitation paddle,
which is dimensionally equivalent to an atmospheric consistometer paddle.
The desired test temperature is maintained by a digital PID temperature
controller, while the necessary pressure is applied to the cell to prevent
evaporation of the liquid phase. When conditioning the cement in accordance
to API (American Petroleum Institute) Specication 10 guidelines, the paddle
is rotated at 150 rpm for 20 minutes. Once the cement is conditioned,
differential pressure is applied to the cell. The ltrate is collected in a back
pressure receiver for 30 minutes. The API denes uid loss as the volume
(ccs) of ltrate that is collected during this 30-minute interval.
-Temperature is maintained by a PID temperature controller
-Variable paddle rotation speed (5 to 200 rpm)
-Filtration portion of cell is dimensionally equivalent to an API approved
HTHP test cell
Setup
Operation
Preparing the Test Cell
1. Connect the instrument to a power source. Be sure to use the correct
voltage for your equipment.
2. Connect the instrument to a nitrogen source using the connector on the
back panel. The nitrogen source should be regulated between 2,000 and
2,500 psi.
3. Connect a drain and water supply to the back of the unit. All connectors
are ¼" NPT.
1. Begin by turning the test cell so that the end labeled "In" is facing up.
2. Apply high-temperature grease (#165-44) to a cell cap o-ring (#171-190-
060) and insert it into the groove inside the test cell.
3. To facilitate cleaning, a thin coat of white lithium high-temperature grease
may be applied to all surfaces that will come in contact with cement. This
includes the inside of the test cell, the paddle, and the inside surfaces of
the two cell caps.
4. Lubricate the threads on the paddle assembly cell cap. Press the poppet
valve into the closed position and insert the paddle into the test cell. Hand
tighten completely.
5. Screw the valve stem (#170-16) into the paddle assembly cell cap and
tighten it completely.
6. Turn the cell over. If possible, place the cell in a vise to prevent damage
to the valve stem.
7. Mix your cement slurry as directed in API
Specication 10 and pour no more than 425
mL into the test cell. Remove any cement
from the o-ring groove.
8. Apply high-temperature grease to another
cell cap o-ring (#171-190-060) and place it