Memmert Vacuum Oven Vo User Manual

VO

OPERATING MANUAL

VACUUM OVEN VO
MADE IN GERMANY.
www.memmert.com
MEMMERT GmbH + Co. KG Willi-Memmert-Straße 90-96 91186 Büchenbach Germany
Phone: +49 (0)9122 925-0 Fax: +49 (0)9122 14585 E-mail: sales@memmert.com Internet: www.memmert.com
Customer service: Service hotline: +49 (0)9171 9792 911 Service fax: +49 (0)9171 9792 979 E-mail: service@memmert.com
When calling for service enquiries, please state the appliance number given on the name­plate (see page 15).
Shipping address for repairs: Memmert GmbH + Co. KG Customer service Willi-Memmert-Str. 90-96 DE-91186 Büchenbach Germany
Please contact our customer service department before sending appliances for repair or before returning equipment, or the shipment may be refused.
© 2019 MEMMERT GmbH + Co. KG D39374 | Date 12/2019 Subject to change without notice

About this manual

About this manual
Purpose and target audience
This manual describes the assembly, function, transport, putting into operation, opera­tion, troubleshooting, maintenance and decommissioning/disposal of the vacuum oven VO. It is intended for use by trained personnel of the owner, who have the task of oper­ating and/or maintaining the respective appliance.
If you are asked to work on the appliance, read this manual carefully before starting. Fa­miliarise yourself with the safety regulations. Only perform work that is described in this manual. If there is something you do not understand, or certain information is missing, ask your manager or contact the manufacturer. Do not do anything without authorisa­tion.
Versions
The appliances are available in different configurations and sizes. If specific equipment features or functions are available only for certain configurations, this is indicated at the relevant points in this manual.
The functions described in this manual refer to the latest firmware version. Due to individual configurations and sizes, illustrations in this manual may be slightly dif-
ferent to the actual appearance. Function and operation are identical.
Other documents to be observed:
► Observe the relevant manual when operating the appliance with MEMMERT Atmo-
CONTROL computer software. Click on open the AtmoCONTROL software manual.
► Please refer to the separate service manual for service and repair work (see page
63).
“Help” on the AtmoCONTROL menu bar to
Storage and resale
This operating manual belongs with the appliance and should always be stored where persons working on the appliance have access to it. It is the owner's responsibility to ensure that persons who are working on or are going to work on the appliance know where to find the operating manual. We recommend that it is always stored in a protect­ed location close to the appliance. Make sure that the operating manual is not damaged by heat or humidity. If the appliance is resold or transported and then set up again at a different location, the operating manual must remain with it.
For the current version of this operating manual in PDF format, please go to http://www. memmert.com/en/service/downloads/user-manual/ .
D39374 | Date 12/2019 3

Contents

Contents
1. For your safety 6
1.1 Terms and signs used ................................................................................................6
1.2 Product safety and dangers ...................................................................................... 6
1.3 Requirements of the operating personnel ................................................................ 7
1.4 Responsibility of the owner ......................................................................................8
1.5 Changes and alterations ........................................................................................... 8
1.6 Behaviour in case of malfunctions and irregularities ................................................8
1.7 Switching off the appliance in an emergency ........................................................... 8
2. Design and description 9
2.1 Design ...................................................................................................................... 9
2.2 Intended use ..........................................................................................................10
2.3 Function .................................................................................................................10
2.4 Materials used ........................................................................................................12
2.5 Electrical equipment ...............................................................................................12
2.6 Connections and interfaces .................................................................................... 12
2.7 Designation (nameplate) ........................................................................................ 15
2.8 Technical data .........................................................................................................16
2.9 Declaration of conformity.......................................................................................17
2.10 Ambient conditions ................................................................................................ 18
2.11 Scope of delivery ....................................................................................................18
2.12 Optional accessories ............................................................................................... 18
3. Delivery, transport and setting up 19
3.1 Delivery ..................................................................................................................20
3.2 Transport ................................................................................................................20
3.3 Unpacking .............................................................................................................. 20
3.4 Storage after delivery .............................................................................................20
3.5 Setting up ..............................................................................................................21
4. Putting into operation 25
4.1 Connecting the appliance ....................................................................................... 25
4.2 Install suction .........................................................................................................27
4.3 Insert thermoshelves ..............................................................................................28
4.4 Switching on .......................................................................................................... 29
5. Operation and control 30
5.1 Operating personnel ...............................................................................................30
5.2 Opening the door ................................................................................................... 30
5.3 Operating the appliance ......................................................................................... 31
5.4 Temperature monitoring ........................................................................................37
5.5 Pressure monitoring ............................................................................................... 41
5.6 Graph ..................................................................................................................... 42
5.7 Ending operation ....................................................................................................43
6. Malfunctions, warning and error messages 44
6.1 Warning messages of the monitoring function ...................................................... 44
6.2 Malfunctions, operating problems and appliance errors ....................................... 45
6.3 Power failure ..........................................................................................................47
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Contents
7. Menu mode 48
7.1 Overview ................................................................................................................ 48
7.2 Basic operation in menu mode using the example of language selection ...............49
7.3 Setup ......................................................................................................................50
7.4 Date and time ........................................................................................................53
7.5 Calibration .............................................................................................................. 54
7.6 Program ................................................................................................................. 59
7.7 Sounds ................................................................................................................... 60
7.8 Logging .................................................................................................................. 61
7.9 USER ID .................................................................................................................. 62
8. Maintenance and Servicing 63
8.1 Cleaning .................................................................................................................63
8.2 Regular maintenance .............................................................................................. 63
8.3 Repairs and Service ................................................................................................. 63
9. Storage and disposal 64
9.1 Storage ................................................................................................................... 64
9.2 Disposal .................................................................................................................. 64
Index 65
D39374 | Date 12/2019 5
For your safety

1. For your safety

1.1 Terms and signs used
In this manual and on the appliance itself, certain common terms and signs are used to warn you of possible dangers or to give you hints that are important in avoiding injury or damage. Observe and follow these notes and regulations to avoid accidents and dam­age. These terms and signs are explained below.
1.1.1 Terms used
WARNING
CAUTION
NOTICE
Warns of a dangerous situation that might lead to death or serious injuries
Warns of a dangerous situation that might lead to moderate or minor injuries
Warns of material damage
1.1.2 Signs used
Signs used
Danger of elec-
trocution
Gas bottles
Danger of
explosion
Follow the
instructions!
Dangerous
gases/vapours
Wear gloves Observe infor-
Danger of burns Danger of top-
mation in sepa-
rate manual
pling over
Disconnect the
mains plug
1.2 Product safety and dangers
The appliances described in this manual are technically sophisticated, manufactured using high-quality materials and subject to many hours of testing in the factory. They reflect the state of the art and comply with recognised technical safety regulations. How­ever, there are still risks involved, even when the appliances are used as intended. These are described below.
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For your safety
WARNING
After removing covers, live parts may be exposed. Touching these can lead to an electric shock. Disconnect the mains plug before removing any covers. Work on the electrical system must only be performed by qualifi ed electricians.
WARNING
Toxic gases or vapours may be produced in certain applications. These can escape from the vacuum pump into the room. This can injure people nearby. The appliance may only be used for such applications if a suction is attached to the vacuum pump used, which reliably keeps toxic gases or vapours away from people. Observe the respective national regu­lations for occupational safety and environmental protection.
WARNING
Depending on operation, the surfaces in the interior of the appliance and the chamber load may still be very hot after the appliance is switched off. Touching these surfaces can cause burns. Wear heat­resistant protective gloves or wait until the appliance cools down before touching.
WARNING
Gas bottles may burst or explode at high temperatures. Keep the gas bottles away from open fl ames. Store gas bottles below 50 °C and ensure that the location is always well ventilated. Prevent water from penetrating as well as backfl ow into the gas bottles. It is es- sential that you read the safety notes and instructions of the gas supplier.
1.3 Requirements of the operating personnel
The appliance may only be operated and maintained by persons who are of legal age and have been instructed accordingly. Personnel who are to be trained, instructed or who are undergoing general training may only work with the appliance under the continuous supervision of an experienced person.
Repairs may only be performed by qualified electricians. The regulations in the separate service manual must be observed.
D39374 | Date 12/2019 7
For your safety
ONN
1.4 Responsibility of the owner
The owner of the appliance
► is responsible for the flawless condition of the appliance and for it being operated in
accordance with its intended use (see page 8);
► is responsible for ensuring that persons who are to operate or service the appliance
are qualified to do this, have been instructed accordingly and are familiar with the operating instructions at hand;
► must know about the applicable guidelines, requirements and operational safety
regulations, and train staff accordingly;
► is responsible for ensuring that unauthorised persons have no access to the appli-
ance;
► is responsible for attaching a suction to the vacuum pump used if toxic gases or
vapours may arise as a result of the process;
► is responsible for ensuring that the maintenance plan is adhered to and that mainte-
nance work is carried out properly (see page 63);
► has to ensure that the appliance and its surroundings are kept clean and tidy, for
example through corresponding instructions and inspections;
► is responsible for ensuring that personal protective clothing is worn by operating
personnel, e.g. work clothes, safety shoes and protective gloves.
1.5 Changes and alterations
No unauthorised changes or alterations may be made to the appliance. No parts may be added or inserted which have not been approved by the manufacturer.
Unauthorised changes or alterations result in the CE declaration of conformity losing its validity, and the appliance may no longer be operated.
The manufacturer is not liable for any damage, danger or injuries that result from un­authorised changes or alterations, or from non-compliance with the provisions in this manual.
1.6 Behaviour in case of malfunctions and irregularities
The appliance may only be used in a flawless condition. If you as the operator notice ir­regularities, malfunctions or damage, immediately take the appliance out of service and inform your superior.
You can find information on troubleshooting from page 44.
1.7 Switching off the appliance in an emergency
Press the main switch on the ControlCOCKPIT (Fig. 1) and disconnect the power plug. This disconnects the appliance from the power supply at all poles.
Fig. 1 Switch off the appliance by pressing the main switch
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ON

2. Design and description

2.1 Design
Design and description
Fig. 2 Design 1 ControlCOCKPIT with capacitive function keys and LCD displays (see page 32) 2 Vacuum oven VO 3 Thermoshelves 4 Main switch Pump module 5 Pump module
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Design and description
2.2 Intended use
Vacuum ovens VO are used for drying, testing, moisture determination, airtight storage, curing and degassing of substances or materials under vacuum, which are used in the procedures and specifications described in the operating instructions.
The appliance is not explosion-proof. The use of explosive substances or materials is abu­sive and can lead to hazards or damage. The appliance may only be loaded with materi­als and substances which cannot form any explosive vapours at the set temperature and which cannot explode, burst or ignite.
2.3 Function
The devices of the VO series (Fig. 3 ) can generate a vacuum in working chamber in conjunction with Memmert pump module or another suitable vacuum pump. The vacuum inlet on the back of appliance evacuates the working chamber through the pump.
Optionally, the working chamber can be supplied with inert gas through a connection on the rear of the appliance ⑤⑥.
For temperature control thermal plates with electronic contacts are inserted into tube . If the electronic contacts are connected to the connections in rear panel , the ther­moshelves can emit heat by direct contact with the load.
If toxic gases or vapours may be produced in the intended application, these must be safely discharged by the customer via an extraction system and cleaned if necessary .
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1
Design and description
0
3
2
7 8
5
N
2
He Ne
Ar Kr
Xe
4
6
0
9
Fig. 3 Function of vacuum ovens VO in conjunction with a pump module 1 VO 2 Vacuum pump 3 VO working chamber 4 Hose connection between VO and vacuum pump 5 Gas cylinder (inert gas, optional) 6 Inert gas supply 7 Thermoshelves 8 Contacting the Thermoshelves in the appliance 9 Suction (required if toxic gases or vapours may be produced as a result of the process) 10 Wall mounting (tilt protection, see page 23)
D39374 | Date 12/2019 11
Design and description
2.4 Materials used
Component Materials
Housing Stainless steel (W.St.Nr. 1.4016)
Piping Stainless steel (W.St.Nr. 1.4571)
Interior Stainless steel (W.St.Nr. 1.4404), which stands out
Thermoshelves Aluminium. The vulcanised heating mat covered with
Plug connection of thermoshelf and rear flange socket
Seals in solenoid valves and flange sockets
Door seal Silicone
A resistance table for all these materials can be requested from the company MEMMERT.
through its high stability, optimal hygienic proper­ties and corrosion-resistance towards many (but not all!) chemical compounds (caution for example with chlorine compounds).
stainless steel on the underside of the thermoshelf is made of silicone.
Ryton R4 (GF-PPS plastic) or Peek 450GL30
Fluorocarbon FKM / FPM (Viton)
2.5 Electrical equipment
Operating voltage and current consumption: See nameplateProtection class I, i.e. operating insulation with PE conductor in accordance with EN
61010
Protection class IP 20 acc. to EN 60529Interference suppression acc. to EN 55011 class BAppliance fuse: Safety fuse 250 V/15 A, quick-blowThe temperature sensor is equipped with a 125 mA miniature fuse.
2.6 Connections and interfaces
2.6.1 Electrical connection
This appliance is intended for operation on an electrical power system with a system impedance Z operator must ensure that the appliance is operated only on an electrical power system that meets these requirements. If necessary, you can ask your local energy supply com­pany what the system impedance is.
Observe the country-specific regulations when making connections (e.g. in Germany DIN VDE 0100 with earth leakage circuit breaker).
12 D39374 | Date 12/2019
of a maximum of 0.292 ohm at the point of transfer (service line). The
max
Design and description
2.6.2 Fresh air, inert gas and vacuum connection
At the left rear post are the connections for the inlet of fresh air or inert gas (optional) and the connection for the vacuum pump (DN 16 KF, Fig. 4 and Fig.
5).
Fresh air
The fresh air connection has two functions. On the one hand, the device is ventilated via the connection and thus the nega­tive pressure is adapted to the atmospheric pressure. On the other hand, the connection is opened by the appliance con­troller for a very short time in order to fine-tune the negative pressure.
Fig. 4 Connections on the back of VO 49 Premium and VO 101 Premium appliances 1 Fresh air supply 2 Inert gas connection 3 Vacuum pump con-
nection
1
2
3
Fig. 5 Connections on the back of VO 29 Premium units and all standard appliances 1 without function
(blanking plug) 2 Fresh air supply 3 Vacuum pump con-
nection
1
2
3
Inert gas (optional)
By applying inert gas to the working chamber, a protective atmosphere can be created which protects the load from contact with ambient air.
Vacuum
The vacuum connection is designed as an ISO-KF connection of size DN 16. Either the supplied pump module or another suitable external vacuum pump are connected to it.
When using an external vacuum pump, make sure that the pump is suitable for the ma­terial being fed and the desired process.
Required parameters of a suitable pump:
► Pumping speed > 30 Nl/min ► Final vacuum 3 mbar ► chemical-resistant version ► temperature resistant (exhaust gas temperature like working temperature)
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Design and description
2.6.3 Communication interfaces
The communication interfaces are intended for appliances which meet the requirements of IEC 60950-1.
USB interface
The appliance is fitted by default with a USB port in accordance with the USB speci­fication. This way, you can
transfer software stored on a USB stor-
age medium to the appliance (see page
59).
export protocol logs from the appliance
to a USB storage medium (see page
61).
Fig. 6 USB interface
transfer user ID data stored on a USB storage medium to the appliance (see page
62).
The USB port is located on the right of the ControlCOCKPIT (Fig. 6).
Ethernet interface
The appliance can be connected to a network via the Ethernet interface, so that you can transfer programmes created with the AtmoCONTROL software to the appliance and read out protocols. The Ethernet interface is located on the rear of the appliance (Fig. 7).
For identification purposes, each appliance con­nected must have its own unique IP address. Configuration of the IP address is described on page 50.
You will find a description of how to transfer programs via Ethernet in the enclosed AtmoCONTROL manual.
Fig. 7 Ethernet interface
The appliance can be directly connected to a computer / laptop using an optional USB to Ethernet converter (see Scope of delivery on page 18).
2.6.4 Switching output for external vacuum pump purge valve and pump control
The 8-pin switching output on the rear right post (Fig. 8) is used to control the vacuum pump of the optional pump module (PM) through the vacuum oven (VO). The switching output is backwards-compatible with the 3-pole contact of older pump modules. For this purpose, plug the 3-pole cable into the 8-pole contact.
Fig. 8 Switching output
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Design and description
Vacuum pump rinsing valve
When drying feed materials with a high moisture content, the pump capacity may de­crease during prolonged operation due to condensation in the pump heads. The dia­phragms are blown free by briefly flushing the pump heads with fresh air.
This improves the efficiency of the drying process. In combination with the optionally available pump modules PM29, PM49 and PM101, this cyclical flushing takes place auto­matically when the pump output decreases. The drying process is thus faster and more energy-saving and the pump is protected.
Speed control and switch-off of the vacuum pump
After completing a drying program or after a long period of operation without a vacuum request from the controller, the vacuum pump installed in the pump module (PM) is switched off via the control line. The demand-controlled pump speed control saves energy, is low-noise and increases the service life of the vacuum pump by protecting the pump diaphragms.
Note: A control signal switches off the pump module (PM) installed in the optional vacuum pump. The operating light in the main switch of the pump module also lights up if the vacuum pump has been switched off via the control line.
2.7 Designation ( nameplate)
The nameplate (Fig. 9) provides information about the appliance model, manufacturer and technical data. It is attached to the front of the appliance, on the right behind the door.
1
2
3
4
5
6
Fig. 9 Nameplate (example) 1 Type designation
2 Operating voltage 3 Applicable standard 4 Protection type 5 CE conformity
D39374 | Date 12/2019 15
Typ: VO49 230 V~ 50/60 Hz DIN12880-2007-Kl.: 1
Schutzart DIN EN 60529 - IP 20
GmbH+Co.KG D-91126 Schwabach FRG

Äußere
Rittersbacher Str. 38 Made in Germany
F-Nr.: S318.3008
8,8 A 202 W
Nenntemp.: 20-200°C
6 Address of manufacturer 7 Disposal note 8 Temperature range 9 Connection / power ratings 10 Appliance number
10
9
8
7
Design and description
p
2.8 Technical data
Appliance size 29 49 101
Appliance width D1 [mm] 550 550 710 Appliance height E1 [mm] 600 680 760 Appliance depth F1 [mm] 400 480 550
th of door lock [mm] 38
De Chamber width A Chamber height B
Chamber depth C
Base
Chamber volume [litres] 29 49 101 Weight [kg] 62 74 100 Power [W] 820 2020 2420 Current consumption [A] 230 V, 50/60 Hz 3.6 8.8 10.5
max. number of ther­moshelves
max. load per Thermoshelf [kg] 20 max. load per appliance [kg] 60 80 150
Temperature
Pressure
1
See Fig. 10
2
The minimum temperature depends on the outdoor temperature (see ambiant conditions on page
18).
1
[mm] 385 385 545
1
[mm] 305 385 465
1
[mm] 250 330 400
Width G [mm] 529 529 689 Height H [mm] 450 290 130 Depth I [mm] 383 463 533
Standard 1 2 2 Premium 2 4 4
Adjustment range 20 °C to 200 °C Adjustment precision 0.1 K Operating temperature range 5°C above room temperature up to 200°C Adjustment range 5 mbar - 1100 mbar Adjustment precision 1 mbar
-2
Leak rate 0.5 x 10
mbar 1/sec
16 D39374 | Date 12/2019
Design and description
80 80
D
A
12
12
F
C
200
80
200
E E
38
200
B
80
40
G
H
40
I
Fig. 10 Dimensions
2.9 Applied directives and standards
Based on the standards and guidelines listed in the following, the products described in this manual have received a CE label from the company Memmert:
► Directive 2014/30/EC amended (Directive of the European Parliament and of the
Council on the approximation of the laws of the Member States relating to electro­magnetic compatibility). Standards complied with: DIN EN 61326:2004-05, EN 61326:1997, EN 61326/A1:1998, EN 61326/A2:2001 EN 61326/A2:2003
D39374 | Date 12/2019 17
Design and description
Directive 2014/35/EC amended (Directive of the European Parliament and of the
Council on the harmonisation of the laws of Member States relating to electrical equipment designed for use within certain voltage limits). Standards complied with: DIN EN 61 010-1 (VDE 0411 part 1) DIN EN 61 010-2-010 (VDE 0411 part 2-010) EN 61 010-1:2001, EN 61 010-2-010
2.10 Declaration of conformity
You can download the EC declaration of conformity of the appliance online: English: http://www.memmert.com/en/service/downloads/ce-statement/ German: http://www.memmert.com/de/service/downloads/eg-konformitaetserklaerung/
2.11 Ambient conditions
The appliance may only be used in enclosed areas and under the following ambient
conditions:
Ambient temperature
Humidity rh max. 80 % non-condensing
Overvoltage category II
Pollution degree 2
Altitude of installation max. 2,000 m above sea level
+5 ºC to +40 ºC
The appliance may not be used in areas where there is a risk of explosion. The ambi-
ent air must not contain any explosive dusts, gases, vapours or gas-air mixtures. The appliance is not explosion-proof.
Heavy dust production or aggressive vapours in the vicinity of the appliance could
lead to sedimentation in the interior and, as a consequence, could result in short circuits or damage to electrical parts. For this reason, sufficient measures to prevent large clouds of dust or aggressive vapours from developing should be taken.
2.12 Scope of delivery
Power cableTilt protectionThermoshelves (Standard and Premium VO 29 1 shelf; Premium VO 49 and VO 101 2
shelves)
USB storage medium with software and AtmoCONTROL manualthe operating instructions at handCalibration certificate
2.13 Optional accessories
With an Ethernet-USB converter (Fig. 11) it is possible to connect the Ethernet port of the appliance (see page 14) to the USB port of a PC/laptop.
Fig. 11 USB to Ethernet converter
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Delivery, transport and setting up

3. Delivery, transport and setting up

WARNING
The appliance may only be lifted and placed with a special lifting de­vice. This lifting device must be used for lifting and carrying. Without a lifting device there is a great risk of injury!
The lifting device can be purchased from the dealer under the order number B04456 (VO29/49) or B04457 (VO101). Either the dealer sends the device to the customer or the dealer assembles the appliances himself with the device.
To set up appliances of the sizes 29 and 49, at least two persons, for appliances of size 101, four persons are needed.
To lift the appliance, guide the lifting device under the appliance from both sides (Fig. 12) and lift the appliance.
29 49 101
Fig. 12 Lifting equipment
WARNING
There is a risk of tipping when stacking on a pump module. Do not move stacked device combinations.
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Delivery, transport and setting up
3.1 Delivery
The appliance is packed in cardboard and is delivered on a wooden palette.
3.2 Transport
The appliance can be transported in three ways:
► With a forklift truck; move the forks of the truck entirely under the pallet. ► On a manual pallet jack ► (only with the lifting device)
3.3 Unpacking
To avoid damage, do not unpack the appliance until you reach the installation site.
Remove the cardboard packaging by pulling it upwards or carefully cutting along an edge.
3.3.1 Checking for completeness and transport damage
► Check the delivery note to ensure that the scope of delivery is complete. ► Check the appliance for damage.
If you notice deviations from the delivery note, damage or irregularities, do not put the appliance into operation but inform the haulage company and the manufacturer.
3.3.2 Remove the transportation lock
Remove the transportation lock. It is located between the door hinge, door and frame and has to be removed after opening the door.
3.3.3 Disposing of packaging material
Dispose of the packaging material (cardboard, wood, foil) in accordance with the appli­cable disposal regulations for the respective material in your country.
3.4 Storage after delivery
If the appliance is first to be stored after delivery: Read the storage conditions from page
64.
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Delivery, transport and setting up
3.5 Setting up
CAUTION
Stacked combinations of appliances can tip over due to their centre of gravity and injure you or someone else. Always attach the appli­ance to a wall with the tilt protection (see page 23). In case there is not enough space, do not put the appliance into operation and do not open the door. Contact the Memmert service (see page 2).
3.5.1 Preconditions
The installation site must be flat and horizontal and must be able to reliably bear the weight of the appliance (see "Technical data" on page 16). Do not place the appliance on a flammable surface.
A 230 V power connection must be available at the installation site. The maximum mains voltage fluctuation is +/- 10%.
The distance between the wall and the rear of the appliance must be at least 15 cm. The clearance from the ceiling must not be less than 20 cm and the side clearance from walls or nearby appliances must not be less than 5 cm (Fig. 13). Sufficient air circulation in the vicinity of the appliance must be guaranteed at all times.
FP
FP FP FP
Fig. 13 Minimum clearance from walls and ceiling
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