2-1.1-ME Gas sampling and gas conditioning technology 3
j
Dear customer,
we have made up this operating manual in such a way that all necessary information about the product can be found and understood quickly and easily.
Should you still have any question, please do not hesitate to contact M&C directly or go through your
appointed dealer. Respective contact addresses are to be found in the annexe to this operating manual.
Please also contact our homepage www.mc-techgroup.com for further information about our prod-
ucts. There, you can read or download the data sheets and operating manuals of all M&C products as
well as further information in German, English and French.
This Operating Manual does not claim completeness and may be sub-
The product described in this operating manual has been examined before delivery and left our works
in perfect condition related to safety regulations. In order to keep this condition and to guarantee a
safe operation, it is important to heed the notes and prescriptions made in this operating manual. Furthermore, attention must be paid to appropriate transportation, correct storage, as well as professional
installation and maintenance work.
All necessary information a skilled staff will need for appropriate use of this product are given in this
operating manual.
2 DECLARATION OF CONFORMITY
CE - Certification
The product described in this operating manual complies with the following EC directives:
EMV-Instruction
The requirements of the EC directive 2004/108/EC “Electromagnetic compatibility“ are met.
Low Voltage Directive
The requirement of the EC directive 2006/95/EC “Low Voltage Directive“ are met.
The compliance with this EC directive has been examined according to DIN EN 61010.
Declaration of conformity
The EU Declaration of conformity can be downloaded from the M&C homepage or directly requested
from M&C.
2-1.1-ME Gas sampling and gas conditioning technology 5
3 SAFETY INSTRUCTIONS
Please take care of the following basic safety procedures when mounting, starting up or operating this equipment:
Read this operating manual before starting up and use of the equipment. The information and warnings given in this operating manual must be heeded.
Any work on electrical equipment is only to be carried out by trained specialists as per the regulations
currently in force.
Attention must be paid to the requirements of VDE 0100 (IEC 364) when setting high-power electrical
units with nominal voltages of up to 1000 V, together with the associated standards and stipulations.
Check the details on the type plate to ensure that the equipment is connected to the correct mains
voltage.
Protection against touching dangerously high electrical voltages:
Before opening the equipment, it must be switched off and hold no voltages. This also applies to any
external control circuits that are connected.
The device is only to be used within the permitted range of temperatures and pressures.
Check that the location is weather-protected. It should not be subject to either direct rain or moisture.
The equipment must not be used in hazardous areas.
Installation, maintenance, monitoring and any repairs may only be done by authorized personnel with
respect to the relevant stipulations.
4 WARRANTY
If the equipment fails, please contact M&C directly or else go through your M&C authorised dealer.
We offer a one year warranty as of the day of delivery as per our normal terms and conditions of sale,
and assuming technically correct operation of the unit. Consumables are hereby excluded. The terms
of the warranty cover repair at the factory at no cost or the replacement at no cost of the equipment
free ex user location. Reshipments must be send in a sufficient and proper protective packaging.
6 Gas sampling and gas conditioning technology 2-1.1-ME
5 USED TERMS AND SIGNAL INDICATIONS
This means that death, severe physical injuries and/or important
material damages will occur in case the respective safety measures
DANGER!
WARNING!
CARE!
CARE! Without the warning triangle means that a material damage may
ATTENTION!
NOTE!
SKILLED STAFF
are not fulfilled.
This means that death, severe physical injuries and/or important
material damages may occur in case the respective safety
measures are not fulfilled.
This means that minor physical injuries may occur in case the re-
spective safety measures are not fulfilled.
occur in case the respective safety measures are not met.
This means that an unintentional situation or an unintentional status
may occur in case the respective note is not respected.
These are important information about the product or parts of the
operating manual which require user’s attention.
These are persons with necessary qualification who are familiar with
installation, use and maintenance of the product.
6 INTRODUCTION
2-1.1-ME Gas sampling and gas conditioning technology 7
Major problems of the extractive continuous gas analysis are the materials contained in the sample
gas e.g. dust, water vapour and also gas components forming corrosive acids with condensing water
vapour.
In order to realize an easy-to-maintain measurement the dust has to be separated without condensation of water vapour. This prevents „baking“ of dust and water and the possible acid formation. This
way a blockage of filters and connected line is prevented and the probe material in contact with the
gas will not be affected.
The solution are heated M&C sample probes like e.g. probes of the series SP2000... This probes
guarantee a minimum of maintenance work if correctly adapted to the process conditions. At the con-
tinuous gas sampling for analytical measurements with M&C gas sample probes a fine dust filtration
already happens at the sample point. Hereby already a majority of necessary maintenance work at
analyser systems is prevented.
Basically, the quantity of sampled gas should be kept to a necessary minimum to guarantee a minimum of maintenance work and a maximum of availability. This is made possible thanks to optimised
downstream gas conditioning using M&C components.
7 SERIAL NUMBERS
The nameplates bearing the serial number are located on the side of the electrical connection box.
NOTE!
Always quote the device's serial number when making enquiries and ordering replacement parts.
8 Gas sampling and gas conditioning technology 2-1.1-ME
8 TECHNICAL DATA
Gas sample probe type SP2000 SP2000-H SP2300-H SP2400-H
Part no. 20S1000 20S2000 20S3000 20S3500
Weather protection shield no yes yes yes
Protection class terminal box IP54 EN60529
Material filter housing Stainless steel SS316/316Ti* PTFE Titanium
Sealing material FPM* /7aT** = PTFE -H320/C** = Graphite
Probe flange sealing material Novapress
Insitu probe tube / prefilter Optional
Sample pressure max. 0,4-6 bar* abs., /7aT**= 2 bar abs.,
/HP** = 25 bar abs.
Ambient temperature 20 °C to +180 °C -20 °C to +60 °C*;
Differential pressure and T90-time at different flow rates
P and T90 at flow of
P with new filter element
S-2K 150/F-0,1GF150
P with new filter element
F-3SS150
T90-time without sample
tube/prefilter
100 200 500 1000 1500 3000 (only /HF) Nl/h
0,007 0,011 0,020 0,058 0,135 0,240/0,225 bar
0,006 0,012 0,040 0,110 0,215 0,405 bar
6,0 3,5 1,0 <0,5 <0,5 <0,5 sec.
2 bar abs. 0,4-6 bar abs.
9 APPLICATION
The M&C gas sample probes type SP2000..., SP2300-H and SP2400-H are used for continuous ex-
traction of gases from dust laden, high-temperature and/or humid processes.
2-1.1-ME Gas sampling and gas conditioning technology 9
10 DESCRIPTION
The sample probes are designed for easy installation, reliable and flexible operation and trouble-free
maintenance. Depending on the problem, different sample tubes or prefilters (see data sheet 2-1.1.0.6
and 2-1.1.0.8) are screwed into the thread (G3/4”) in the mounting flange. This equipment is not included in the scope of delivery of the probe.
The large-surface ceramic deep filter element (fibre glass or glass wadding fillings are also available)
is placed in a housing with small dead volume outside the process area. The probes are designed so
that no tools are necessary for changing the filter element, the sample line needs not to be dismounted and no contamination on the clean gas side will occur. Cleaning or back purging of the sample tube
is possible from outside. Due to the special execution of the heating element of the SP2000-H, SP2300-H and SP2400-H (with protection cover), the complete filter housing including mounting
flange is heated, adjustable up to 180°C (version H320/C up to 320°C), so that a safe operation without shortfall below the dew point in the out-of-process area is guaranteed. The temperature adjustment of the standard version is made via an integrated capillary sensor thermostate with exess temperature limiter and alarm function in compact configuration. Calibration gas feeding and comparison
sampling at the probe are possible.
Depending on the gas composition, it may be possible that the standard material of the probe body
(stainless steel 1.4404) is not sufficient with respect to ist corrosion resistance. For this case, the
SP2300-H of PTFE is available or alternatively for a heating above 180°C the SP2400-H out of Titane.
The following filter elements are available:
Filter elements Type Porosity Material
Filter element S-2K 150 2µm
Filter element S-3G 150 3µm Glass
Filter element S-3SS 150 3µm Stainless steel SS316
Filter element S-0,1GF 150 0,1µm Glass fiber
Filter element FW -------- Spun glass
* = Standard
The following sealing agents are applied:
Material Type Max. temperature
Viton Standard max. 180°C
PTFE Type /7aT max. 180°C
Graphite Type -H320/C max. 320°C
The following types of partial filter heating and regulation are possible:
Type Version
-H
/PT100
/Fe-CuNi
/Ni-CrNi
/D
* = Standard
Electrical heating and control with incorporated capillary thermostat*
Electical heating and control with external electronic temperature controller
Steam heating, not controlled
Ceramic*
10 Gas sampling and gas conditioning technology 2-1.1-ME
11 PROBE DESIGN OF THE HEATED VERSION
A complete gas sample probe consists of the heated filter part and a sample tube or prefilter. The filter
housing with its all-round heating element forms a unit with the standard mounting flange DN65
PN6 and the laterally mounted electrical connection box .
The heat-insulated shield is mounted on the stainless steel angle sheet which is mounted on the
mounting flange. It is secured with 2 pressure clamps. The cover ensures a uniform distribution of heat
over the probe heater and at the same time serves as protection against weather and accidental contact.
Figure 1 Design of basic version SP2000-H
11.1 SAMPLE GAS CONNECTION
The connecting clamp for attaching heated M&C sample lines with external dimensions of between
40mm and 50mm is located at the aperture on the underside of the angle sheet, which is closed with a
silicon lid . The clamp is mounted on an adjustable mounting bracket which allows adjustment for
various sample line diameters.
The standard probe's sample gas outlet connection has a ¼" NPT internal thread to which the customer must connect a suitable size of temperature resistant and threaded connector to connect the
sample line in a gas tight manner. These connectors can be supplied by M&C.
In the high-temperature version -H320/C..., the sample gas outlet connection is fitted with a welded 6
mm threaded pipe connection (optional 8mm).
After the threaded pipe connector and sample line have been mounted, the sample gas outlet connection is enclosed in special heat-conducting jaws in order to avoid temperature failures in the critical
connection areas. The size of the heat-conducting jaws allows connection joints up to an external pipe
dimension of 10mm.
2-1.1-ME Gas sampling and gas conditioning technology 11
1)
11.2 TEMPERATURE CONTROLLER
In standard version -H, or with option –H320/C temperature control is ensured by way of the capillary
tube thermostat which is built into the connection box and which has a regulation range between 0°C
to 180°C (-H) or 0°C to 320°C (-H320/C). Rated values can be set to a maximum 180°C resp. 320°C.
The temperature has an excess temperature limiter which permanently switches off the heating if the
set temperature is exceeded by 30°C. The heating can be switched back on again by pressing the
green RESET-button which is located below the aperture in the thermostats mounting.
The thermostat has a temperature failure alarm which activates a contact if the temperature falls 30°C
below the set temperature. This status alarm is located on the terminal strip as a potential-free switch
over contact.
If temperature control is to be achieved using external electronic equipment, a PT100 (a max. of two
can be built in) or an Fe-CuNi resp. Ni-CrNi thermoelement is provided as a temperature sensor.
M&C also supplies suitable temperature controller, e.g. Type 70304G (see data sheet 2-5.1) which
also can be mounted directly at the gas sample probe (max. ambient temperature +45°C).
11.3 SAMPLE TUBE AND PREFILTER POSSIBILITIES
Depending on the process gas temperature and composition, probe tubes made of different materials
are used with ¾" connections.
* Sample tube with support adapter. Max.Temperature concern the area of the support adapter on approx. 200 mm length depend on material 600/900 °C.
** For gas sampling downstream wet scrubbers for droplet separation
1)
standard
2)
Please pay attention to the characteristic feature of ceramic in case of high and changing temperatures!
Other materials or executions on request.
Part no. Temperature
max. °C
Material
tube / connection part
Length
mm
Length
max. mm
Tube ø
o/i „d1“ mm
For more information about sample tubes see data sheet 2-1.1.0.6
To prevent condensation between sample point and heated gas sample probe or in case of condensation in the area of the connection piece heated sample tubes made of stainless steel with flange
connection DN65 PN6 are used.
12 Gas sampling and gas conditioning technology 2-1.1-ME
Type Max. process temperature Length max. Tube ø o. Temperature sensor
SP-30H1.1, heating max. 320°C bis max. 550 °C
SP-30H1.1V, heating max. 320°C bis max. 550 °C
SP30-H2, heating max. 320°C bis max. 550 °C
SP35-H1.1, heating max. 320°C bis max. 550 °C 0,175 m ø 42,2mm Fe-CuNi
SP35-H2, heating max. 320°C bis max. 550 °C 0,175 m ø 42,2mm PT100
* = standard
2,0 m *
2,0 m *
2,0 m *
ø 42,2mm Fe-CuNi
ø 42,2mm Fe-CuNi
ø 42,2mm PT100
For more information about heated sample tubes see data sheet 2-1.9.5
In case of heavier dust loading of the process gas, we recommend using a prefilter under all circumstances in order to prolong service life. This can be supplied with or without dead volume displacer
depending on the response times required. These filters can be screwed directly into the probe flange
or via extension tubes fitted with volume displacers.
2-1.1-ME Gas sampling and gas conditioning technology 13
The following prefilters can be selected :
Prefilter
Type
SP2000/20SS 150 20S9160 600 SS316/316Ti 20 2-10
SP2000/V20 20S9085 600 SS316/316Ti 2 2-10
SP2000/V20-0 20S9105 600 SS316/316Ti 2 2-10 X 220 46 G 3/4"a
SP2000/V20/HC 20S9095 900 Hastelloy-C 2 2-10
SP2000/V20-0/HC 20S9115 900 Hastelloy-C 2 2-10 X 220 46 G 3/4"a
SP2000/V20-T 20S9315 200 PTFE / SS316Ti 3 > 10
SP2000/V20-2 20S9125 600 SS316/316Ti 2 > 10
SP2000/V20-1 20S9145 600 SS316/316Ti 2 > 10 X 520 60 G 3/4"a
SP2000/V20-2/HC 20S9135 900 Hastelloy-C 2 > 10
SP2000/V20-1/HC 20S9155 900 Hastelloy-C 2 > 10 X 520 60 G 3/4"a
SP2000/V20-41) 20S9290 600 SS316/316Ti 2 2-10
SP2000/V20-31) 20S9300 600 SS316/316Ti 2 2-10 X
SP2000/V20-5 20S9127 500 SS316/316Ti 3 2-10
SP2000/V20-6 20S9128 500 SS316/316Ti 3 > 10
SP2000/V12-1 20S9500 1000
SP2000/V12-3 20S9510 1000
SP2000/V12-2 20S9505 1000
SP2000/V12-1/SS2) 20S9525 600
SP2000/V12-3/SS3) 20S9535 600
SP2000/V12-2/SS3) 20S9530 600
SP2000/V12-1/IC2) 20S9540 1000
SP2000/V12-3/IC3) 20S9550 1000
SP2000/V12-2/IC3) 20S9545 1000
1)
Prefilter V20-3, V20-4 optional up to 1000 mm length available.
2)
With protection tube V12-1.
3)
With protection tube V12-2/3.
4)
Prefilter with special construction for efficient back purge.
5)
Please pay attention to the characteristic feature of ceramic in case of high and changing temperatures!
For more information about prefilters see data sheet 2-1.1.0.8
12 RECEIPT OF GOODS AND STORAGE
The gas sample probe and any special accessories should be removed carefully from the packag-
ing and checked immediately for completeness against the delivery note.
Check the goods for any damage incurred during transport and if necessary inform your transport
insurer of any damage.
The gas sample probe is normally delivered in two packaging units:
1. The gas sample probe with the screws, nuts and flange seal required for mounting.
2. Sample tube or prefilter, if applicable with extension tube.
14 Gas sampling and gas conditioning technology 2-1.1-ME
The equipment should be stored in a protected, frost-free room!
NOTE!
13 PREPARATION FOR INSTALLATION
Select the optimal sampling point in accordance with the generally applicable guidelines or consult
the competent persons.
Locate the sampling point in such a way that there is adequate space for inserting and removing
the probe and pay attention to the insertion length of the probe tube.
Make certain that the probe is easily accessible so that you can carry out any subsequent mainte-
nance work without trouble.
Locate the probe connections in such a way that the connections' temperature is always above the
acid dew point in order to avoid corrosion and blockage problems. If this is not possible, a heated
SP35/SP30 probe tube is recommended for cold connections.
If the ambient temperature in the area of the connections is >80°C as a result of radiated heat, then
a radiated-heat deflector must be mounted to protect the probe.
The connection's mounting flange connection should comply with DN65 PN6. If other connection
sizes are required, a special adapter flange /S010 can be supplied as an option. Instead of flange
connection mounting, the probe can also be mounted using an R2" adapter on a corresponding
threaded sleeve connection. This adapter can be supplied. The necessary minimum flange size
and the minimum connection diameter depends on the diameter of the probe tube or prefilter used.
2-1.1-ME Gas sampling and gas conditioning technology 15
Before mounting, the probe must be adjusted to the existing operating conditions.
The existing operational parameters are to be checked accordingly prior to commencing
mounting work.
Low-excess pressure situation
Process temperature
Dust loading
Dust composition – grain size
Gas composition
Parameters to be measured, e.g. O2, CO, SO2,
,..,
NO
X
Necessary gas flow
Necessary T90-time
mbar bar
°C, Min. °C Max.
g/m³
µm
corrosive toxic explosive
Vol.% mg/Nm³ ppm
l/hr, Min. l/hr, Max.
s
14 MOUNTING
M&C SP2000 probes are designed for stationary use and if properly selected and mounted a long
service life and minimum maintenance are guaranteed.
It is advisable to mount the probe in an operational position which is at a 10% inclination to the process.
14.1 CHECK OF THE FILTER ELEMENT
Before starting the filter element has to be checked for tight fit.
Figure 3 Cross-sectional drawing SP2000-H
Removing the filter housing lid to check or change the filter element has to be done as follows :
16 Gas sampling and gas conditioning technology 2-1.1-ME
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