Martini Instruments MI 413 User Manual

USER MANUAL
MI 413
Free & Total Chlorine
High Range Meter
Dear Customer, Thank you for choosing a Martini product. This manual will provide you with the necessary infor­mation for the correct use of the instrument. Please read it carefully before using the meter.
This instrument is in compliance with directives.
Range 0.00 to 10.00 mg/L Cl
2
Resolution 0.01 mg/L (0.00-3.50 mg/L);
0.10 mg/L (above 3.50 mg/L) Precision ±0.10 mg/L @ 5.00 mg/L Light Source Tungsten lamp Light Detector Silicon Photocell and 525 nm
narrow band interference filter
Method Adaptation of the USEPA
method 330.5 and Standard Method 4500-Cl G.
Environment 0 to 50°C (32 to 122°F);
100% RH max. Battery Type 1 x 9 volt Auto-Shut off After 10' of non-use Dimensions 192 x 104 x 52 mm
(7.5 x 4.1 x 2”) Weight 380 g
SPECIFICATIONS:
ISTMI413 02/08
MEASUREMENT PROCEDURE:
1• Turn the meter on by pressing ON/OFF. 2• When the LCD displays “- - -”,
the meter is ready.
3• Fill the cuvet with 10 mL of
unreacted sample, up to the mark and replace the cap.
4• Place the cuvet into the holder
and ensure that the notch on the cap is positioned securely into the groove.
5• Press ZERO and “SIP” will blink
on the display.
6• After a few seconds the dis-
play will show “-0.0-”. The meter is now zeroed and ready for measurement.
7• For free chlorine measurement:
Add 3 drops of DPD 1 reagent to an empty cuvet.
8• Add 5 mL of DPD 0 reagent by using a
syringe.
9 • Fill the cuvet up to the 10 mL mark with 5
mL of unreacted sample using a pipette.
10• Replace the cap and shake gentily for a
few seconds.
11• Immediately insert the cuvet into the holder
and ensure that the notch on the cap is positioned securely into the groove.
12• Press READ and “SIP” will blink
during measurement.
13• The instrument directly displays con-
centration in mg/L of chlorine.
14• Then, for total chlorine measurement,
remove the cuvet and add to the reacted sample 3 drops of DPD 3. Replace the cap and swirl gently.
15• Reinsert the cuvet into the holder and en-
sure that the notch on the cap is posi­tioned securely into the groove.
16• Wait for 2 minutes and
30 seconds then press READ and “SIP” will blink during measurement.
17• The instrument directly displays concentra-
tion in mg/L of total chlorine.
Interferences
Bromine (positive error)
Chlorine dioxide (positive error)
Iodine (positive error)
Oxidized Manganese and Chromium (positive
error)
Ozone (positive error)
Alkalinity above 250 mg/L CaCO3 or acidity
above 150 mg/L CaCO3 will not reliable de­velop the full amount of color or it may rapidly fade. To resolve this, neutralize the sample with diluted HCl or NaOH.
GUIDE TO DISPLAY CODES:
This prompt appears for 1 second each time the instru­ment is turned on.
The dashes “- - -” indicate that the meter is in a ready state and zeroing can be performed.
Sampling In Progress. Flash­ing “SIP” prompt appears each time the meter is performing a measurement.
“-0.0-”, the meter is in a zeroed state and measure­ment can be performed.
The blinking "BAT" indicates that the battery voltage is getting low and the battery needs to be replaced.
“-bA-”, the battery is dead and must be replaced. Once this indication is displayed, the meter will lock up. Change the battery and restart the meter.
“Conf”, the meter has lost its configuration. Contact your dealer or the nearest Martini Customer Service Center.
ERROR MESSAGES
On zero reading
Blinking “-0.0-” indicates
that the zeroing procedure failed due to a low signal­to-noise ratio. In this case press ZERO again.
“no L”, the instrument can-
not adjust the light level. Please check that the sample does not contain any debris.
“L Lo”, there is not enough
light to perform a measure­ment. Please check the preparation of the zero cuvet.
“L Hi”, there is too much
light to perform a measure­ment. Please check the preparation of the zero cuvet.
On sample reading
“-SA-”, there is too much
light for the sample measurement. Please check if the right sample cuvet is inserted.
“Inv”, the sample and the
zero cuvet are inverted.
“ZErO”, a zero reading was
not taken. Follow the instruction in the measure­ment procedure for zero­ing the meter.
BATTERY REPLACEMENT
Battery replacement must only take place in a non-hazardous environment.
Simply rotate the battery cover on the back of the meter.
Detach the battery from the termi­nals and attach a fresh 9V battery while paying attention to the correct polarity. Insert the battery and replace the cover.
Under range. A blinking
“0.00” indicates that the sample absorbs less light than the zero reference. Check the procedure and make sure you use the same cuvet for reference (zero) and measurement.
A flashing value of the
maximum concentration in­dicates an over range con­dition. The concentration of the sample is beyond the programmed range: dilute the sample and re-run the test.
ACCESSORIES:
MI513-045 Free & Total Chlorine
reagent set (45 tests)
MI0001 Glass cuvets (2 pcs) MI0002 Caps for cuvets (2 pcs) MI0003 Stoppers for cuvets (2 pcs) MI0004 Tissue for wipping cuvets
(4 pcs)
MI0005 9V battery (1 pc)
WARRANTY
This instrument is warranted against defects in mate­rials and manufacturing for a period of two years from the date of purchase. If during this period the repair or replacement of parts is required, where the damage is not due to negli­gence or erroneous operation by the user, please return the meter to either distributor or our office in the original packing and the repair will be free of charge. Damages due to accidents, misuse, tampering or lack of prescribed maintenance are not covered.
ISTMI413 03/05
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