MRC MH-4D Operation Manual

3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Digital Hotplate
With Stirrer
MH-4D
Operation Manual
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Important Before using this product, read this entire operation manual carefully. Users should follow all of the operational guidelines contained in this manual and take all necessary safety precautions while using this product. Failure to follow these guidelines could result in potentially irreparable bodily harm and/or property damage.
Caution All internal adjustments and maintenance must be performed by qualified service personnel.
Material in this manual is for information purposes only. MRC is committed to a continuing program of product development and improvement, and reserves the right to change information, such as specifications, appearance, and dimensions, described in this document without notice. MRC makes no representations or warranties with respect to this manual. In no event shall MRC be held liable for any damages, direct or incidental, arising out of or related to the use of this manual.
This manual contains important safety and operation information. You must carefully read, understand, and follow all the instructions in this manual prior to operating this instrument. Keep this manual in a safe place nearby for reference and make it easily available to all users.
1) This manual highlight DANGER/WARNING/CAUTION/NOTICE
alerts to prevent injury or property damage and also to achieve optimum performance of your instrument.
2) These alerts are classified into four types in this manual
depending on the importance and the risk levels as described below
3) The claim which is out of the quality guarantee published by
the Manufacturer is out of Manufacturer’s responsibility.
4) The damage which is from unexpected fault or damage of user
by Acts of God is out of Manufacturer’s responsibility.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
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Table of content
Section 1 Warning and Cautions………….…..……………………………1-1
Section 2 General Description ………….………………..…………………2-1
Features Safety Convenience Construction
Section 3 Unpacking and installation…………………….……….………3-1 Installation environment Connecting to Power Supply Location Condition Connecting to the main power
Section 4 Operation……………………………………….…………………….4-1
Power On Change the Set Value (SV) Change the Alarm Value Autotuning (AT) Temperature Offsetting (OFFSET) Stir Control Knob External Temperature Probe Input (optional)
Section 5 Maintenance………………………..…………….……….….………5-1
Cleaning Product Relocation Keeping Product
Section 6 Troubleshooting …………….……………………………….….…6-1
Section 8 Warranty Information………….…………………………..….….7-1
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Section 1 Warnings and Cautions
DANGER
Ignoring the following warnings could cause serious injuries or even fatal accidents.
Understand all alert labels prior to operating this equipment. Never remove or damage the alert labels. Never move this equipment while under operation. Never install or use this equipment in explosive or flammable
atmospheres.
Never use or store flammable or hazardous substances near to
this equipment.
Never use the equipment to heat flammable or hazardous
substances.
Always wear proper protective gear (such as goggles, gloves,
masks or an apron) when using this equipment.
Never allow water, organic solvents, dust, or corrosive gases to
get inside the equipment.
Never immerse this equipment in water or operate it under
water.
Never reach for this equipment if it has fallen into water. Check electrical requirements described in this operation
manual or on the ID plate of this equipment before use. Connect this equipment to a dedicated power outlet nearby.
Connect this equipment only to properly grounded power
outlets to protect you and your instrument. Do not ground to gas pipes or water pipes.
Never install this equipment closer than 30 cm (12 inches) to a
wall of combustible material. Observe minimum distances (in general, 30 cm) from other devices.
If you observe strange smoke, odor or noise from the
instrument, unplug the power cord immediately and turn off the main power switch. After the smoke or odor disappears, contact your dealer or MRC if any repair is required.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Never disassemble, repair, or modify this equipment on your
own. Doing so will void your warranty and may result in injuries or product damages.
Do not heat any substances above temperature which will
cause hazards of explosion, implosion or release of toxic or flammable gases from the material being heated.
Do not use in the presence of pressurized or sealed containers.
Fire or explosion may result causing injury or death
Do not operate the plate with external temperature probe
in the air or out of the liquid.
The external probe must be properly placed into a liquid
on the top surface during the whole process, to prevent damage to the plate
The plate might be covered with aluminum foil to protect
it, DO NOT cover any other parts of the device and make sure the radiation sheets underneath are not covered.
The Aluminum topped plates are not designed to be used with
metal containers. For heating of such containers it's advisable to use a ceramic top hot plate.
To avoid electric shock, always use a property grounded
electrical outlet of correct voltage, and correct handling capacity equipment
CAUTION
Ignoring the following cautions could cause injuries or property damages.
Keep away the power cord from the hot plate, to prevent
melting and damages.
Do not touch the top plate or any object near it even when the
heater is turned off. You may get burned due to residual heat.
After using this equipment, make sure to turn off the main
power switch and also to disconnect the power cord from the power outlet for the safety of other users.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Do not place heavy objects, including this equipment, on top
of the power cord and do not strip, scratch, bend, twist, pull, or heat the power cord. A damaged power cord is a fire and electrical shock hazard.
Make sure to set up this equipment on a flat, stable, clean,
non-slip, dry, and fireproof surface inside a lab with proper safety measures.
Do not touch the power outlet, power socket, or power cord
with wet hands. And make sure to connect the power cord directly and firmly to the power outlet and power socket.
Do not put or insert any objects (especially if conductive or
flammable) inside this equipment.
Do not expose this equipment to any heat sources including
direct sunlight.
Mechanical shock or vibration can damage this equipment. Pay
extra attention while moving it. Damages caused by mechanical shock or vibration may result in injury or fire.
Do not impact the top plate or heat sink. You can damage the
equipment or get injured.
Do not install this equipment near any device that generates
high frequency noise such as high frequency welding machines, high frequency sewing machines, or SCR power controllers.
Before cleaning, make sure to unplug the power cord to avoid
electric shock or fire.
Do not use chlorine bleach, ammonia-based cleaners,
abrasives, ammonia, or metal scouring pads. Wipe with a soft damped cloth or a sponge soaked in water or diluted neutral detergent.
The user shall be aware that, if the equipment is used in a
manner not specified by the manufacturer, the protection provided by the equipment may be impaired.
The instrument should be placed so, that handy operation of
the ON-OFF Switch is possible.
Service only by a qualified Service engineer.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Always disconnect from power supply prior to maintenance
and servicing.
Connect the instrument to a ground mains outlet, after
ensuring that the Voltage is the same as given on the name plate
The Instrument must be connected to an earthen (grounded)
supply
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Section 2 General Description
Congratulations of your purchase of MRC hotplate which is specially designed to provide maximum benefit for your investment with respect to performance, safety, ease of use, and durability.
Item/Model MH-4D
Dimension (W x D x H, mm) 200 X 250 X 130
Top plate dimension (mm) 175 X 175 mm
Maximum heating capacity 800W
Current consumption (110V) 7.3A
Temp. range Up to 300°C
Temp. control Digital
Magnetic stirrer 100 – 1200 rpm
Features Performance
Microprocessor PID Feedback Control
Fast and precise temperature control is provided by the microprocessor PID controller
Quick Heat Up Time
Ample heating capacity and superb heat transfer rate of the tightly integrated structure of heater and top plate allow quick heat up time (up to 300°C).
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
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Auto-tuning (AT)
Automatic tuning of the PID parameters provides more accurate temperature control.
Temperature Offsetting
In case your own thermometer is to be used for temperature control for specific applications, there can be some differences between the temperature of your thermometer and the displayed temperature of this unit.
Safety
High and Low Temperature Limits
The high temperature limit of the top plate is set to 300°C to protect you and your media. However, you can set your own high and low temperature limits to reduce operation time and also to avoid inadvertent mistakes.
Convenience
Two large digital displays on the control panel clearly show
both set and actual temperatures of the top plate side by side.
You can easily set your own temperature limit at any value
between 0 and 300°C.
Heating rate can be set from 0 to 100% at 1% interval for
delicate temperature control.
One support rod (optional) can be attached to hold various
kinds of devices such as temperature sensors, thermometers, and so on.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Construction
(1) Top Plat (2) Radiation Sheets (3) Main Power Switch (4) FY-400 Temperature Controller (5) Stirring Control Knob (6) Stirring Switch (7) Stirring motor
(8) Socket for Temperature Probe (9) Identification Label
(10) Threaded Holes for Support Rod (Optional)
(11) Power Cord
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Section 3 Unpacking and Installation
Upon receiving the instrument, check to ensure that no damage has occurred during shipment. It is important that any damage that occurred during shipment must be detected before unpacking. If such damage is found, notify the carrier immediately.
After unpacking, check to ensure that all the following parts and accessories are included in the package. If not, contact your dealer or MRC immediately.
Item Quantity
Main Body 1 Operation Manual 1 External Probe 1 Stirring magnet (option) 1 Support Rod (option) 1 RS232 or RS485 Communication (option) 1 Programmer (option) 1 Separate Control box (option) 1
Installation Environment
It should be installed in suitable environment as described below.
Avoid direct sunlight.
Room temperature should be 5°C ~ 40°C
Relative Humidity (RH%) should be less 80%.
Altitude should be less than 2,000m.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
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Location Conditions
DANGER
Never install or use this equipment in explosive atmospheres. Never install or use this equipment with or near to hazardous
or flammable substances.
Never expose this equipment to any heat sources including
direct sunlight.
Never install this equipment closer than 20 cm (8 inches) to a
wall of combustible material.
Never install this equipment near any device that generates
high frequency noises.
Set up this equipment on a flat, stable, clean, non-slip, dry, and
fireproof surface inside a lab with proper safety measures.
Observe the minimum distances (in general, 30 cm or 12
inches) from other devices. In addition, any device which can be affected by the motor vibrations should not be placed near this equipment.
Connecting to Power Supply
When connecting power, use only the power cord that came with your instrument. The power connection procedures are as follows:
(1) Before connecting the power cord, make sure that the main
power switch is turned off.
(2) Plug the other end into a properly grounded and dedicated
power outlet nearby.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Connecting to Main Power
DANGER
Check electrical requirements in the operation manual or on
the ID plate attached to the back of this equipment before use.
Make sure to connect this equipment only to properly
grounded as well as dedicated power outlets to protect you and your equipment.
In order to prevent fire or power cord damage due to
overloading, do not use power strips or improper extension cords.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Section 4 Operation
FY-401 Digital controller
SYMBOL NAME FUNCTION
PV 1
Measured value (PV) display
Displays PV or various parameter symbols (Red)
SV 2
Set value (SV) display
Displays SV or various parameter set values (Green)
3
Set key
Used for parameter calling up and set value registration
4 Auto/Manual key Switches between Auto (PID) output mode and Manual output mode.
5 Shift key Shift digits when settings are changed
6
Down key *Program hold
Decrease numbers (-1000, -100, -10, -1) * Program hold (Programmable controller)
7
Up key *Program run
Decrease numbers (+1000, +100, +10, +1) * Program run (Programmable controller)
OUT1 8 OUT1 lamp Lights when OUT1 is activated
OUT2 9 OUT2 lamp Lights when OUT2 is activated
AT 10 Auto tuning lamp Lights when Auto tuning is activated
AL1 11 Alarm 1 lamp Lights when Alarm 1 is activated
AL2 12 Alarm 2 lamp Lights when Alarm 2 is activated
AL3 13 Alarm 3 lamp Lights when Alarm 3 is activated
MAN 14 Manual output lamp Lights when manual output is activated
PRO 15
*Program running lamp
*Flashes when program is running (Programmable controller)
OUT1% 16
OUT% bar-graph display
Output% is displayed on 10-dot LED.
AUTO
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
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Operations
Power On
Controller will display as below
Change the Set Value (SV)
Change SV for example from 0 to 100
NOTICE
You can change the temperature setting even during
operation.
Changing the temperature setting is allowed only within the
low and high temperature limits.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Change the Alarm Value
Change AL1 value for example to "5.0" (AL1 active, if PV exceeds SV over 5.0)
Autotuning (AT)
Temperature control using digital PID controllers have automatic auto-tune functions. During the auto-tune period the PID controller controls the power to the process and measures the rate of change, overshoot and response time of the plant. This is often based on the Zeigler-Nichols method of calculating controller term values. Once the auto-tune period is completed the P, I ,D values are stored and used by the PID controller. Use AT function to automatically calculate and set the optimize PID value for your system
DO NOT touch the plate or the temperature controller or
add media during autotuning process.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Temperature Offsetting (OFFSET)
The temperature shown on the Actual Temperature Display is measured by a temperature sensor inside the unit. However, this temperature can be different from the temperature of your own thermometer which you may use as a standard for your specific applications. If needed, you can offset such temperature differences at 0.1°C interval
NOTICE
If, for example, the actual temperature of the top plate is 100°C but the displayed temperature is 98°C, you can match the displayed temperature with the actual temperature of the unit by selecting the offset value of +2°C
Stir Control Knob
Turn it clockwise to set desired stirring speed. Turn it all the way counterclockwise to turn off stirring function.
Stirring Instructions
1. Fill vessel with liquid to be stirred.
2. Place stir bar into vessel.
3. Place vessel in the center of the top surface.
4. Turn Stir Control Knob
5. Stir bar to cease rotation before removing the vessel from the
unit.
NOTICE
Please note that the viscosity of the stirred material will affect the ability of the stir bar to remain coupled to the rotating ring magnet. Materials of high viscosity must be stirred at slower speed settings.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
External Temperature Probe Input
Connect the K type optional External Temperature probe into the back socket.
To Connect the External Temperature Controller
1. Turn the Stir Control Knob and the main switch to the OFF
position.
2. Disconnect power cord.
3. Connect the External Temperature probe to the socket on the
back of the unit.
4. Fill vessel with liquid to be heated.
5. Place vessel in the center of the top surface.
6. Place stir bar into vessel.
7. Put the temperature external probe in vessel.
8. Reconnect power cord.
9. Turn the main switch and the stirring switch to the ON
position.
10. Product is now ready for use with External Temperature
Controller.
11. Repeat the above process when disconnecting the
temperature controller.
CAUTION
Do not use the plate with external temperature probe in
the air or out of the liquid, this can cause serious damage to the plate, due to lack of control.
The external probe must be properly placed into a liquid
on the top surface during the whole process, to prevent damage to the plate
The top surface and the vessel used may be at substantially
higher temperatures than indicated by the setting on the Heating Temperature Display as the controller regulates the liquid temperature inside the vessel.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Section 5 Maintenance
Inspection Interval
Item
Daily Weekly
Connection status of power cord or plug Damages in power cord or plug Cleanliness of top plate Cleanliness of main body and accessories Damages in plate, switches, buttons, Controller
Heating capability check (up to 300℃)
Stirring capability check (up to 1200 rpm) Assembly status of all parts or accessories
Cleaning Product
WARNING
Never immerse this unit in water or any other liquid. Do not allow any liquid or wet material to get inside the unit
when cleaning.
Do not reconnect this unit to power outlets until all cleaned
surfaces have dried.
CAUTION
DO NOT use of caustic soda in cleaning reagent
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Cleaning Product (continued)
Always make sure to keep top plate, main body, and accessories clean. Dirt and other foreign substances can cause fire or electric shock. Before attempting cleaning,
(1) Disconnect the power cord from the power outlet and ensure
that the equipment is cool enough,
(2) Wipe with a soft dry cloth first to remove any foreign matter
and, if not enough,
(3) Wipe with a soft damp cloth or a sponge soaked in water or
diluted neutral detergent when necessary.
Relocation
If you need to move the equipment to another place,
(1) Disconnect the power cord from the power outlet, (2) Pack the equipment and its accessories into the original
packaging or any other suitable container before moving.
CAUTION
Pay attention to avoid mechanical shock or vibration while
moving the instrument. Damages caused by mechanical shock or vibration may result in injury or fire.
Keeping Product
If you know you will not use this equipment for an extended period of time,
(1) Disconnect the power cord from the power outlet and clean
the equipment with soft cloth.
(2) Pack the equipment properly and make sure to store it in dry
place.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
com.mrclab@mrc
Section 6 Troubleshooting
Power troubles
Cause Corrective action
Unsuitable power supply
Meet the electrical requirements of this equipment before use.
Loose power connection
Reconnect the power cord firmly to the power outlet as well as to the power
socket at the back of the instrument. Damages in power cords, Power outlets, plug, controller
Replace the damaged part with a
proper one.
No Power
Internal circuit failure Contact MRC for service
Electrical overload
Disconnect all the appliances connected
to the breaker first and reconnect them
one by one to find the reason for the
overload.
Damages in heating element Contact MRC for service.
Repetitive tripping of circuit breaker
Internal circuit failure Contact MRC for service.
Main switch failure Contact MRC for service. Controller failure Contact MRC for service.
No operation with power on
Internal circuit failure Contact MRC for service.
Operation troubles
Cause Corrective action
Temperature sensor is disconnected
Connect the temperature sensor
Too low setting of the temperature controller
Increase the temperature setpoint
Heating element failure Contact MRC for service.
No heat
Internal circuit failure Contact MRC for service.
Too low setting of the heating rate
Increase the temperature setpoint
Too much media Reduce the media volume.
No or too slow temperature change during heating to increase the heating rate
Internal circuit failure Contact MRC for service.
Internal circuit failure Contact MRC for service
Switches malfunction
Damaged switches Contact MRC for service.
3, Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529
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Stirring knob malfunction Damaged knob Contact MRC for service.
Controller display malfunction
Damage due to chemical spill or overheating or technical problem
Contact MRC for service.
Section 7 Warranty Information
The warranty provided for one year and begins from the date
of the purchase by the user
The warranty protection extends to any subsequent owner
during the first-year warranty period.
This warranty does not apply if the product has been damaged
by accident, abuse, misuse, or misapplication, or from ordinary wear and tear.
The Technical Services Department must be contacted for
warranty determination and direction prior to performance of any repairs.
Expendable items, glass, filters and gaskets are excluded from
this warranty. Replacement or repair of components parts or equipment under this warranty shall not extend the warranty to either the equipment or to the component part beyond the original warranty period.
The Technical Services Department must give prior approval
for return of any components or equipment.
Your MRC Sales Office is ready to help with comprehensive site
preparation information before your equipment arrives. Printed instruction manuals carefully detail equipment installation, operation and preventive maintenance.
If equipment service is required, please call our Technical
Services Department at +972(0)3-5595252 (office) or +972(0)3­6227732/1 (Service Laboratory)
We're ready to answer your questions on equipment warranty,
operation, maintenance, service and special application.
Outside the Israel, contact your local distributor for warranty
information.
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