NIVELCO AnaCONT LE-100, AnaCONT LP-100, AnaCONT LG-100 Installation And Programming Manual

Download

BKI 11 ATEX 0012 X le00100a0600p_05  1 / 60

AnaCONT

Manufacturer

Phone (36-1) (36-1)

E-mail: sales@nivelco.com www.nivelco.com

H-1043 Budapest, Dugonics u. 11.

: 889-0100 Fax: 889-0200

NIVELCO Process Control Co.

LE-100 LP-100

LG-100

Two-wire compact analytical transmitters

2 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

pH- and ORP- Dissolved oxygen

sensors and transmitters (compact type)

pH- and ORP- Dissolved oxygen

sensors and transmitters (integrated type)

BKI 11 ATEX 0012 X le00100a0600p_05  3 / 60

TABLE OF CONTENTS

1. INTRODUCTION.............................................................................................................................................................................................................................. 5

1.1. APPLICATION ............................................................................................................................................................................................................................ 5

1.2. OPERATION PRINCIPLE............................................................................................................................................................................................................... 5

1.2.1. Characteristics of an ideal pH electrode .......................................................................................................................................................................................................... 5

1.2.2. Characteristics of an ideal ORP electrode....................................................................................................................................................................................................... 6

1.2.3. Characteristics of an ideal DO sensor ............................................................................................................................................................................................................. 6

2. ORDER CODES............................................................................................................................................................................................................................... 7

2.1. CONFIGURATIONS.................................................................................................................................................................................................................... 11

3. TECHNICAL DATA........................................................................................................................................................................................................................ 16

3.1. TECHNICAL DATA OF THE PH ELECTRODES (INCLUDING EX VERSIONS) FOR LP-- INSTRUMENTS ................................................................................. 18

3.2. TECHNICAL DATA OF THE ORP ELECTRODES (INCLUDING EX VERSIONS) FOR LR-- INSTRUMENTS............................................................................. 20

3.3. TECHNICAL DATA OF THE DO SENSORS (INCLUDING EX VERSIONS) FOR LD-- INSTRUMENTS ..................................................................................... 22

3.4. ACCESSORIES......................................................................................................................................................................................................................... 22

4. MAINTENANCE AND REAPAIR................................................................................................................................................................................................... 23

4.1. STORAGE ............................................................................................................................................................................................................................... 23

4.2. PERIODIC SETTING, CALIBRATION AND VERIFICATION .................................................................................................................................................................. 23

4.2.1. Periodic calibration of the pH electrode ......................................................................................................................................................................................................... 24

4.2.2. Verification of the ORP electrode .................................................................................................................................................................................................................. 25

4.2.3. Periodic calibration of the DO sensor ............................................................................................................................................................................................................ 25

4.3. MAINTENANCE OF THE PH AND ORP ELECTRODES .................................................................................................................................................................... 27

4.4. MAINTENANCE OF THE DO SENSOR .......................................................................................................................................................................................... 29

4.5. SOFTWARE UPDATE................................................................................................................................................................................................................. 29

5. INSTALLATION............................................................................................................................................................................................................................. 30

5.1. MOUNTING.............................................................................................................................................................................................................................. 30

5.1.1. Installation of pH and ORP electrodes........................................................................................................................................................................................................... 30

5.1.2. Installation of DO sensor ............................................................................................................................................................................................................................... 31

5.1.3. Special application possibilities of the Integrated type instruments............................................................................................................................................................... 33

5.2. WIRING................................................................................................................................................................................................................................... 34

5.2.1. Wiring of Compact instruments...................................................................................................................................................................................................................... 34

5.2.2. Wiring of Integrated instruments.................................................................................................................................................................................................................... 35

5.3. LOOP CURRENT CHECKING WITH HAND INSTRUMENT.................................................................................................................................................................. 35

5.4. CONDITIONS OF EX APPLICATION .............................................................................................................................................................................................. 35

4 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6. PROGRAMMING ........................................................................................................................................................................................................................... 36

6.1. THE SAP-300 DISPLAY UNIT.................................................................................................................................................................................................... 36

6.2. MEASURING WITH THE SAP-300 DISPLAY UNIT.......................................................................................................................................................................... 37

6.3. PROGRAMMING WITH THE SAP-300 DISPLAY MODULE ............................................................................................................................................................... 40

6.3.1. Components of the programming interface ....................................................................................................................................................................................................40

6.3.2. Menu structure................................................................................................................................................................................................................................................41

6.4. PROGRAMMABLE FEATURES DESCRIPTION................................................................................................................................................................................. 42

6.4.1. Basic measurement settings ..........................................................................................................................................................................................................................42

6.4.2. Analogue output .............................................................................................................................................................................................................................................44

6.4.3. Relay output ...................................................................................................................................................................................................................................................45

6.4.4. Digital output...................................................................................................................................................................................................................................................47

6.4.5. Service functions ............................................................................................................................................................................................................................................47

6.5. PH SENSOR CALIBRATION........................................................................................................................................................................................................ 53

6.5.1. Editing one item of the calibration table..........................................................................................................................................................................................................53

6.5.2. Adding an item to the calibration table ...........................................................................................................................................................................................................55

6.5.3. Deleting an element of the calibration table ...................................................................................................................................................................................................55

6.5.4. Reset the calibration table to default ..............................................................................................................................................................................................................55

6.5.5. Calibration procedure .....................................................................................................................................................................................................................................55

6.6. DO SENSOR CALIBRATION....................................................................................................................................................................................................... 56

6.6.1. Calibration of saturated value (100%) ............................................................................................................................................................................................................56

6.6.2. Calibration of Zero point (0%).........................................................................................................................................................................................................................57

6.6.3. Calibration with referential DO instrument......................................................................................................................................................................................................57

6.6.4. Reset the calibration table to default ..............................................................................................................................................................................................................57

6.6.5. Reset Timer....................................................................................................................................................................................................................................................57

6.7. ERROR CODES ........................................................................................................................................................................................................................ 58

BKI 11 ATEX 0012 X le00100a0600p_05  5 / 60

Thank you for choosing a NIVELCO instrument.

We are sure that you will be satisfied throughout its use!

1. INTRODUCTION

1.1. APPLICATION

The AnaCONT compact transmitters, liquid analytical instruments are suitable for high precision measurement and transmission of acidity or alkalinity - pH (Hydrogen ion concentration) value -, reducing and oxidizing capability - ORP (Oxidation Reduction Potential) value -, or Dissolved Oxygen content of process water, wastewater, surface water, ground water and drinking water. These measurements can be widely used in industrial practice and could be of great relevance. In the field of environmental protection or sewage treatment, instruments like that are suitable for measuring the concentration of hazardous substances (chromium, cyanide). In chemical- and pharmaceutical industry, high precision measurement has utmost importance in the aspect of the technology (e.g. solvent feed), in many cases it is quality specification standard.

1.2. OPERATION PRINCIPLE

The intelligent signal processing of the electronics calculates the output signal from the voltage output values of the electrode and the temperature probe, and compensates it to 25°C. This value composes the basis of all output signals of the instrument.

1.2.1. Characteristics of an ideal pH electrode

he pH electrode immersed into the measured liquid measures a voltage value which is proportional to the hydrogen

ion concentration of the liquid.

 0mV output at neutral pH value (pH=7.00)  Positive voltage output in acidic liquids (pH<7)  Negative voltage output in alkaline liquids (pH>7)  Total measuring range is 0-14pH  -59.16mV/pH (Nernst potential) slope at 25 °C

 The temperature dependency of the Nernst potential is -0.001984 mV / °C.

600 500 400 300 200 100

0 100 200 300 400 500 600

100° C (74.04 mV/pH)

25° C (59.16 mV/pH)

0° C (54.20 mV/pH)

2 4 6 8 10 12 14

1 3 5 7 9 1 1 13

Because the pH electrodes in deed are not ideal (their properties depend on the design of the electrode, manufacturing tolerances and most of all the age of the electrode) the parameters differ from the given values above. To achieve reliable pH measurement and accuracy these electrodes must be calibrated from time to time. The time interval between two calibrations depends on the application conditions where the pH probes are used. Calibration of pH electrodes means offsetting the displayed value (7.00pH) when gauging neutral buffer solution, and adjusting the slope (pH/mV) by measuring buffer solutions with other pH value (usually with 4.00pH and 10.00pH value) by adjusting the displayed value to exact 4.00 and 10.00pH, respectively.

6 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

1.2.2. Characteristics of an ideal ORP electrode

 Negative voltage output in liquids with reduction potential,  Positive voltage output in liquids with oxidation potential,  Output voltage is equal to the redox potential (according to the Nernst equation)  pH independent measurement with certain types

To achieve reliable measurement and accuracy, these electrodes have to be thoroughly checked before installation and during usage from time to time. The time interval between two calibrations depends on the application and conditions where the ORP probes are used.

1.2.3. Characteristics of an ideal DO sensor

The dissolved oxygen level indicates the amount (in mg/l or ppm) of physically dissolved gas-form oxygen in liquid phase. Oxygen-permeable membrane amperometric DC sensor wetted in the measurement medium gives output

urrent proportional to the dissolved oxygen concentration of the medium.

air

zero

utp

ut c

rre

of the DO sensor

Dissolved oxygen (DO), ppm

sat´n0

Slope =

/ppm oxygen

Output current of the

DO sensor

The ideal DO sensor has:

 I

zero=0,

 Temperature independent output current

Real DO sensor gives off a minimal I

zero

≠0ppm current in case of 0 ppm dissolved oxygen concentration and its oxygen-permeable capability is temperaturedependent. Oxygen-permeable capability of the membrane is increasing according to the increase of the temperature, at 25 °C it can be 4%/°C. Temperature proportional correction is necessary for reliable measurement.

The DO sensors in deed are not ideal (their properties depend on the design of the electrode, manufacturing tolerances and most of all the age of the electrode), so the parameters differ from the given values above. To give reliable DO measurement and accuracy these electrodes must be calibrated from time to time. In case of DO sensors the calibration means that 0 ppm output value have to be set by offsetting in an oxygen-free solution. For DO measurement of other mediums (for example dry air 20.95%@25°C or oxygen-saturated water) adjustment of slope (nA/ppm) has to done accurately according to the properties of these mediums.

BKI 11 ATEX 0012 X le00100a0600p_05  7 / 60

2. ORDER CODES

Not all combinations possible!

AnaCONT instruments:

AnaCONT L - -

TYPE CODE FUNCTION CODE HOUSING CODE PROBE**

PROC. CONN. / MATERIAL

CODE OUTPUT CODE

Transmitter E pH P Plastic 1

BSP 1½ “ / PP 1 4 … 20 mA 2

Transmitter + display

G ORP R Aluminium 2

BSP 1½ “ / PVDF 2 4 … 20 mA / HART 4

Integrated P DO D

NPT 1½ “ / PP 4 4 … 20 mA / Ex 6 NPT 1½ “ / PVDF 5 4 … 20 mA / HART / Ex 8

4 … 20 mA / Relay R 4 … 20 mA / HART / Realy H

PH PROBE CODE ORP PROBE CODE DO PROBE CODE

4xpher112seph 1

4xorrherpseor 1 4x085g0023ydo

/ 20ppm

4xphed112seph 2

4xorrhexpseor 2 4x085g0022ydo

/ 10ppm

4xphex112seph 3

4xorrheptseor 3

4xpheph314sph 4

4xorrhespseor 4

4xphe1120seph 5

4xorrheppseor 5

4xphes112seph 6

4xorrheklseor 6 4xphep112seph 7 4xphekl112seph 8

* The order code of an Ex version should end in “Ex”! ** Probe selection is detailed in 3rd chapter.

8 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

The extension unit, adjustment unit and the sensor housing can be ordered to every analytical device, apart from the type of the electrode, measurement principal and measured quantity. Sensor protection tube is available only for LP--, or LR-- instruments.

EXTENSIONS L A – – 0

TYPE CODE MATERIAL CODE CODE LENGTH (L) CODE

Pipe R PP 1 0 0 m 0 m 0

Cable K PVDF 2 1 1 m 0.1 m 1

Suspended pipe F 2 2 m 0.2 m 2

3 3 m 0.3 m 3

4 4 m 0.4 m 4

5 5 m 0.5 m 5

6 6 m 0.6 m 6

7 7 m 0.7 m 7

8 8 m 0.8 m 8

9 9 m 09 m 9

A 10 m

PIPE EXTENSION: LAR--0 CABLE EXTENSION: LAK--0 SUSPENDED PIPE EXTENSION: LAF--0

BSP2"

Ø63

101

L = 0,2 - 3m

Ø3

Ø63

BSP2"

BKI 11 ATEX 0012 X le00100a0600p_05  9 / 60

SLIDING SLEEVE: L A A – 1 0 – 0

CODE

DN80 PN16 / PP 2

DN100 PN16 / PP 3

DN125 PN16 / PP 4

DN150 PN16 / PP 5

DN200 PN16 / PP 6

Console mounting bracket, 200 mm K

Mounting bracket, 200 mm T

SLIDING SLEEVE WITH FLANGE: LAA-10-0

DN80 - DN200

pH/ORP

CONSOLE MOUNTING BRACKET:

LAA-10K-0

MOUNTING BRACKET: LAA-10T-0

20 mm0

105

101

pH/ORP

FOR EXTENSION TYPE

ØA

=63.5MM

FOR BASIC TYPE

ØA

=70.5MM

BKI 11 ATEX 0012 X le00100a0600p_05  10 / 60

MATERIAL

SIZE

SENSOR PROTECTION TUBE: L A P

–

1 PP 1 1½”

0–0

2 PVDF 2 2”

PROTECTION TUBE 1½”: LAP-10-0

FOR EXTENSION TYPE

PROTECTION TUBE 2”: LAP-20-0

FOR BASIC TYPE

BSP1 1/2"

130

Ø51

BSP1 1/2"

112

BSP 2"

Sensor protection tube is available only for LP--, or LR-- instruments

BKI 11 ATEX 0012 X le00100a0600p_05  11 / 60

2.1. CONFIGURATIONS

COMPACT STANDARD TYPE: ANACONT LE--, LG--

(+SENSOR PROTECTION TUBE: LAP-20-0)*

INTEGRATED STANDARD TYPE: ANACONT LP --

(+SENSOR PROTECTION TUBE: LAP-20-0)*

BSP1 1/2"

120 160

~90

120

~200

Ø95

BSP1 1/2"

*Further configuration drawings show only compact types, however many accessories are available to order with integrated types. Essential dimension values are shown in the drawings of the standard types.

12 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

STANDARD TYPE: ANACONT L--

(+SENSOR PROTECTION TUBE: LAP-20-0)*

STANDARD TYPE: ANACONT L--

+ PIPE EXTENSION: LAR--0

(+SENSOR PROTECTION TUBE: LAP-10-0)*

~90

BSP1 1/2"

pH/ORP

112

BSP2"

BSP1 1/2"

108

As per order

codes

BSP 1 ½"

120

pH/ORP

Ø51

Ø63

* Sensor protection tube is available only for LP--, or LR-- instruments.

BKI 11 ATEX 0012 X le00100a0600p_05  13 / 60

STANDARD TYPE : ANACONT L--

+ PIPE EXTENSION : LAR--0

+ SLIDING SLEEVE WITH FLANGE: LAA-10-0

(+SENSOR PROTECTION TUBE: LAP-10-0)*

STANDARD TYPE: ANACONT L--

+ PIPE EXTENSION: LAR--0

+ CONSOLE MOUNTING BRACKET: LAA-10K-0

(+SENSOR PROTECTION TUBE: LAP-10-0)*

As per order codes

BSP 1 ½"

120

Ø51

108

pH/ORP

108

As per order codes

BSP 1 ½"

120

pH/ORP

Ø51

* Sensor protection tube is available only for LP--, or LR-- instruments.

14 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

STANDARD TYPE ANACONT L--

+ CABLE EXTENSION: LAK--0

(+SENSOR PROTECTION TUBE: LAP-20-0)*

STANDARD TYPE: ANACONT L--

+ CABLE EXTENSION: LAK--0

+ SUSPENDED PIPE EXTENSION: LAF--0

(+SENSOR PROTECTION TUBE: LAP-10-0)*

BSP 1 ½"

120

pH/ORP

112

BSP2"

BSP1 1/2"

175

s per order

codes

120

175

As per order codes

As per order

codes

1 ½"

110

Ø63

Ø51

BSP1 ½"

pH/ORP

* Sensor protection tube is available only for LP--, or LR-- instruments.

BKI 11 ATEX 0012 X le00100a0600p_05  15 / 60

STANDARD TYPE: ANACONT L--

+ CABLE EXTENSION: LAK--0

+ SUSPENDED PIPE EXTENSION: LAF--0

+ SLIDING SLEEVE WITH FLANGE: LAA-10-0

(+SENSOR PROTECTION TUBE: LAP-10-0)*

STANDARD TYPE: ANACONT L--

+ CABLE EXTENSION: LAK--0

+ SUSPENDED PIPE EXTENSION: LAF--0

+ CONSOLE MOUNTING BRACKET: LAA-10K-0

(+SENSOR PROTECTION TUBE: LAP-10-0)*

As per order codes

BSP 1 ½"

120

pH/ORP

175

s per order

codes

from DN80

Ø51

BSP1 ½"

As per order codes

BSP 1 ½"

120

pH/ORP

Ø51

BSP1 ½"

175

s per order

codes

* Sensor protection tube is available only for LP--, or LR-- instruments.

16 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

3. TECHNICAL DATA

GENERAL DATA

Material of sensor housing Polypropylene (PP), PVDF Electrode As per order code

Housing material

Compact type: Plastic: Glass fibre plastic PBT Metal: Powder paint coated Aluminium Integrated type: Same as the sensor housing

Medium temperature (pressure dependent) *

PP sensor housing: –10 °C ... +90 °C, PVDF sensor housing: -15 °C …. +100 °C with DO probe: 0 °C ... +50 °C

Ambient temperature Metal housing: -30 °C …+70 °C, Plastic housing: -25 °C … +70 °C, both with display: -20 °C … +70 °C

Pressure (absolute)*

With pH and ORP probe: 0.05 … 1 MPa (0.5 … 10 bar) @25°C With DO probe: 0,1…0,2 MPa (1…2 bar)@25°C

Sealing PP sensor housing: EPDM. all other sensor housing: FPM (Viton)

Ingress protection

Compact type: Sensor housing: IP 68, Housing: IP 67 (NEMA 6) Integrated type: IP 68

Power supply / Consumption 12 … 36 V DC / 48 mW … 720 mW, galvanic isolation, protection against surge transients

Electrode input

With pH and ORP probe: Combined electrode, galvanic isolation, input impedance: >10

ohm, connection: SN6.

With DO probe: Galvanic isolated current input, 0.725V polarisation voltage, connection: SN6

Liquid potential (complementary) electrode** Stainless steel housing of the temperature sensor (1.4571) , connection: SN6 Temperature measuring

(semiconductive sensor)

Range: -50…130°C, Accuracy: ±0.5°C, Resolution: 0.1°C

Analogue: 4 … 20 mA, (3.9 … 20.5 mA), R

tmax

= 1200 Ώ ( [Ut – 12 V] / 0.022 A)

galvanic isolation, protection against surge transients Relay: SPDT 30 V DC, 1A DC Display: SAP-300 (128x64 pixels monochrome LCD, 41x24mm with effective display interface)

Outputs

Serial line: (optional) HART interface, terminal resistor  250 ohm

Electrical connections

Compact type: 2 x M20x1.5 metal cable gland, cable diameter: 7 … 13 mm, or 2 x M20x1.5 plastic cable gland, cable

diameter: 6 … 12 mm; connecting cable cross section: 0.5 ... 1.5 mm

(shielded cable is recommended) +

internal thread 2x NPT 1 / 2" cable protective pipe

Integrated type: 6x0.5mm

shielded cable  6 mm x 5 m (up to max. 30 m cable length)

Electrical protection Class III. electric shock protection, less than 24V voltage feed

* Depends on the selected electrode! **In case of LP-- and LR-- instruments.

BKI 11 ATEX 0012 X le00100a0600p_05  17 / 60

EASUREMENT DATA

pH measurement

Range: 0…14pH, Reserve: ±2pH, Accuracy*: 0.1% of the measured value ±1 digit ±0.01% /°C, Linearity: ±0.004pH, Resolution: 0.01pH, (internal resolution 0.004pH), Measuring cycle: 300msec, on display: 1 sec

ORP measurement

Range: ±1000mV, Reserve: ±200mV, Accuracy*: 0.1% of the measured value ±1 digit ±0.01% /°C, Linearity: ±0.001%, Resolution: 0.1mV, Measuring cycle: 300msec, on display: 1sec

DO measurement

Range: 0…20ppm v. 0…10ppm, Reserve: 20%, Accuracy*: 0.5% of the measurement range ±1 digit ±0.01% /°C, Linearity: ±0.05ppm, Resolution: 0.01ppm, (internal resolution 0.005ppm), Measuring cycle: 300msec, on display: 1sec

* Depends on the selected electrode / sensor!

PECIAL DATA FOR EX APPROVED MODELS

Ex marking

II1G Ex ia IIB T6 Ga

Intrinsically safe data

Ci ≤ 15 nF, Li ≤ 200



H, Ui ≤ 30 V, Ii ≤ 140 mA, Pi ≤ 1 W

For Ex transmitter only Ex ia power supply should be used

Ex power supply Uo < 30 V, Io < 140 mA, Po < 1 W, power supply voltage range 12 V … 30 V, Rt

max

= [Ut – 12 V] / 0.022 A

Medium temperature

With pH and ORP probe: for PP sensor housing: –10... +70 °C, PVDF sensor housing: –15... +80 °C With DO probe: : 0… +50 °C

Ambient temperature Metal housing: -30 °C … +70 °C with display: -20 °C … +70 °C, Plastic housing : -20 °C … +70 °C

18 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

3.1. TECHNICAL DATA OF THE PH ELECTRODES (INCLUDING EX VERSIONS) FOR LP-- INSTRUMENTS

Type 4xpher112seph 4xphed112seph 4xphex112seph

Range [pH] 1...12 1...12 1...12 Process temperature °C 0…80 0…80 0…100 Max. process pressure [bar] 6 8 16 (<25°C), 6 (<100°C) Min. conductivity µs/cm 50 150 500 Diaphragm (the conductive aperture of the reference electrode)/electrolyte in closed glass-house

PTFE (Teflon) ring / 3 mol KCl 2 pcs ceramic rod / 3 mol KCl Concentrical gap/ 3 mol KCl

Connection / insertion length [mm] SN6 & PG13,5 / 120 SN6 & PG13,5 / 120 SN6 & PG13,5 / 120

Main application areas

Public and industrial

wastewater, process water,

drinking water, water in

chemical industry, water with

suspended solid particles.

Industrial water, drinking water,

slightly contaminated

wastewater, cooling tower

water, galvanic industry,

technologic water with Cr 6+,

Wastewater, process water, water

in chemical industry, emulsions,

suspensions, mediums containing

proteins or sulphides, water with

high concentration of solid

particles.

Not applicable for

Steam sterilization, water with

low conductivity, sudden

temperature changes.

Steam sterilization, water with

low conductivity, sudden

temperature changes.

Steam sterilization, water with low

conductivity, sudden temperature

changes. Clear water!!

Type 4xpheph314sph 4xphe112seph 4xphes112seph

Range [pH] 3...14 1...12 1...12 Process temperature °C 0…100 0…60 0…60 Max. process pressure [bar] 6 (<25°C), 3 (<100°C) 0.5 3 Min. conductivity µs/cm 150 150 150 Diaphragm (the conductive aperture of the reference electrode)/electrolyte in closed glass-house

Ceramic / 3 mol KCl Ceramic / 3 mol KCl Ceramic / 3 mol KCl

Connection / insertion length [mm] SN6 & PG13.5 / 120 SN6 & PG13,5 / 120 SN6 & PG13,5 / 120

Main application areas

Monitoring or controlling of

chemical processes of

mediums from neutral to very

alkaline.

Swimming pools, applications

in atmospheric pressure,

drinking water, slightly

contaminated wastewater.

Swimming pools, applications under pressure, drinking water, slightly contaminated industrial

and wastewater.

Not applicable for

Steam sterilization, water with

low conductivity, sudden

temperature changes.

Steam sterilization, water with

low conductivity, sudden

temperature changes, above

atmospheric pressure.

Steam sterilization, water with low

conductivity, sudden temperature

changes

BKI 11 ATEX 0012 X le00100a0600p_05  19 / 60

TYPE 4xphep112seph 4xphekl112sph

Range [pH] 1...12

1...12

Process temperature °C 0…80

0…60

Max. process pressure [bar] 6

Min. conductivity µs/cm 150

150

Diaphragm (the conductive aperture of the reference electrode)/electrolyte in closed glass-house

Ceramic / 3 mol KCl

Ceramic (polycarbonate)

Connection / insertion length [mm] SN6 & PG13,5 / 120

SN6 & PG13,5 / 120

Main application areas

Swimming pools, drinking water, process water,

slightly contaminated wastewater, electrolytic

metallization.

Swimming pools, drinking water, process water,

slightly contaminated wastewater.

Not applicable for

Steam sterilization, water with low conductivity,

sudden temperature changes.

Steam sterilization, water with low conductivity,

sudden temperature changes.

20 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

3.2. TECHNICAL DATA OF THE ORP ELECTRODES (INCLUDING EX VERSIONS)

FOR LR-- INSTRUMENTS

TYPE 4xorrherpseor 4xorrhexpseor 4xorrheptseor

Process temperature °C 0…80 0…100 0…60 Max. process pressure [bar] 6 16 (<25°C), 6 (<100°C) 1 Min. conductivity µs/cm 50 500 150 Diaphragm (the conductive aperture of the reference electrode)/electrolyte in closed glass-house

PTFE (teflon) ring / KCl Circular recess / solid electrolyte Ceramic

Connection / insertion length [mm] SN6 & PG13,5 / 120 SN6 & PG13,5 / 120 SN6 & PG13,5 / 120

Main application areas

public and industrial wastewater

process water drinking water

water in chemical industry

water with suspended solid particles

polluted water

emulsions, mediums containing

sulphides

high pressure applications

drinking water

pools in atmospheric pressure

slightly polluted water

Not applicable for

steam sterilization

water with low conductivity

sudden temperature changes

steam sterilization

water with low conductivity

sudden temperature changes

clean water

steam sterilization

water with low conductivity

sudden temperature changes

BKI 11 ATEX 0012 X le00100a0600p_05  21 / 60

TYPE 4xorrhespseor 4xorrheppseor 4xorrheklseor

Process temperature [°C] 0…60 0…80 0…60 Max. process pressure [bar] 3 6 3 Min. conductivity [µs/cm] 150 150 150 Diaphragm / electrolyte Ceramic Ceramic Ceramic (polycarbonate housing) Connection / insertion length [mm] SN6 & PG13,5 / 120 SN6 & PG13,5 / 120 SN6 & PG13,5 / 120

Main application areas

swimming pools

drinking water

slightly polluted water

drinking water process water

swimming pools

metallization

chemical applications

swimming pools

drinking water

slightly polluted water

Not applicable for

steam sterilization

water with low conductivity

sudden temperature changes

steam sterilization

water with low conductivity

sudden temperature changes

above atmospheric pressure

mediums containing ozone

steam sterilization

water with low conductivity

sudden temperature changes

22 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

3.3. TECHNICAL DATA OF THE DO SENSORS (INCLUDING EX VERSIONS) FOR LD-- INSTRUMENTS

TYPE 4x085g0023ydo (20 ppm) 4x085g0022ydo (10 ppm)

DO range [ppm] 0...20 0...10 Process temperature [°C] 0…50 0…50 Max. process pressure [bar] 1 1 Min. speed of medium-flow [m/s] 0,05 0,05 Response time [sec] 110 22 Accuracy [%; ppm] ±0.5 ; 0.1 ±0.5 ; 0.05 Life-span [year] 2-3 2-3 Material/thickness of the membrane PTFE / 125µm PTFE / 50µm

Other materials

PBT/PC, gold, silver, silver-chloride, potassium-

chloride

PBT/PC, gold, silver, silver-chloride, potassium-

chloride

Application area

Fish- and crawfish farms, water conditioning of large

aquariums, Controlling of oxygen concentration in

water-plants, determination of biological condition in

surface water

Potable water production, river monitoring, water

treatment sites, controlling of dissolved oxygen

level in wastewater plants, determination of

biological condition in surface water.

SAP-300 DISPLAY UNIT

Display 128 x 64 pixels monochrome LCD, with 41x24mm effective display surface

Ambient temperature – 20°C…+70°C

Storage temperature – 30°C…+80°C

Housing material PBT fibre glass plastic

3.4. ACCESSORIES

 Installation and programming manual,  Warranty Card  Declaration of Conformity,  2 pcs M20x1.5 cable glands,

 pH/ORP electrode (as per order code, separately packed with user manual)  DO sensor (as per order code, separately packed with user manual)  SAP-300 display unit (optional)  CD (EViewLight, DataScope softwares)

BKI 11 ATEX 0012 X le00100a0600p_05  23 / 60

4. MAINTENANCE AND REAPAIR

The AnaCONT series do not require maintenance on a regular basis, but the electrode (depending on the application) may need to be checked, cleaned, calibrated and replaced regularly. Repairs during or after the warranty period are carried out exclusively at the Manufacturer’s. Equipments sent back for repairs should be cleaned or neutralised (disinfected) by the User.

All sensors and electrodes including the NIVELCO recommended ones need proper storage, handling and calibration to have long life-time and give reliable measurement. Improper handling and lack of calibration will lead to unreliable measurement

4.1. STORAGE

DO sensors can be stored (under normal storage conditions) for a period of 12 month without shortening its lifecycle. The lifetime of pH and ORP electrodes is maximum one year (storage + usage). Prominent ships the electrodes hydrated in a well sealed container with a 3mol/l KCl solution in it. As a result, the membrane remains wet and the electrode is in ready-to-use state. It is important to keep these containers as they are needed for storing the electrodes during calibration or in case of transportation. If for any reason the electrodes are taken out of the process they must be put back into the storage containers containing storage liquid.

Notes: Never let the membrane and the diaphragm desiccated. Do not leave the electrode on open air longer than 10 minutes. If the electrode is warm it can desiccate even within a shorter period of time!

4.2. PERIODIC SETTING, CALIBRATION AND VERIFICATION

The electrode is exposed to different stresses, dependent on the measured medium, its ORP and pH value and the medium temperature. That is why the electrode needs to be recalibrated (its accuracy needs to be checked) between certain time intervals depending on the application utilizations. The calibration intervals may vary from few days to several weeks (max. 8 weeks).

24 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

4.2.1. Periodic calibration of the pH electrode

The calibration has to be done minimum in two measuring points (using two different buffer solutions). The calibration points have to be selected so that the widest measuring range is covered. The common calibration points are 4.00pH and 10.00pH, 4.00pH and 7.00pH, 7.00pH and 10.00pH, or even more points for example

4.00pH, 7.00pH and 10.00pH. Recommended solutions:

ORDER CODE DENOMINATION

4vpuf4ph50mph Buffer solution pH4 / 50 ml 4vpuf4ph250ph Buffer solution pH4 / 250 ml 4vpuf4ph100ph Buffer solution pH4 / 1 l 4vpuf7ph50mph Buffer solution pH7 / 50 ml 4vpuf7ph250ph Buffer solution pH7 / 250 ml 4vpuf7ph100ph Buffer solution pH7 / 1 l 4vpuf10ph50ph Buffer solution pH10 / 50 ml 4vpuf10ph25ph Buffer solution pH10 / 250 ml 4vpuf10ph10ph Buffer solution pH10 / 1 l 4vtarkcI 350ph Storage solution KCl 3 mol / 50 ml 4vtarkcl 250ph Storage solution KCl 3 mol / 250 ml 4vtarkcl 310ph Storage solution KCl 3 mol / 1 l 4vtiszold 25ph Cleaning solution / 250 ml

The given pH values refer to 25°C. The temperature dependency is given by the manufacturer, usually in a table on the label of the bottle.

The calibration procedure is described in chapter 6.5

BKI 11 ATEX 0012 X le00100a0600p_05  25 / 60

4.2.2. Verification of the ORP electrode

The calibration can be done (for example) with a 465 mV buffer solution. After the electrode is rinsed with distilled water put the electrode into the buffer solution. The electrode should reach the correct measurement value in 30 seconds. If the measured value is less with more than (the acceptable) 20mV the electrode should be cleaned. If the electrode does not give the desired measurement after cleaning it has to be replaced

Recommended solutions:

ORDER CODE DENOMINATION

4vpuf22050mor Buffer solution ORP 220 mV / 50 ml 4vpuf220100or Buffer solution ORP 220 mV / 1 l 4vpuf46550mor Buffer solution ORP 465 mV / 50 ml 4vpuf465250or Buffer solution ORP 465 mV / 250 ml 4vpuf465100or Buffer solution ORP 465 mV / 1 l 4vtarkcI 350ph Storage solution KCl 3 mol / 50 ml 4vtarkcl 250ph Storage solution KCl 3 mol / 250 ml 4vtarkcl 310ph Storage solution KCl 3 mol / 1 l 4vtiszold 25ph Cleaning solution / 250 ml

The given (mV) values refer to 25°C. The temperature dependency is given by the manufacturer, usually in a table on the label of the bottle.

4.2.3. Periodic calibration of the DO sensor

The calibration has to be done minimum in two measuring points. Calibration points should be selected according to the required range to cover almost or fully. In every case it is necessary for the calibration: one solution which does not contain any oxygen – may be a neutral gas – for the zero standard calibration, and an other solution which has a known oxygen concentration for the full-scale standard calibration.

Zero calibration is necessary, because DO sensor gives output current when the measured medium does not contain any dissolved oxygen. This current is called residual-current. The required zero-standard is an aqueous solution of sodium-sulphite (Na

2S03

) and cobalt(II)-chloride hexahydrate (CoCl2-6H2O) prepared

according to the followings. Oxygen-free nitrogen gas can be also used as zero-standard. The zero point calibration determines the offset of the calibration line.

Required items:

 1 clean pot  1 mixer  1 dl distilled water  1g sodium-sulphite (Na

2S03

)

 1mg cobalt(II)-chloride hexahydrate –Analytical Reagent– (CoCl

-6H2O)

26 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

Before the calibration pour the salts in the distilled water with continuous mixing.

For sensitivity calibration it is necessary a full-scale standard to determine the slope of the calibration line. Water solubility of oxygen at atmospheric pressure is well known dependent on temperature and pressure, so air-saturated water is a natural choice for full-scale standard. The air-saturated water is difficult to prepare and use. Usage of water-saturated air is a more general practice as a full-scale standard, because air-saturated water and water-saturated air are the same for the DO sensor. These are same standards, because the sensor is actually measuring the chemical potential of the oxygen. This chemical potential is a force driving through oxygen molecules from the sample through the membrane into the sensor. Output current of the sensor is proportional to the amount of oxygen driving through the membrane, so this current is determined by the chemical potential of the oxygen in the sample. The amount of oxygen is the same in air-saturated water and watersaturated air, so the chemical potential of the oxygen are also the same in both phases. Consequently the output current of the sensor is also the same in both cases.

Automatic calibration on air: The sensor should be simply hold in water-saturated air. The instrument measures the output current of the DO sensor, then store the measured value if stabilized and measures the temperature of the sample. It determines the saturation vapor pressure of the water from the temperature. Then it calculates the pressure of the dry air as the difference of atmospheric pressure and the saturation vapor pressure of the water. (Value of atmospheric pressure should be entered in the menu of the instrument as a parameter, default value is 1013mbar=101,3kPa) Considering the fact, that oxygen concentration of dry air is

20.95%, it calculates the partial pressure of the oxygen. Knowing the partial pressure of the oxygen, it calculates the amount of atmospheric dissolved oxygen in

equilibrium at a current temperature using the Bunsen solubility coefficient. This calculated value is assigned to the stored output current of the sensor.

Usually it is has many difficulties to dismount the instrument or the sensor from the technologic process for the calibration. In case of this, the sensor can be calibrated to a measurement value of a portable laboratory instrument in the same technologic process. Before this type of calibration, the laboratory instrument (usually also using oxygen-permeable membrane amperometric sensor) should be calibrated in water-saturated air. The calibration procedure is described in 6.6.

BKI 11 ATEX 0012 X le00100a0600p_05  27 / 60

4.3. MAINTENANCE OF THE PH AND ORP ELECTRODES

In this chapter you can find some recommendations regarding re-hydration, chemical cleaning and reactivation of the electrodes.

Disassembling the electrode

During this operation be careful not to expose the fragile electrode to mechanical (bending, squeezing, tensile) forces!

 Hold the electrode housing with one hand and the flare nut (right-threaded) with the other one

and loosen it completely.

 Then detach carefully the electrode housing from the instrument housing.  Loosen the electrode carefully using a socket-wrench (size 17) and screw it off completely.

Don't use a pipe- or a double-end wrench!

Put the electrode into the storage solution or perform the following steps below.

size 17

Re-hydration

If the electrode was desiccated due to incorrect use or storage it needs to be re-hydrated. This has to be done by soaking the electrode in 3mol/l KCl storage solution at 20°C for 24 hours. The process can be shortened to 6 hours if the KCl solution is at 60°C. Note: long time desiccation or desiccation after measuring crystallizating mediums may have an irreversible effect on the electrode and thus the re-hydration may not be successful.

Chemical cleaning

The deposits and obstructions on the surface of the electrode’s membrane and on the diaphragm have to be eliminated from time to time:

1. General deposits

 Rinse the electrode with warm water then dry up gently using a soft rag!  Soak the electrode for 15 mins in 1.5mol/l (5%) hydrochloric acid (HCl)!  Rinse the electrode again with warm water then dry up gently using a soft swab!  Soak the electrode for 1 hour in 3mol/l KCl solution then perform the calibration procedure!

28 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

2. Non-organic deposits

 Rinse the electrode with warm water then dry up gently using a soft rag!  Soak the electrode for 15 mins in 0.1 mol/l EDTA (ethylenediaminetetraacetic acid) solution!  Rinse the electrode again with warm water then dry up gently using a soft rag!  Soak the electrode for 1 hour in 3mol/l KCl solution then perform the calibration procedure!

3. Protein deposits

 Rinse the electrode with warm water then dry up gently using a soft rag!  Soak the electrode for 15 mins in 0.5 mol/l hydrochloric acid (HCl) or in 0.1 mol/l HCl and 0.1% pepsin mixture!  Rinse the electrode again with warm water then dry up gently using a soft rag!  Soak the electrode for 1 hour in 3mol/l KCl solution then perform the calibration procedure!

4. Silver sulphide deposits

 Rinse the electrode with warm water then dry up gently using a soft rag!  Soak the electrode for 15 mins in 0.1 mol/l thiourea and 1.5 mol/l (5 %) hydrochloric acid (HCl)!  Rinse the electrode again with warm water then dry up gently using a soft rag!  Soak the electrode for 1 hour in 3mol/l KCl solution then perform the calibration procedure!

Note: when deposits are hard to remove try using hydrogen peroxide or sodium hypochlorite solutions.

Reactivation

Regeneration of the glass membrane: The physical or chemical damage of the glass membrane slows down the operation of the electrode. The reactivation of the membrane helps restoring the normal operation of the electrode.

 Immerse ONLY the spherical part of the glass electrode into ammonium bifluoride with 10% concentration for 60 seconds then immediately

into 50-50% mixture of undiluted HCl and water for 10 seconds. This will neutralize the strong base!

 Soak the electrode for 12 hours in 3 mol/l hydrochloric acid (HCl)!  Rinse the electrode with water then dry up gently using a soft rag!  Soak the electrode for 1 hour in 3mol/l KCl solution then perform the calibration procedure!

BKI 11 ATEX 0012 X le00100a0600p_05  29 / 60

Reassembling the electrode

During this operation be careful not to expose the fragile electrode to mechanical (bending, squeezing, tensile) forces!

 Insert the electrode to its place carefully, screw it in with your hand and then with a socket-wrench

(size 17) carefully, until it reaches the level of the connector of the temperature sensor (

5.0

5.9

 

,see figure). Don't use a pipe-wrench or a double-end wrench!

 Assemble the instrument housing and the electrode housing then fasten the flare nut with your

hand. Pay attention to the encasement of the anti-rotation guides.

9.5

+ 0

- 0.5

s=17mm

4.4. MAINTENANCE OF THE DO SENSOR

During this operation be careful not to expose the fragile electrode to mechanical forces! Do not scratch, finger or touch the membrane of the sensor!

 Dismount the instrument from the technology process.  While holding the instrument in one hand rinse the membrane of the sensor with clean water.

If necessary some detergents could be used.

 Dry up the sensor gently using a soft rag.

4.5. SOFTWARE UPDATE

Based on the observation and needs of our customers NIVELCO constantly improves the operating software of the device. The software can be upgraded with the help of the ELink (USB) communication adapter plugged into the socket of the SAP-300 display. For software updates and for more information about software updates please contact NIVELCO.

30 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

5. INSTALLATION

5.1. MOUNTING

 When choosing the installation place please ensure proper space for later calibrations, verification or maintenance service. (see placement on page 32. )  Make sure that the transmitter is protected against overheating that can be caused by direct sunshine.  Assemble the electrode with the instrument prior to the installation.  It is advised to check the operation of the instrument prior to the installation in the control room.  If factory settings need to be modified do it according to the Programming Description.  The process connection should be selected according to the type to be installed.

ATTENTION!

When mounting or dismounting the instrument, avoid exposing the electrodes, DO sensors and temperature sensors to mechanical impacts because these can cause malfunctioning of the unit. The unit should not be loosened if the process is under pressure, in this case user should take care of depressurization first!

5.1.1. Installation of pH and ORP electrodes

Prior to mounting into the process the instrument should be put into operation-ready state. For this the user has to insert the electrode (packed separately) into the instrument as described below:

During this operation be careful not to expose the fragile electrode to mechanical (bending, squeezing, tensile) forces!

The housing of the instrument can be disassembled as described in chapter 4.3.

 Remove the plug in the electrode housing from the connector

of the electrode.

 Open the box and screw the electrode off the container.  Insert the electrode to its place carefully, screw in with your hand and

using a socket-wrench (size 17) until it reaches the level of the connector of the temperature sensor (

5.0

5.9





 Don't use a pipe-wrench or a double-end wrench!

size 17

9.5

+ 0

- 0.5

s=17mm

Assemble the instrument as described in Chapter 4.3. If the instrument is not installed immediately into the process the electrode should be put into storage solution to keep it wet.

BKI 11 ATEX 0012 X le00100a0600p_05  31 / 60

5.1.2. Installation of DO sensor

Prior to mounting into the process the instrument should be put into operation-ready state. For this the user has to insert the DO sensor (packed separately) into the instrument as described below:

During this operation be careful not to expose the fragile DO sensor to mechanical (bending, squeezing, tensile) forces!

 Remove the threaded protector- basket and the sponge-disc protector of the contacts.  Unpack the DO sensor and place it into a flat surface, downward with the plastic cap. Do not wipe the out the silione grease from the back of the

membrane! Silicone grease protect the contacts against short-circuit, even if water is infliltrated.

 With one hand hold the instrument upwards with its sensor, with other hand remove the (right-threaded) protector- basket of the sensor.  Place the sensor into the instrument with its cap that the pins of the sensor-nest can fit into the holes in the rear side of the sensor.  Remove the cap from the sensor and replace the protector- basket of the sensor.

TEMPERATURE

As it is shown in the diagram below – there may be a drop in the pressure-resistance according to the changes of the medium temperature, - which, in any case, should be considered, prior to the installation of the instrument into the technology process:

Depending on the location of the installation the instrument should be protected against any heat source or direct sunlight to avoid higher temperatures than specified!

32 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

PLACEMENT The instrument should be mounted within a max. 45° angle, compared to vertical position.

Types mounted with 4xphekl112seph / 4xorrheklseor electrode may be positioned horizontally as well!

If the unit is installed using a fitting piece the user has to assure that before and after the fitting piece there is a straight pipe with the appropriate length to minimalize sedimentation and turbulency. The influent section has to have min. 10xDN length while the effluent section has to have min. 3xDN length. It is advised to create a by-pass line so during the service of the instrument the electrode is kept wet or a calibration can be done without stopping the process.

>10 DN

>3 DN

LIQUID CONTINUITY

Near the electrode (sensor), the pipeline should always be filled with liquid:

BKI 11 ATEX 0012 X le00100a0600p_05  33 / 60

BUBBLE, FOAM Near the electrode (sensor), liquid in the pipeline should be free of bubbles or foam.

Installation of the threaded models

 Screw the unit into its place and tighten by hand. Don’t use any tool!  After tightening, the enclosure can be rotated to the proper position. (Safety bolt prevents rotation more than 350°).

5.1.3. Special application possibilities of the Integrated type instruments

Integrated type instruments can be installed in the same place with the medium to be measured. In this case of application, the maximal process pressure can not exceed 0.5 bar!

34 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

5.2. WIRING

The instrument operates from 12.5 … 36 V galvanic isolated and not grounded DC power supply in two wire system. (For Ex version: 12.5 … 30 V DC!) Sum of the resistance of the equipped instruments, between the transmitter and the power supply, mainly depends on the supply voltage of power supply applied, and the overall resistance value cannot exceed 1200 ohms. In case of using HART interface – to achieve proper communication between the transmitter’s interface and the power-supply – a minimal 250 ohms resistance should be maintained within the network.

5.2.1. Wiring of Compact instruments

The instrument should be wired with shielded cable led through the cable gland. The wiring of cables can be done after removing the cover of the instrument and the SAP display unit.

 Make sure that the power supply is turned off at the source.  After removal of the cover of the housing and taking the display module (if any) out,

the wiring cables can be connected. (Recommended cable: shielded, two-wire, with

0.5 ... 1.5 mm2 cross section. Connect shielding to grounding by the inner or outer grounding screw first.

 Switch on the unit. After switching of the unit, necessary programming can be done.  After the wiring, adjustment and programming, check proper sealing and close the

cover carefully.

IMPORTANT: - The housing of the transmitter should be grounded to the EPH network. Resistance of the EPH network should be R  2 ohm measured from the neutral. Shielding of the cable should be grounded at the control room side to the EP network. To avoid disturbing noises, keep away of closeness to high-voltage cables. Especially critical can be the inductive couplings of harmonics (which are present at frequency converter control) because even cable shielding does not supply effective protection against these cases.

RELAY

Display unit connector

Loop current measuring connect or

4...20 mA loop current and supply (HART)

GND

1/2” NPT

M20x1,5

23456

4 6

(Only normal version)

2 3

The instrument may be damaged by electrostatic discharge (ESD) via its terminal, thus apply the precautions commonly used to avoid electrostatic discharge e.g. by touching a properly grounded point before removing the cover of the enclosure.

BKI 11 ATEX 0012 X le00100a0600p_05  35 / 60

5.2.2. Wiring of Integrated instruments

The insrument can be connected directly to the suitable power suply unit. When extending the cable, a junction box is needed to use for this purpouse. Shielding should be connected with the shield of the extending cable and should be grounded at the signal processing device.

 Make sure that the power supply is turned off at the source.  (Recommended cable: shielded cable with 6 x 0.5 mm

or greater cross section).

 Turn on the power supply. After switching of the unit, necessary programming can be

done.

Colour codes of the wires:

Green – C1 relay output White – I One point (polarity-independent) of loop current, power supply and HART Yellow – CC relay output Brown – I Other point (polarity-independent) of loop current, power supply and HART Grey – C2 relay output Black – GND Grounding and shielding point

White

Green

Yel lo w

Grey

Braun

Black

Function box

Power supply

Power supply +HART +Current output

HART modem

white (brown) brown (white)

green

black

C1 C2

yellow

grey

TRA NSM IT TER

IMPORTANT: The shielding of the transmitter should be grounded at the control room side to the EPH network. Resistance of the EPH network should be R  2

ohm measured from the neutral. To avoid disturbing noises, keep away of closeness to high-voltage cables. Especially critical can be the inductive couplings of harmonics (which are present at frequency converter control) because even cable shielding does not supply effective protection against these cases.

5.3. LOOP CURRENT CHECKING WITH HAND INSTRUMENT

After removing the cover and lifting the Display Module, the actual loop current can be measured with an accuracy of ~ 5% by connecting a voltmeter (in the range of 200 mV) to the points indicated on the drawing above.

5.4. CONDITIONS OF EX APPLICATION

 Intrinsically safe units with Ex ia IIB marking can only be used in certified intrinsically safe loops with the previously given technical data. (see values in special

data for Ex approved models under Point 3).

 The size of the macrolon window of intrinsical safe equipment with metallic enclosure exceeds the limit, thus the devices must be protected against electrostatic

charges.

 Equipment with plastic housing are susceptible to electrostatic charges, thus the deivces must be protected against electrostatic charges.  The aluminium content of equipment with metallic enclosure exceeds the limit, the devices must be protected against impact and friction effects.  Devices should be grounded by connecting their grounding screws to the equipotential system.

36 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6. PROGRAMMING

The AnaCONT instruments can be programmed with the SAP-300 display unit. Without SAP-300 the following LEDs can be seen:

 RELAY Indicates the energised state of the relay (C2 closed, C1 open)  VALID Indicates the measuring capability of the unit. If lit, the input signal is stabilised.

If blinking,the input signal is changing.

 COM Indicates digital (HART) communication. During Remote programming LEDs are

continuously illuminated.

When SAP-300 display is present, LEDs are not visible; functions are taken over by the display. In default state SAP display shows the primary measured value (which the output current is calculated from). Programming is supported by a text-based menu. Navigation is done by using the

/ / / buttons.

The instrument can operate without the SAP-300 module as well. Programming can be done only by using SAP-300 display module locally or by HART (REMOTE PROGRAMMING) communication system remotely.

6.1. THE SAP-300 DISPLAY UNIT

The SAP-300 is a 64x128 dot-matrix LCD display which can be plugged into the transmitter. (Universal – usable in other NIVELCO devices as well – provided that the system software supports SAP-300.)

Warning!

The SAP-300 module is based on LCD technology, so please make sure it is not exposed to permanent heat or direct sunlight, in order to avoid damage of the display unit. If the instrument cannot be protected against direct sunlight or high temperature that is beyond the standard operating temperature range of the SAP-300, please do not leave the SAP display in the instrument.

BKI 11 ATEX 0012 X le00100a0600p_05  37 / 60

6.2. MEASURING WITH THE SAP-300 DISPLAY UNIT

Elements of the display:

1. Primary value (PV), in a dimension depended on the type of the instrument

2. SENSOR VOLTAGE – informative data in case of pH measurement

3. Trend direction arrows. The empty triangle shows when the measured value is small, the filled triangle shows

large-scale change. If none of the arrows are shown the measured value is constant.

4. Measured value in relation to measurement range (Sensor range) in a bargraph.

5. Temperature is shown for temperature compensation (measured by internal sensor).

After the dimension, the temperature compensation mode is indicated by inverse inscription: Any possible errors during measurement are shown in the lower part of the display.

Manual mode (see 6.4.1.3)

Temperature simulation active (see 6.4.5.8)

Temperature sensor error. In this case the instrument will compensate to 25 ºC.

6. Indication of primary value simulation. In this case the display and output will show the values of the simulation

and not the measured value.

7. Measured value normalized to 25˚C, 760Hgmm and Salinity=0 – informative data (only for DO transmitters)

8. Oxygen saturation (only for DO transmitters)

During active simulation the critical measurement errors will be displayed to give information to the user.

pH measurement

ORP measurement

DO measurement

38 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

A. Calculated value of the output current. After the dimension, the mode of current output is indicated by inverse inscription:

Manual mode (see 6.4.2.1)

HART address is not 0, so output current has become overwritten to 4mA (see 6.4.2.1)

Analogue transmission reacts to a programmed failure condition if an upper or lower fault current is programmed. (see 6.4.2.4)

B. Output range (4…20mA) indicated in a bargraph.

C. Relay state indication: if deenergized – C1 closed, C2 open, there is no indication. If RELAY message is visible, the relay is energised – C2 closed, C1 open.

D. Indication of Menu Lock:

 If key symbol is visible, the unit is protected with a password. When entering the menu, the instrument asks for the correct password.  If REM message is visible, the instrument is in remote programming mode and the menu cannot be accessed.

Errors occurred during the measurement can be seen at the bottom line of the display.

BKI 11 ATEX 0012 X le00100a0600p_05  39 / 60

Information displays:

Press button to cycle between the information displays.

1. The general information display (DEV. INFO): overall

running time (OV. RUN TIME), run time after power on (RUN TIME), type of interface (INTERFACE), relay (RELAY) and logger (LOGGER) indication.

2. Sensor information: time passed after last sensor

change, slope and offset after sensor change, time passed after last calibration, slope and offset at last calibration, minimum / maximum temperature of the sensor.

In case of DO measurement in addition to these: atmospheric pressure (PRESSURE) and salinity (SALINITY).

3. Relay information: number of switchings, total energised

time (C2 closed) (only if there is a relay in the unit).

The informative display switches back to main screen after 30 seconds.

By pressing the

button the user can get back to main screen at

any time.

Pressing the E button in any of the displays the user can enter to menu. After exiting the menu always the main screen will be shown.

Information display of pH

measurement

RUN TIME: 0.1h

OV. RUN TIME: 1.0h

RELAY: YES

INTERFACE: HART

- DEV. INFO ---0:1.00

LOGGER: NO

EN. TIME 15.2h

SW. COUNT 11

STATE: ON

--- RELAY INFO ------

T : 26.5°C Io: 12.00mA

RELAY

700mV

S1: 00mV

RUN TIME: 42d

RUN TIME: 5d

-- LAST CALIBRATION -

--- SENSOR INFO -----

SC: 03mV T: -5°C/ 70°C

Information display of ORP

measurement

Information display of DO

measurement

40 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.3. PROGRAMMING WITH THE SAP-300 DISPLAY MODULE

When entering the menu the instrument makes a copy of the actual parameters, all changes are done to this duplicated parameter set. During programming the instrument keeps measuring and transmitting with the current (and intact) parameter set. After exiting the menu the instrument replaces the original parameters with the new parameter set and will measure according the new parameters. This means that the change of the parameters does not become immediately effective when pressing the E button!

Entering the menu can be done by pressing the E button while exiting the menu can be done by pressing the button. If the instrument is left in programming mode after 30 mins it will automatically return to measuring mode. If the SAP display is removed during programming the instrument immediately returns to measuring mode.

As programming with SAP-300 (manual programming) and HART (remote mode) programming is not possible at the same time use only one programming method at a time. Measured values can be read out through HART at any time

6.3.1. Components of the programming interface

The parameters of the instrument are grouped according to their functions. The programming interface consists of lists, dialog windows, edit windows and report windows.

Lists

Navigation between the lines of a list can be done by pressing / buttons. Pressing the E button activates a list item. Selected list item is marked with inverse colour. Exit from a list by pressing the

button.

Menu list

Menu list is a specialized list. Its characteristic is that upon selecting a list item we directly get into another list, and these lists are opening from each other in different levels.

The menu header (1) helps to navigate.

Entering the menu can be done by pressing the E button. Navigation between the menu items can be done by pressing the

/ buttons. Enter to the selected menu by pressing the E button. The selected list item

is marked with inverse colour.

Exit from a submenu with

button. Pressing the button in the main menu will exit programming mode and

the instrument will return to measuring mode.

BKI 11 ATEX 0012 X le00100a0600p_05  41 / 60

Dialog window

The system sends messages or warnings using dialog windows. These usually can be acknowledged by pressing the

button or the user can choose between two options (usually YES or NO) by pressing /

buttons. In some cases to correct an error one of the parameters has to be changed

WARNING LOAD DEFAULT TO PARAMETER TABLE! ARE YOU SURE?

[YES] [NO]

Edit window

An edit window is used for modifying a numeric parameter value. The selected character can be changed using the

/ buttons. The cursor can be moved to left, using the button. The direction of the cursor movement through the digits is right to left. Changed value can be validated by pressing the E button. The software checks if the entered value is appropriate, exiting the edit window is only possible after entering a correct value. If the entered value is uninterpretable the software sends an error message in the bottom line (1) of the display. The display gives the same error message, independently of the measured value and the measurement principle.

PV: primary Value

Edit window – button combinations

In the edit window the following button combinations are available:

1. Recalling the parameters to the state before editing ( + , pressed for 3 secs);

2. Recalling default parameters (

+ , pressed for 3 secs);

3. Inserting (currently) measured value to the edit window (

+ , pressed for 3 secs)

Only for certain parameters!

6.3.2. Menu structure

Main menu

BASIC SETUP Parameter group of the basic measurement parameters

OUTPUT SETUP Parameter group of the output parameters

SERVICE Service functions, calibration, test and simulation

42 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.4. PROGRAMMABLE FEATURES DESCRIPTION

6.4.1. Basic measurement settings

6.4.1.1 Measuring unit (Only for DO measurement)

Parameter: P02: b Menu path: BASIC SETUP / MEASURING UNIT Default value:

Dimension of PV: primary value. ppm

 ppm  mg/l  %sat

Description:

Primary values are the same in case of displaying ppm and mg/l, only displayed and transmitted dimension changes. Large number on the screen follows the dimension of ppm and mg/l in the setting of ppm and mg/l. In case of choosing %sat, large numbered primary value indicates the oxygen saturation.

6.4.1.2 Damping time

Parameter: P20 Menu path: BASIC SETUP / DAMPING TIME Default value:

measurement

ORP

measurement

Description: Damping time is used to damp the unwanted fluctuations of the output and

display. If the measured value changes rapidly the new value will settle with 1% accuracy after this set time

2 sec 2 sec 2 sec

6.4.1.3 Temperature compensation mode

Parameter: P06: a Menu path: BASIC SETUP / TEMP. COMPENSATION / MODE Default value:

AUTO

Description: Mode of the temperature compensation

 AUTO Compensation is done with the value measured by the temp. sensor.  MANUAL Compensation is done with a predefined temperature value

(see 6.4.1.5)

 OFF No compensation

BKI 11 ATEX 0012 X le00100a0600p_05  43 / 60

6.4.1.4 Temperature compensation unit

Parameter: P02: a Menu path: BASIC SETUP / TEMP. COMPENSATION / UNIT Default value: Description: Dimension of the temperature measurement

 ºC  ºF

ºC

6.4.1.5 Temperature compensation fixed value

Parameter: P07 Menu path: BASIC SETUP / TEMP. COMPENSATION / MANUAL VALUE Default value: Description: Value of the manual temperature compensation (see 6.4.1.3)

25 ºC

6.4.1.6 Salinity correction value (Only for DO measurement)

Parameter: P23 Menu path: BASIC SETUP / SALTINITY CORRECTION / MANUAL VALUE Default value: Description: Value of the salinity correction in ppt (parts per thousand)

0 ppt

6.4.1.7 Pressure correction unit (Only for DO measurement)

Parameter: P02: c Menu path: BASIC SETUP / PRESSURE CORRECTION / UNIT Default value:

Hgmm

Description: Dimension of the atmospheric pressure correction

 Hgmm Compensation is performed by the measured value of the

temperature sensor

 bar Compensation is performed by a fix given temperature value.  kPa Compensation is off

Measurement unit is required to be selected first and value should be entered after this.

6.4.1.8 Pressure correction value (Only for DO measurement)

Parameter: P22 Menu path: BASIC SETUP / PRESSURE CORRECTION / MANUAL VALUE Default value: Description: Value of the atmospheric pressure correction

Measurement unit is required to be selected first and value should be entered after this.

760 Hgmm

44 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.4.2. Analogue output

6.4.2.1 Output current mode

Parameter: P12: b Menu path: OUTPUT SETUP / ANALOG OUTPUT / CURRENT MODE Default value:

AUTO

Description: Transmission mode of the current output [AUTO, MANUAL]

 AUTO The output current is calculated from the measured value, output is

active.

 MANUAL The output current is fixed at a constant (set) value (see 6.4.2.5). In

this mode the setting of the error current (see 6.4.2.4) is irrelevant. The set (current) value overwrites the 4mA output of HART multidrop mode!

6.4.2.2 Output current value 4mA

Parameter: P10 Menu path: OUTPUT SETUP / ANALOG OUTPUT / 4mA VALUE Default value:

pH measurement ORP measurement DO measurement

Description: Measured value assigned to 4mA

0 pH - 1000 mV 0 ppm

6.4.2.3 Output current value 20 mA

Parameter: P11 Menu path: OUTPUT SETUP / ANALOG OUTPUT / 20mA VALUE Default value:

pH measurement ORP measurement DO measurement

Description: Measured value assigned to 20mA

14 pH 1000 mV 8.24 ppm

6.4.2.4 Output current error mode

Parameter: P12: a Menu path: OUTPUT SETUP / ANALOG OUTPUT / ERROR MODE Default value:

HOLD

Description: Error indication by the current output

 HOLD Error indication has no effect on the output current.  3.8 mA Error indication: the output current gets 3.8mA.  22 mA Error indication: the output current gets 22mA

Attention! Also see chapter 6.4.2.1!

BKI 11 ATEX 0012 X le00100a0600p_05  45 / 60

6.4.2.5 Fixed output current

Parameter: P08 Menu path: OUTPUT SETUP / ANALOG OUTPUT / MANUAL VALUE Default value:

4 mA

Description: Parameter for setting the fixed output current

Values between 3.8 and 20.5 can be entered. The output current will be set to the entered value and analogue transmission will be suspended. . (see 6.4.2.1) The set (current) value overwrites the 4mA output of HART multidrop mode!

6.4.3. Relay output

6.4.3.1 Relay output mode

Parameter: P13: a Menu path: OUTPUT SETUP / RELAY OUTPUT / MODE Default value:

OFF

Description: Relay operating mode:

 OFF Relay off (C1 closed, C2 open)  PH/ORP/DO Relay operation assigned to the measured pH / ORP / DO value  TEMP Relay operation assigned to the measured temperature  ON ERROR Relay operates on critical errors

6.4.3.2 Relay output functions

Parameter: P13: b Menu path: OUTPUT SETUP / RELAY OUTPUT / FUNCTION Default value: Description: Relay operation functions: HYSTERESIS

HYSTERESIS

Differential control. (ex.: for controlling tasks)

If the two switching values are close to each other it will operate as a limit switch.

C2 OPEN

, T

EN < DEN

DEN EN

C2 CLOSED

C2 OPEN

PV, T

EN > DEN

EN DEN

WINDOW

Window comparator mode (ex.: for monitoring a range).

H1=H2=0.05pH or 0.05 ºC

, T

EN < DE N

DEN EN

C2 CLOSED

C2 OPEN

, T

EN > DE N

EN DEN

C2 CLOSED

C2 OPEN

PV: Primary Value – pH measurement: pH, ORP measurement: mV, DO measurement: ppm

46 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.4.3.3 Relay output energised value

Parameter: P14 Menu path: OUTPUT SETUP / RELAY OUTPUT / ENERGIZED VALUE (EN) Default value:

pH measurement ORP measurement DO measurement

Description: Value of the relay when it will become energised (C1 open, C2

closed)

0 pH - 1000 mV 0 ppm

6.4.3.4 Relay output de-energised value

Parameter: P15 Menu path: OUTPUT SETUP / RELAY OUTPUT / DEENERGIZED VALUE (DEN) Default value:

pH measurement ORP measurement DO measurement

Description: Value of the relay when it become deenergised at (C1 closed,

C2 open)

14 pH 1000 mV 8.24 ppm

6.4.3.5 Relay switching (ON/OFF) delay

Parameter: P16 Menu path: OUTPUT SETUP / RELAY OUTPUT / DELAY Default value: Description: Delay time of the relay switching On or Off (0 – 99 sec)

0 sec

6.4.3.6 Relay inverted operation

Parameter: P13: c Menu path: OUTPUT SETUP / RELAY OUTPUT / INVERTING Default value: Description: Relay operation

 NO Normal operation  YES Inverted operation

BKI 11 ATEX 0012 X le00100a0600p_05  47 / 60

6.4.4. Digital output

6.4.4.1 HART polling address

Parameter: P19 Menu path: OUTPUT SETUP / SERIAL OUTPUT / ADDRESS Default value:

Description: HART polling address (only HART capable types)

The polling address can be set between 0 and 15. For a single instrument the polling address is 0 and the output is 4...20mA (analogue output). If multiple units are used in HART Multidrop mode (max. 15pcs) the polling addresses should differ from 0 (1-15), in this case the output current will be fixed at 4mA. The fixed 4mA output can be overwritten as described in chapter

6.4.2.5.

6.4.5. Service functions

6.4.5.1 Security codes

User security code

Parameter: - Menu path: SERVICE / SECURITY / USER LOCK Default value:

Description: Setting or unlocking the user security code.

The instrument can be protected against unauthorized programming with a 4 digit PIN (Personal Identification Number) code. If either of the digits differs from 0 the code is active. If zero is specified, then the secret code has been deleted! In case of Active code, this code is requested at menu entry.

Service code

Parameter: Menu path: SERVICE / SECURITY / SERVICE LOCK

Description: Setting of the service code (only for trained personnel)!

48 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.4.5.2 Loop test

Parameter: P80 Menu path: SERVICE/OUTPUT TEST / ANALOG OUTPUT Description: Loop current test (mA)

Values between 3.9 and 20.5 can be entered. The output current will be set to the entered value. The measured current on the output should be equal to the set value. In test mode a dialog window warns the user of the fixed output current until the user exits the warning message window. Exiting can be done by pressing the

button.

6.4.5.3 Relay output test

Parameter: P81 Menu path: OUTPUT SETUP / TEST / RELAY OUTPUT Description:

Used for the testing of the relay output. Pressing the

and buttons the relay will change state.

When in this menu point the programmed relay operation is not taken into consideration.

 DEENERGIZED Relay is de-energised  ENERGIZED Relay is energised

6.4.5.4 pH Sensor calibration

Parameter: Menu path: SERVICE / SENSOR CALIBRATION Description: Calibration of the pH sensor (electrode) (see 6.5).

 VIEW/EDIT TABLE Table overview  ADD ITEM Addition of a calibration point  DELETE ITEM Deletion of a calibration point  RESET TO DEFAULT Resets the calibration table to default  RESET TIMER Resets the inner timer of the pH electrode life-time monitoring routine. This timer is NOT a real-time

clock. It only counts when the instrument is powered. Its value is saved in a non-volatile memory

BKI 11 ATEX 0012 X le00100a0600p_05  49 / 60

6.4.5.5 ORP Sensor calibration

Parameter: - Menu path: SERVICE / SENSOR CALIBRATION Description: Calibration of the ORP sensor.

 SET ZERO POINT Setting the zero point of the sensor

1. Measured value (without setting).

2. Real (measured) value at the zero point of the sensor

Use a 0 mV buffer solution. Dip the sensor into the buffer solution and wait until the measured value (1) becomes stabilised! Set the uncalibrated measured value (1) in the edit field using the

, and buttons. By pressing and simultaneously the measured value can

be entered to the edit field.

SENSOR SETUP

PARAMETER EDITOR

SET ZERO POINT

3mV mV

00053

1 2

Entering the SERVICE / SENSOR CALIBRATION menu the instrument will display a warning message that the user is about to change critical parameters of the measurement system. The user can enter the menu by pressing the

(OK) button or exit to the previous menu by

pressing the

(NO) button. In the next dialogue the software asks the user if the calibration of the sensor is the „first” calibration (after a

new sensor is installed) or not. Select OK or NO buttons. If OK button is selected the stored informational parameters of the previous sensor are reset to default values. Select (NO) button if it is not a „first” setting.

6.4.5.6 DO Sensor calibration

Parameter: - Menu path: SERVICE / SENSOR CALIBRATION Description: Calibration of the DO sensor. Calibration process is described at chapter 6.6.

Calibration shall be performed in air or referential liquid, sanity is zero in both cases.

 CAL. IN AIR (SPAN) Calibration of saturated value (100%sat) with sensor in air (8.24ppm / [25˚C, 760Hgmm])  CAL. IN ZERO SOL. Calibration of the Zero point in referential liquid.  CAL. IN SPAN SOL. Calibration of the saturated value (100%sat).  RESET TO DEFAULT Resets the calibration table to default  RESET TIMER Resets the inner timer of the pH electrode life-time monitoring routine.

This timer is NOT a real-time clockIt only counts when the instrument is powered. Its value is saved in a non-volatile memory

50 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.4.5.7 Simulation

This function helps the user to check the outputs and the additional processing instruments connected to the output. (Irrespectively of the instruments) To start simulation the instrument must return to Measuring mode.

Simulation mode

Parameter: P84: a Menu path: SERVICE / SIMULATION / MODE Default value:

OFF

Description: Simulation mode: OFF No simulation FIX VALUE Its value is set according to the lower range value of pH / ORP

simulation

TRIANGLE WAVE

The simulated value changes linearly between the set low and high values with an adjustable cycle time.

PV: Primary Value

SQUARE WAVE The simulated value jumps between the set low and high values

with an adjustable cycle time.

Simulation cycle

Parameter: P85 Menu path: SERVICE / SIMULATION / TIME Default value: Description: Cycle time of the simulation

60 sec

Bottom value of the simulation

Parameter: P86 Menu path: SERVICE / SIMULATION / BOTTOM VALUE Default value:

pH measurement ORP measurement DO measurement

Description: Lowest value of the simulation

0 pH - 1000 mV 0 ppm

BKI 11 ATEX 0012 X le00100a0600p_05  51 / 60

Upper value of the simulation

Parameter: P87 Menu path: SERVICE / SIMULATION / UPPER VALUE Default value:

pH measurement ORP measurement DO measurement

Description: Highest value of the simulation

14 pH 1000 mV 8.24 ppm

6.4.5.8 Temperature simulation

This function helps the user to check the outputs and the additional processing instruments connected to the output. To start simulation the instrument must return to Measuring mode.

Temperature simulation mode

Parameter: P84: b Menu path: SERVICE / TEMP. SIMULATION / MODE Default value:

OFF

Description: Temperature simulation mode: OFF No temperature simulation FIX VALUE Simulation of a fixed lower range temperature value TRIANGLE WAVE The simulated value changes linearly between the set low

and high values with an adjustable cycle time

52 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

Temperature simulation cycle

Parameter: P88 Menu path: SERVICE / TEMP. SIMULATION / TIME Default value: Description: Cycle time of the temperature simulation

60 sec

Bottom value of the temperature simulation

Parameter: P89 Menu path: SERVICE / TEMP. SIMULATION / BOTTOM VALUE Default value: Description: Lowest value of the temperature simulation

0 ºC

Upper value of the temperature simulation

Parameter: P90 Menu path: SERVICE / TEMP. SIMULATION / UPPER VALUE Default value: Description: Highest value of the temperature simulation

50 ºC

6.4.5.9 Load default values

Parameter: - Menu path: SERVICE / DEFAULTS / LOAD DEFAULT Default value:

Description: This command loads all default values of the instrument.

After loading the default values the parameters can freely be changed, the effect of the changes does not affect the measurement until the user exits programming mode and returns to measurement mode. Before loading the defaults the software asks for a confirmation warning the user that all user parameters will be lost!

6.4.5.10 Restart

Parameter: - Menu path: SERVICE / RESTART Default value: Description: Restarts the instrument (Cold boot) (Reloads parameters from the non-volatile memory)

–

BKI 11 ATEX 0012 X le00100a0600p_05  53 / 60

6.5. PH SENSOR CALIBRATION

This function is for periodic calibration of the pH sensor. Entering the SERVICE / SENSOR CALIBRATION menu the instrument will display a warning message that the user is about to change critical parameters of the

measurement system. The user can enter the menu by pressing the

(OK) button or exit to the previous menu by pressing the (NO) button. In case of calibration, after sensor replacement, please handle first calibration with high priority. The system will inquire this in the next dialog box. In the event of initial calibration, press the OK button. In this case, all parameters and counters related to the sensor will be reset to default. We should press

NO button, in case it is not the first calibration.

In the SENSOR INFO page the slope and offset voltage of the sensor can be checked (see chapter 6.2). The calibration can be performed within ±0.8 pH sensor error. When this error is greater then ±0.8 pH the unit shows a warning message that the sensor should be

replaced.

6.5.1. Editing one item of the calibration table

(SERVICE | SENSOR CALIBRATION | VIEW/EDIT TABLE) Calibration of the pH sensor is done using this table with min. 2 or max. 8 elements. By default the table contains

2 elements (0 and 14pH). The instrument is ready to measure with these two elements in the table. Any change in the calibration table applies instantly! The two minimal elements of the table cannot be erased only edited.

The selected element of the list (table) can be edited by pressing the

button. Then we get a special box editor.

One line of the list consists of two values. The left one (BUFFER VALUE) shows the nominal value of the used pH buffer solution. The right one (SENSOR VALUE) indicates the uncalibrated but temperature compensated value measured with this buffer solution.

VIEW/EDIT TABLE

0: 0.00 0.00

1: 14.00 14.00

54 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

Adding, modifying a calibration point

The following special screen helps the user to set a calibration point. The user can see the uncalibrated measured values and also the pair values of the selected table line.

1. Value, measurable without sensor calibration

2. Trend display for monitoring installation. The upper part of the bargraph symbolizes the increasing trend, the bottom part of

the bargraph symbolizes the decreasing trend. The filling rate is in accordance with the measure of change. If the bargraph is empty, the measured value is constant.

3. Measured value with calibration.

4. The BUFFER VALUE is editable using the

, and buttons. The user has to

enter the nominal pH value of the measured buffer solution.

5. The measured value can be copied to the stored SENSOR VALUE by pressing the

+ buttons simultaneously. Then the software starts an algorithm to check if the measured value is stable or not. When the value is stored in the SENSOR VALUE field, a READY message appears on the bottom of the display.

The measured value can be copied to the stored SENSOR VALUE by pressing the + buttons simultaneously. If the two values of the data pair differ in more than ±0.8 pH from each other the software shows an error message at the bottom line of the screen.

By pressing the

button the instrument checks the edited calibration data pair and if it is OK the software returns to the calibration table. If not a dialogue window

will appear and inform the user.

Exit from the calibration table by pressing the

button.

Damping check:

When pressing the

+ buttons the software checks if the calibration value to be stored is constant. After the buttons are pressed the measured pH value must be stabilized in 30 seconds otherwise the value will not be stored and a FAILED! message will appear on the screen. Change in the measured value (1) can be followed on the trend bargraph (2). If the cause of a fluctuation or error is eliminated, storing of the calibration points can be repeated by pressing the

buttons again.

BKI 11 ATEX 0012 X le00100a0600p_05  55 / 60

6.5.2. Adding an item to the calibration table

(SERVICE | SENSOR CALIBRATION | ADD ITEM)

This menu point adds a line to the table and enters to view/edit table display at the same time. Editing is done as described above.

6.5.3. Deleting an element of the calibration table

(SERVICE | SENSOR CALIBRATION | DELETE ITEM)

This menu point lets the user delete a line (element) of the table. Pressing the

on the selected line deletes

it from the table. Exit from the list by pressing the

button.

6.5.4. Reset the calibration table to default

(SERVICE | SENSOR CALIBRATION | RESET TO DEFAULT)

This function resets the sensor calibration data to default (0 and 14 pH). It is ineffective to other operating parameters.

6.5.5. Calibration procedure

1. Enter to menu point „SENSOR CALIBRATION - VIEW / EDIT TABLE” as described in Chapter 6.5.1

2. Rinse the pH electrode and temperature sensor with distilled water then dry up gently using a soft rag.

3. Immerse the electrode as well as the temperature sensor into the buffer solution.

4. Select one existing line of the calibration table or add a new item to the table.

5. In the „BUFFER VALUE:” field enter the pH value of the first buffer solution corrected to the actual temperature – use the

, and buttons - . (The

temperature corrected pH values of the buffer solution usually are listed on the label of the bottle.)

6. Observe the damping of „SENSOR:” and „MEASURED:” values. This is helped by the bargraph near them. If values are settled press

+ buttons

simultaneously to store the actual measured value which will appear in the „SENSOR VALUE:” field. If user cannot get a clear measurement (the value is constantly changing) the sensor should be cleaned as described in chapter 4.3 and recalibrated again. If the electrode still cannot be calibrated it has to be replaced with a new one!

7. Exit to „VIEW / EDIT TABLE” by pressing the

button.

8. Repeat steps 2…6 for every desired calibration point (max. 8)

9. Exit programming mode by pressing the display, and check the calibrated measurement state („UNCAL” message disappears from the display.

56 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.6. DO SENSOR CALIBRATION

This function is for periodic calibration of the DO sensor. The sensor is aging during the usage of the instrument. When the life-time of the sensor is over the sensor should be replaced. In case of sensor replacement the

sensor should be calibrated compensating the aging. Calibration of the sensor has to be done in two points: (ZERO – zero point and SPAN – saturated value) ZERO calibration can be performed with 5% sodium sulphite referential liquid, SPAN (saturated value) calibration can be performed with saturated zero salinity

referential liquid or air. Value of atmospheric pressure should be set before calibration process (see 6.4.1.8.) Entering the SERVICE / SENSOR CALIBRATION menu the instrument will display a warning message that the user is about to change critical parameters of the

measurement system. The user can enter the menu by pressing the (OK) button or exit to the previous menu by pressing the (NO) button. In case of calibration, after sensor replacement, please handle first calibration with high priority. The system will inquire this in the next dialog box. In the event of initial calibration, press the

OK button. In this case, all parameters and counters related to the sensor will be reset to default.

We should press

NO button, in case it is not the first calibration.

6.6.1. Calibration of saturated value (100%)

(SERVICE / SENSOR CALIBRATION / CAL. IN AIR (SPAN)) Rinse the DO sensor with distilled water then dry up gently using a soft rag. Immerse the sensor into

saturated, zero salinity referential liquid or hold the sensor into air. Please wait until the measured value (2) get stabilized. Change in the measured value (2) can be

followed on the trend bargraph (1). Achieving proper calibration atmospheric pressure (3) and relative humidity (4) should be entered. In accordance to these values and the measured temperature the instrument calculates the DO concentration, which can be edited in the last line (5).

Damping check:

When pressing the E button at the last line, a warning message appears asking do we really want to store the calibration data. By pressing the

[yes – OK] button, the instrument checks the stability of the measured value and if it remains unchanged during a given time period, the instrument stores the calibration. Changes of the measured value can be checked on the display (2) and the trend bargraph (1) also indicates changes of the measured value. When the measured value got stabilized, READY! message will appear on the bottom of the screen. If damping check procedure is unsuccessful, FAILED! message will appear on the bottom of the screen. When the error caused by changes or fluctuations became resolved, then calibration-point storing procedure can be repeated.

BKI 11 ATEX 0012 X le00100a0600p_05  57 / 60

6.6.2. Calibration of Zero point (0%)

(SERVICE / SENSOR CALIBRATION / CAL. IN ZERO SOL.) Rinse the DO sensor with distilled water then dry up gently using a soft rag. Immerse the sensor into

5% sodium sulphite referential liquid. Please wait until the measured value (2) get stabilized. Change in the measured value (2) can be

followed on the trend bargraph (1).

When pressing the E button at the last line, a warning message appears asking do we really want to store the calibration data. By pressing the [yes – OK] button we enter the damping check procedure described in the previous point.

6.6.3. Calibration with referential DO instrument

(SERVICE / SENSOR CALIBRATION / CAL. IN SPAN SOL.) With this function the instrument can be calibrated to a referential (already calibrated) instrument.

In this case basic settings (atmospheric pressure, temperature) should be the same. Rinse the DO sensor with distilled water then dry up gently using a soft rag. Immerse the sensor into

saturated referential liquid with zero salinity or hold the sensor into air. Please wait until the measured value (2) get stabilized. Change in the measured value (2) can

be followed on the trend bargraph (1). Read the measurement value of the referential instrument and enter this value to the edit field (3).

When pressing the E button at the last line, a warning meassage appears asking do we really want to store the calibration data. By pressing the [yes – OK] button we enter the damping check procedure described in 6.6.1 point.

6.6.4. Reset the calibration table to default

(SERVICE | SENSOR CALIBRATION | DELETE ITEM)

This function resets the sensor calibration data to default. It is ineffective to other operating parameters.

6.6.5. Reset Timer

This function resets the inner timer of the DO electrode life-time monitoring routine.

58 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

6.7. ERROR CODES

Code Message on the screen Error description Procedure

1 MEMORY ERROR Memory error in the electronics Contact the service! 2 NO INPUT SIGNAL Hardware error Contact the service! 3 EE COM. ERROR Hardware error Contact the service! 4 MATH. OVERLOAD Display overflow Check the programming!

SENS. SERVICE! Sensor slope and offset are out of

tolerance limit.

Check or clean the sensor and do a calibration. Check the correct operation of the sensor and the installation!

16 EE CHK ERROR Parameter checksum error. Restart the unit in SERVICE / RESTART menu (or power off and

on the instrument) and check / repeat programming! If the problem persists contact the service!

17 INTEGRITY ERROR Incorrect parameter values. Stored

parameters are damaged.

Restart the unit in SERVICE / RESTART menu (or power off and on the instrument) and check / repeat programming! If the problem persists contact the service!

18 AC COM. ERROR Hardware error Contact the service! 19 RELAY ERROR Hardware error Contact the service!

- TEMP. ERROR Temperature sensor error Check the connection of the temperature sensor.

The unit will compensate to 25ºC!

- CALIBRATION ERROR Logic error Check the sensor calibration table!

- POINT PAIR ERR. Logic error Check the sensor calibration table!

le00100a0600p_05

2015. October

Nivelco reserves the right to change technical data without notice!

BKI 11 ATEX 0012 X le00100a0600p_05  59 / 60

BASIC SETUP

-----------------------------------

MEASURING UNIT(DO)

DAMPING TIME.

TEMP. COMPENSATION

SALINI TY CORRECT ION(DO)

PRESSURE CORRECTION(DO)

DAMPING TIME

MEASURING UNIT

--------------------------------

ppm

mg/l

%sat

MODE

---------------------------------

AUTO

MANUAL

OFF

UNIT

---------------------------------

C°

MANUAL VALUE

MAIN MENU

----------------------

BASIC SETUP

OUTPU T SETUP

SERV ICE

OUTPUT SETUP

-----------------------------------

ANALOG OUTPUT

RELAY OUTPUT

SERIAL OUTPUT

ANALOG OUTPUT

---------------------------------

CURRENT MODE

4 mA VALUE

20 mA VALUE

ERROR MODE

MANUAL VALUE

CURRENT MODE

---------------------------------

AUTO

MANUAL

4 mA VALUE

ERROR MODE

---------------------------------

HOLD

3.8 mA

22 mA

MANUAL VALUE

ADDRESS

SERIAL OUTPUT

---------------------------------

ADDRESS

RELAY OUTPUT

---------------------------------

FUNCTION

---------------------------------

HYSTERESIS

WINDOW

DELAY TIM E

MODE

---------------------------------

OFF

pH/ORP/DO

TEMP

ON ERROR

INVERTING

---------------------------------

YES

20mA VALUE

MODE

FUNCTION

4 mA VALUE

20 mA VALUE

DELAY TIME

INVERTING

6. MEN8UMAP

PRESSURE CORRECTION

--------------------------------

UNIT

MANUAL VALUE

UNIT

---------------------------------

C°

F°

MANUAL VALUE

TEMP. COMPENSATION

--------------------------------

MODE

UNIT

MANUAL VALUE

60 / 60  le00100a0600p_05  BKI 11 ATEX 0012 X

------------------ -----------------

SECURITY

---------------- -----------------

USER LOCK

SERVICE LOCK

USER LOCK

SERVICE LOCK

OUTPUT TEST

---------------- -----------------

ANALOG OUTPUT

RELAY OUTPUT

SERIAL OUTPUT

---------------- -----------------

1200Hz

2200Hz

CURRENT VALUE

SENSOR SETUP CALIBRATION /

VIEW/EDIT TABLE

ADD ITEM

DELETE ITEM

RESET TO DEFAULT

RESET TIMER

pH/OR P/DO SIMULATION

-------------- -------------------

MODE

TIME

BOTTOM VAL UE

UPPER VALUE

MODE

------------ ---------------------

OFF

MANUAL VALUE

TRIANGLE WAVE

SQUARE WAVE

TIME

BOTTOM VALUE

UPPER VALUE

------------------ ---------------

LOAD DEFAULT

CLEAR TIMERS

-------------- -------------------

TEMP. SIMULATION

MODE

TIME

BOTTOM VALUE

UPPER VALUE

MODE

---------------- -----------------

OFF

MANUAL VALUE

TRIANGLE WAVE

TIME

BOTTOM VALUE

UPPER VALUE

SERVICE

SECURITY

OUTPUT TEST

SENSOR CALIBRATION

pH/O RP/DO SIMU LATION

TEMP. SIMULATION

DEFAULTS

RESTART

pH:

SET ZERO POINT

ORP:

ZERO CAL. IN LIQUID

SPAN CAL. IN AIR

SPAN C AL. IN LIQUID

RESET TO DEFAULT

RESET TIMER

DO:

RELAY OUTPUT

------------- --------------------

DEENER GISED

ENERGISED

le00100a0600p_05  Menumap

BASIC SETUP

----------------------------------MEASURING UNIT(DO)

DAMPING TIME.

TEMP. COMPEN SATION SALINITY CORRECTION(DO) PRESSURE CORRECTION(DO)

DAMPING TIME

MEASURING UNIT

-------------------------------ppm mg/l

%sat

MODE

--------------------------------AUTO

MANUAL

OFF

UNIT

---------------------------------

C° F

MANUAL VALUE

MAIN MENU

---------------------BASIC SETUP

OUTPUT SETUP

SERVICE

OUTPUT SETUP

----------------------------------ANALOG OUTPUT

RELAY OUTPUT

SERIAL OUTPUT

ANALOG OUTPUT

--------------------------------CURRENT MODE

4 mA VALUE

20 mA VALUE

ERROR MODE

MANUAL VALUE

CURRENT MO DE

--------------------------------AUTO

MANUAL

4 mA VALUE

ERROR MODE

--------------------------------HOLD

3.8 mA 22 mA

MANUAL VALUE

ADDRESS

SERIAL OUTPUT

--------------------------------ADDRESS

RELAY OUTPUT

---------------------------------

FUNCTION

--------------------------------HYSTERESIS

WINDOW

DELAY TIME

MODE

---------------------------------

OFF

pH/ORP/DO

TEMP

ON ERROR

INVERTING

---------------------------------

YES

20mA VALUE

MODE

FUNCTION

4 mA VALUE

20 mA VALUE

DELAY TIME

INVERTING

--------------------- --------------

SECURITY

--------------------- ------------

USER LOCK

SERVICE LOCK

USER LOCK

SERVICE LOCK

OUTPUT TEST

(

KIMENETI TESZT)

--------------------- ------------

ANALOG OUTPUT

RELAY OUTPUT

SERIAL OUTPUT

--------------------- ------------

1200Hz 2200Hz

CURRENT VALUE

SENSOR SETUP CALIBRATION /

VIEW/EDIT TABLE

ADD ITEM

DELETE ITEM

RESET TO DEFAULT

RESET TIMER

pH/ORP/DO SIMULATION

--------------------- ------------

MODE

TIME

BOTTOM VALUE

UPPER VALUE

MODE

--------------------- ------------

OFF

MANUAL VALUE

TRIANGLE WAVE

SQUARE WAVE

TIME

BOTTOM VALUE

UPPER VALUE

--------------------- ------------

LOAD DEFAULT CLEAR TIMERS

--------------------- ------------

TEMP. SIMULATION

MODE

TIME

BOTTOM VALUE

UPPER VALUE

MODE

--------------------- ------------

OFF

MANUAL VALUE

TRIANGLE WAVE

TIME

BOTTOM VALUE

UPPER VALUE

SERVICE

SECURITY

OUTPUT TEST

SENSOR CALIBRATION

pH/ORP/DO SIMULATION

TEMP. SIMULATION

DEFAULTS

RESTART

pH:

SET ZERO POINT

ORP:

ZERO CAL. IN LIQUID

SPAN CAL. IN AIR

SPAN CAL. IN LI QUID

RESET TO DEFAULT

RESET TIMER

DO:

PRESSURE CORRECTION

-------------------------------UNIT

MANUA L VALUE

UNIT

--------------------------------C° F°

MANUAL VALUE

TEMP. COMPENSATION

-------------------------------MODE

UNIT

MANUAL VALUE

RELAY OUTPUT

--------------------- ------------

DEENERGISED

ENERGISED

6. MEN8UMAP

NIVELCO AnaCONT LE-100, AnaCONT LP-100, AnaCONT LG-100 Installation And Programming Manual

Specifications and Main Features

Frequently Asked Questions

User Manual