Mettler Toledo Thornton 2000 Instruction Manual

Part No. 84401
2000 Two-Channel Instrument
for pH, ORP, Conductivity, Resistivity,
Dissolved Oxygen, Dissolved Ozone
IMPORTANT SAFETY INFORMATION
Follow all warnings, cautions, and instructions indicated on and supplied with this product.
Install equipment as specified in this instruction manual. Follow appropriate local and national
codes.
Use only factory documented components for repair. Tampering or unauthorized substitution of parts and procedures can affect the performance and cause unsafe operation of your process.
Protective covers must be in place unless qualified personnel are performing maintenance.
If this equipment is used in a manner not specified by the manufacturer, the protection provided by
it against hazards may be impaired.
WARNINGS:
Installation of cable connections and servicing of this product require access to shock hazard voltage levels.
Main power and relay contacts wired to separate power source must be disconnected before servicing.
Main power must employ a switch or circuit breaker as the disconnecting device for the equipment.
Electrical installation must be in accordance with the National Electrical Code and/or any other
applicable national or local codes.
Safety and performance require that this instrument be connected and properly grounded through a three-wire power source.
RELAY CONTROL ACTION: the 2000 instrument relays will always de-energize on loss of power, equivalent to normal state, regardless of relay state setting for powered operation. Configure any control system using these relays with fail-safe logic accordingly.
PROCESS UPSETS: Because process and safety conditions may depend on consistent operation of this instrument, provide appropriate means to maintain operation during sensor cleaning, replacement or sensor or instrument calibration.
This manual includes specific safety information with the following designations and formats:
WARNING: OF POTENTIAL FOR PERSONAL INJURY. CAUTION: of possible instrument damage or malfunction. NOTE: important operating information.
On the instrument indicates: Caution, risk of electric shock
On the instrument indicates: Caution (refer to accompanying documents)
TABLE OF CONTENTS
Chapter 1: Getting Started............................................................................................ 1
Introduction..................................................................................................................1
Features ...................................................................................................................... 1
Overview of Operation................................................................................................. 1
Installation & Setup Procedure....................................................................................2
Chapter 2: Installing the 2000 ...................................................................................... 3
Unpacking.................................................................................................................... 3
Installation ...................................................................................................................3
Electrical Connections.................................................................................................3
Chapter 3: Using the 2000............................................................................................ 7
Applying Power to the 2000......................................................................................... 7
The Display.................................................................................................................. 7
The Keypad................................................................................................................. 8
Using the Menus.......................................................................................................... 9
Installing a Sensor..................................................................................................... 10
Measurement Designations.......................................................................................10
Displaying Measurements ......................................................................................... 10
Alarm Indications.......................................................................................................12
Chapter 4: Making Measurements............................................................................. 13
Measurement Process ............................................................................................... 13
Measurement Types.................................................................................................. 13
Selecting a Measurement Type.................................................................................17
Cell Constants........................................................................................................... 17
Conductivity Temperature Compensation.................................................................. 18
pH/ORP Temperature Compensation ........................................................................ 19
Dissolved Oxygen Temp and Pressure Compensation. ............................................ 20
AC Power Frequency.................................................................................................20
Chapter 5: Using Setpoints ........................................................................................ 21
Overview.................................................................................................................... 21
Setpoint Signal .......................................................................................................... 21
Setpoint Value........................................................................................................... 21
Setpoint State............................................................................................................21
Assigned Relay.......................................................................................................... 22
Programming a Setpoint............................................................................................ 22
USP & EP Setpoints.................................................................................................. 23
Chapter 6: Using Relays.............................................................................................24
Description................................................................................................................. 24
Electrical Connections............................................................................................... 24
Delay Time ................................................................................................................ 24
Hysteresis.................................................................................................................. 24
Relay State................................................................................................................24
Programming a Relay................................................................................................ 24
Chapter 7: Using Analog Outputs .............................................................................. 27
Description................................................................................................................. 27
Programming the Analog Outputs ............................................................................. 27
Analog Output Calibration.......................................................................................... 29
Chapter 8: Meter Calibration...................................................................................... 30
Overview.................................................................................................................... 30
Calibration Verification...............................................................................................30
Calibration Procedure................................................................................................ 31
Chapter 9: Sensor Calibration.................................................................................... 34
Conductivity/Resistivity Cell Constants......................................................................34
Conductivity/Resistivity Sensor Calibration................................................................ 34
pH/ORP Sensor Calibration....................................................................................... 36
pH Sensor Diagnostics.............................................................................................. 38
Dissolved Oxygen Sensor Calibration ....................................................................... 38
Dissolved Ozone Sensor Calibration......................................................................... 42
Chapter 10: Security/Lockout.....................................................................................44
Security Features ...................................................................................................... 44
Changing the Password............................................................................................. 44
Enabling the Lockout................................................................................................. 44
Accessing a Locked Menu......................................................................................... 44
Chapter 11: Other Functions...................................................................................... 46
Averaging .................................................................................................................. 46
System Reset............................................................................................................ 46
Setting the Temperature Source................................................................................ 47
Sending Data to a Printer or Computer ..................................................................... 47
Chapter 12: Troubleshooting ..................................................................................... 49
Off-Line Self-Diagnostics...........................................................................................49
On-Line Diagnostics ................................................................................................. 49
Troubleshooting......................................................................................................... 50
Recovery Procedure ................................................................................................. 50
Chapter 13: Service..................................................................................................... 51
Fuse Replacement .................................................................................................... 51
Reducing 2000 Patch Cord Length............................................................................ 51
Recommended Spare Parts List................................................................................ 52
Accessories............................................................................................................... 52
Chapter 14: Technical Illustrations............................................................................ 53
Menu Trees ............................................................................................................... 54
Overall Dimensions.................................................................................................... 57
Panel Cutout.............................................................................................................. 58
Exploded Assembly................................................................................................... 58
Pipe Mounting............................................................................................................ 59
Sealed Back Cover Assembly ................................................................................... 59
Printed Circuit Board Layout...................................................................................... 60
Rear Panel Wiring and Patch Cords.......................................................................... 61
Conductivity Calibrators.............................................................................................62
Meter Calibration Connections .................................................................................. 62
SPECIFICATIONS........................................................................................................ 63
RATINGS......................................................................................................................65
WARRANTY ................................................................................................................. 66
CHAPTER 1: GETTING STARTED
Setpoints (alarms): 4 independent alarms
INTRODUCTION
The 2000 is an analytical and process control instrument for measuring solution properties. It can process two sensor inputs for pH, ORP (redox potential), conductivity or resistivity, or one sensor input for dissolved oxygen or dissolved ozone, in all combinations except for ozone and four-electrode conductivity. A liquid crystal display conveys measuring data and setup information. The display is backlit for viewing in all lighting conditions. The menu structure allows the operator to modify all operational parameters by using keys on the front panel. A menu-lockout feature, with password protection, is available to prevent the unauthorized use of the meter. The 2000 can have up to four relays for process control.
The 2000 instrument is equipped with a communication interface that can be configured as either an RS422 or an RS232. This interface provides real-time data output and complete instrument configuration capabilities for central monitoring via personal computer or Programmable Logic Controller (PLC). An external isolator for the digital communications signal is required if measurements other than conductivity with 0.1/cm cell constants are being made. For coverage of communications, see Manual 84423.
FEATURES
Display: 16 character backlit LCD. Measurements: pH, ORP (redox potential),
resistivity, conductivity, dissolved oxygen, dissolved ozone, °C, °F, total dissolved solids, %rejection, difference, ratio, %HCl, %NaOH, %H2SO4.
Measurement Channels: 2. Signal Inputs per channel: 2 (total of 4 signals
for measurement). Measurement Cycle Time: 1 second (4
measurements processed per second). Programmable: all setup information is stored in
non-volatile memory.
programmable as high, low, USP, or EP limits. Relays: up to 4 with programmable delay time
and hysteresis.
Outputs: 2 analog outputs (0/4-20mA). Communications: RS232/RS422 interface, bi-
directional; external isolator recommended with measurements other than conductivity with
0.1/cm cell constants.
Security: keypad lockout with password. Calibration: complete instrument, output, and
sensor calibration; can be NIST traceable. Built-In Diagnostics: several self tests can be
initiated at any time.
OVERVIEW OF OPERATION
When power is applied to the 2000, the initialization process begins. The instrument will perform a number of self tests. Any problems detected during these tests will be reported by a displayed message.
Next, all setup parameters (setpoints, states, relay conditions, etc.) are restored from a non­volatile memory.
The meter will then begin the measurement process. A complete measurement cycle is performed once per second and consists of the following:
1. Measure four signals and compute four measurements.
2. Check setpoints against the measurements.
3. Control the relays.
4. Update analog output signals.
5. Transmit measurement data over the communication port.
6. Display data (if not displaying a menu).
At any time during this process the menus can be accessed by pressing one of the menu keys. The display of a menu will not affect the measurement process.
Chapter 1 Getting Started 1
INSTALLATION & SET UP PROCEDURE
The following guideline shows the steps necessary to install a 2000 meter and begin operation.
1. Follow the meter installation procedure for physically mounting the meter, as outlined in Chapter 2. The meter may be mounted in a panel, on a pipe, or on a wall.
Optional: the rear cover is required for wall and pipe mounting. Drill holes as needed for conduit or cable grips, install the cover and wire the meter before wall or pipe mounting.
2. Make all necessary electrical connections to the meter after panel mounting. The wiring procedure is outlined in Chapter 2.
3. Required wiring: input power and sensor
cables.
CAUTION: Be certain that patch cord is wired specifically for the type of sensor to be connected or damage could result.
12. Optional: program the relays as shown in Chapter 6.
13. Optional: program other features such as averaging method, special temperature compensation, security/password, etc, as needed.
4. Optional wiring: relays, analog outputs, and serial port.
5. Set appropriate input line frequency to reduce measurement noise. See AC POWER FREQUENCY in Chapter 4.
6. Instrument calibration is performed at the factory to specifications. Re-calibration is not necessary. If QA/QC practice requires it, meter calibration may be verified as outlined in Chapter 8.
7. Connect sensors to the patch cords.
8. Select the desired measurements for each sensor as shown in SELECTING A MEASUREMENT TYPE in Chapter 4.
9. Enter sensor constants from the label of each cell as outlined in ENTERING/EDITING CELL CONSTANTS in Chapter 9. DO NOT PERFORM A SENSOR CALIBRATION except for pH, dissolved oxygen or ozone.
10. Optional: program the analog outputs as shown in Chapter 7. DO NOT AN OUTPUT CALIBRATION.
PERFORM
11. Optional: program the setpoints as shown in Chapter 5.
2 Getting Started Chapter 1
CHAPTER 2: INSTALLING THE 2000
UNPACKING
Each 2000 is packed in an individual biodegradable carton. Retain the packaging in the event that the instrument must be returned to Thornton for service or calibration.
This carton should contain: 1 - 2000 Instrument 1 - Set of panel mounting hardware with
gasket 1 - 02192 kit of 2 ferrite bead noise
suppression modules 1 - 84401 Instruction Manual 1 - 84402 Startup Instruction Sheet 1 - Certificate of Calibration
INSTALLATION
The 2000 can be mounted in a panel, on a pipe or attached to a wall.
Panel Mounting Cutout and Installation
The panel cutout should measure 7.56 inches wide by 3.780 inches high (192 mm X 96 mm). Drill four holes for the #10 mounting screws. See Figure 14.3 for panel cutout size and mounting screw hole spacing. When mounting multiple instruments on the same panel, note the front flange dimensions in Figure 14.2 in order to allow enough space between instruments.
Panel cutouts should be clean and free of burrs and sharp edges. The proper dimensions allow an instrument to slide freely into the cutout.
Install the panel gasket (supplied with instrument) on the instrument mounting flange. Slide the instrument into the cutout and secure it with the mounting screws.
CAUTION: Do not over tighten the screws as this may crack the case.
If the rear cover is used in a panel mounted installation, the 2000 unit must be installed in the panel opening before the rear cover is installed.
Wall Mounting
The 2000 can be easily mounted to a wall when the rear cover is installed. The flanges on the ends of the cover contain holes for screws to fasten the assembly to the wall. A layout for drilling mounting holes is included in the wall mount kit.
Pipe Mounting
The 2000 can be mounted to a pipe with the pipe mounting accessory kit. The assembly is shown in Figure 14.5.
ELECTRICAL CONNECTIONS
All electrical connections are made at plug-in terminal blocks at the rear of the 2000 case.
WARNING: MAKE SURE POWER TO ALL WIRES IS TURNED OFF BEFORE PRO­CEEDING WITH THE INSTALLATION. HIGH VOLTAGE MAY BE PRESENT ON THE INPUT POWER WIRES AND RELAY WIRES.
CAUTION: A good power earth ground connection is required for safety and for proper operation of the instrument. To prevent electrostatic discharge (ESD) from damaging the instrument during installation, the installer must also be electrically grounded i.e., wear a conductive wrist strap connected to earth ground.
Do not run power and relay wiring in the same conduit or parallel with sensor and output signal wiring to prevent interference.
Input Power and Relay Connections
Terminal block TB1 contains connections for the input line power and relay contacts. Depending upon the model number, the 2000 will have either 2 or 4 relays. Table 2.1 shows the wiring sequence.
All relays have “dry contacts”; they are potential­free and require external power to be wired in series with the load and instrument terminals. Relays 3 and 4, if specified, are solid state AC-
Chapter 2 Installation 3
only relays (triacs) and require a minimum current of 10 mA to switch reliably. With very small loads such as a neon bulb, test meter or PLC, a load resistor is required in parallel with the load, e.g. a 10K ohm, 2 watt resistor, for operation with 115 VAC.
WARNING: IF THE INPUT VOLTAGE JUMPERS ARE CHANGED YOU MUST LABEL THE UNIT WITH THE NEW VOLTAGE REQUIREMENT. ALSO, THE FUSE MUST BE CHANGED TO THE PROPER RATING TO AVOID RISK OF FIRE HAZARD
TB1 Label
Input Power & Relay Function
L 115V/230 VAC Line N 115V/230 VAC Neutral
Earth Ground
NC1 Relay1: Normally Closed C1 Relay1: Common NO1 Relay1: Normally Open
NC2 Relay 2: Normally Closed C2 Relay 2: Common NO2 Relay 2: Normally Open
C3 Relay 3: Common NO3 Relay 3: Normally Open
C4 Relay 4: Common NO4 Relay 4: Normally Open
Table 2.1: Input Power & Relay Connections
WARNING: MISWIRING THE AC POWER MAY DAMAGE THE INSTRUMENT AND WILL VOID ALL WARRANTIES.
Setting Input Voltage for 115 VAC or 230 VAC
The input voltage for a 2000 can be set for either 90-130 VAC or 180-250 VAC operation. The input voltage is preset at the factory and is indicated on the serial number label on the side of the unit. Jumpers on the printed circuit board can be changed to change the input voltage. See Figure
14.7. W4 jumper pins are located between the
power transformer and the fuse. For 90-130 VAC operation jumper pins 1-2 and 3-4 must be used. For 180-250 VAC operation only a jumper on pins 2-3 must be installed. The jumpers can be accessed by removing two screws from the back panel and carefully lifting the panel off.
Fuse requirements: For 90-130 VAC: 1/8 Amp, SB, 250 VAC For 180-250 VAC: 1/16 Amp, SB, 250 VAC NOTE: If the line power frequency is changed,
select the correct setting (see AC POWER FREQUENCY in Chapter 4).
Setting Input Voltage for 24 VDC
The 2000 can be operated from a +24 VDC power supply instead of the typical 90-130 VAC or 180-250 VAC source.
NOTE: 24 VDC power supply must be isolated from earth ground and between instruments. Use a DC/DC power isolator if necessary.
Remove any AC power connections from terminal block TB1.
1. Move circuit board jumper W6 to the 24V position (left two pins) as shown in Figure
14.7.
2. Connect + 24V DC power to the connection labeled PS+ on terminal block TB3. Connect the power supply ground to the connection labeled PS- on TB3.
WARNING: AC POWER CONNECTIONS MUST BE REMOVED WHEN USING THE +24V POWER INPUT.
NOTE: The +24 VDC input is not fused within the
meter. Use an external fuse.
AC Power Wiring
In order to maintain safety for the electrical installation, no more than 6 mm of insulation is to be removed from each conductor before fully inserting into the electrical terminal.
The plug-in terminal blocks for all connections will accept wire sizes from 26 AWG (0.126 mm to 14 AWG (2.08 mm to 12 AWG (3.31 mm
2
), solid or stranded and up
2
) stranded only.
2
)
4 Installation Chapter 2
Output Connections
Connections for all outputs are made to terminal block TB4. The serial port can be configured as an RS232 port (shown in Table 2.2.) or an RS422 port (shown in Table 2.3). An external isolator for digital communications is strongly recommended to prevent ground loop problems.
TB2 Label
AO2- Output 2 (-) AO2+ Output 2 (+) AO1- Output 1 (-) AO1+ Output 1 (+)
Analog Output Function
TB2 Label RS232 Function
DGND Ground TXD+ Not Used TXD- Transmit Data RXD+ Not Used RXD- Receive Data
Table 2.2: RS232 Connections
TB2 Label RS422 Function
DGND Ground TXD+ Transmit Data Positive TXD- Transmit Data Negative RXD+ Receive Data Positive RXD- Receive Data Negative
Table 2.3: RS422 Connections
Each analog output has + and – connections. Analog outputs are self-powered with a maximum load resistance of 500 ohms.
CAUTION: Do not connect analog outputs to circuits supplying power.
CAUTION: Do not connect analog output cable shield(s) to the adjacent DGND terminals. Connect shield(s) only to one of the earth ground terminals next to AC line power.
Table 2.4: Analog Output Connections
Sensor Patch Cord Connections
The sensors are connected to plug-in terminal blocks TB2 and TB3. Each channel has nine terminals for the sensors plus earth ground. Patch cords, 1XXX-67 or 58 080 20X series, for the 2000 have a connector on one end and tinned leads on the other end. Table 2.5. shows the wiring pattern for each type of sensor.
CAUTION: Wiring for each type of sensor is different. Miswiring patch cords may damage sensors and will void all warranties. Verify wire colors in table 2.5. Disconnect power before wiring sensors to prevent damage to the input circuit.
If sensors other than conductivity must be wired with the instrument powered, make the PS- connection first to prevent damage to the input circuit.
To meet CE electromagnetic compatibility requirements for emissions Class B, install a
ferrite suppression module from kit 02192 on each sensor patch cord as close to the instrument as possible.
NOTE: For ultrapure water conductivity measurements with all-plastic piping, especially semiconductor wet benches, it is recommended to connect a jumper from one of the three earth ground terminals to sensor ground terminal SIG6(6) on TB3 for Channel A. This will prevent possible instrument damage due to electrostatic charges that build up in plastic piping systems. Do not use a ground jumper with higher conductivity water, with metal piping or with pH or ORP measurements.
Chapter 2 Installation 5
Terminal Cond/
Resistivity
EARTH GND*
PS-
+5V (9) I/O (8) Ch A** I/O (8) Ch B**
SIG7(7) SIG6(6) SIG5(5)
SHIELD
BLACK
-
-
-
-
BLUE
RED
pH/ORP Dissolved
Oxygen
SHIELD
BLACK
BLUE
-
-
WHT/BLU
-
RED
-
BLACK
BLUE
WHT/BLU
RED
SHIELD
-
CLEAR
Ozone
SHIELD
BLACK
BLUE
WHT/BLU
RED
JUMP-5***
-
CLEAR
Alternative 3-Lead Conductivity Sensor Connections
Tinned-lead cells with 1000 Pt or 500 Ni-Fe RTDs may be used with the 2000. These sensors, with integral leadwire and no connector, enable the lead to pass through small openings. The sensor/instrument separation is limited to less than 50 feet (20 feet recommended).
Somewhat lower accuracy may result. Connections are given in Table 2.6. Jumpers should be 22 gauge to match the conductor size in the cable, for secure terminal connections.
SIG4(4) SIG3(3) SIG2(2) SIG1(1)
* Connect to any of three earth ground terminals. ** Connections for dissolved oxygen and ozone use
both channel A and B I/O terminals regardless of
which channel is assigned for that measurement. *** Install a wire jumper between terminals 5 and 7. For instruments with firmware version 2.0 and earlier
(before April 2004), pH, ORP and dissolved oxygen connections must connect the black wire to SIG6(6) instead of PS-. Ozone measurement requires firmware version 4.0 or higher.
GREEN
WHITE CLEAR
WHT/BLUE
GREEN
WHITE CLEAR
GREEN
WHITE
-
GREEN
WHITE
-
-
-
-
Table 2.5: Sensor Patch Cord Connections
Voltage and current measuring terminals are rated for overvoltage category II.
Sensor Models/Types
240-, 243- 2-Electrode Conductivity 244- 4-Electrode Conductivity 363- & 1200- pH or ORP 367- dissolved oxygen
Terminals Three-lead Conductivity
Sensor Wiring
+5V (9) I/O (8) SIG7(7) SIG6(6) SIG5(5) SIG4(4) SIG3(3) SIG2(2) SIG1(1)
-
­Jumper to SIG(6) Jumper to SIG(5) CLEAR (shield) WHITE Jumper to SIG(1)
­RED
Table 2.6: Alternative Sensor Connections
With these 2_8 Series Dot Two sensors there is no label with factory-supplied precision calibration constants. Only the nominal value 0.1/cm for cell constant and 1.0 for temperature constant are entered into the 2000.
With all tinned-lead sensors, when meter calibration is desired, the cell must be disconnected and a patch cord installed in its place to accept a calibrator.
368- dissolved ozone
6 Installation Chapter 2
CHAPTER 3: USING THE 2000
APPLYING POWER TO THE 2000
After applying power to the meter, the display will show an introduction message for three seconds and then begin making measurements. This message shows the model number and the software version number as follows:
In the menus, an underline cursor and flashing (bold) characters will indicate a field that can be changed. A typical menu appears as follows:
SP1=17.00 M High
68XX Ver X.X
While the message is being displayed the instrument is performing self diagnostics. Various circuits are tested during this process and any failure will be noted with a message. The diagnostics can be repeated at any time via the menus.
The default measurement display is the primary readings from the sensors on channel A and B as shown below:
A1.76µS B2.11µS
All 2000 meters are calibrated from the factory and normally require no further calibration. If QA/QC practice requires it, the instrument be calibrated after installation. See Chapter 8 for more information on meter calibration.
THE DISPLAY
The 2000 uses a 1 line by 16 character alphanumeric display to convey all measurement and setup information. This instrument will display one or two measurements, each with channel indication and unit of measure. A typical display of measurement data is:
This menu indicates that setpoint #1 is programmed at a value of 17.00 M (million) and is set as a high limit. The cursor is under the digit “7” indicating that the UP and DOWN keys can be used to change it. The RIGHT and LEFT keys will move the cursor to the next or previous field.
Display Contrast Adjustment
The contrast quality of the display can change with ambient temperature. The display contrast is adjusted from the factory for operation at standard room temperature (25°C). If the meter is operated at an ambient temperature that is much different then it may be necessary to make an adjustment. A potentiometer is accessible from the back side of the instrument to change the contrast. Use a small slotted screwdriver to gently turn the potentiometer. A counter-clockwise turn will increase the contrast and a clock-wise turn will decrease the contrast. The rear panel is shown in Figure 3.1.
A7.76pH B2.10µS
This display indicates that channel A is measuring 7.76pH and channel B is measuring
2.10µS/cm. The display of the other measurements can be achieved by pressing the UP or DOWN keys.
Chapter 3 Using the 2000 7
Figure 3.1: 2000 Rear Panel
THE KEYPAD
The 2000 is equipped with an 11-key keypad as shown in Figure 3.2.
THORNTON
A1.076µS
Figure 3.2: 2000 Front Panel
8 Using the 2000 Chapter 3
B1.055µS
2000
The keypad has 6 keys that provide direct access to specific menus as follows:
instrument to accept the options that are displayed and move to the next menu.
1. MEASURE MODE - menus to change
measurement modes.
2. SETPOINTS - menus for programming
setpoints.
3. RELAYS - menus for programming relays.
4. OUTPUTS - menus for programming
outputs.
5. CALIBRATE - menus to perform calibration.
6. MENUS - all other menus (cell constants,
security, compensation, averaging, etc.).
The other keys are referred to as control keys and are used to make changes within a menu.
1. OK/NEXT Key - used to accept a selection
and proceed to the next menu level.
2. UP Key - up arrow is used to scroll up
through a list of options.
3. DOWN Key - down arrow is used to scroll
down through a list of options.
4. LEFT Key - left arrow is used to move the
cursor to the left within a menu.
5. RIGHT Key - right arrow is used to move the
cursor to the right within a menu.
USING THE MENUS
There are six menu keys across the bottom of the 2000 front panel. The first five of these keys (MEASURE MODE, SETPOINTS, RELAYS, OUTPUTS, AND CALIBRATION) are used to enter specific menus. These menus allow the modification of parameters most frequently used by the operator. The sixth key labeled MENUS allows access to all other menus for various functions such as setting compensation methods, security levels, etc.
The UP and DOWN arrow keys scroll vertically through the menus. Part or all of the display changes to the next option whenever an UP or DOWN arrow key is pressed. A field is defined as a section of the display that can be changed. The characters of the field will also blink. The LEFT and RIGHT arrow keys move the underline cursor across the display from one field to the next. Pressing the OK/NEXT arrow key causes the
Numbers are set one digit at a time using the arrow keys. The LEFT and RIGHT arrow keys are used to position the underline cursor below the digit to be changed. The UP and DOWN arrow keys are then used to change the value of the digit. Each digit can be scrolled through the values: .(decimal point), 0, 1, 2, 3, 4, 5, 6, 7, 8, and 9 The first digit of any number can also be set to a negative sign (-).
To exit the menus either scroll completely through a set of menus with the OK/NEXT key or press any of the six menu keys at any time. The meter will display a prompt asking if the recent changes should be saved.
Save Changes Yes
To save the changes press the OK/NEXT key with “Yes” on the display. To discard the changes use the UP or DOWN arrow keys to change “Yes” to “No”, then press the OK/NEXT arrow key.
If the instrument is displaying a menu and a key is not pressed for two minutes, the instrument will
automatically exit the menus without saving any changes. When performing a calibration the
operator may need to wait for a measurement to stabilize so the menu time-out feature is automatically disabled.
Menu Example
Press the MEASURE MODE key and the display will show:
A=S/cm (AUTO)
This menu indicates that the Channel A primary measurement is set for conductivity (S/cm) with auto ranging. The section “S/cm” is the field to be changed and will be flashed as long as the cursor is under it. Pressing the UP arrow key will change the “S/cm” to “-cm”. The RIGHT arrow key will move the cursor to the “(AUTO)” field.
A=/cm (AUTO)
Chapter 3 Using the 2000 9
The OK/NEXT key is used to accept the entry and move to the next menu. When the last menu level is reached the following message is displayed:
b = channel B secondary measurement Upper case letters are used to indicate the
primary measurements and lower case letters are used to indicate the secondary measurements.
Save Changes Yes
Pressing the OK/NEXT key will save the changes and exit the menus. The UP and DOWN arrow keys can be used to change the “Yes” to “No”. Pressing the OK/NEXT key with “No” will discard the changes and exit the menus.
INSTALLING A SENSOR
Each sensor is equipped with a cell and temperature sensor (except ORP). Conductivity sensors have calibration constants for these elements that must be programmed into the meter for proper operation. These factors are printed on the sensor (as well as a Certificate of Calibration supplied with each conductivity sensor). The label may look like this:
RES M=1.0034 TEMP M=1.0015
RES M is the conductivity cell constant, and TEMP M is the temperature sensor constant. pH preamps will have a pH A (adder) constant. Long life 367-110 dissolved oxygen sensors have Cell M (multiplier), Cell A (adder) and TEMP M (multiplier) constants. See ENTERING/ EDITING CELL CONSTANTS in Chapter 9 for information on entering cell constants.
Each of the four calculated measurements can be one of the following:
1. pH
2. ORP (redox potential)
3. Resistivity
4. Conductivity
5. Total Dissolved Solids (TDS)
6. Degrees C
7. Degrees F
8. % Rejection
9. Difference (A-B or B-A)
10. Ratio (A/B or B/A)
11. %HCl
12. %NaOH
13. %H2S0
14. Dissolved Oxygen
15. Dissolved Ozone
16. Power plant calculations of pH, CO chlorides or sulfates from conductivity
4
2
DISPLAYING MEASUREMENTS
,
MEASUREMENT DESIGNATIONS
The 2000 instrument will measure four fundamental signals during each measurement cycle. These measurements are the conductivity, pH or dissolved oxygen and temperature of the probe on channel A and the conductivity or pH and temperature of the probe on channel B.
The 2000 can process and display four calculated measurements. They are referred to as A primary, A secondary, B primary and B secondary. These measurements are designated by a single letter as follows:
A = channel A primary measurement a = channel A secondary measurement B = channel B primary measurement
10 Using the 2000 Chapter 3
Changing the Display of Measurements
The 2000 display can show either one or two measurements at a time. The display of measurements can be changed by using the UP or DOWN arrow keys. Pressing one of these keys will cause the meter to change the display mode (show an alternative set of data).
The display modes for two measurements per line are:
Mode #1: A primary and B primary (three significant digits displayed for each parameter):
A1.76µS B2.11µS
Mode #2: A secondary and B secondary (three significant digits displayed for each parameter).
Press the MENUS key and the following menu will appear:
a25.2°C b25.1°C
Mode # 3: A Primary and A Secondary (four significant digits displayed for each parameter):
A1.764µS 25.10°C
Mode #4: B primary and B Secondary (four significant digits displayed for each parameter):
B2.109µS 25.12°C
Note that when two measurements from the same channel are displayed, the secondary measurement indicator ( a or b) is not displayed. This allows for greater precision in the display of the primary measurement.
The default display setting (after a system reset) is mode #1 (A Primary & B Primary).
The display modes for one measurement per line are:
Mode #1: A Primary:
Menus use arrows
Press the UP arrow key until “Display Menus” is displayed.
Display Menus
Press the OK/NEXT key to access this menu. Use the Up or DOWN keys to toggle the field until “Disp Format” appears. Press OK/NEXT to access this menu.
Set: Disp Format
Use the UP and DOWN keys to toggle the field between “1” and “2”.
Measure per Line: 1
Press OK/NEXT when done. The meter will ask if changes should be saved.
Save Changes Yes
A 1.765µS/cm
Mode #2: A Secondary:
a 25.25 deg C
Mode #3: B Primary:
B 2.109µS/cm
Mode # 4: B Secondary:
b 25.12 deg C
Setting the Number of Measurements per Display Line
The 2000 can be set to display either one or two measurements per line.
To change this feature:
Press OK/NEXT key to save the changes and return to the display of measurement data.
Measurement Display Scrolling
The 2000 has an automatic display scrolling feature for measurement data. With this feature enabled, the display will show channel A data for 5 seconds and then show channel B data for 5 seconds. Secondary measurements are not shown if a single measurement is selected per display line. The process is repeated indefinitely.
To enable or disable this feature: Press the MENUS key and the following menu
will appear:
Menus use arrows
Press the UP arrow key until “Display Menus” is displayed.
Display Menus
Chapter 3 Using the 2000 11
Press the OK/NEXT key to access this menu
Set: Auto Scroll
Use the Up or Down arrow keys to toggle the field until “Auto Scroll” appears. Press OK/NEXT to access this menu.
Auto Scroll=off
Use the UP or DOWN arrow keys to toggle the field from “Off” to “On”. Press the OK/NEXT key when done. The meter will ask if changes should be saved.
Save Changes Yes
Press the OK/NEXT key to save the changes and return to the display of measurement data.
ALARM INDICATIONS
A setpoint can be programmed as a high limit, a low limit, USP or EP (temperature-dependent pharmaceutical water conductivity) limits. When a measurement is higher than a high, USP or EP point or lower than a low point then the setpoint is in alarm state. This condition is indicated by flashing the corresponding measurement value in the normal operating display. See Chapter 5: Using Setpoints.
12 Using the 2000 Chapter 3
CHAPTER 4: MAKING MEASUREMENTS
MEASUREMENT PROCESS
The 2000 will process two measurements from each of the two channels. The measurements of each channel are referred to as the primary and the secondary measurement. The instrument will process a total of four different measurements per cycle.
Measurements are designated as follows: A = channel A primary measurement a = channel A secondary measurement B = channel B primary measurement b = channel B secondary measurement
Upper case letters indicate primary measurements and lower case letters indicate secondary measurements.
MEASUREMENT TYPES
Each of the four measurements (channel A primary, etc.) is programmed as one of the following with corresponding 1 or 2-character display:
Measurement
pH ORP (redox potential) Resistivity
Conductivity – siemens/cm, siemens/m Total Dissolved Solids (TDS), ppm, ppb
Dissolved Oxygen – g/L, ppm, ppb, % saturation
Dissolved Ozone – ppm (mg/L), ppb (µg/L)
Temperature – Deg C, Deg F % Rejection Difference (A-B or B-A) Ratio (A/B or B/A) %HCl - Hydrochloric Acid %NaOH - Sodium Hydroxide %H2S04 - Sulfuric Acid
Display
pH
V
S, Σ
PM, PB
g, pm,
pb, %
Z,
z
°C, °F
%R
d
r %H %N %S
Power cycle chemistry calculations of pH, CO
, Chloride, Sulfate
2
PH, CD,
Cl, Sf
pH and ORP (Redox potential)
pH is displayed with fixed range. ORP is displayed in fixed range millivolts (mV).
Resistivity
Resistivity is expressed in ohms-centimeter (Ω- cm). This measurement can be displayed with a prefix in front of the units. The prefixes are k (kilo or 1,000) and M (Mega or 1,000,000).
The display can be set for a fixed range such as -cm, K-cm (1,000-cm), or M-cm (Mega or 1,000,000-cm). The 2000 can also be set for auto ranging where the range will be automatically adjusted for the most appropriate display. The range is set via the measure mode menus.
1,000,000 -cm = 1,000 K-cm = 1 M-cm
Conductivity
Conductivity is expressed in siemens per centimeter (S/cm) and is the reciprocal of resistivity. This measurement can be displayed with a prefix in front of the units. The prefixes are m (milli or 1/1,000) and µ (micro or 1/1,000,000). The 2000 can also be set for auto ranging where the range will be automatically adjusted for the most appropriate display. The range is set via the measure mode menus.
1 S/cm = 1,000 mS/cm = 1,000,000 µS/cm Conductivity may also be expressed in siemens
per meter units as described above. To clearly distinguish these units in the 2000 display, the symbol “Σ” is used in place of “S”. In operation, microsiemens per meter is displayed as µΣ.
(S/m) with a multiplier in front of the
Total Dissolved Solids
Total Dissolved Solids (TDS) is another way to measure and display conductivity/resistivity data. TDS is the equivalent of Sodium Chloride (NaCl) required to produce the measured conductivity-­approximately 0.46 ppm TDS per µS/cm. If some
Chapter 4 Making Measurements 13
other conversion is desired, it is necessary to adjust the cell constant to give direct readout. For example, if a conversion of 0.6 ppm TDS per µS/cm is desired, the cell multiplier to be entered into the 2000 is 0.6/0.46 x Multiplier on sensor label. See Chapter 9, Entering/Editing Sensor Constants.
TDS is measured in parts per billion (ppb), parts per million (ppm), or parts per thousand (ppk). A TDS reading of 10 ppm is equivalent to 10 milligrams per liter. Because of space limitations, the following abbreviations are used to display TDS units:
PB = parts per billion
Temperature
Temperature can be measured in degrees Celsius (°C) or degrees Fahrenheit (°F). The 2000 normally works with a 1000 ohm DIN platinum RTD sensor which is built into Thornton most conductivity, dissolved oxygen, dissolved ozone and most pH sensors. Alternatively, the 2000 can automatically recognize and measure with a 500 ohm Ni-Fe RTD temperature sensor. When configured for a 50/cm constant cell only, the 2000 automatically changes its characteristic to measure from the 262 ohm @ 25°C thermistor supplied in those sensors.
PM = parts per million PK = parts per thousand
Dissolved Oxygen
Dissolved oxygen can be measured in units of parts per billion (ppb), parts per million (ppm), and grams per liter (g/L), with or without auto­ranging between micro and milli (grams per liter). Abbreviations used in the display mode are pb, pm, µg and mg, respectively. Note that dissolved oxygen uses lower case pb and pm to distinguish it from TDS which uses upper case PB and PM.
NOTE: Select dissolved oxygen as a measurement after connecting the probe. This initiates an automatic internal preamp calibration for highest accuracy at startup and will display “Saving Changes” for an extended period. Otherwise, the system will initiate calibration by itself 1 hour later.
Dissolved Ozone
Dissolved ozone can be measured in units of parts per billion (ppb) with resolution of 1 ppb or in units of parts per million (ppm) with resolution of 0.01 ppm. Abbreviations for units in the normal display mode are z and Z respectively.
NOTE: Select dissolved ozone as a measurement after connecting the preamp. This initiates an automatic internal preamp calibration for highest accuracy at startup and will display “Saving Changes” for an extended period. Otherwise, the system will initiate calibration by itself 1 hour later.
% Rejection
For reverse osmosis (RO) applications, percent rejection is measured in conductivity to determine the ratio of impurities removed from product water to the total impurities in the incoming feed water. The formula for obtaining Percent Rejection is:
[1 - (Product/Feed)] X 100 = % Rejection
Where Product is the conductivity measurement of the first sensor and Feed is the conductivity of the second sensor. Figure 4.1 shows a diagram of an RO installation with sensors installed for Percent Rejection.
CONDUCTIVIY
SENSOR
REVERSE OSMOSIS MEMBRANE
B
FEED PRODUCT
Figure 4.1: % Rejection
IMPORTANT: When preparing the system to perform a percent rejection measurement, the product monitoring sensor must be installed in the channel that will measure percent rejection. If the product conductivity sensor is installed in channel A, then percent rejection must be measured in channel A. Likewise if the product sensor is installed in channel B, then the percent rejection
REJECT
CONDUCTIVITY
SENSOR
A
14 Making Measurements Chapter 4
measurement must also be programmed in channel B.
Difference (A-B or B-A)
The difference measurement is computed as:
Difference on channel A = A-B.
or
Difference on channel B = B-A.
When the difference is assigned to one channel, the meter will measure the same type of measurement mode of the other channel as a basis. For example, if channel A is set to measure the difference and channel B is measuring conductivity, then the 2000 will measure conductivity on both channels before computing the difference. The displayed unit for difference is ‘d’.
Ratio (A/B or B/A)
This measurement is similar to the difference measurement.
Ratio on channel A = A/B. Ratio on channel B = B/A. The displayed unit for ratio is ‘r’.
Concentrations (%HCl, %NaOH, %H2SO4)
All concentrations are displayed as percent by weight. Setting a measurement for concentration automatically activates specialized temperature compensation for that particular material. The compensation setting is ignored for that channel.
Power Plant Calculated Parameters
The following derived parameters are valid only for power plant cycle chemistry samples conditioned by a cation exchanger (and sometimes a degasifier) as illustrated in Figure
4.2. They are not applicable to other samples and would give very erroneous results elsewhere. Because the 2000 can provide two measurements from a single sensor channel, it can be configured to display two conductivity measurements, sample temperature and calculated pH or CO
measurements.
2
Calculated pH may be obtained very accurately from specific and cation conductivity values when the pH is between 7.5 and 10.5 due to ammonia or amines and when the specific conductivity is significantly greater than the cation conductivity. The 2000 uses this algorithm when CALCPH is selected using the Measure Mode key for the channel measuring cation conductivity.
For example, set up measurement ‘A’ to be specific conductivity, measurement ‘a’ to be temperature, measurement ‘B’ to be cation conductivity and measurement ‘b’ to be calculated pH. Set the temperature compensation mode to “Ammonia” for measurement ‘A’ and to “Cation” for measurement ‘B.’
Note that if operation goes outside the recommended conditions, a glass electrode pH measurement is needed to obtain an accurate value. On the other hand, the calculated pH provides an accurate standard for one-point trim calibration of the electrode pH measurement when sample conditions are within the ranges noted above.
Carbon dioxide may be calculated from cation conductivity and degassed cation conductivity using tables from ASTM Standard D4519. The 2000 has these tables stored in memory which it uses when units of CO2ppb are selected under the Measure Mode key.
For example, set up measurement ‘A’ to be cation conductivity, measurement ‘a’ to be CO2ppb, measurement ‘B’ to be degassed cation conductivity and measurement ‘b’ to be temperature. Set the temperature compensation mode to “Cation” for both conductivity measurements.
Total anions as chlorides or sulfates may be readout on a degassed cation conductivity sample using tables from ASTM Standard D4519. The 2000 has these tables stored in memory which it uses when selected under the Measure Mode key by choosing units of “Clppb” or “SO4ppb” for parts per billion chlorides or sulfates. Conductivity is non-specific and cannot determine the actual anions present—it merely converts the conductivity value as if they were all chlorides or all sulfates. Set the temperature compensation mode to “Cation”.
The display units for these derived parameters are given below.
Chapter 4 Making Measurements 15
Measurements Menu Normal Display
PHCALC ( ) PH CO2ppb ( ) CD
pH calculated from conductivity is designated by all upper case ‘PH’. pH measured by electrode is designated by the conventional lower/upper case
‘pH’. Clppb ( ) Cl SO4ppb ( ) Sf
Specific Conductivity
+
NH
, OH-, Na+, H+, Cl-, HCO
4
-
3
CO
2
Degassed Cation Conductivity
+
H
, Cl
+
R–NH
R–Na
4
+
Degas Unit
Cation Exchanger
+
R–H
-
, OH-
3
Cation Conductivity
+
H
, Cl-, CO2, HCO
Fig. 4.2: Sample conditioning for specific, cation and degassed cation conductivity measurements used to calculate pH, CO
and anion concentration on power plant cycle chemistry
2
samples
-
, OH
-
16 Making Measurements Chapter 4
SELECTING A MEASUREMENT TYPE
To set or change a measurement type for each of the four measurements:
Press the MEASURE MODE key and the display will show the measurement type assigned to channel A primary. The display may appear as:
The field on the right half side of the display is the
range field. Some measurements can be set for a
fixed range, others can be set only for auto
ranging. For example, conductivity can be set for
micro, milli, units, or auto ranging. To change the
field, use the RIGHT arrow key to move the
cursor under “(Auto)”. Use the UP and DOWN
arrow keys to select the desired range.
A = -cm (AUTO)
This menu indicates that channel A primary measurement is set for resistivity (-cm) with auto ranging. The section -cm” is the first field to be changed and will be flashed as long as the cursor is under it. Pressing the UP arrow key will change the -cm” to “S/cm”.
The OK/NEXT key is used to accept the entry for
channel A primary and move to the next menu for
setting channel “a” secondary. Press the
OK/NEXT key a third and fourth time to set the
measurement types for channel B primary and
channel “b” secondary, respectively.
When the last menu level is reached (after setting
channel “b” secondary), the following message is
displayed:
A = S/cm (AUTO)
Use the UP and DOWN arrow keys to select the desired measurement type.
For dissolved oxygen, the sensor should be connected to the 2000 before selecting this parameter because the 2000 performs a DO preamplifier calibration when it is saved (and at hourly intervals thereafter). Also for this reason there is a long delay in the saving process.
For conductivity, both temperature compensated and uncompensated measurement are available. Uncompensated readings are needed to meet pharmaceutical water requirements. Select units of “S/cm” for compensated measurement or “s/cm U” for uncompensated measurement. Using both primary and secondary parameters, both compensated and uncompensated measurements are available simultaneously. In normal operation, uncompensated measurements are identified by a flashing cursor under the units, for example, “µ are identified by “µS”.
Another option for conductivity is to display in units of siemens per meter SI metric system. The Menu setting is
s”. Normal compensated readings
in accordance with the
Pressing the OK/NEXT key will save the changes
and exit the menus. The UP and DOWN arrow
keys can be used to change the “Yes” to “No”.
Pressing the OK/NEXT key with “No” will discard
the changes and exit the menus.
CELL CONSTANTS
The calibration of each measurement is defined
by a set of constants known as cell constants.
There are two cell constants for each
measurement: a Multiplier Factor and an Adder
Factor. They are used to derive an accurate
measurement from the sensor’s output signal. As
an example, the output of a conductivity sensor
can be represented by the following equation:
R = x / M + A
Where:
R = resistivity value
x = output from cell
M = multiplier factor
Save Changes Yes
A = S/m (AUTO)
The measurement mode will display it as “µΣ” or “mΣ”.
Chapter 4 Making Measurements 17
A = adder factor
Example: for a typical two-electrode conductivity
sensor the multiplier (M) is 0.1 and the adder (A)
is 0. If the sensor output is 120,000 ohms, then
the actual resistivity of the solution measured is
1.2 Mohm-cm and is calculated as follows:
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