CentriVap micro IR Vacuum
Centrifugal Concentrators
Models
77010 Series
Copyright © 2017 Labconco Corporation. The information contained in this manual and the accompanying
Warranty
Labconco Corporation provides a warranty to the original buyer for the repair or replacement of parts and
reasonable labor as a result of normal and proper use of the equipment with compatible chemicals. Broken
glassware and maintenance items, such as filters, gaskets, light bulbs, finishes and lubrication are not
warranted. Excluded from warranty are products with improper installation, erratic electrical or utility supply,
unauthorized repair and products used with incompatible chemicals.
The warranty for CentriVap® micro IR Vacuum Centrifugal Concentrators will expire one year from date of
installation or two years from date of shipment from Labconco, whichever is sooner. Warranty is nontransferable and only applies to the owner (organization) of record.
Buyer is exclusively responsible for the set-up, installation, verification, decontamination or calibration of
equipment. This limited warranty covers parts and labor, but not transportation and insurance charges. If the
failure is determined to be covered under this warranty, the dealer or Labconco Corporation will authorize
repair or replacement of all defective parts to restore the unit to operation. Repairs may be completed by 3rd
party service agents approved by Labconco Corporation. Labconco Corporation reserves the rights to limit this
warranty based on a service agent’s travel, working hours, the site’s entry restrictions and unobstructed access
to serviceable components of the product.
Under no circumstances shall Labconco Corporation be liable for indirect, consequential, or special damages
of any kind. This warranty is exclusive and in lieu of all other warranties whether oral, or implied.
products are copyrighted and all rights reserved by Labconco Corporation. Labconco Corporation reserves
the right to make periodic design changes without obligation to notify any person or entity of such change.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be
accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier.
Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery
carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by
various federal, state, or local regulations. All users of this equipment are required to become familiar with
any regulations that apply in the user’s area concerning the dumping of waste materials in or upon water,
land, or air and to comply with such regulations. Labconco Corporation is held harmless with respect to
user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact
Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821-5525
or 1-816-333-8811, between the hours of 7:30 a.m. and 5:30 p.m., Central Standard Time.
Part #7539801, Rev. A
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CHAPTER 1: INTRODUCTION 1
Safety Symbols 2
CHAPTER 2: PREREQUISITES 5
Electrical Requirements 5
Location and Exhaust Requirements 6
Space Requirements 6
CHAPTER 3: GETTING STARTED 7
Unpacking Your CentriVap micro IR 7
CentriVap micro IR Components 8
Setting Up Your CentriVap micro IR 8
Emergency Access Into the Chamber 8
Electrical Connection 9
Rotor Installation 9
Installing a CentriZap IR Strobe Light 9
Chemical Resistance of CentriVap micro IR Components 10
Solvent Safety Precautions 11
CHAPTER 4: USING YOUR CENTRIVAP MICRO IR 12
Planning 12
Sample Vial Selection 12
Loading Glassware Into the CentriVap micro IR 12
Temperature Setting Guidelines 13
Time Setting Guidelines 13
CentriVap micro IR Controls 13
Operating the CentriVap micro IR Controls 14
Operating the CentriVap micro IR 15
Operational Notes 16
Interrupting a Cycle After it Has Begun 16
Safety Precautions 16
CHAPTER 5: MAINTAINING YOUR CENTRIVAP MICRO IR 17
CHAPTER 6: ACCESSORIES FOR YOUR CENTRIVAP
MICRO IR 19
CHAPTER 7: TROUBLESHOOTING 20
APPENDIX A: CENTRIVAP MICRO IR COMPONENTS 22
APPENDIX B: CENTRIVAP MICRO IR DIMENSIONS 23
APPENDIX C: CENTRIVAP MICRO IR SPECIFICATIONS 24
Electrical Specifications 24
Environmental Conditions 24
Evaporation Rates 25
1
CChhaapptteerr 11::
IInnttrroodduuccttiioonn
Congratulations on your purchase of a Labconco CentriVap® micro IR Vacuum
Concentrator.
The CentriVap micro IR Concentrator uses centrifugal force with heat and
vacuum to rapidly evaporate and condense solvents from biological and analytical
samples. Centrifugation eliminates bumping and foaming as vacuum is applied
and also concentrates the solute in the bottom of the vial. This allows recovery of
solutes from sample volumes as small as a few microliters. The concentrator is
equipped with two separate heaters to speed evaporation by warming the chamber
during processing. The clear lid heater uses radiant heat to efficiently heat
samples under vacuum conditions. An additional heater is provided for
applications were samples maybe sensitive to radiant heat. A PTFE coated
diaphragm vacuum pump is included which requires no maintenance. The
vacuum pump pulls vapor out through the center of the chamber to minimize
cross contamination. A glass trap is also provided to condense and collect solvent
exiting the chamber. The CentriVap micro IR Concentrator has a standby
function to preheat or maintain the chamber temperature. A safety switch
prevents the concentrator from starting when the lid is in the open position and a
latch prevents the lid from being opened while the rotor is turning. The compact,
low profile design allows the concentrator to be placed on a bench top or other
laboratory work surface. The CentriVap micro IR Concentrator also comes
standard with a CentriZap IR LED strobe light for viewing the samples during the
run.
The microprocessor controls the operation of the heaters from 35°C to 65°C. The
rotor speed of 1700 RPM and vacuum down to 120 mbar provides excellent
regulation and reproducibility of protocols.
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Chapter 1: Introduction
2
Safety Symbols
Your CentriVap micro IR Concentrator was designed with safety in mind,
however conditions may exist that could be hazardous.
Throughout this manual potentially hazardous conditions are identified using the
following words and symbols.
It is important that you understand the warnings listed throughout this manual
before you operate the CentriVap micro IR Concentrator.
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Chapter 1: Introduction
3
Warning: Precautions for installation
Connect to proper supply voltage.
Verify that the supply voltage matches the voltage and hertz written on serial tag.
Failure to do so could damage the unit or affect performance.
Do not operate in environment with relative humidity exceeding 80% for
temperatures up to 88°F (31°C), decreasing linearly to 50% relative humidity at
104°F (40°C). Doing so could cause electric leakage or corrosion.
Do not expose unit to direct sun light or high temperatures.
The recommended indoor operating temperature is 20°C - 30°C.
Do not use flammable substances near the product. Doing so could create a fire
hazard.
Provide a minimum space of 7.8 inches (20cm) behind the unit for clearance of
the power cord.
Install unit on solid level surface. Failure to do so can result in excessive
vibration.
Do not lay the unit down on its sides or top. Doing so can result in damage to the
unit.
Secure lid and any other moveable parts when moving the unit. Failure to do so
can result in injury or damage to the unit.
When moving the unit always lift, do not slide. Failure to do so may result in
damage to the unit.
Warning: Precautions for use.
3. Precaution for use
Do not disassemble, or attempt to repair the unit without proper training, or
personal injury or damage to the unit could occur.
Do not use the product for anything other than what it was intended for, or
personal injury or damage to the unit could occur.
Product Service 1-800-522-7658
Chapter 1: Introduction
4
Do not use flammable sprays near the product. Doing so could cause fire.
Protect the control panel from spills by wiping off any water or solvent with a
clean dry cloth. Failure to do so could cause an unsafe condition or create a fire
hazard.
Do not clean the product with excessive quantities of water, thinner,
benzene or petroleum-based products. Failure to do so could cause an unsafe
condition or create a fire hazard.
Product Service 1-800-522-7658
5
CChhaapptteerr 22::
PPrreerreeqquuiissiitteess
Before you install your CentriVap micro IR, you need to prepare your site for
installation. Carefully examine the location where you intend to install your
CentriVap. You must be certain that the area is level and of solid construction. In
addition, an exhaust means must be provided. An electrical source must also be
located near the installation site.
Carefully read this chapter to learn:
The electrical supply requirements.
The exhaust requirements.
Space requirements.
Refer to Appendix C: CentriVap micro IR Specifications for complete CentriVap
electrical and environmental conditions, specifications and requirements.
Electrical Requirements
The CentriVap micro IR Concentrator requires a grounded electrical outlet. This
outlet requires a 15 Amp circuit breaker or fuse for models rated at 115V (60 Hz).
An 8 Amp circuit breaker or fuse is required for models rated at 230V (50/60 Hz).
Various models are available for use in different locations throughout the world.
Each has a unique plug suitable for the specific location. See CentriVap
Components in Chapter 3 for detail plug specifications. If the plug supplied with
the CentriVap Does not match the available receptacle, remove this plug and
replace it with an approved plug of the suitable style.
It is recommended that an emergency switch for disconnecting the power in the
case of a malfunction be located remote from the CentriVap micro IR, preferably
outside the room in which the unit is housed, or adjacent to the exit from that
room.
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Chapter 2: Prerequisites
6
Location and Exhaust Requirements
The CentriVap micro IR Concentrator should be located on a surface that is
stable, flat and level.
WARNING: The CentriVap Concentrator should be located within a fume
hood if hazardous or flammable solvents are used. Heating of materials
could lead to the liberation of hazardous gases. In all cases, regardless of the
solvent used, it is strongly recommended that the vacuum pump is vented in
a fume hood. A glass trap is included with the unit to minimize the
exhausting of solvents into the atmosphere but if flammable solvent are used
a secondary trap is recommended. See Chapter 6 for available accessories.
The use of the glass traps does not negate the need to exhaust the vacuum
pump into a fume hood. Failure to properly vent the CentriVap will expose
personnel to potentially harmful chemicals.
The CentriVap has not been evaluated by an approval agency for the use of
biological, radio toxins or flammable liquids or materials.
Space Requirements
Refer to Appendix C: CentriVap micro IR Specifications for dimensional
drawings of the CentriVap micro IR.
No person or any hazardous material should be within 12 inches of the CentriVap
Concentrator while it is operating.
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7
CChhaapptteerr 33::
GGeettttiinngg SSttaarrtteedd
Now that the site for your CentriVap micro IR is properly prepared, you are ready
to unpack, inspect, install, and test the unit. Read this chapter to learn how to:
Unpack and move your CentriVap micro IR.
Set up your CentriVap micro IR.
Connect the electrical supply source to your CentriVap micro IR.
Properly exhaust your CentriVap micro IR.
Safely use solvents with your CentriVap micro IR.
Unpacking Your CentriVap micro IR
Carefully unpack your CentriVap micro IR and inspect it for damage that may
have occurred in transit. If your CentriVap is damaged, notify the delivery carrier
immediately and retain the entire shipment intact for inspection by the carrier.
The United States Interstate Commerce Commission rules require that claims be
filed with the delivery carrier within fifteen (15) days of delivery.
NOTE: Do not return goods without the prior authorization of Labconco.
Unauthorized returns will not be accepted. If your CentriVap micro IR was
damaged in transit, you must file a claim directly with the freight carrier.
Labconco Corporation and its dealers are not responsible for shipping
damage.
Do not discard the carton or packing material for your CentriVap micro IR until
you have checked all of the components and installed and tested the unit.
Product Service 1-800-522-7658
Chapter 3: Getting Started
8
Catalog #
Product Description
7701020
CentriVap micro IR Concentrator – 115V – USA
1334500
Power Cord with NEMA 5-15P Plug
7548500
Rotor 1.5ml x 24
7539801
User’s Manual
7548900
Wrench, Rotor
7549000
CentriZap micro IR LED Strobe Light
7701030
CentriVap micro IR Concentrator – 230V – EU
1336100
Power Cord with CEE 7/7 Plug
7548500
Rotor 1.5ml x 24
7539801
User’s Manual
7548900
Wrench, Rotor
7549000
CentriZap micro IR LED Strobe Light
7701035
CentriVap micro IR Concentrator – 230V – UK
1332600
Power Cord with BS 1363 Plug
7548500
Rotor 1.5ml x 24
7539801
User’s Manual
7548900
Wrench, Rotor
7549000
CentriZap micro IR LED Strobe Light
7701037
CentriVap micro IR Concentrator – 230V – CHINA
1332700
Power Cord with CHI-10P Plug
7548500
Rotor 1.5ml x 24
7539801
User’s Manual
7548900
Wrench, Rotor
7549000
CentriZap micro IR LED Strobe Light
CentriVap micro IR Components
As previously mentioned, the CentriVap micro IR System is available in 115V or
230V. Locate the model of CentriVap you received in the following table. Verify
that the components listed are present and undamaged.
If you do not receive one or more of the components listed for your CentriVap
micro IR, or if any of the components are damaged, contact Labconco
Corporation immediately for further instructions.
Setting Up Your CentriVap micro IR
After you verify receipt of the proper components, move your CentriVap micro
IR to the level and sturdy location where you want to install it. There is no need
to secure the CentriVap micro IR Concentrator to the work surface. Then, follow
the steps listed below.
Emergency Access Into the Chamber
The CentriVap micro IR is designed to prevent access to the chamber in the event of a
power disruption. If it is necessary to open the lid when there is no electrical power
connected to the unit, you can unlock the latch by pulling on cable release located in the
top left-hand rear corner of the back panel. Pulling the cable out will unlock the lid
latch mechanism. While holding the latch open, raise the lid with the other hand.
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Chapter 3: Getting Started
9
CAUTION: Never attempt to defeat the latch or open the lid while the
CentriVap micro IR is running. Personal injury can result from moving
parts and chemicals.
Electrical Connection
Plug the power cord into the receptacle on the back of the CentriVap micro IR
Concentrator and plug the other end into a suitable power receptacle.
Rotor Installation
The CentriVap micro IR Concentrator comes with a 1.5ml rotor installed. If a
different rotor is required you may remove the standard rotor and replace it with
one of the other available rotors. To remove the rotor, loosen the left handed
19mm hex nut using the rotor wrench. The rotor nut is left handed so turn the nut
clockwise to remove. Once the nut is removed the rotor can be lifted off of the
drive hub. Place the alternate rotor on the drive hub making sure the drive pins are
properly engaged with the drive holes in the rotor. Replace the 19mm hex nut by
turning counter-clockwise; secure the nut using the rotor wrench. Do not over
tighten the hex nut.
IMPORTANT: Do not leave the rotor wrench in the chamber. Do not use a
rotor if it shows any signs of damage.
Installing a CentriZap™ micro IR Strobe
Light
An LED strobe light comes standard with each CentriVap micro IR Concentrator.
This light will enable you to see the samples as they are rotating in the chamber.
Attach the connector on the strobe light harness into the receptacle on the back of
the CentriVap micro IR marked “STROBE.”
To use the strobe light while the unit is operating, press the pushbutton on the
light and shine the light on the samples in the rotor.
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Chapter 3: Getting Started
10
COMPONENT
MATERIAL
Acetic Acid 20% Boric Acid Formic Acid Hydrobromic Acid 20% Hydrochloric Acid 20% Nitric Acid 20% Sulfuric Acid 10%
Ammonium Hydroxide
Acetone Acetonitrile Chloroform Dimethyl Formamide Dimethyl Sulfoxide (DMSO) Ethanol Ethyl Acetate Hexanes Isoproponal Methanol Methylene Chloride
Toluene Water
Chamber
Hub/nut
NI-Chrome plate
D D D D D A D A A A A A
A
Chamber
PTFE coated
Aluminum
A A A A A A A A A A A A A A A A A A
A
Rotor
PTFE coated
Aluminum
A A A A A A A A A A A A A A A A A A
A
Lid Gasket
Silicone
C A C D D D A D D D A C C C A A D
A
Tubing
Silicone
C A C D D D A D D D A C C C A A D
A
Motor shaft
Stainless Steel
C C C D D A A A A A A A A A A A A A A Bearings
Stainless Steel
C C C D D A A A A A A A A A A A A A
A
Vacuum pump
EPDM
FPM
PPS
PTFE
A
C
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
D
A
C
A
A
A
A
D
A
A
D
D
A
A
D
D
A
D
A
A
A
A
A
A
A
A
C
A
A
A
A
A
A
C
A
A
A
C
A
A
A
D
C
A
A
D
A
A
A
A
A
A
A
Chemical Resistance of CentriVap micro
IR Components
Your CentriVap micro IR Vacuum Concentrator is designed to be chemical
resistant to compounds that are commonly used in the concentration processes.
However, by necessity, the CentriVap is comprised of a number of different
materials, some of which may be attacked and degraded by certain chemicals. The
degree of degradation is obviously dependent on the concentration and duration of
exposure. Some major components of the CentriVap that are susceptible to
degradation are as follows:
Acids Bases Solvents
A- Acceptable
C-Moderate Degradation-Questionable use
D-Severe Degradation-Infrequent use recommended-immediate thorough
cleaning required.
When using compounds in the CentriVap micro IR that are hostile to the materials
of construction, it is imperative that the equipment is appropriately maintained.
After each run, clean up all residues, spills and materials that might have
splashed in the chamber using agents suitable for the substance involved.
Remove the contents and clean the glass trap after each use.
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Chapter 3: Getting Started
11
Solvent Safety Precautions
CAUTION: The CentriVap micro IR is not classified as “explosion proof.”
It has been designed with safety as a primary consideration and should be
used in a prudent manner using “good laboratory practices.” It has been
designed for use with compounds as described in the United States National
Electrical Code Class I, Group D. The heater may be programmed to run
as hot as 65°C, however, the heater elements may be hotter. An over
temperature protection device limits the heater to a maximum temperature
of 80°C. It is important that the solvents used are compatible with these
temperatures. Do not evaporate solvents that have an autoignition
temperature below 180°C. Do not evaporate solvents that are classified as
Group A, B, or C by the National Electrical Code. Evaporate only nonflammable or Group D solvents with autoignition temperatures 180°C or
above. Use of other compounds could cause an explosion.
CAUTION: Solvents used in the CentriVap micro IR may be flammable or
hazardous. Use extreme caution and keep sources of ignition away from the
solvents. When using flammable or hazardous solvents, the CentriVap micro
IR should be operated inside a fume hood.
If a sample is spilled in the chamber it must immediately be cleaned up.
Hazardous materials such as strong acids or bases, radioactive substances
and volatile organics, must be handled carefully and promptly cleaned up if
spilled.
Do not store flammable or hazardous solvents within 12 inches (300 mm) of
the CentriVap micro IR.
IMPORTANT: The disposal of substances used in connection with this
equipment may be governed by various Federal, State or local regulations.
All users of this equipment are urged to become familiar with any
regulations that apply in the user’s area concerning the dumping of waste
materials in or upon water, land or air and to comply with such regulations.
Product Service 1-800-522-7658
12
CChhaapptteerr 44::
UUssiinngg YYoouurr CCeennttrriiVVaapp m
miiccrroo IIRR
After your CentriVap micro IR has been installed as detailed in Chapter 3:
Getting Started, you are ready to begin using your CentriVap. Read this chapter
to learn how to:
Set operating parameters.
Operate the controls.
Properly select and position glassware inside your CentriVap micro IR.
Understand the display.
Interrupt a cycle after it has begun.
NOTE: Do not store or stack supplies or equipment on top of the CentriVap
micro IR.
Planning
Thoroughly understand procedures and the equipment operation prior to
beginning work. The unique performance of the CentriVap micro IR is dependent
upon the proper balance of heat, vacuum and centrifugal force. If the proper
balance is not established, it is possible to damage or lose a portion of the sample.
Therefore, if you are unfamiliar with the CentriVap micro IR or are attempting a
new protocol, it may be helpful to make a trial run using a representative sample.
Sample Vial Selection
Normally, sample vials should be filled no more than approximately half full.
Select the size of the sample vial so it is compatible with the rotor and the desired
sample size. Vials should not be loose in the rotor. Rotors are available with
holes for various size vials. Refer to Chapter 6: Accessories for your CentriVap
micro IR Concentrator for available rotor sizes.
Loading Glassware into the CentriVap
micro IR
Smooth operation of the CentriVap micro IR is dependent upon proper balance of
the machine. Therefore, if less than a full load of samples is run, it is important to
load samples in a fairly symmetrical manner distributing the weight of the
samples evenly in the rotor.
Product Service 1-800-522-7658
Chapter 4: Using Your CentriVap micro IR
13
Temperature Setting Guidelines
The evaporation rate achieved by the CentriVap micro IR is dependent upon a
variety of factors. These include the nature of the solvent, the temperature set
point, the temperature mode and the pressure in the vacuum system.
The Centrivap micro IR was designed to quickly evaporate small samples at
elevated temperatures. The temperature can be set from 35°C to 65°C. As a
general guideline, to speed the evaporation process, the CentriVap temperature
should be set as high as possible as long as the temperature will not damage the
sample or cause the sample to bump. Typically the fastest evaporation rates will
be obtained using the IR heat mode, IR/Heat second, then Heat. At lower
temperatures, depending on the mode of heat and the type of samples, vapor can
sometimes condense inside the chamber slowing the evaporation process. For
instance, at temperatures below 50°C aqueous samples can begin to condense
inside of the chamber, becoming worse at lower set points. When evaporating at
lower temperatures we recommend running in the IR/Heat mode. This mode
distributes the heat more evenly around the chamber reducing the potential for
condensation. As always when attempting a new protocol, it is recommended that
a trial run be made.
Time Setting Guidelines
The CentriVap micro IR Concentrator has a timer that can be set from 00:00 to 99
hours and 59 minutes. The run time setting is used to turn the concentrator off
after a set period of time. This stops the rotation, turns off the heater, vacuum
pump and bleeds vacuum from the system. The 00:00 setting allows the unit to
run at the set point temperature until manually turned off.
The tables in Appendix C: CentriVap micro IR Specifications indicate
approximate times required to evaporate various common solvents. Actual times
must be determined by the user.
CentriVap micro IR Controls
The control panel for the CentriVap micro IR is shown below with a description
of its functions.
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Chapter 4: Using Your CentriVap micro IR
14
65.0
102 4 1 5 6 7 9 3 8
1. Display – Shows set point parameters and actual measured conditions.
2. Start/Stop Button – Used to start or stop a run and reset the timer.
3. Time Button – Used to display time remaining.
4. Set Button – Use to program temperature and time.
5. Increase Button – Use to increase temperature and time in set up mode.
6. Decrease Button – Use to decrease temperature and time in set up mode.
7. Standby Light – Indicates that the selected heater is on and cycling.
8. Power Light – Indicates the unit is in Standby or Run mode.
9. Heat Mode Selector – Use to select IR, IR/Heat, or Heat only modes.
10. Run Mode Selector – Use to select Off, Standby (Preheat) or Run modes.
Operating the CentriVap micro IR Controls
Change “Temperature” and “Run Time” Set Point:
To change the temperature set point, press the “SET” button. The current temperature
set point will flash on the display. Press the increase or decrease button until the desired
temperature set point is displayed. Press “SET” button and the current hour set point
will flash. Press the increase or decrease button until the desired run hours (00: to 99:)
is displayed. Press “SET” button and the current minutes set point will flash. Press the
increase or decrease button until the desired run minutes (:00 to :59) is displayed. Press
the “SET” button and save will flash on the display. The new program is now entered,
the display will show the current chamber temperature. Setting the run time to 00:00
will turn off the program timer. With the timer off the unit will operate at the set point
temperature until manually turned off.
The temperature set point range is 35°C to 65°C.
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Chapter 4: Using Your CentriVap micro IR
15
The time set point range is 00:00 (on) to 99:59 (99 hrs 59 min.)
Preheat:
To preheat the chamber, program the desired temperature and time. Make sure the
chamber door is closed. Select the desired heat mode. IR/HEAT is recommended
for preheating. Turn the Run Mode Selector to Standby. The heaters will raise the
chamber temperature to the programmed set point. The actual chamber
temperature will be displayed. The chamber will continue to preheat until either
the “START/STOP” button is pressed or the mode selector is turned to the off
position. Opening the lid will also turn the heater off.
Operating the CentriVap micro IR
CAUTION: To avoid personnel injury; Do not operate the CentriVap micro
IR if the lid is scratched or nicked, or shows signs of damage. A damaged lid
could fail under vacuum.
While the CentriVap micro IR Concentrator is operating, do not lean on the lid,
and do not place hazardous materials within 12 inches (305mm).
1. Turn “ON” the CentriVap micro IR power switch located on the right side of
the back panel. Turn the run mode switch to “STANDBY.”
2. Program the desired temperature set point and run time.
3. Preheat the chamber if desired.
4. Place samples in vials. Normally the vials should be no more than half full.
Place vials in the rotor. Use caution as the lid and rotor could be hot.
5. Close the lid.
6. Turn the Run mode selector switch to “RUN.” The rotor and vacuum pump
will start. The display will show the actual chamber temperature.
7. Set point parameters can be altered at any time during a run.
8. If the run time set point is used, at the end of the set time the display will
show “END.”
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Chapter 4: Using Your CentriVap micro IR
16
9. Select “OFF” or “STANDBY” to terminate operation if the CentriVap micro
IR rotor and to release the vacuum. Selecting “OFF” will turn the system off
and reset the timer. Selecting “STANDBY” will turn the vacuum pump and
rotor off and pause the timer.
10. When the evaporation is complete, allow the rotor to stop moving, lift the lid
and remove the samples. Use caution as the lid and rotor could be hot.
Operational Notes
Turn the mode switch to “OFF” before turning the power switch off. When the
CentriVap micro IR power is turned on, the program returns to the same mode
that it was in when the power was turned off. The timer will reset.
Pressing the “START/STOP” during a run will turn the system off and reset the
timer. Pressing it again will restart the program from the beginning.
To display the time remaining press the “TIME” button.
Interrupting a Cycle After it has Begun
To interrupt the cycle during a run, select “STANDBY.” This shuts off the rotor,
vacuum pump, releases vacuum and unlatches the lid. After the rotor stops, the lid
may be opened. If it is necessary to re-start the CentriVap micro IR, close the lid
and select “RUN.” The cycle resumes operation at the same set point parameters
and the timer continues to count down from the time at which the cycle was
stopped.
Safety Precautions
Special precautions must be observed if the materials used in the CentriVap micro
IR Concentrator are known to be hazardous, toxic, radioactive, or contaminated
with pathogenic microorganisms. These actions should include but are not
limited to the following:
Refer to the World Health Organization Laboratory Biosafety Manual,
paying special attention to information about centrifuges and the handling
of hazardous materials.
Operate or vent the CentriVap micro IR Concentrator inside a suitable
fume hood or ventilation device. Load rotors in a ventilation device.
Periodically inspect all parts of the CentriVap micro IR Concentrator
including the lid, gasket, chamber, plumbing components and rotors.
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Under normal operation, the CentriVap micro IR requires little maintenance. The
following maintenance schedule is recommended. Before servicing disconnect
electrical power. Special precautions must be observed if materials used in the
CentriVap micro IR Concentrator are known to be hazardous, toxic, radioactive or
contaminated with pathogenic microorganisms. Before servicing, the CentriVap
micro IR Concentrator must be suitably decontaminated. Wear appropriate
eyewear, gloves and other safety apparel.
As needed:
Before using any cleaning or decontamination method except those recommended
by the manufacturer, users should check with the manufacturer that the proposed
method will not damage equipment.
1. Clean up all spills; remove liquids from the chamber. Clean or decontaminate
all surfaces using agents suitable for the substance spilled.
2. Clean lid and gasket using soft cloth, sponge or chamois and a mild, non-
abrasive soap or detergent.
3. At the end of the run, liquid collected in the glass traps should be removed. To
empty the trap, remove the glass from the mounting bracket, remove the
silicone stopper. Dispose of the liquid in accordance with all codes. Reinstall
the silicone stopper and replace the glass trap to its mounting bracket.
4. To prolong the life of the vacuum pump and to optimize its performance, it is
important to purge all liquid from within it. Once the concentration process is
completed and the glass trap has been emptied, open the CentriVap micro IR
lid and turn the Mode selector switch to “ON.” The pump will operate and
will draw air through the system. The rotor will not turn with the lid open. The
length of the liquid purge time is dependent on the volatility of the solvents
used. Once all of the liquid is purged from the vacuum lines, turn the mode
selector switch to “OFF.”
5. Check rotors for loose or missing parts. Tighten or replace as required. Do
not use defective rotors.
6. Inspect the chamber to insure that there are no cracks or structural damage.
Call Labconco if defects exist.
Product Service 1-800-522-7658
Chapter 5: Maintaining Your CentriVap micro IR
18
7. Check the continuity of the protective earth ground between the ground
terminal on the power inlet and a bare metal housing panel. Contact
Labconco if there is no continuity.
8. Repair any defects to the surface where the unit is installed.
Monthly:
1. The rubber and silicone components on the CentriVap may eventually
deteriorate and require replacement. The effective life of those parts depends
upon both their usage and the surrounding environment. Check all hoses and
gaskets and replace any that show signs of hardening, permanent set or
deterioration.
2. Using a soft cloth, sponge or chamois and a mild, non-abrasive soap or
detergent, clean the glass lid.
3. Using a soft cloth, sponge, or chamois and a mild, non-abrasive soap or
detergent, clean the exterior surfaces of the unit. Liquid spray cleaners and
polishes may be used on the exterior surfaces. Do not use solvents to remove
stains from the exterior surfaces as they may damage the finish.
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PART #
DESCRIPTION
7548400
Rotor, .5 ml x 24
Holds (24) 0.5 ml microcentrifuge tubes
7548500
Rotor, 1.5 ml x 24
Holds (24) 1.5 ml microcentrifuge tubes
7548600
Rotor, 10 ml x 16
Holds (16) 10ml 18mm x 65mm vials
7548700
Rotor 15 ml x 12
Holds (12) 15ml 20mm x 70mm vials
7548800
Rotor 30 ml x 8
Holds (8) 30ml 30mm x 73vials
7548300
Secondary Glass Trap Assembly
The following accessories are available for the CentriVap micro IR Concentrator.
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PROBLEM
CAUSE
CORRECTIVE ACTION
Unit will not operate
Unit not connected to
electrical power
Connect unit to proper electrical receptacle.
Circuit breaker blown
Correct electrical problem and reset circuit
breaker.
Lid open
Close lid.
Excessive vibration
Sample vials not located
symmetrically in rotor
Reposition sample vials.
Sample odor in lab
Vent hose exhausting into
lab area
Redirect hose to fume hood.
Evaporation rate is
reduced
Heater inoperable
Contact Labconco.
Vacuum pump failure
Check pump.
Liquid in vacuum line
Clear vacuum line
Refer to the following if your CentriVap micro IR fails to operate properly. If the
suggested corrective actions do not solve your problem, contact Labconco for
additional assistance.
CAUTION: Disconnect power before corrective action is taken.
Product Service 1-800-522-7658
Chapter 7: Troubleshooting
21
PROBLEM
CAUSE
CORRECTIVE ACTION
Evaporation rate is
reduced (continued)
Obstruction in hose
Remove obstruction or replace hose.
Lack of adequate vacuum
See below.
Temp set point too low
Increase temperature set point.
No vacuum/poor vacuum
Liquid in glass trap
Empty trap.
Leaks in lines or
connectors or gasket
Locate and repair.
Foreign material on lid
gasket
Clean gasket and lid.
Product Service 1-800-522-7658
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Quantity
Part No.
Description
1
7549000
CentriVap micro IR Strobe Light
1
7549100
Drive Motor
1
7549200
Control Board IR Pus
1
7549300
SS Relay Set micro IR
1
7549400
Display board micro IR
1
7549500
Vacuum Pump micro IR
1
7549600
Transformer, 100VA
1
7549700
Transformer, 50VA
1
7549800
Fan Motor micro IR
1
7549900
Selector Switch
1"
1624100
Silicone Tubing
1
7548200
Lid Gasket
The following pages list components that are available for your CentriVap micro
IR. The parts shown are the most common replacement parts. If other parts are
required, contact Product Service.
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This Appendix contains technical information about the CentriVap including
specifications, environmental operating conditions, wiring diagrams and
evaporation rates.
Electrical Specifications
Nominal amperage for 115V CentriVap (model 7701020) (including
vacuum pump): 5A
Nominal amperage for 230V CentriVap (models 7701030,-35,-37)
(including vacuum pump): 3A
Frequency (all models): 50/60 Hz.
Phase: Single
Heater power: 300 watts
Rotor Speed: Up to 1,700 RPM
The vacuum pump is capable of achieving an ultimate vacuum pressure of
160 MBAR
Environmental Conditions
Indoor use only.
Maximum altitude: 6562 feet (2000 meters).
Ambient temperature range: 41° to 104°F (5° to 40°C).
Maximum relative humidity: 80% for temperatures up to 88°F (31°C),
decreasing linearly to 50% relative humidity at 104°F (40°C).
Main supply voltage fluctuations not to exceed ±10% of the nominal
voltage.
Transient overvoltages according to Installation Categories II
(Overvoltage Categories per IEC 1010). Temporary voltage spikes on the
AC input line that may be as high as 1500V for 115V models and 2500V
for 230V models are allowed.
Used in an environment of Pollution degrees 2 (i.e., where normally only
non-conductive atmospheres are present). Occasionally, however, a
temporary conductivity caused by condensation must be expected, in
accordance with IEC 664.
Product Service 1-800-522-7658
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Solvent
Tube Size
(ml)
Number of
Samples
Sample
Size (ml)
Temp
(C)
Time to
Dry (min.)
Heat
Mode
Methanol
1.5
24 1 35
104
IR 1.5
24 1 35
110
IR/Heat
1.5
24 1 50
59
Heat
1.5
24 1 65
36
Heat
1.5
24 1 65
32
IR 1.5
24 1 65
33
IR/Heat
Water
1.5
24 1 50
240
IR 1.5
24 1 50
330
IR/Heat
1.5
24 1 60
225
Heat
1.5
24 1 60
145
IR
1.5
24 1 60
180
IR/Heat
1.5
24 1 65
129
IR
Isopropanol
1.5
24 1 40 IR 1.5
24 1 50
49
IR/Heat
1.5
24 1 60
34
IR/Heat
1.5
24 1 60
30
IR 1.5
24 1 65
31
IR/Heat
Ethanol
1.5
24 1 40
270
IR/Heat
1.5
24 1 50
60
IR/Heat
1.5
24 1 60
39
IR/Heat
1.5
24 1 65
32
IR/Heat
Evaporation Rates
Appendix C: Specifications
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